DTA measure 2Olom2 Date: 20251119:1017 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.25 s Mass = 1367.000 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3260 -2.0997 209.5081 211.6078 247.9184 2.1130 -2.0986 209.6430 211.7416 247.9051 2.9205 -2.0968 209.7910 211.8879 247.8529 3.7383 -2.0989 209.9637 212.0626 247.8106 4.5048 -2.1000 210.0643 212.1643 247.7878 5.3635 -2.0986 210.1944 212.2930 247.7511 6.1300 -2.0981 210.3740 212.4721 247.7221 6.9478 -2.1006 210.5246 212.6253 247.6448 7.7453 -2.0981 210.6578 212.7559 247.6103 8.5320 -2.1005 210.7764 212.8769 247.5745 9.3505 -2.1024 210.9384 213.0407 247.5175 10.1275 -2.1024 211.0532 213.1556 247.4951 10.9760 -2.1021 211.1764 213.2785 247.4810 11.7425 -2.1029 211.2849 213.3878 247.4609 12.5705 -2.1015 211.4256 213.5271 247.4434 13.3268 -2.0996 211.5522 213.6518 247.4204 14.1548 -2.0975 211.6824 213.7799 247.3926 14.9520 -2.0965 211.8189 213.9154 247.3591 15.7493 -2.0979 211.9499 214.0478 247.3270 16.5773 -2.0959 212.0883 214.1842 247.2922 17.3335 -2.0943 212.1972 214.2915 247.2669 18.1923 -2.0939 212.3345 214.4284 247.2613 18.9588 -2.0911 212.4732 214.5643 247.2556 19.7765 -2.0890 212.6192 214.7081 247.2259 20.5843 -2.0868 212.7286 214.8154 247.2188 21.3713 -2.0847 212.8809 214.9656 247.2413 22.1998 -2.0822 213.0007 215.0829 247.2194 22.9665 -2.0807 213.1417 215.2224 247.1918 23.8253 -2.0805 213.2703 215.3509 247.1942 24.5918 -2.0786 213.4040 215.4826 247.1930 25.4095 -2.0717 213.5305 215.6022 247.2082 26.2170 -2.0680 213.6387 215.7067 247.2140 27.0040 -2.0645 213.7836 215.8481 247.2314 27.8320 -2.0613 213.9329 215.9942 247.2073 28.5985 -2.0577 214.0343 216.0920 247.2578 29.4573 -2.0561 214.1698 216.2259 247.3345 30.2238 -2.0523 214.2979 216.3502 247.3281 31.0415 -2.0471 214.4307 216.4778 247.3683 31.8490 -2.0483 214.5620 216.6103 247.4169 32.6463 -2.0477 214.7245 216.7722 247.4676 33.4640 -2.0471 214.8521 216.8992 247.5126 34.2308 -2.0425 214.9341 216.9766 247.5817 35.0903 -2.0385 215.0612 217.0997 247.6562 35.8568 -2.0362 215.1805 217.2168 247.7861 36.6745 -2.0332 215.3117 217.3449 247.8169 37.4820 -2.0326 215.4378 217.4704 247.8946 38.2690 -2.0349 215.5401 217.5750 247.9570 39.0868 -2.0293 215.6628 217.6920 248.0166 39.8635 -2.0281 215.7959 217.8240 248.0902 40.7120 -2.0245 215.9462 217.9707 248.1830 41.4683 -2.0210 216.0881 218.1091 248.2397 42.3065 -2.0173 216.2255 218.2428 248.3061 43.0935 -2.0160 216.3258 218.3418 248.3886 43.8805 -2.0119 216.4498 218.4617 248.4853 44.7195 -2.0082 216.5828 218.5910 248.6029 45.4760 -2.0069 216.7097 218.7166 248.7129 46.3245 -2.0020 216.8533 218.8553 248.8752 47.1013 -1.9992 216.9480 218.9472 248.9894 47.9190 -1.9950 217.0622 219.0572 249.1354 48.6855 -1.9885 217.1842 219.1726 249.2579 49.5135 -1.9863 217.3313 219.3175 249.3853 50.3108 -1.9830 217.4665 219.4495 249.4972 51.1080 -1.9799 217.5612 219.5411 249.6086 51.9258 -1.9774 217.6867 219.6641 249.7227 52.7025 -1.9759 217.7928 219.7687 249.8449 53.5510 -1.9744 217.9219 219.8963 250.0143 54.3175 -1.9720 218.0520 220.0240 250.1417 55.1455 -1.9712 218.1759 220.1471 250.2855 55.9428 -1.9681 218.3013 220.2694 250.4248 56.7400 -1.9668 218.4031 220.3699 250.5615 57.5583 -1.9694 218.5180 220.4874 250.7213 58.3355 -1.9676 218.6422 220.6098 250.8654 59.1840 -1.9640 218.7827 220.7467 250.9934 59.9300 -1.9629 218.9155 220.8784 251.1423 60.7785 -1.9631 219.0324 220.9955 251.2853 61.5553 -1.9629 219.1748 221.1377 251.4468 62.3730 -1.9590 219.3120 221.2710 251.5782 63.1703 -1.9639 219.4507 221.4146 251.7493 63.9675 -1.9646 219.5934 221.5580 251.8945 64.7955 -1.9582 219.6916 221.6498 252.0261 65.5620 -1.9533 219.7836 221.7369 252.1546 66.4108 -1.9551 219.9050 221.8601 252.3274 67.1883 -1.9526 220.0396 221.9922 252.4537 68.0060 -1.9506 220.1967 222.1474 252.6193 68.8033 -1.9496 220.3230 222.2726 252.7980 69.6005 -1.9511 220.4593 222.4104 252.9419 70.3978 -1.9534 220.5718 222.5252 253.1240 71.1848 -1.9515 220.6908 222.6423 253.2664 72.0128 -1.9567 220.8037 222.7604 253.4332 72.7793 -1.9604 220.9021 222.8625 253.5654 73.6278 -1.9552 221.0339 222.9891 253.7314 74.3943 -1.9556 221.1272 223.0828 253.8590 75.2128 -1.9554 221.2927 223.2481 254.0091 75.9795 -1.9547 221.4037 223.3584 254.1680 76.8075 -1.9521 221.5193 223.4714 254.2832 77.6048 -1.9494 221.6551 223.6045 254.4327 78.3918 -1.9460 221.7264 223.6724 254.5854 79.2198 -1.9406 221.8680 223.8086 254.7250 79.9863 -1.9354 221.9718 223.9072 254.8317 80.8450 -1.9296 222.0879 224.0175 254.9570 81.6013 -1.9254 222.2088 224.1342 255.0876 82.4395 -1.9216 222.3580 224.2795 255.2255 83.2270 -1.9196 222.5000 224.4196 255.3657 84.0248 -1.9236 222.6064 224.5300 255.5066 84.8528 -1.9227 222.7474 224.6700 255.6526 85.6090 -1.9227 222.8660 224.7887 255.7924 86.4678 -1.9226 222.9812 224.9038 255.9527 87.2035 -1.9189 223.0950 225.0139 256.0366 88.0623 -1.9167 223.2439 225.1606 256.1765 88.8288 -1.9190 223.3709 225.2899 256.3008 89.6465 -1.9197 223.4760 225.3957 256.4070 90.4540 -1.9179 223.6136 225.5315 256.4881 91.2420 -1.9173 223.7648 225.6821 256.6120 92.0700 -1.9204 223.8988 225.8192 256.7481 92.8365 -1.9195 224.0189 225.9385 256.8307 93.7055 -1.9170 224.1585 226.0755 256.9423 94.4618 -1.9141 224.2405 226.1545 257.0550 95.3000 -1.9152 224.3871 226.3023 257.1798 96.0460 -1.9161 224.4826 226.3987 257.3121 96.8945 -1.9147 224.5686 226.4833 257.4462 97.6713 -1.9163 224.6614 226.5777 257.5566 98.4900 -1.9163 224.8151 226.7314 257.6856 99.2873 -1.9213 224.9737 226.8950 257.7985 100.0845 -1.9230 225.1164 227.0394 257.9029 100.9125 -1.9240 225.2175 227.1415 257.9905 101.6790 -1.9263 225.3281 227.2544 258.1122 102.5275 -1.9206 225.4532 227.3738 258.2494 103.3043 -1.9147 225.6010 227.5157 258.3575 104.1220 -1.9164 225.7107 227.6271 258.4495 104.9090 -1.9172 225.8327 227.7499 258.5387 105.7063 -1.9211 225.9533 227.8744 258.6179 106.5240 -1.9214 226.0762 227.9976 258.7293 107.2905 -1.9192 226.1508 228.0699 258.8347 108.1398 -1.9171 226.2712 228.1884 258.9528 108.9065 -1.9161 226.3867 228.3028 259.0476 109.7345 -1.9157 226.5053 228.4210 259.1274 110.5215 -1.9170 226.6217 228.5388 259.2025 111.3188 -1.9160 226.7387 228.6547 259.2508 112.1468 -1.9127 226.8804 228.7931 259.3041 112.9133 -1.9144 226.9971 228.9115 259.4057 113.7720 -1.9150 227.1273 229.0423 259.5129 114.4975 -1.9143 227.2480 229.1623 259.5838 115.3665 -1.9153 227.3860 229.3013 259.6450 116.1228 -1.9130 227.4601 229.3731 259.7157 116.9508 -1.9149 227.5922 229.5071 259.8494 117.7480 -1.9154 227.7123 229.6277 259.9623 118.5453 -1.9124 227.8260 229.7384 260.0365 119.3743 -1.9128 227.9824 229.8952 260.1173 120.1305 -1.9137 228.1205 230.0342 260.1998 120.9995 -1.9130 228.2511 230.1641 260.2827 121.7558 -1.9132 228.3660 230.2792 260.3505 122.5838 -1.9089 228.4983 230.4072 260.4845 123.3810 -1.9065 228.5984 230.5049 260.5674 124.1783 -1.9068 228.7433 230.6500 260.6555 125.0063 -1.9080 228.8689 230.7768 260.7287 125.7625 -1.9106 229.0039 230.9145 260.7945 126.6320 -1.9110 229.1541 231.0651 260.8808 127.3888 -1.9113 229.2819 231.1931 260.9670 128.2168 -1.9117 229.3804 231.2921 261.0636 129.0140 -1.9093 229.4728 231.3820 261.1423 129.8113 -1.9012 229.5961 231.4972 261.2549 130.6393 -1.9024 229.7216 231.6240 261.3488 131.3955 -1.9036 229.8239 231.7274 261.4236 132.2645 -1.9056 229.9145 231.8201 261.5169 133.0208 -1.9074 230.0094 231.9169 261.6245 133.8495 -1.9021 230.1300 232.0321 261.7207 134.6470 -1.9011 230.2670 232.1681 261.8073 135.4443 -1.9038 230.3671 232.2710 261.8872 136.2620 -1.9005 230.4834 232.3839 261.9716 137.0285 -1.8953 230.6111 232.5064 262.0767 137.8770 -1.8952 230.7323 232.6275 262.2022 138.6435 -1.8943 230.8357 232.7300 262.2956 139.4715 -1.8979 230.9815 232.8795 262.3923 140.2585 -1.9017 231.1046 233.0063 262.4571 141.0455 -1.9036 231.2073 233.1109 262.5258 141.8838 -1.9027 231.3694 233.2721 262.6209 142.6400 -1.9014 231.5172 233.4186 262.7171 143.4888 -1.8994 231.6419 233.5413 262.8226 144.2663 -1.8961 231.7131 233.6092 262.8294 145.0840 -1.8968 231.8339 233.7308 262.9307 145.8813 -1.8942 231.9611 233.8553 263.0416 146.6785 -1.8932 232.0667 233.9598 263.1321 147.5065 -1.8939 232.1862 234.0801 263.2344 148.2730 -1.8914 232.3173 234.2087 263.3433 149.1215 -1.8887 232.4509 234.3396 263.4620 149.8983 -1.8891 232.5617 234.4508 263.6017 150.7160 -1.8891 232.6824 234.5715 263.7358 151.5030 -1.8876 232.7683 234.6559 263.8445 152.3105 -1.8859 232.8730 234.7589 263.9398 153.1283 -1.8837 233.0142 234.8979 264.0303 153.8948 -1.8829 233.1566 235.0396 264.1251 154.7543 -1.8813 233.2972 235.1785 264.2433 155.5210 -1.8801 233.4242 235.3043 264.3522 156.3490 -1.8763 233.5451 235.4214 264.4173 157.1155 -1.8780 233.6912 235.5691 264.5193 157.9640 -1.8804 233.8325 235.7130 264.6690 158.7305 -1.8820 233.9581 235.8402 264.7730 159.5585 -1.8794 234.0559 235.9353 264.8319 160.3558 -1.8783 234.1683 236.0465 264.9493 161.1530 -1.8821 234.3054 236.1875 265.0550 161.9708 -1.8808 234.4333 236.3141 265.1460 162.7475 -1.8800 234.5427 236.4227 265.2728 163.5970 -1.8801 234.6745 236.5546 265.4009 164.3635 -1.8808 234.7704 236.6512 265.4965 165.1915 -1.8780 234.8834 236.7614 265.6127 165.9888 -1.8744 235.0025 236.8769 265.7545 166.7860 -1.8773 235.1425 237.0198 265.8643 167.6038 -1.8773 235.2385 237.1159 265.9648 168.3703 -1.8751 235.3458 237.2208 266.0270 169.2188 -1.8690 235.4461 237.3152 266.1361 169.9863 -1.8674 235.4973 237.3647 266.2583 170.8040 -1.8703 235.5907 237.4610 266.3898 171.6013 -1.8691 235.6982 237.5674 266.5041 172.3985 -1.8723 235.8202 237.6925 266.6479 173.2163 -1.8733 235.9450 237.8183 266.7447 173.9828 -1.8775 236.0611 237.9387 266.8671 174.8108 -1.8812 236.1558 238.0371 266.9999 175.5773 -1.8773 236.2844 238.1618 267.1230 176.4258 -1.8779 236.4461 238.3240 267.2182 177.1933 -1.8769 236.5531 238.4300 267.3010 178.0213 -1.8779 236.6883 238.5662 267.4235 178.8185 -1.8731 236.7576 238.6307 267.5424 179.6055 -1.8686 236.8862 238.7548 267.6661 180.4335 -1.8672 237.0273 238.8944 267.7844 181.2000 -1.8701 237.1351 239.0052 267.9296 182.0485 -1.8735 237.2762 239.1496 268.0430 182.7945 -1.8749 237.3874 239.2623 268.1390 183.6430 -1.8728 237.5061 239.3789 268.2684 184.4095 -1.8694 237.6464 239.5158 268.3973 185.2375 -1.8720 237.7617 239.6336 268.5226 186.0350 -1.8733 237.8840 239.7572 268.6108 186.8330 -1.8763 237.9525 239.8288 268.7508 187.6610 -1.8746 238.0855 239.9601 268.8544 188.4275 -1.8712 238.2147 240.0859 268.9294 189.2863 -1.8725 238.3444 240.2169 268.9982 190.0528 -1.8765 238.4538 240.3303 269.1043 190.8705 -1.8799 238.5803 240.4602 269.2241 191.6473 -1.8816 238.6924 240.5739 269.3791 192.4650 -1.8751 238.7956 240.6708 269.4915 193.2623 -1.8731 238.8938 240.7669 269.6154 194.0595 -1.8729 239.0021 240.8750 269.7335 194.8883 -1.8784 239.1207 240.9992 269.8696 195.6550 -1.8812 239.2434 241.1246 269.9955 196.5035 -1.8815 239.3822 241.2637 270.1241 197.2803 -1.8831 239.5444 241.4275 270.2655 198.0980 -1.8823 239.6562 241.5385 270.3446 198.8953 -1.8777 239.7527 241.6304 270.4792 199.6925 -1.8774 239.8505 241.7279 270.6086 200.5205 -1.8783 239.9644 241.8426 270.7242 201.2768 -1.8784 240.0739 241.9523 270.8252 202.1048 -1.8781 240.1839 242.0620 270.9211 202.8610 -1.8742 240.2897 242.1639 271.0326 203.7208 -1.8727 240.4185 242.2912 271.1429 204.4873 -1.8699 240.5302 242.4001 271.2456 205.3050 -1.8686 240.6303 242.4990 271.3407 206.1023 -1.8689 240.7086 242.5775 271.4283 206.8995 -1.8737 240.8143 242.6880 271.5602 207.7275 -1.8752 240.9531 242.8283 271.6493 208.4940 -1.8680 241.0648 242.9328 271.7120 209.3118 -1.8672 241.2050 243.0722 271.8437 210.0885 -1.8670 241.3252 243.1921 271.9608 210.9370 -1.8652 241.4036 243.2688 272.0954 211.7035 -1.8685 241.5091 243.3777 272.1935 212.5325 -1.8715 241.6135 243.4850 272.2884 213.3298 -1.8699 241.7810 243.6510 272.3503 214.1270 -1.8663 241.8969 243.7632 272.4685 214.9448 -1.8680 242.0282 243.8962 272.5586 215.7215 -1.8674 242.1871 244.0545 272.5843 216.5700 -1.8687 242.3250 244.1937 272.6440 217.3365 -1.8692 242.4265 244.2957 272.7297 218.1645 -1.8698 242.5051 244.3749 272.8319 218.9618 -1.8682 242.6378 244.5060 272.9787 219.7590 -1.8656 242.7579 244.6234 273.0927 220.5460 -1.8663 242.8681 244.7344 273.1901 221.3535 -1.8676 242.9967 244.8643 273.2848 222.1713 -1.8691 243.1108 244.9799 273.3688 222.9378 -1.8691 243.2260 245.0952 273.4472 223.7968 -1.8706 243.3791 245.2497 273.5670 224.5640 -1.8749 243.4641 245.3390 273.6604 225.3920 -1.8741 243.5442 245.4183 273.7269 226.1790 -1.8708 243.6538 245.5246 273.8169 226.9865 -1.8753 243.7978 245.6731 273.9022 227.8145 -1.8781 243.9285 245.8066 273.9928 228.5810 -1.8802 244.0755 245.9557 274.0526 229.4295 -1.8735 244.1936 246.0671 274.1440 230.2063 -1.8721 244.2663 246.1384 274.2630 231.0240 -1.8735 244.3748 246.2483 274.3558 231.8315 -1.8700 244.4823 246.3523 274.4314 232.6185 -1.8720 244.6104 246.4824 274.5016 233.4160 -1.8747 244.7560 246.6307 274.6092 234.2038 -1.8797 244.8659 246.7456 274.7276 235.0318 -1.8781 244.9791 246.8572 274.8318 235.7880 -1.8778 245.0744 246.9521 274.9091 236.6468 -1.8817 245.2260 247.1077 274.9976 237.4133 -1.8842 245.3025 247.1867 275.0759 238.2310 -1.8779 245.3907 247.2686 275.1750 238.9975 -1.8750 245.4736 247.3486 275.2605 239.8563 -1.8756 245.6029 247.4785 275.3642 240.6125 -1.8809 245.7165 247.5973 275.4628 241.4405 -1.8795 245.8370 247.7165 275.5507 242.2383 -1.8773 245.9146 247.7919 275.6106 243.0360 -1.8801 246.0387 247.9188 275.7289 243.8845 -1.8833 246.1659 248.0492 275.8048 244.6305 -1.8867 246.3024 248.1891 275.8759 245.4790 -1.8804 246.4458 248.3262 275.9614 246.2455 -1.8788 246.5620 248.4408 276.0823 247.0735 -1.8775 246.6483 248.5258 276.1961 247.8708 -1.8742 246.7794 248.6536 276.3058 248.6680 -1.8724 246.8869 248.7593 276.4326 249.4858 -1.8710 246.9789 248.8499 276.5240 250.2625 -1.8644 247.1125 248.9769 276.6166 251.1110 -1.8663 247.2063 249.0726 276.7467 251.8778 -1.8680 247.3069 249.1749 276.7925 252.7065 -1.8741 247.4115 249.2856 276.9244 253.5038 -1.8701 247.5229 249.3930 277.0512 254.3010 -1.8695 247.6210 249.4905 277.1367 255.1188 -1.8715 247.7516 249.6231 277.2334 255.8955 -1.8736 247.9014 249.7750 277.3387 256.7440 -1.8732 248.0254 249.8986 277.4656 257.5105 -1.8771 248.1258 250.0028 277.5697 258.3385 -1.8792 248.2373 250.1165 277.6399 259.1358 -1.8786 248.3256 250.2042 277.7313 259.9333 -1.8802 248.4407 250.3209 277.8646 260.7518 -1.8771 248.5578 250.4348 277.9671 261.5285 -1.8811 248.6705 250.5517 278.0459 262.3770 -1.8879 248.7781 250.6661 278.1690 263.1435 -1.8866 248.8724 250.7590 278.2718 263.9715 -1.8834 249.0040 250.8874 278.4129 264.7688 -1.8809 249.1091 250.9901 278.5193 265.5558 -1.8805 249.2241 251.1046 278.6131 266.3838 -1.8800 249.3369 251.2169 278.7071 267.1400 -1.8798 249.4274 251.3072 278.8091 267.9890 -1.8830 249.5465 251.4294 278.9187 268.7663 -1.8807 249.6580 251.5386 278.9647 269.5840 -1.8771 249.7905 251.6676 279.0963 270.3710 -1.8753 249.9140 251.7893 279.2062 271.1683 -1.8728 250.0250 251.8977 279.3282 271.9963 -1.8720 250.1798 252.0518 279.4404 272.7525 -1.8730 250.3146 252.1875 279.5226 273.6113 -1.8740 250.4416 252.3156 279.6878 274.3778 -1.8738 250.5515 252.4253 279.7730 275.1960 -1.8713 250.6750 252.5463 279.8593 276.0040 -1.8726 250.8006 252.6732 279.9439 276.7910 -1.8735 250.8882 252.7616 280.0962 277.6190 -1.8797 250.9910 252.8707 280.2350 278.3855 -1.8829 251.0864 252.9693 280.3300 279.2135 -1.8857 251.1983 253.0840 280.4068 279.9800 -1.8856 251.3123 253.1979 280.4961 280.8285 -1.8844 251.4386 253.3231 280.5466 281.6053 -1.8849 251.5590 253.4438 280.6258 282.4230 -1.8857 251.6437 253.5294 280.7849 283.2203 -1.8814 251.7562 253.6376 280.9306 284.0180 -1.8781 251.9027 253.7808 281.0193 284.8465 -1.8772 251.9653 253.8425 281.1117 285.6130 -1.8748 252.0706 253.9454 281.2024 286.4718 -1.8799 252.1659 254.0458 281.3140 287.2383 -1.8813 252.2509 254.1322 281.4387 288.0663 -1.8793 252.3749 254.2541 281.5795 288.8328 -1.8775 252.5024 254.3799 281.7061 289.6608 -1.8795 252.6277 254.5072 281.8287 290.4580 -1.8799 252.7384 254.6183 281.9178 291.2660 -1.8781 252.8189 254.6970 282.0530 292.0843 -1.8796 252.9512 254.8308 282.1509 292.8508 -1.8815 253.0765 254.9580 282.2839 293.6788 -1.8828 253.1962 255.0790 282.3721 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