DTA measure 13_Pb_updown Date: 2026923:918 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.27 s Mass = 1178.700 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2503 -3.4372 210.0406 213.4778 247.9218 2.0885 -3.4399 210.3706 213.8106 247.9507 2.8753 -3.4385 210.4780 213.9165 247.9409 3.6718 -3.4346 210.6329 214.0675 247.8368 4.4998 -3.4252 210.9051 214.3303 247.7444 5.2760 -3.4300 211.0735 214.5035 247.7110 6.1240 -3.4405 211.1614 214.6020 247.6746 6.8803 -3.4333 211.3029 214.7362 247.6313 7.7075 -3.4214 211.4616 214.8830 247.6097 8.4943 -3.4203 211.6147 215.0349 247.5567 9.2915 -3.4191 211.8128 215.2319 247.5302 10.1190 -3.4161 211.9367 215.3528 247.5316 10.8748 -3.4085 212.0259 215.4344 247.3808 11.7028 -3.4107 212.1834 215.5941 247.2739 12.4580 -3.4106 212.3380 215.7487 247.2296 13.3168 -3.4025 212.5586 215.9610 247.1969 14.0833 -3.3842 212.7490 216.1332 247.1534 14.9000 -3.3766 212.8463 216.2229 247.1280 15.6973 -3.3812 212.9614 216.3426 247.1094 16.4945 -3.3773 212.9922 216.3696 247.1935 17.3113 -3.3783 213.0843 216.4626 247.2142 18.0778 -3.3721 213.1820 216.5540 247.3069 18.9058 -3.3573 213.2549 216.6122 247.2650 19.6713 -3.3550 213.4614 216.8164 247.1656 20.5198 -3.3529 213.6652 217.0181 247.1635 21.2863 -3.3485 213.9054 217.2539 247.0917 22.1133 -3.3528 214.0352 217.3880 247.0562 22.9105 -3.3475 214.2050 217.5526 247.0280 23.6973 -3.3507 214.3855 217.7363 247.0882 24.5348 -3.3564 214.4783 217.8347 247.1512 25.2910 -3.3489 214.5593 217.9082 247.2183 26.1495 -3.3363 214.6841 218.0203 247.2832 26.8845 -3.3352 214.7518 218.0870 247.2912 27.7433 -3.3223 214.8784 218.2007 247.3134 28.5093 -3.3142 215.0987 218.4129 247.3491 29.3265 -3.3060 215.3832 218.6892 247.3152 30.1340 -3.2958 215.5018 218.7976 247.3887 30.9303 -3.2953 215.5679 218.8632 247.4992 31.7583 -3.2852 215.6959 218.9811 247.5725 32.5140 -3.2884 215.8189 219.1073 247.5950 33.3825 -3.2875 216.0505 219.3380 247.6581 34.1080 -3.2798 216.2345 219.5143 247.6165 34.9665 -3.2750 216.3697 219.6447 247.6074 35.7323 -3.2709 216.4311 219.7020 247.6583 36.5603 -3.2671 216.5101 219.7772 247.7408 37.3568 -3.2604 216.6377 219.8981 247.8461 38.1435 -3.2471 216.7457 219.9928 247.9991 38.9818 -3.2347 216.9005 220.1352 248.1013 39.7373 -3.2240 217.1231 220.3471 248.1750 40.5958 -3.2072 217.2936 220.5008 248.3391 41.3623 -3.1995 217.4562 220.6557 248.4214 42.1893 -3.1933 217.5336 220.7269 248.4879 42.9865 -3.1880 217.6954 220.8834 248.6899 43.7735 -3.1811 217.7806 220.9617 248.8532 44.6108 -3.1814 217.8804 221.0619 248.9684 45.3670 -3.1851 218.0243 221.2093 249.0511 46.2255 -3.1806 218.1865 221.3670 249.2275 46.9913 -3.1721 218.3545 221.5266 249.3158 47.8193 -3.1696 218.4238 221.5934 249.4081 48.6158 -3.1641 218.5645 221.7286 249.5913 49.4025 -3.1592 218.7012 221.8604 249.7514 50.2408 -3.1493 218.8060 221.9554 249.9388 50.9960 -3.1499 218.9710 222.1209 250.1331 51.8548 -3.1545 219.1278 222.2823 250.3189 52.6213 -3.1550 219.2115 222.3665 250.5038 53.4488 -3.1561 219.3530 222.5091 250.6314 54.2455 -3.1455 219.5682 222.7137 250.7795 55.0325 -3.1314 219.6595 222.7909 250.9626 55.8705 -3.1340 219.7987 222.9327 251.1075 56.6363 -3.1372 219.9741 223.1113 251.2282 57.4950 -3.1312 220.0936 223.2248 251.2926 58.2508 -3.1227 220.2023 223.3250 251.3647 59.0885 -3.1135 220.3126 223.4261 251.5739 59.8755 -3.1138 220.4186 223.5324 251.7739 60.6823 -3.1207 220.5337 223.6544 251.9587 61.4998 -3.1126 220.5679 223.6805 252.1821 62.2765 -3.1098 220.7032 223.8130 252.3600 63.0933 -3.1053 220.8351 223.9404 252.5954 63.8598 -3.1024 221.0153 224.1177 252.8026 64.7185 -3.0996 221.2482 224.3477 253.1065 65.4945 -3.0885 221.3828 224.4714 253.3421 66.3120 -3.0860 221.4639 224.5499 253.5282 67.1093 -3.0868 221.6490 224.7358 253.6591 67.9055 -3.0860 221.7609 224.8469 253.8383 68.7335 -3.0827 221.9492 225.0319 253.9654 69.4998 -3.0840 222.0760 225.1600 254.0755 70.3475 -3.0891 222.1362 225.2253 254.2344 71.1243 -3.0879 222.2905 225.3785 254.4005 71.9418 -3.0855 222.3405 225.4260 254.5746 72.7383 -3.0904 222.4864 225.5768 254.7844 73.5355 -3.0910 222.6316 225.7226 254.9442 74.3528 -3.0881 222.8273 225.9154 255.1917 75.1085 -3.0858 223.0617 226.1475 255.3892 75.9673 -3.0797 223.2272 226.3070 255.5527 76.7230 -3.0700 223.3903 226.4603 255.6922 77.5505 -3.0628 223.3848 226.4476 255.8709 78.3478 -3.0476 223.4068 226.4544 256.0311 79.1440 -3.0503 223.4341 226.4844 256.1558 79.9618 -3.0392 223.5899 226.6292 256.3959 80.7280 -3.0320 223.7222 226.7542 256.4846 81.5860 -3.0313 223.8574 226.8887 256.7265 82.3423 -3.0378 224.0494 227.0872 257.0103 83.1698 -3.0375 224.2089 227.2465 257.1401 83.9665 -3.0405 224.4205 227.4610 257.2407 84.7535 -3.0376 224.5661 227.6037 257.3335 85.5908 -3.0428 224.8079 227.8507 257.4656 86.3573 -3.0387 224.8562 227.8950 257.6147 87.2160 -3.0379 225.0072 228.0452 257.8073 87.9713 -3.0389 225.1326 228.1716 257.9766 88.8095 -3.0304 225.1969 228.2273 258.1838 89.5965 -3.0222 225.3293 228.3515 258.2691 90.3930 -3.0207 225.5159 228.5366 258.3730 91.2208 -3.0164 225.7099 228.7263 258.5764 91.9870 -3.0102 225.7726 228.7828 258.7768 92.8450 -3.0118 225.7538 228.7656 258.9358 93.6013 -3.0204 225.8616 228.8820 259.0548 94.4390 -3.0189 226.0183 229.0372 259.1838 95.1948 -3.0251 226.0839 229.1089 259.2905 96.0228 -3.0295 226.2399 229.2695 259.3939 96.8190 -3.0235 226.3580 229.3815 259.5203 97.6163 -3.0337 226.4336 229.4672 259.6616 98.4443 -3.0245 226.5799 229.6044 259.8836 99.1995 -3.0115 226.6546 229.6661 260.0545 100.0685 -3.0143 226.9009 229.9152 260.2679 100.8248 -3.0176 227.0823 230.0999 260.4036 101.6520 -3.0035 227.1957 230.1992 260.5925 102.4490 -3.0014 227.3943 230.3958 260.7587 103.2463 -3.0086 227.4906 230.4992 260.8734 104.0738 -3.0011 227.5800 230.5811 260.9636 104.8295 -3.0030 227.7266 230.7297 261.0868 105.6985 -3.0011 227.9646 230.9657 261.1555 106.4543 -3.0068 228.1182 231.1249 261.2261 107.2818 -3.0033 228.2685 231.2718 261.2619 108.0790 -3.0028 228.4180 231.4208 261.3576 108.8758 -3.0084 228.5372 231.5456 261.4880 109.7033 -3.0112 228.7364 231.7476 261.5795 110.4595 -3.0160 228.9453 231.9613 261.7199 111.3283 -3.0122 229.0071 232.0193 261.8484 112.0838 -3.0016 229.1207 232.1223 262.0270 112.9118 -2.9957 229.2495 232.2452 262.1451 113.7088 -3.0056 229.3177 232.3233 262.2592 114.5053 -2.9963 229.3217 232.3180 262.3522 115.3333 -2.9938 229.5424 232.5362 262.4353 116.0890 -2.9993 229.6522 232.6515 262.5231 116.9575 -3.0018 229.7907 232.7924 262.6028 117.7138 -2.9969 229.9207 232.9176 262.7300 118.5515 -2.9953 230.0652 233.0605 262.8657 119.3380 -2.9903 230.1888 233.1791 262.9681 120.1455 -2.9829 230.2763 233.2592 263.1029 120.9318 -2.9889 230.4501 233.4390 263.2350 121.7288 -2.9850 230.6388 233.6238 263.3665 122.5568 -2.9844 230.7616 233.7460 263.5195 123.3223 -2.9823 230.7753 233.7576 263.6534 124.1810 -2.9803 230.8729 233.8532 263.7849 124.9373 -2.9796 230.9769 233.9565 263.8899 125.7745 -2.9865 231.1897 234.1762 263.9234 126.5615 -2.9930 231.4752 234.4682 263.9686 127.3585 -2.9904 231.6438 234.6342 264.1194 128.1858 -2.9938 231.8242 234.8180 264.2756 128.9523 -2.9926 231.8341 234.8266 264.4703 129.8110 -2.9935 231.9354 234.9289 264.6425 130.5663 -2.9952 231.9843 234.9796 264.7106 131.4045 -2.9971 232.1972 235.1944 264.8421 132.2015 -2.9823 232.3308 235.3131 264.9796 132.9980 -2.9756 232.3062 235.2818 265.0476 133.8158 -2.9790 232.4685 235.4476 265.1829 134.5920 -2.9769 232.7334 235.7104 265.2588 135.4400 -2.9759 232.8561 235.8320 265.3593 136.1758 -2.9783 232.9682 235.9465 265.4502 137.0338 -2.9791 233.0663 236.0454 265.5561 137.7898 -2.9721 233.1129 236.0850 265.6021 138.6075 -2.9748 233.2823 236.2570 265.6699 139.4040 -2.9726 233.4293 236.4018 265.7594 140.2010 -2.9607 233.5088 236.4695 265.9025 141.0188 -2.9600 233.6294 236.5895 266.0274 141.7843 -2.9637 233.7595 236.7232 266.1303 142.6430 -2.9624 233.9231 236.8855 266.2042 143.3683 -2.9715 234.0184 236.9899 266.2338 144.2263 -2.9788 234.1717 237.1505 266.4024 144.9928 -2.9793 234.3923 237.3716 266.4944 145.8105 -2.9883 234.5185 237.5068 266.5401 146.6068 -2.9847 234.6324 237.6171 266.6631 147.4040 -2.9805 234.8179 237.7984 266.8132 148.2218 -2.9691 234.8711 237.8402 266.9703 148.9975 -2.9729 234.9007 237.8736 267.0464 149.8460 -2.9723 235.1245 238.0968 267.2591 150.6123 -2.9702 235.3079 238.2781 267.3580 151.4395 -2.9660 235.4551 238.4211 267.5161 152.2368 -2.9624 235.6113 238.5737 267.6569 153.0335 -2.9573 235.8346 238.7919 267.8117 153.8508 -2.9586 235.9097 238.8683 267.8777 154.6173 -2.9572 236.0195 238.9767 267.9701 155.4755 -2.9592 236.2223 239.1815 268.1074 156.2313 -2.9672 236.3223 239.2895 268.1925 157.0695 -2.9626 236.4367 239.3992 268.3113 157.8558 -2.9607 236.6001 239.5608 268.4533 158.6528 -2.9572 236.6766 239.6338 268.6334 159.4500 -2.9694 236.8097 239.7791 268.7416 160.2463 -2.9728 236.9338 239.9066 268.8780 161.0743 -2.9633 237.1173 240.0806 268.9912 161.8303 -2.9587 237.1517 240.1104 269.0989 162.6985 -2.9584 237.2097 240.1681 269.1841 163.4548 -2.9536 237.3595 240.3131 269.2395 164.2825 -2.9491 237.4813 240.4304 269.4333 165.0790 -2.9537 237.6137 240.5674 269.6310 165.8763 -2.9538 237.7329 240.6867 269.8675 166.7043 -2.9644 237.8811 240.8455 270.0244 167.4595 -2.9749 237.9858 240.9608 270.1141 168.3285 -2.9687 238.0720 241.0407 270.2781 169.0843 -2.9757 238.1883 241.1640 270.3074 169.9118 -2.9767 238.3542 241.3309 270.3813 170.7090 -2.9696 238.4832 241.4528 270.5490 171.5060 -2.9767 238.6060 241.5827 270.6860 172.3333 -2.9701 238.8167 241.7868 270.8468 173.0895 -2.9595 238.9811 241.9406 270.9999 173.9583 -2.9520 239.1603 242.1123 271.1082 174.7138 -2.9613 239.3140 242.2752 271.2056 175.5520 -2.9593 239.3856 242.3449 271.3168 176.3390 -2.9583 239.5341 242.4924 271.4835 177.1455 -2.9602 239.6886 242.6488 271.6444 177.9633 -2.9508 239.8786 242.8293 271.6663 178.7295 -2.9429 239.9616 242.9045 271.7928 179.5875 -2.9397 240.0178 242.9575 271.9399 180.3540 -2.9264 240.0445 242.9708 272.0926 181.1818 -2.9280 240.1288 243.0568 272.1941 181.9680 -2.9314 240.3807 243.3121 272.4102 182.7755 -2.9353 240.5083 243.4437 272.5251 183.6030 -2.9404 240.6327 243.5732 272.6325 184.3690 -2.9479 240.7764 243.7243 272.7446 185.2175 -2.9496 240.9345 243.8842 272.8336 185.9935 -2.9484 241.1036 244.0520 272.9098 186.8110 -2.9512 241.3143 244.2655 273.1189 187.6185 -2.9499 241.5097 244.4596 273.2750 188.4048 -2.9635 241.5528 244.5164 273.4484 189.2428 -2.9678 241.7198 244.6876 273.5281 189.9990 -2.9684 241.8541 244.8225 273.6167 190.8568 -2.9652 241.9394 244.9046 273.7115 191.6233 -2.9668 241.9765 244.9433 273.8767 192.4613 -2.9690 242.0642 245.0332 274.0860 193.2475 -2.9738 242.2180 245.1918 274.2467 194.0448 -2.9672 242.3239 245.2911 274.3347 194.8723 -2.9677 242.4627 245.4304 274.4118 195.6383 -2.9642 242.6133 245.5775 274.5604 196.4970 -2.9629 242.7502 245.7130 274.7413 197.2525 -2.9655 242.9130 245.8785 274.8401 198.0905 -2.9683 243.1376 246.1058 274.9815 198.8775 -2.9683 243.2617 246.2299 275.1138 199.6740 -2.9642 243.3457 246.3099 275.3005 200.5018 -2.9714 243.4132 246.3845 275.4998 201.2580 -2.9804 243.6043 246.5848 275.5816 202.0748 -2.9887 243.7701 246.7588 275.6847 202.8515 -2.9843 243.9841 246.9684 275.8102 203.7000 -2.9794 244.0961 247.0755 276.0256 204.4553 -2.9849 244.2255 247.2104 276.2015 205.2833 -2.9837 244.2700 247.2536 276.3806 206.0700 -2.9858 244.3365 247.3223 276.4848 206.8665 -2.9906 244.4760 247.4666 276.6185 207.6945 -3.0027 244.6125 247.6151 276.6685 208.4605 -3.0033 244.7363 247.7395 276.8076 209.3085 -3.0013 244.9024 247.9037 276.9005 210.0750 -3.0010 245.0414 248.0424 277.0286 210.9025 -3.0004 245.2214 248.2217 277.2432 211.6890 -3.0006 245.2760 248.2766 277.3836 212.4863 -2.9947 245.4170 248.4118 277.4815 213.3133 -2.9871 245.6404 248.6275 277.5622 214.0695 -2.9946 245.7734 248.7679 277.6757 214.9385 -3.0062 245.9948 249.0010 277.8614 215.6938 -3.0061 246.1042 249.1103 277.9616 216.5115 -3.0028 246.3118 249.3146 278.1313 217.3188 -2.9966 246.3678 249.3644 278.3545 218.1050 -2.9916 246.4854 249.4770 278.5482 218.9023 -3.0010 246.5721 249.5731 278.6823 219.6993 -3.0112 246.7322 249.7435 278.8488 220.5265 -3.0049 246.8789 249.8838 278.9492 221.2930 -2.9927 247.0008 249.9935 279.0950 222.1410 -2.9910 247.1648 250.1558 279.2544 222.9173 -3.0021 247.3158 250.3179 279.3424 223.7350 -3.0086 247.4777 250.4863 279.5006 224.5315 -2.9930 247.5724 250.5653 279.6238 225.3285 -2.9975 247.7288 250.7263 279.6729 226.1565 -3.0032 247.9219 250.9251 279.8095 226.9223 -2.9975 248.0160 251.0135 279.9101 227.7398 -2.9991 248.1082 251.1073 279.9795 228.5165 -3.0080 248.2489 251.2570 280.1229 229.3640 -3.0114 248.3531 251.3646 280.2165 230.1305 -3.0057 248.5301 251.5358 280.3215 230.9585 -3.0005 248.7294 251.7300 280.5563 231.7548 -2.9991 248.8456 251.8447 280.7066 232.5520 -3.0000 248.9953 251.9954 280.9179 233.3800 -3.0022 249.1136 252.1157 280.9384 234.1458 -2.9966 249.2116 252.2082 280.9989 235.0043 -3.0054 249.2517 252.2572 281.1201 235.7708 -3.0087 249.3449 252.3536 281.2324 236.5875 -3.0066 249.5746 252.5811 281.3940 237.3643 -3.0035 249.7610 252.7645 281.5402 238.1818 -3.0131 249.8688 252.8819 281.5248 238.9783 -3.0200 249.9051 252.9251 281.6335 239.7755 -3.0223 250.0813 253.1036 281.7779 240.6033 -3.0221 250.2148 253.2369 281.9337 241.3690 -3.0162 250.3026 253.3188 282.0719 242.2175 -3.0131 250.5832 253.5962 282.1627 242.9938 -3.0010 250.8215 253.8225 282.2065 243.8110 -3.0035 250.9429 253.9464 282.3981 244.6083 -3.0058 250.9396 253.9454 282.4367 245.4048 -2.9965 251.0587 254.0551 282.5395 246.2325 -2.9889 251.1734 254.1623 282.7686 246.9990 -2.9891 251.1835 254.1726 282.8579 247.8568 -2.9933 251.4335 254.4267 283.0627 248.6233 -2.9979 251.5890 254.5869 283.2563 249.4513 -2.9965 251.7486 254.7450 283.3919 250.2475 -2.9883 251.9004 254.8887 283.5332 251.0345 -2.9976 252.0375 255.0352 283.6960 251.8728 -2.9988 252.1162 255.1150 283.7981 252.6280 -2.9903 252.1861 255.1763 283.9059 253.4868 -2.9856 252.1389 255.1245 284.1010 254.2530 -2.9844 252.1540 255.1384 284.2384 255.0803 -2.9783 252.3259 255.3043 284.3725 255.8775 -2.9850 252.5613 255.5464 284.4861 256.6640 -2.9849 252.7741 255.7590 284.5750 257.5018 -2.9879 252.8975 255.8854 284.6462 258.2683 -2.9799 253.1257 256.1056 284.7789 259.1260 -2.9745 253.1906 256.1651 284.9448 259.8823 -2.9716 253.3259 256.2975 285.1026 260.7203 -2.9777 253.4793 256.4570 285.2229 261.5065 -2.9826 253.6436 256.6261 285.3063 262.3038 -2.9876 253.7868 256.7744 285.4777 263.1313 -2.9844 253.8173 256.8016 285.5744 263.8973 -2.9818 253.9719 256.9537 285.7266 264.7458 -2.9754 254.1309 257.1063 285.8349 265.4808 -2.9632 254.2846 257.2478 285.9463 266.3290 -2.9661 254.5107 257.4768 286.1629 267.0955 -2.9654 254.5719 257.5374 286.3617 267.9225 -2.9586 254.7329 257.6915 286.5647 268.7095 -2.9619 254.8955 257.8574 286.7174 269.5065 -2.9680 255.0475 258.0155 286.9002 270.3338 -2.9898 255.1830 258.1727 287.0840 271.0900 -3.0000 255.3101 258.3102 287.1592 271.9483 -3.0001 255.4514 258.4515 287.1491 272.7143 -2.9884 255.6637 258.6521 287.2328 273.5320 -2.9935 255.8399 258.8334 287.3797 274.3285 -2.9902 255.9457 258.9359 287.4621 275.1255 -2.9829 256.0672 259.0501 287.5841 275.9535 -2.9967 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