DTA measure 1Pb_updown4 Date: 2026923:1016 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.17 s Mass = 1178.700 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2943 -1.9149 220.8041 222.7190 249.3139 2.0505 -1.9005 220.9523 222.8528 249.3736 2.9103 -1.9195 221.0468 222.9663 249.1121 3.6460 -1.8918 221.2341 223.1259 248.9946 4.4945 -1.8989 221.1843 223.0832 249.0712 5.2713 -1.9340 221.3575 223.2914 248.9238 6.0890 -1.9452 221.4789 223.4241 248.8644 6.8760 -1.9457 221.4881 223.4338 248.7082 7.6835 -1.9281 221.6581 223.5862 248.8345 8.5013 -1.9467 221.6677 223.6145 248.7602 9.2575 -1.9514 221.7679 223.7193 248.7279 10.1268 -1.9690 221.8841 223.8531 248.7179 10.8835 -1.9537 221.8435 223.7972 248.7105 11.7118 -1.9475 221.9423 223.8898 248.7483 12.4783 -1.9363 222.1073 224.0436 248.5502 13.2960 -1.9204 222.3123 224.2327 248.5056 14.0933 -1.9132 222.4177 224.3309 248.2857 14.8905 -1.9372 222.5491 224.4863 248.2462 15.7185 -1.9200 222.6462 224.5663 248.2759 16.4850 -1.9030 222.7714 224.6745 248.2259 17.3335 -1.8816 222.9069 224.7885 248.4208 18.1105 -1.8843 222.9149 224.7992 248.3643 18.9290 -1.8833 223.0205 224.9037 248.4417 19.7263 -1.8987 223.1192 225.0180 248.4133 20.5235 -1.8896 223.1537 225.0434 248.2229 21.3208 -1.8660 223.3397 225.2056 248.1312 22.1180 -1.8700 223.5333 225.4032 248.2163 22.9358 -1.8712 223.7009 225.5721 248.0839 23.7125 -1.8878 223.8506 225.7384 248.1957 24.5620 -1.8928 223.9195 225.8123 248.0487 25.3285 -1.8607 224.0142 225.8749 248.2308 26.1565 -1.8431 224.0913 225.9344 248.2648 26.9538 -1.8497 224.2465 226.0962 248.2042 27.7510 -1.8629 224.3440 226.2069 248.3203 28.5688 -1.8579 224.3332 226.1911 248.4447 29.3455 -1.8674 224.4165 226.2839 248.7002 30.1940 -1.8484 224.5009 226.3493 248.7686 30.9400 -1.8436 224.5448 226.3884 248.7411 31.7885 -1.8411 224.5975 226.4387 248.8199 32.5655 -1.8315 224.5406 226.3721 248.8541 33.3840 -1.8250 224.6267 226.4517 248.7858 34.1813 -1.8415 224.7032 226.5447 248.7146 34.9785 -1.8633 224.7998 226.6631 248.6193 35.8065 -1.8687 224.9995 226.8682 248.6506 36.5730 -1.8667 225.1782 227.0449 248.6466 37.4215 -1.8657 225.4211 227.2868 248.9071 38.1983 -1.8405 225.4817 227.3221 248.8954 39.0160 -1.8555 225.4792 227.3347 248.9296 39.8143 -1.8620 225.6624 227.5244 248.9576 40.6115 -1.8505 225.8280 227.6785 248.9933 41.4498 -1.8519 225.9316 227.7835 249.1334 42.2060 -1.8361 226.1051 227.9412 249.4224 43.0648 -1.8483 226.2086 228.0569 249.6574 43.8313 -1.8722 226.3370 228.2092 249.6065 44.6593 -1.8796 226.4375 228.3172 249.6850 45.4565 -1.8573 226.6753 228.5326 249.6552 46.2435 -1.8301 226.7577 228.5878 249.7618 47.0818 -1.8315 226.9031 228.7346 249.7188 47.8383 -1.8347 226.9564 228.7910 249.8046 48.6670 -1.8240 226.9452 228.7692 249.9366 49.4335 -1.8229 226.9040 228.7269 250.1654 50.2923 -1.8042 226.9939 228.7981 250.3502 51.0588 -1.7767 227.0574 228.8341 250.4530 51.8765 -1.7610 227.2131 228.9740 250.5692 52.6840 -1.7866 227.2618 229.0484 250.7404 53.4710 -1.7849 227.3999 229.1848 250.9581 54.2990 -1.7830 227.5645 229.3475 251.0689 55.0658 -1.7896 227.8344 229.6240 251.1044 55.9253 -1.7907 227.9158 229.7065 251.0404 56.7225 -1.7894 227.9757 229.7650 251.2760 57.5095 -1.8110 228.1112 229.9222 251.4155 58.3478 -1.7981 228.3729 230.1710 251.5607 59.1040 -1.7884 228.2960 230.0843 251.7386 59.9525 -1.8161 228.3873 230.2034 251.8661 60.7190 -1.8368 228.5220 230.3588 251.8067 61.5470 -1.8392 228.7161 230.5553 252.0579 62.3340 -1.8245 228.8400 230.6645 252.2032 63.1313 -1.8346 228.8625 230.6971 252.3296 63.9490 -1.8322 228.8917 230.7239 252.4648 64.7155 -1.8195 229.0045 230.8241 252.5493 65.5753 -1.7936 229.0511 230.8446 252.7176 66.3008 -1.7677 229.1635 230.9312 252.7867 67.1595 -1.7591 229.2085 230.9676 252.9403 67.9158 -1.7481 229.2003 230.9484 253.2137 68.7438 -1.7413 229.2223 230.9636 253.3906 69.5410 -1.7402 229.3358 231.0760 253.5689 70.3383 -1.7390 229.5284 231.2674 253.8113 71.1560 -1.7548 229.6922 231.4470 254.0170 71.9328 -1.7588 229.8931 231.6519 254.0440 72.7510 -1.7681 230.0070 231.7751 254.1351 73.5488 -1.7870 229.9748 231.7618 254.1866 74.3768 -1.7871 230.0348 231.8219 254.2463 75.1330 -1.7933 229.9845 231.7778 254.3111 75.9918 -1.7832 229.9015 231.6847 254.6082 76.7583 -1.7753 230.0419 231.8172 254.7579 77.5760 -1.7864 230.2259 232.0123 254.9963 78.3733 -1.7925 230.4575 232.2500 255.2893 79.1705 -1.8099 230.5603 232.3702 255.4599 79.9985 -1.7997 230.6594 232.4590 255.6283 80.7650 -1.8152 230.8417 232.6569 255.7538 81.5828 -1.7964 230.9013 232.6978 256.0101 82.3605 -1.8034 230.9750 232.7785 256.2380 83.2090 -1.8211 231.1212 232.9422 256.5246 83.9755 -1.8156 231.2062 233.0218 256.6587 84.8035 -1.8305 231.3183 233.1488 256.7007 85.6008 -1.8322 231.4347 233.2669 256.8232 86.3980 -1.8365 231.6108 233.4473 256.8023 87.2158 -1.8445 231.7072 233.5517 256.8097 87.9925 -1.8474 231.6980 233.5454 256.9054 88.8420 -1.8584 231.8488 233.7072 257.0446 89.5880 -1.8639 231.9724 233.8363 257.1046 90.4365 -1.8574 232.1755 234.0329 257.1491 91.2133 -1.8468 232.2177 234.0645 257.1862 92.0310 -1.8147 232.1531 233.9677 257.2769 92.8180 -1.8079 232.0993 233.9072 257.2398 93.6255 -1.7977 232.1284 233.9262 257.2265 94.4433 -1.8010 232.2246 234.0256 257.4253 95.2098 -1.8038 232.3983 234.2020 257.5246 96.0695 -1.8038 232.7571 234.5609 257.6825 96.8360 -1.8095 232.9122 234.7217 257.8988 97.6640 -1.8174 233.0443 234.8617 258.1866 98.4510 -1.8372 232.9413 234.7785 258.3926 99.2585 -1.8274 232.8848 234.7122 258.7200 100.0763 -1.8214 232.9654 234.7868 258.9303 100.8428 -1.8398 233.1088 234.9487 258.8682 101.7015 -1.7995 233.2174 235.0169 258.8883 102.4680 -1.8137 233.2445 235.0582 258.9703 103.2968 -1.8132 233.3733 235.1865 259.1057 104.0840 -1.8055 233.4771 235.2826 259.2280 104.8915 -1.7917 233.6500 235.4417 259.1638 105.6785 -1.8085 233.6840 235.4926 259.3279 106.4758 -1.8181 233.7000 235.5181 259.3727 107.3038 -1.8080 233.8086 235.6166 259.5141 108.0703 -1.8077 233.8907 235.6984 259.6802 108.9290 -1.8398 233.9462 235.7860 259.8355 109.6853 -1.8404 234.0263 235.8667 260.0219 110.5238 -1.8576 234.1790 236.0366 260.0857 111.3115 -1.8556 234.4274 236.2830 260.2395 112.1088 -1.8437 234.4885 236.3322 260.2129 112.9368 -1.8341 234.5922 236.4263 260.2863 113.7135 -1.8108 234.7243 236.5351 260.4841 114.5620 -1.8143 234.9001 236.7143 260.6375 115.3285 -1.8151 234.9674 236.7825 260.6576 116.1565 -1.8110 235.0252 236.8362 260.6937 116.9538 -1.8174 235.0484 236.8658 260.7105 117.7510 -1.8423 235.2002 237.0425 260.7825 118.5688 -1.8441 235.2945 237.1385 261.0999 119.3460 -1.8257 235.4252 237.2510 261.2750 120.1643 -1.8168 235.4669 237.2837 261.3210 120.9308 -1.8141 235.6888 237.5029 261.3087 121.7895 -1.8272 235.8184 237.6457 261.2379 122.5560 -1.8183 235.9761 237.7944 261.2584 123.3738 -1.8227 236.0474 237.8700 261.4181 124.1710 -1.8060 236.1187 237.9247 261.6650 124.9580 -1.8203 236.1310 237.9513 261.8323 125.7758 -1.8226 236.1609 237.9835 261.8460 126.5530 -1.8417 236.3500 238.1917 261.8783 127.4020 -1.8332 236.5254 238.3586 261.9385 128.1583 -1.8309 236.5742 238.4051 261.8871 128.9863 -1.8445 236.6366 238.4810 261.8926 129.7835 -1.8316 236.6501 238.4817 261.9394 130.5705 -1.8551 236.7857 238.6409 261.9527 131.3985 -1.8655 236.9961 238.8616 261.9462 132.1650 -1.8421 237.0567 238.8988 262.0185 133.0135 -1.8586 237.2337 239.0923 262.2328 133.7595 -1.8673 237.2943 239.1617 262.3612 134.6090 -1.8966 237.2657 239.1622 262.4744 135.3755 -1.8905 237.4334 239.3238 262.6674 136.2035 -1.9074 237.5150 239.4224 262.7899 136.9905 -1.8903 237.5135 239.4038 262.9672 137.7878 -1.8810 237.5845 239.4654 263.0229 138.6158 -1.8630 237.7175 239.5805 263.2536 139.3823 -1.8624 238.0365 239.8989 263.4843 140.2308 -1.8640 238.2148 240.0788 263.5811 140.9978 -1.8468 238.2511 240.0980 263.6067 141.8263 -1.8414 238.4396 240.2810 263.7454 142.6235 -1.8203 238.4789 240.2992 263.8691 143.4105 -1.8131 238.4666 240.2797 263.9625 144.2488 -1.8189 238.5564 240.3753 264.0728 145.0050 -1.8328 238.8238 240.6566 264.0038 145.8535 -1.8678 238.8940 240.7617 263.9010 146.6303 -1.8810 238.9121 240.7930 263.9489 147.4480 -1.8932 239.0047 240.8979 264.0255 148.2453 -1.8779 239.0091 240.8870 264.0046 149.0430 -1.8680 239.0674 240.9354 264.1446 149.8715 -1.8914 239.1817 241.0731 264.2495 150.6380 -1.9126 239.1711 241.0837 264.1999 151.4558 -1.9121 239.3154 241.2275 264.2536 152.2325 -1.8897 239.4256 241.3153 264.3946 153.0810 -1.8836 239.5084 241.3920 264.6593 153.8475 -1.9081 239.7973 241.7053 264.8456 154.6755 -1.9178 240.1187 242.0365 264.8606 155.4728 -1.8903 240.2349 242.1252 264.9484 156.2700 -1.8871 240.1569 242.0440 265.1546 157.0883 -1.8768 240.2958 242.1726 265.2636 157.8655 -1.8856 240.4496 242.3352 265.4225 158.7140 -1.9041 240.7879 242.6920 265.4708 159.4805 -1.8870 241.0685 242.9555 265.4328 160.3085 -1.9045 241.2644 243.1688 265.6118 161.1058 -1.8737 241.2521 243.1258 265.6237 161.9030 -1.8681 241.3496 243.2177 265.5896 162.7208 -1.8585 241.4628 243.3214 265.6839 163.4975 -1.8487 241.3954 243.2441 265.8821 164.3460 -1.8662 241.3245 243.1906 265.9661 165.1125 -1.8433 241.4781 243.3214 266.0546 165.9405 -1.8243 241.6801 243.5044 266.1859 166.7383 -1.8019 241.8657 243.6676 266.3530 167.5360 -1.8071 241.8868 243.6939 266.4514 168.3538 -1.8488 241.9612 243.8100 266.5486 169.1305 -1.8574 242.3660 244.2234 266.6925 169.9790 -1.8602 242.4175 244.2777 266.8267 170.7455 -1.8489 242.4105 244.2594 266.8931 171.5735 -1.8501 242.4589 244.3090 267.2350 172.3710 -1.8599 242.4416 244.3016 267.3299 173.1688 -1.8645 242.5417 244.4062 267.6188 173.9868 -1.8665 242.7083 244.5748 267.6752 174.7635 -1.8798 242.8122 244.6920 267.6885 175.6120 -1.8925 242.7467 244.6392 267.9595 176.3785 -1.8922 242.9933 244.8855 267.9954 177.2065 -1.8869 243.2834 245.1703 268.0589 178.0038 -1.9005 243.2361 245.1365 268.1104 178.8010 -1.9033 243.2527 245.1560 268.1667 179.6193 -1.9008 243.2705 245.1713 268.3834 180.3958 -1.9087 243.2203 245.1290 268.4669 181.2450 -1.8897 243.4398 245.3295 268.3704 182.0115 -1.8961 243.4876 245.3837 268.6161 182.8395 -1.9084 243.5177 245.4260 268.9531 183.6368 -1.9093 243.6816 245.5909 269.2176 184.4340 -1.9141 243.7960 245.7101 269.4870 185.2518 -1.9198 244.1421 246.0619 269.4582 186.0285 -1.9290 244.1956 246.1247 269.4635 186.8770 -1.9410 244.4019 246.3429 269.5282 187.6435 -1.9242 244.3548 246.2790 269.6499 188.4715 -1.9040 244.4129 246.3169 269.5745 189.2590 -1.9037 244.3672 246.2708 269.5706 190.0465 -1.8720 244.3463 246.2183 269.6912 190.8745 -1.8882 244.5526 246.4407 269.8177 191.6410 -1.8950 244.6711 246.5662 269.7890 192.4895 -1.9025 244.8128 246.7153 269.7074 193.2253 -1.9057 244.8293 246.7349 269.9014 194.0738 -1.9186 244.8633 246.7819 270.0932 194.8403 -1.9230 244.9832 246.9062 270.1774 195.6683 -1.9030 245.2510 247.1540 270.1546 196.4553 -1.8972 245.4137 247.3109 270.3040 197.2525 -1.9017 245.6269 247.5286 270.4003 198.0813 -1.8868 245.7585 247.6452 270.5897 198.8480 -1.8646 245.9786 247.8431 270.8003 199.6658 -1.8754 246.0836 247.9590 270.9743 200.4323 -1.8801 246.2735 248.1536 271.1181 201.2910 -1.8887 246.3389 248.2277 271.1538 202.0473 -1.9056 246.3644 248.2701 271.0838 202.8753 -1.9263 246.3536 248.2799 271.2558 203.6725 -1.9339 246.3194 248.2533 271.3738 204.4595 -1.9358 246.4334 248.3692 271.4617 205.2978 -1.9454 246.4204 248.3658 271.5539 206.0548 -1.9535 246.4303 248.3838 271.7452 206.9035 -1.9542 246.4463 248.4005 271.8635 207.6803 -1.9503 246.6756 248.6259 272.0275 208.4980 -1.9441 246.7550 248.6991 272.2411 209.2953 -1.9666 246.9107 248.8773 272.2340 210.0925 -1.9711 246.8671 248.8382 272.2173 210.8898 -1.9586 247.0356 248.9941 272.3268 211.6870 -1.9489 247.1110 249.0600 272.5212 212.5048 -1.9546 247.2843 249.2388 272.7473 213.2815 -1.9758 247.4246 249.4005 272.6995 214.1300 -1.9896 247.6619 249.6515 272.7134 214.8965 -1.9614 247.9572 249.9186 272.8750 215.7255 -1.9607 247.8620 249.8227 273.0000 216.5125 -1.9687 247.9111 249.8799 272.9330 217.3098 -1.9579 247.9114 249.8693 273.1082 218.1378 -1.9788 248.0651 250.0440 273.4227 218.9043 -1.9712 248.1476 250.1188 273.5980 219.7630 -1.9357 248.3365 250.2722 273.7458 220.5193 -1.9365 248.4382 250.3747 273.7106 221.3575 -1.9541 248.5687 250.5228 273.9781 222.1140 -1.9794 248.6437 250.6231 274.0795 222.9418 -1.9906 248.7731 250.7636 274.2177 223.7398 -1.9715 248.8464 250.8179 274.3539 224.5373 -1.9092 248.8561 250.7653 274.2787 225.3653 -1.8983 249.0892 250.9875 274.2041 226.1215 -1.9344 249.1003 251.0348 274.2168 226.9905 -1.9560 249.3176 251.2737 274.2447 227.7468 -1.9787 249.4084 251.3872 274.3724 228.5748 -1.9792 249.4356 251.4149 274.5011 229.3720 -1.9739 249.4814 251.4553 274.5718 230.1703 -1.9890 249.4660 251.4550 274.7047 230.9983 -1.9608 249.7081 251.6689 274.6943 231.7545 -1.9484 249.8748 251.8232 274.7148 232.6235 -1.9574 250.1564 252.1138 274.8700 233.3798 -1.9369 250.3395 252.2765 275.0436 234.2078 -1.9492 250.4767 252.4259 275.2998 234.9743 -1.9659 250.5444 252.5103 275.2767 235.8023 -1.9579 250.7655 252.7234 275.3581 236.5995 -1.9453 251.0103 252.9556 275.5043 237.3865 -1.9440 251.0199 252.9639 275.6802 238.2248 -1.9579 251.0126 252.9705 275.8098 238.9818 -1.9720 251.1062 253.0782 275.9085 239.8408 -1.9772 251.1516 253.1289 276.0039 240.6073 -1.9564 251.1972 253.1536 276.1456 241.4353 -1.9255 251.1928 253.1183 276.2851 242.2325 -1.9031 251.3243 253.2273 276.2955 243.0195 -1.9028 251.4509 253.3537 276.4385 243.8578 -1.9272 251.5114 253.4386 276.5197 244.6140 -1.9474 251.5807 253.5282 276.6581 245.4738 -1.9729 251.5891 253.5621 276.9524 246.2403 -1.9854 251.5949 253.5802 277.0262 247.0785 -1.9818 251.5219 253.5036 277.1395 247.8655 -1.9736 251.7571 253.7307 277.1797 248.6628 -1.9682 251.8089 253.7770 277.1328 249.4908 -1.9567 251.9963 253.9530 277.1453 250.2573 -1.9283 252.1481 254.0764 277.2250 251.1160 -1.9289 252.4277 254.3565 277.4706 251.8725 -1.9647 252.3406 254.3053 277.6986 252.7010 -1.9760 252.5357 254.5117 277.7477 253.4880 -1.9793 252.8857 254.8650 277.9227 254.2855 -2.0046 253.0798 255.0844 278.0586 255.1135 -1.9911 253.0299 255.0210 278.1405 255.8698 -1.9656 253.0281 254.9936 278.1920 256.7285 -1.9666 253.2303 255.1969 278.1000 257.4540 -1.9506 253.2992 255.2498 278.2706 258.3128 -1.9551 253.3811 255.3361 278.3679 259.0793 -1.9477 253.4160 255.3637 278.4200 259.8970 -1.9287 253.5473 255.4760 278.4342 260.6943 -1.9320 253.6965 255.6286 278.4789 261.4918 -1.9124 253.6183 255.5307 278.4134 262.3103 -1.9048 253.7446 255.6494 278.5800 263.0768 -1.9307 253.8850 255.8157 278.9377 263.9355 -1.9714 253.9783 255.9497 279.1590 264.6918 -1.9865 254.0646 256.0510 279.2522 265.5198 -1.9700 254.2231 256.1931 279.2574 266.3170 -1.9464 254.2778 256.2242 279.3379 267.1040 -1.9529 254.3165 256.2694 279.5314 267.9320 -1.9787 254.4193 256.3980 279.5299 268.6985 -2.0048 254.5020 256.5068 279.4436 269.5573 -1.9746 254.6755 256.6501 279.6041 270.3143 -1.9816 254.9828 256.9643 279.8609 271.1425 -1.9820 255.1707 257.1527 279.7615 271.9398 -1.9758 255.1688 257.1446 280.0000 272.7370 -1.9757 255.1531 257.1287 280.0662 273.5548 -1.9735 255.1667 257.1402 280.1689 274.3315 -1.9717 255.1569 257.1286 280.2261 275.1800 -1.9813 255.2877 257.2690 280.4577 275.9158 -1.9856 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