DTA measure 1gyors Date: 2026317:1056 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.67 s Mass = 1173.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2513 -3.9693 184.3660 188.3354 247.2604 2.0683 -3.9566 184.6485 188.6051 247.2203 2.8653 -3.9390 184.8925 188.8315 247.1584 3.6625 -3.9279 185.1352 189.0631 247.1031 4.4895 -3.9189 185.4004 189.3193 247.0469 5.2560 -3.9043 185.6674 189.5717 246.9825 6.1045 -3.8865 185.9440 189.8305 246.8849 6.8803 -3.8734 186.2081 190.0815 246.8586 7.7083 -3.8567 186.4136 190.2703 246.7958 8.5055 -3.8388 186.6380 190.4768 246.6963 9.3018 -3.8233 186.8870 190.7103 246.6355 10.0990 -3.8093 187.1773 190.9866 246.5923 10.8963 -3.7965 187.4013 191.1978 246.5299 11.7233 -3.7848 187.6699 191.4547 246.4785 12.4898 -3.7713 187.9217 191.6930 246.4187 13.3485 -3.7607 188.1928 191.9535 246.3623 14.1140 -3.7554 188.4406 192.1960 246.3356 14.9420 -3.7433 188.7003 192.4437 246.2759 15.7288 -3.7301 188.9379 192.6680 246.2598 16.5355 -3.7176 189.1714 192.8890 246.1770 17.3533 -3.6990 189.4587 193.1577 246.1186 18.1195 -3.6862 189.7109 193.3971 246.0605 18.9775 -3.6775 189.9383 193.6159 246.0535 19.7543 -3.6667 190.1247 193.7914 246.0294 20.5720 -3.6521 190.3572 194.0093 246.0188 21.3683 -3.6417 190.5843 194.2260 246.0047 22.1655 -3.6323 190.8498 194.4821 245.9764 22.9935 -3.6192 191.1002 194.7194 245.9641 23.7595 -3.6070 191.3336 194.9407 245.9432 24.6178 -3.5907 191.6199 195.2106 245.9701 25.3535 -3.5718 191.8385 195.4103 246.0001 26.2115 -3.5502 192.0975 195.6477 246.0255 26.9778 -3.5322 192.2959 195.8281 246.0088 27.8058 -3.5177 192.5243 196.0419 246.0687 28.6023 -3.5051 192.7427 196.2479 246.0913 29.3993 -3.4913 192.9510 196.4422 246.1067 30.2273 -3.4799 193.2128 196.6927 246.1675 30.9835 -3.4719 193.4257 196.8976 246.2240 31.8518 -3.4616 193.6764 197.1381 246.2904 32.6078 -3.4499 193.9025 197.3524 246.3534 33.4460 -3.4348 194.1553 197.5902 246.4324 34.2320 -3.4231 194.3915 197.8146 246.5102 35.0293 -3.4157 194.6428 198.0585 246.5888 35.8470 -3.4060 194.8686 198.2745 246.6724 36.6128 -3.3925 195.0741 198.4665 246.7286 37.4610 -3.3764 195.3168 198.6932 246.8238 38.2275 -3.3623 195.5465 198.9088 246.9135 39.0545 -3.3488 195.7844 199.1332 247.0330 39.8210 -3.3359 195.9799 199.3158 247.1486 40.6383 -3.3206 196.1916 199.5122 247.2560 41.4350 -3.3097 196.4242 199.7339 247.3963 42.2220 -3.2958 196.6139 199.9097 247.5748 43.0500 -3.2884 196.8318 200.1201 247.7122 43.8158 -3.2799 197.0454 200.3253 247.8361 44.6640 -3.2679 197.2876 200.5555 248.0024 45.4305 -3.2551 197.4876 200.7426 248.1696 46.2578 -3.2409 197.7400 200.9810 248.3409 47.0548 -3.2259 197.9755 201.2014 248.4874 47.8520 -3.2178 198.2320 201.4498 248.6265 48.6688 -3.2013 198.4721 201.6733 248.7540 49.4353 -3.1858 198.6764 201.8623 248.8902 50.2940 -3.1710 198.9051 202.0761 249.0656 51.0495 -3.1644 199.1293 202.2936 249.2506 51.8875 -3.1516 199.3431 202.4948 249.4241 52.6745 -3.1410 199.5561 202.6971 249.5719 53.4713 -3.1255 199.7831 202.9086 249.7259 54.2988 -3.1092 200.0106 203.1198 249.9278 55.0653 -3.1036 200.2138 203.3174 250.0869 55.9233 -3.0937 200.3985 203.4922 250.2664 56.6793 -3.0865 200.6262 203.7127 250.4717 57.5175 -3.0763 200.8633 203.9395 250.6958 58.2733 -3.0691 201.0952 204.1643 250.9176 59.1110 -3.0640 201.2810 204.3450 251.1249 59.8980 -3.0620 201.5077 204.5697 251.3137 60.7050 -3.0509 201.7471 204.7980 251.5282 61.5223 -3.0438 201.9329 204.9767 251.7189 62.2888 -3.0310 202.1365 205.1675 251.9187 63.1470 -3.0217 202.3508 205.3725 252.1251 63.9130 -3.0080 202.5498 205.5578 252.2841 64.7410 -2.9998 202.7630 205.7629 252.4345 65.5278 -2.9920 202.9584 205.9504 252.6210 66.3345 -2.9855 203.1533 206.1388 252.8087 67.1523 -2.9817 203.3665 206.3481 252.9786 67.9183 -2.9785 203.5764 206.5549 253.1691 68.7765 -2.9738 203.8082 206.7820 253.3789 69.5430 -2.9669 204.0169 206.9838 253.5040 70.3705 -2.9624 204.2722 207.2346 253.7360 71.1570 -2.9553 204.4648 207.4200 253.9237 71.9645 -2.9490 204.6559 207.6048 254.1378 72.7920 -2.9393 204.8924 207.8317 254.3497 73.5580 -2.9325 205.0805 208.0130 254.5346 74.4065 -2.9229 205.2693 208.1922 254.7356 75.1828 -2.9185 205.4831 208.4016 254.9049 76.0000 -2.9147 205.6850 208.5997 255.0570 76.8075 -2.9109 205.8941 208.8050 255.2466 77.5943 -2.9054 206.1003 209.0057 255.4205 78.4010 -2.8952 206.3002 209.1954 255.5907 79.1880 -2.8867 206.5047 209.3914 255.7843 80.0263 -2.8812 206.7154 209.5965 255.9734 80.7815 -2.8706 206.9156 209.7862 256.1358 81.6505 -2.8652 207.1201 209.9853 256.3175 82.4068 -2.8574 207.3036 210.1610 256.4854 83.2443 -2.8490 207.4895 210.3385 256.6822 84.0310 -2.8446 207.7158 210.5604 256.8764 84.8385 -2.8411 207.9399 210.7810 257.0365 85.6555 -2.8340 208.1513 210.9853 257.1838 86.4218 -2.8276 208.3246 211.1522 257.3297 87.2805 -2.8190 208.5439 211.3629 257.5150 88.0460 -2.8111 208.7174 211.5285 257.6621 88.8740 -2.7961 208.8785 211.6747 257.8004 89.6610 -2.7870 209.0278 211.8147 257.9535 90.4680 -2.7762 209.2534 212.0296 258.0880 91.2955 -2.7664 209.4802 212.2466 258.2181 92.0620 -2.7608 209.6711 212.4319 258.2858 92.9098 -2.7572 209.8898 212.6470 258.4446 93.6555 -2.7498 210.0973 212.8471 258.5940 94.5040 -2.7463 210.2556 213.0020 258.7466 95.2698 -2.7425 210.4397 213.1822 258.8785 96.0975 -2.7458 210.6467 213.3925 259.0205 96.9050 -2.7430 210.8575 213.6006 259.1536 97.6915 -2.7332 211.0452 213.7784 259.2575 98.5088 -2.7270 211.2360 213.9630 259.3646 99.2855 -2.7216 211.4167 214.1382 259.4958 100.1333 -2.7195 211.6645 214.3841 259.6300 100.8585 -2.7185 211.8424 214.5609 259.7404 101.7275 -2.7127 212.0956 214.8083 259.8864 102.4830 -2.7058 212.2844 214.9902 259.9864 103.3005 -2.7025 212.4624 215.1649 260.1066 104.1080 -2.6958 212.6729 215.3688 260.2522 104.8940 -2.6854 212.8750 215.5604 260.3836 105.7118 -2.6785 213.0704 215.7489 260.5076 106.4885 -2.6710 213.2379 215.9090 260.6103 107.3053 -2.6648 213.4478 216.1126 260.7246 108.0718 -2.6594 213.6124 216.2718 260.8398 108.9305 -2.6610 213.8203 216.4813 260.9418 109.6858 -2.6561 213.9907 216.6468 261.0351 110.5138 -2.6502 214.1755 216.8257 261.1658 111.3110 -2.6462 214.3796 217.0258 261.2810 112.1073 -2.6382 214.6048 217.2430 261.4031 112.9250 -2.6327 214.8495 217.4821 261.4840 113.6915 -2.6288 215.0213 217.6500 261.5764 114.5493 -2.6218 215.2157 217.8375 261.6745 115.2850 -2.6220 215.3904 218.0124 261.7775 116.1335 -2.6198 215.5730 218.1928 261.9211 116.9093 -2.6167 215.7405 218.3572 262.0155 117.7270 -2.6117 215.9526 218.5642 262.1439 118.5240 -2.6064 216.1627 218.7691 262.2392 119.3205 -2.6003 216.3351 218.9354 262.3390 120.1485 -2.5955 216.4996 219.0951 262.4459 120.9145 -2.5943 216.6476 219.2419 262.5586 121.7625 -2.5908 216.8528 219.4436 262.6863 122.5393 -2.5787 217.0090 219.5877 262.7714 123.3565 -2.5729 217.1888 219.7617 262.8782 124.1533 -2.5670 217.3806 219.9476 262.9781 124.9505 -2.5663 217.5937 220.1600 263.0919 125.7780 -2.5660 217.7865 220.3525 263.1947 126.5440 -2.5615 217.9611 220.5227 263.3194 127.3720 -2.5593 218.1513 220.7106 263.4478 128.1383 -2.5558 218.3296 220.8854 263.5658 128.9963 -2.5537 218.5225 221.0761 263.6950 129.7628 -2.5491 218.6986 221.2477 263.8347 130.5805 -2.5460 218.8729 221.4189 263.9445 131.3870 -2.5360 219.0982 221.6342 264.0697 132.1740 -2.5322 219.2978 221.8300 264.1798 133.0123 -2.5250 219.4815 222.0065 264.2972 133.7675 -2.5192 219.6661 222.1852 264.4109 134.6365 -2.5121 219.8723 222.3844 264.4936 135.3928 -2.5084 220.0788 222.5872 264.5804 136.2198 -2.5039 220.2548 222.7587 264.7059 137.0170 -2.5038 220.4524 222.9562 264.8522 137.8143 -2.4981 220.6086 223.1067 264.9873 138.6413 -2.4927 220.7559 223.2486 265.1367 139.3975 -2.4894 220.9179 223.4073 265.2864 140.2665 -2.4836 221.1214 223.6050 265.4180 141.0223 -2.4729 221.3201 223.7930 265.5410 141.8498 -2.4668 221.4678 223.9346 265.6317 142.6470 -2.4667 221.6231 224.0898 265.7510 143.4543 -2.4647 221.8000 224.2647 265.8729 144.2405 -2.4625 221.9866 224.4491 266.0144 145.0378 -2.4606 222.1684 224.6290 266.1427 145.8655 -2.4589 222.3734 224.8323 266.2911 146.6313 -2.4588 222.5705 225.0292 266.4072 147.4900 -2.4585 222.7848 225.2433 266.5349 148.2563 -2.4530 222.9086 225.3616 266.6409 149.0835 -2.4464 223.0389 225.4853 266.7596 149.8808 -2.4430 223.1991 225.6421 266.8822 150.6778 -2.4392 223.3938 225.8330 266.9913 151.4948 -2.4301 223.5685 225.9986 267.1525 152.2715 -2.4295 223.7349 226.1643 267.2660 153.1200 -2.4245 223.9306 226.3551 267.3665 153.8855 -2.4196 224.1360 226.5557 267.5142 154.7135 -2.4174 224.2921 226.7095 267.6454 155.5108 -2.4152 224.4871 226.9024 267.7603 156.3075 -2.4054 224.6611 227.0665 267.8705 157.1248 -2.4008 224.8800 227.2808 268.0220 157.9015 -2.3966 225.0431 227.4397 268.1583 158.7595 -2.3909 225.2118 227.6028 268.3153 159.5258 -2.3850 225.3540 227.7391 268.4181 160.3435 -2.3827 225.5495 227.9322 268.5870 161.1503 -2.3546 225.6869 228.0415 268.7047 161.9370 -2.3568 225.8291 228.1859 268.8547 162.7855 -2.3599 226.0430 228.4029 269.0413 163.5308 -2.3570 226.1913 228.5483 269.1821 164.3790 -2.3525 226.3904 228.7429 269.3349 165.1353 -2.3486 226.5581 228.9067 269.4430 165.9623 -2.3466 226.7561 229.1026 269.6020 166.7493 -2.3460 226.9390 229.2850 269.7184 167.5465 -2.3457 227.1657 229.5114 269.8502 168.3735 -2.3438 227.3817 229.7254 270.0164 169.1400 -2.3468 227.5457 229.8925 270.1554 169.9885 -2.3414 227.7380 230.0795 270.2975 170.7540 -2.3362 227.8754 230.2117 270.4587 171.5820 -2.3348 228.0255 230.3603 270.5762 172.3380 -2.3342 228.1820 230.5162 270.7279 173.1653 -2.3326 228.3682 230.7008 270.8915 173.9625 -2.3313 228.5337 230.8650 271.0499 174.7495 -2.3184 228.7092 231.0276 271.1822 175.5868 -2.3188 228.8895 231.2084 271.3548 176.3430 -2.3169 229.0489 231.3658 271.5053 177.2015 -2.3135 229.2111 231.5246 271.6719 177.9365 -2.3125 229.4077 231.7202 271.7918 178.7850 -2.3116 229.5839 231.8955 271.9890 179.5510 -2.3102 229.7857 232.0959 272.1635 180.3785 -2.3030 229.9099 232.2129 272.3239 181.1758 -2.3015 230.0536 232.3551 272.4775 181.9728 -2.2987 230.2424 232.5411 272.6119 182.7898 -2.2994 230.4127 232.7121 272.7510 183.5665 -2.2978 230.5757 232.8735 272.8948 184.4250 -2.2963 230.7719 233.0682 273.0206 185.1600 -2.2945 230.9355 233.2300 273.1427 186.0085 -2.2909 231.1314 233.4223 273.2935 186.7848 -2.2890 231.3015 233.5905 273.4310 187.6020 -2.2840 231.4571 233.7411 273.5980 188.3993 -2.2791 231.6072 233.8863 273.7271 189.1963 -2.2745 231.7872 234.0618 273.8934 190.0235 -2.2740 231.9855 234.2596 274.0270 190.7900 -2.2742 232.1408 234.4150 274.1349 191.6383 -2.2726 232.2824 234.5550 274.2975 192.4143 -2.2713 232.4049 234.6761 274.4127 193.2423 -2.2715 232.6076 234.8791 274.5385 194.0393 -2.2699 232.7614 235.0313 274.6413 194.8255 -2.2676 232.9350 235.2026 274.7664 195.6330 -2.2665 233.1323 235.3988 274.9092 196.4195 -2.2687 233.2825 235.5511 275.0038 197.2470 -2.2624 233.4557 235.7181 275.1330 198.0135 -2.2589 233.6248 235.8837 275.2492 198.8723 -2.2559 233.8188 236.0747 275.4147 199.6378 -2.2511 233.9592 236.2103 275.5599 200.4555 -2.2515 234.1578 236.4094 275.6782 201.2630 -2.2494 234.3537 236.6031 275.7984 202.0490 -2.2489 234.5084 236.7573 275.9156 202.8770 -2.2511 234.6896 236.9407 276.0408 203.6435 -2.2533 234.8595 237.1128 276.1807 204.5015 -2.2473 235.0458 237.2931 276.3234 205.2678 -2.2418 235.1999 237.4417 276.4295 206.0855 -2.2379 235.3871 237.6250 276.5659 206.8925 -2.2356 235.5522 237.7878 276.7100 207.6790 -2.2337 235.6953 237.9290 276.8058 208.5070 -2.2299 235.8642 238.0941 276.9563 209.2733 -2.2350 236.0267 238.2617 277.0606 210.1005 -2.2322 236.2183 238.4505 277.1508 210.8670 -2.2274 236.3840 238.6114 277.2736 211.7153 -2.2266 236.5490 238.7756 277.3832 212.4913 -2.2237 236.7342 238.9578 277.4784 213.3193 -2.2244 236.8857 239.1101 277.6316 214.1158 -2.2207 237.0409 239.2616 277.6792 214.9025 -2.2202 237.2023 239.4225 277.7874 215.7408 -2.2201 237.3817 239.6017 277.9328 216.4968 -2.2175 237.5558 239.7733 278.0455 217.3548 -2.2134 237.7183 239.9316 278.1783 218.1213 -2.2108 237.8622 240.0730 278.3301 218.9590 -2.2112 237.9788 240.1900 278.4559 219.7455 -2.2141 238.1494 240.3635 278.5801 220.5428 -2.2109 238.2816 240.4925 278.7214 221.3705 -2.2094 238.4774 240.6869 278.8710 222.1363 -2.2034 238.6555 240.8589 279.0329 222.9950 -2.1950 238.8131 241.0080 279.1592 223.7610 -2.1854 238.9467 241.1321 279.2864 224.5885 -2.1878 239.0935 241.2813 279.3994 225.3858 -2.1843 239.2590 241.4433 279.5087 226.1825 -2.1851 239.4550 241.6401 279.6249 226.9998 -2.1854 239.6447 241.8301 279.7248 227.7663 -2.1819 239.8182 242.0001 279.8105 228.5835 -2.1818 239.9769 242.1587 279.9296 229.3495 -2.1809 240.1153 242.2961 280.0382 230.1980 -2.1823 240.2859 242.4682 280.1506 230.9640 -2.1855 240.4076 242.5931 280.2816 231.7915 -2.1868 240.5591 242.7459 280.4042 232.5888 -2.1858 240.7210 242.9068 280.5455 233.3753 -2.1832 240.8839 243.0671 280.6947 234.2028 -2.1781 241.0899 243.2680 280.8176 234.9795 -2.1772 241.2464 243.4236 280.9635 235.7968 -2.1760 241.4081 243.5841 281.1250 236.5628 -2.1717 241.5674 243.7391 281.2398 237.4215 -2.1675 241.7544 243.9220 281.3718 238.1770 -2.1653 241.8894 244.0547 281.4961 239.0048 -2.1611 242.0804 244.2415 281.6401 239.8020 -2.1583 242.2449 244.4032 281.7760 240.5988 -2.1542 242.4162 244.5705 281.8805 241.4263 -2.1501 242.5694 244.7195 281.9722 242.1825 -2.1537 242.7317 244.8855 282.0882 243.0513 -2.1553 242.8923 245.0476 282.2759 243.8068 -2.1511 243.0637 245.2148 282.4087 244.6245 -2.1513 243.2305 245.3818 282.5270 245.4318 -2.1531 243.3653 245.5184 282.6664 246.2180 -2.1500 243.5241 245.6741 282.8225 247.0460 -2.1543 243.6549 245.8092 282.9831 247.8120 -2.1582 243.8105 245.9687 283.1123 248.6703 -2.1592 243.9842 246.1434 283.2366 249.4368 -2.1551 244.1282 246.2833 283.3842 250.2538 -2.1524 244.2628 246.4152 283.5054 251.0303 -2.1546 244.3940 246.5486 283.6400 251.8480 -2.1518 244.5284 246.6802 283.7654 252.6448 -2.1460 244.7065 246.8525 283.8923 253.4415 -2.1477 244.8686 247.0163 284.0197 254.2695 -2.1518 245.0042 247.1560 284.1931 255.0353 -2.1556 245.1242 247.2798 284.3460 255.8835 -2.1526 245.2853 247.4379 284.4746 256.6603 -2.1487 245.4332 247.5819 284.6122 257.4770 -2.1435 245.6490 247.7925 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