DTA measure 1lassu Date: 2026317:1156 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.21 s Mass = 1173.000 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2840 -1.5859 212.0141 213.6000 248.1133 2.0505 -1.5864 212.1224 213.7088 248.0356 2.9093 -1.5848 212.2644 213.8492 247.9671 3.6758 -1.5861 212.3942 213.9803 247.9163 4.4935 -1.5878 212.5140 214.1018 247.8618 5.3010 -1.5815 212.6607 214.2423 247.8137 6.0880 -1.5780 212.7968 214.3748 247.7890 6.8858 -1.5743 212.9153 214.4896 247.7497 7.6835 -1.5737 213.0242 214.5978 247.7196 8.5115 -1.5721 213.1700 214.7421 247.6725 9.2780 -1.5683 213.3106 214.8789 247.6200 10.1265 -1.5667 213.4307 214.9974 247.5659 10.9033 -1.5653 213.5537 215.1190 247.5361 11.7210 -1.5675 213.6603 215.2278 247.4906 12.5183 -1.5688 213.7801 215.3489 247.4432 13.3155 -1.5688 213.9181 215.4869 247.4180 14.1445 -1.5725 214.0189 215.5914 247.3901 14.9110 -1.5754 214.1207 215.6961 247.3505 15.7595 -1.5724 214.2750 215.8473 247.3103 16.5363 -1.5729 214.3475 215.9204 247.2551 17.3540 -1.5741 214.4846 216.0587 247.2412 18.1513 -1.5730 214.6004 216.1734 247.2491 18.9485 -1.5693 214.7452 216.3145 247.2816 19.7765 -1.5667 214.8885 216.4551 247.2715 20.5430 -1.5650 215.0072 216.5723 247.2654 21.3920 -1.5644 215.1822 216.7465 247.2684 22.1693 -1.5619 215.3202 216.8821 247.2563 22.9870 -1.5611 215.4555 217.0165 247.2438 23.7843 -1.5564 215.5977 217.1541 247.2446 24.5815 -1.5550 215.7074 217.2624 247.2117 25.4095 -1.5549 215.8388 217.3937 247.2901 26.1760 -1.5522 215.9812 217.5333 247.3225 27.0245 -1.5471 216.1182 217.6652 247.3709 27.8018 -1.5376 216.2421 217.7797 247.4009 28.6200 -1.5343 216.3410 217.8753 247.4646 29.4173 -1.5363 216.4568 217.9930 247.5323 30.2145 -1.5305 216.5877 218.1182 247.5864 31.0425 -1.5263 216.7084 218.2347 247.6211 31.8090 -1.5238 216.8107 218.3345 247.6730 32.6575 -1.5183 216.9637 218.4821 247.7385 33.4343 -1.5136 217.0758 218.5894 247.7890 34.2528 -1.5132 217.2230 218.7362 247.8779 35.0503 -1.5133 217.3357 218.8490 247.9542 35.8475 -1.5092 217.4217 218.9309 248.0486 36.6858 -1.5096 217.5424 219.0519 248.1048 37.4420 -1.5009 217.6301 219.1309 248.1681 38.3008 -1.4804 217.7427 219.2230 248.2571 39.0673 -1.4781 217.8616 219.3397 248.3455 39.8953 -1.4803 217.9709 219.4512 248.4036 40.6618 -1.4797 218.0990 219.5786 248.4834 41.4795 -1.4784 218.2436 219.7221 248.5686 42.2768 -1.4797 218.3618 219.8415 248.6199 43.0740 -1.4822 218.4496 219.9318 248.7435 43.8918 -1.4839 218.5574 220.0413 248.8616 44.6583 -1.4846 218.6639 220.1485 248.8981 45.5068 -1.4841 218.7698 220.2539 248.9814 46.2738 -1.4807 218.9028 220.3835 249.0855 47.0920 -1.4727 219.0244 220.4971 249.2314 47.8893 -1.4738 219.1152 220.5890 249.3576 48.6865 -1.4695 219.2407 220.7102 249.5052 49.5043 -1.4699 219.3741 220.8440 249.6271 50.2605 -1.4691 219.5024 220.9715 249.7636 51.1295 -1.4658 219.6494 221.1152 249.9034 51.8550 -1.4620 219.7840 221.2460 250.0229 52.7035 -1.4595 219.9115 221.3710 250.1712 53.4803 -1.4582 220.0113 221.4695 250.3055 54.2988 -1.4544 220.1189 221.5734 250.4388 55.0860 -1.4563 220.2840 221.7403 250.5527 55.8935 -1.4526 220.4288 221.8814 250.6904 56.7113 -1.4501 220.5366 221.9868 250.8127 57.4778 -1.4513 220.6291 222.0804 250.9397 58.3365 -1.4449 220.7518 222.1967 251.0645 59.0928 -1.4427 220.8292 222.2719 251.2198 59.9208 -1.4431 220.9494 222.3926 251.3488 60.7180 -1.4411 221.0621 222.5031 251.4368 61.5153 -1.4404 221.1475 222.5879 251.5860 62.3440 -1.4410 221.2735 222.7145 251.7266 63.1005 -1.4407 221.3852 222.8259 251.8704 63.9388 -1.4341 221.5435 222.9776 252.0099 64.6950 -1.4274 221.6827 223.1101 252.1678 65.5538 -1.4221 221.8040 223.2261 252.3580 66.3203 -1.4229 221.9122 223.3351 252.4741 67.1483 -1.4240 222.0385 223.4625 252.6078 67.9455 -1.4226 222.1649 223.5876 252.7497 68.7325 -1.4234 222.2554 223.6788 252.8907 69.5708 -1.4281 222.4000 223.8281 253.0266 70.3270 -1.4254 222.4980 223.9234 253.1524 71.1453 -1.4230 222.6078 224.0308 253.3421 71.9225 -1.4209 222.7026 224.1235 253.4782 72.7710 -1.4185 222.8086 224.2271 253.6360 73.5273 -1.4136 222.9190 224.3326 253.7913 74.3860 -1.4091 223.0033 224.4124 253.9248 75.1525 -1.4067 223.0783 224.4850 254.0745 75.9805 -1.4062 223.1943 224.6005 254.2229 76.7470 -1.4067 223.3147 224.7214 254.3543 77.5750 -1.4056 223.4155 224.8211 254.4971 78.3620 -1.4073 223.5242 224.9315 254.5789 79.1700 -1.4082 223.6794 225.0875 254.7006 79.9883 -1.4077 223.8099 225.2176 254.8520 80.7548 -1.4193 223.9206 225.3399 254.9832 81.6135 -1.4208 224.0362 225.4571 255.1124 82.3800 -1.4217 224.1166 225.5383 255.2257 83.2080 -1.4249 224.2822 225.7071 255.3997 83.9745 -1.4139 224.4428 225.8567 255.5159 84.8025 -1.3334 224.5927 225.9261 255.6591 85.5998 -1.3449 224.6992 226.0440 255.7777 86.3970 -1.3586 224.7742 226.1328 255.8745 87.2148 -1.3734 224.8738 226.2472 256.0033 87.9915 -1.3778 225.0024 226.3802 256.0797 88.8400 -1.3850 225.1420 226.5270 256.2208 89.6068 -1.3925 225.2610 226.6535 256.3561 90.4355 -1.4027 225.3266 226.7293 256.4969 91.2328 -1.3997 225.4232 226.8228 256.6374 92.0300 -1.3966 225.5643 226.9610 256.7759 92.8478 -1.4041 225.6892 227.0933 256.9062 93.6348 -1.4089 225.8116 227.2205 257.0481 94.4320 -1.4165 225.9496 227.3661 257.1716 95.2600 -1.4142 226.0941 227.5083 257.2850 96.0470 -1.4139 226.1880 227.6019 257.3701 96.8553 -1.4145 226.3006 227.7151 257.4745 97.6733 -1.4189 226.4318 227.8507 257.5764 98.4500 -1.4180 226.5462 227.9642 257.7021 99.2985 -1.4144 226.6559 228.0703 257.7945 100.0753 -1.4181 226.7452 228.1633 257.8701 100.8930 -1.4189 226.8328 228.2516 257.9585 101.6903 -1.4196 226.9577 228.3773 258.0729 102.4875 -1.4196 227.0922 228.5118 258.1714 103.2848 -1.4217 227.1899 228.6116 258.3044 104.0820 -1.4235 227.2864 228.7099 258.3911 104.8998 -1.4240 227.4533 228.8772 258.4779 105.6765 -1.4181 227.5535 228.9715 258.5713 106.5258 -1.4177 227.6754 229.0932 258.7050 107.2823 -1.4244 227.7861 229.2105 258.7967 108.1103 -1.4265 227.9026 229.3291 258.8970 108.8973 -1.4289 228.0423 229.4712 258.9734 109.6945 -1.4285 228.1742 229.6027 259.0743 110.5225 -1.4271 228.3404 229.7675 259.1508 111.2788 -1.4264 228.4407 229.8671 259.2330 112.1375 -1.4243 228.5624 229.9867 259.3601 112.8733 -1.4229 228.6735 230.0964 259.4602 113.7218 -1.4271 228.7928 230.2199 259.5754 114.4883 -1.4282 228.8681 230.2963 259.7022 115.3163 -1.4255 228.9761 230.4016 259.8198 116.1033 -1.4240 229.0705 230.4945 259.9041 116.9005 -1.4227 229.1576 230.5803 260.0096 117.7295 -1.4161 229.2827 230.6988 260.1261 118.4960 -1.3959 229.4046 230.8004 260.2277 119.3445 -1.3772 229.5008 230.8781 260.3111 120.1110 -1.3833 229.6278 231.0111 260.4078 120.9390 -1.3924 229.7414 231.1337 260.5311 121.7260 -1.4003 229.8775 231.2778 260.6217 122.5335 -1.4003 229.9906 231.3909 260.6954 123.3513 -1.4004 230.1186 231.5190 260.7833 124.1075 -1.4024 230.2451 231.6475 260.8705 124.9775 -1.4024 230.4002 231.8026 260.9566 125.7338 -1.4065 230.5077 231.9142 261.0259 126.5618 -1.4084 230.6190 232.0274 261.0969 127.3590 -1.4070 230.7429 232.1498 261.1969 128.1460 -1.4061 230.8503 232.2564 261.2977 128.9740 -1.4095 230.9543 232.3637 261.3666 129.7405 -1.4119 231.0466 232.4584 261.4202 130.5685 -1.4097 231.2007 232.6104 261.5087 131.3350 -1.4099 231.2847 232.6946 261.5982 132.1835 -1.4103 231.4048 232.8152 261.7128 132.9813 -1.4143 231.5156 232.9299 261.7684 133.7790 -1.4166 231.6146 233.0312 261.8563 134.5968 -1.4145 231.7499 233.1643 261.9703 135.3735 -1.4175 231.9114 233.3290 262.0709 136.2220 -1.4089 232.0353 233.4442 262.1926 136.9680 -1.4034 232.1230 233.5265 262.2883 137.8165 -1.4065 232.2439 233.6503 262.3811 138.5933 -1.4129 232.3661 233.7790 262.4590 139.4110 -1.4135 232.4769 233.8905 262.5370 140.2083 -1.4123 232.6009 234.0132 262.6264 141.0055 -1.4099 232.7071 234.1170 262.7359 141.8335 -1.4075 232.8093 234.2169 262.8501 142.6008 -1.4074 232.9187 234.3262 262.9120 143.4495 -1.3911 233.0180 234.4091 263.0509 144.2263 -1.3938 233.1387 234.5325 263.1425 145.0440 -1.3981 233.2385 234.6365 263.2492 145.8413 -1.4013 233.3484 234.7497 263.3516 146.6385 -1.4033 233.4530 234.8564 263.3912 147.4665 -1.3818 233.5454 234.9272 263.4782 148.2330 -1.3250 233.7042 235.0292 263.5623 149.0815 -1.3394 233.8517 235.1911 263.6411 149.8583 -1.3497 233.9677 235.3174 263.6841 150.6760 -1.3518 234.0421 235.3939 263.7929 151.4740 -1.3656 234.1671 235.5327 263.9198 152.2715 -1.3729 234.2893 235.6623 264.0151 153.0995 -1.3754 234.4334 235.8088 264.1017 153.8660 -1.3789 234.5359 235.9148 264.2126 154.7145 -1.3824 234.6748 236.0572 264.2955 155.4810 -1.3875 234.7892 236.1766 264.3836 156.3295 -1.3915 234.8999 236.2914 264.4906 157.1063 -1.3914 235.0171 236.4085 264.6301 157.9240 -1.3932 235.1008 236.4939 264.7207 158.7215 -1.3931 235.2160 236.6091 264.8195 159.5188 -1.3996 235.3429 236.7424 264.9208 160.3163 -1.3968 235.4544 236.8513 265.0149 161.1140 -1.4002 235.5744 236.9746 265.1174 161.9420 -1.4032 235.6889 237.0922 265.2241 162.7085 -1.4057 235.7718 237.1775 265.3349 163.5673 -1.4020 235.9056 237.3076 265.4271 164.3338 -1.3991 235.9913 237.3904 265.5393 165.1515 -1.4055 236.1352 237.5407 265.6606 165.9590 -1.4012 236.2603 237.6616 265.7812 166.7460 -1.3997 236.3627 237.7624 265.8834 167.5740 -1.3942 236.5227 237.9169 266.0156 168.3405 -1.3959 236.6254 238.0213 266.1163 169.1993 -1.3947 236.7236 238.1183 266.1862 169.9660 -1.3913 236.8284 238.2197 266.2814 170.7843 -1.3955 236.9526 238.3481 266.4248 171.5818 -1.3997 237.0442 238.4439 266.5563 172.3683 -1.4009 237.1807 238.5816 266.6779 173.1968 -1.4004 237.3007 238.7012 266.7778 173.9530 -1.3962 237.3974 238.7936 266.8544 174.8015 -1.3946 237.5162 238.9109 266.9605 175.5475 -1.3966 237.6194 239.0160 267.0290 176.3960 -1.3966 237.7399 239.1366 267.1697 177.1523 -1.3939 237.8499 239.2438 267.2709 177.9803 -1.3886 237.9499 239.3385 267.3788 178.7775 -1.3908 238.0644 239.4552 267.4617 179.5645 -1.3954 238.1685 239.5638 267.5880 180.3925 -1.3972 238.2961 239.6933 267.6914 181.1590 -1.3984 238.3980 239.7964 267.7940 182.0080 -1.3988 238.5004 239.8992 267.8713 182.7850 -1.3967 238.6032 239.9999 267.9751 183.6030 -1.3962 238.7319 240.1281 268.1119 184.3593 -1.3931 238.8073 240.2004 268.2131 185.1975 -1.3902 238.9312 240.3214 268.3077 185.9845 -1.3898 239.0314 240.4211 268.4324 186.7715 -1.3884 239.1386 240.5270 268.5267 187.6098 -1.3913 239.2741 240.6654 268.6757 188.3660 -1.3929 239.3971 240.7900 268.7893 189.2148 -1.3952 239.5232 240.9185 268.8917 189.9913 -1.3940 239.6547 241.0486 268.9965 190.8090 -1.3876 239.7664 241.1540 269.0943 191.6068 -1.3833 239.8905 241.2738 269.2596 192.4038 -1.3833 240.0028 241.3861 269.3783 193.2318 -1.3879 240.1313 241.5192 269.4996 193.9980 -1.3850 240.2349 241.6199 269.6293 194.8473 -1.3866 240.3400 241.7266 269.7177 195.5930 -1.3898 240.4438 241.8335 269.8082 196.4420 -1.3923 240.5545 241.9468 269.8900 197.2083 -1.3883 240.6820 242.0703 270.0050 198.0365 -1.3855 240.8369 242.2224 270.1242 198.8338 -1.3815 240.9290 242.3104 270.2440 199.6310 -1.3804 241.0186 242.3991 270.3678 200.4488 -1.3786 241.1271 242.5057 270.4985 201.2255 -1.3764 241.2381 242.6144 270.5813 202.0740 -1.3780 241.3329 242.7109 270.6607 202.8405 -1.3803 241.4497 242.8300 270.7423 203.6685 -1.3835 241.6142 242.9976 270.8344 204.4453 -1.3874 241.7235 243.1109 270.9276 205.2630 -1.3888 241.8155 243.2043 271.0328 206.0603 -1.3915 241.9461 243.3376 271.1532 206.8575 -1.3904 242.0523 243.4427 271.2685 207.6855 -1.3886 242.1641 243.5527 271.3945 208.4520 -1.3932 242.2796 243.6728 271.5299 209.3005 -1.3879 242.4036 243.7915 271.6625 210.0773 -1.3899 242.5038 243.8938 271.7374 210.8950 -1.3921 242.6214 244.0135 271.8595 211.6923 -1.3923 242.7242 244.1165 271.9803 212.4895 -1.3955 242.8548 244.2503 272.0697 213.3183 -1.3926 242.9780 244.3706 272.2000 214.0850 -1.3907 243.0745 244.4652 272.3188 214.9335 -1.3924 243.1626 244.5551 272.4534 215.7103 -1.3902 243.2542 244.6444 272.5536 216.5280 -1.3871 243.3497 244.7368 272.6173 217.3048 -1.3879 243.4629 244.8508 272.7103 218.1328 -1.3932 243.5797 244.9728 272.7925 218.9300 -1.3971 243.7016 245.0987 272.8804 219.7273 -1.3932 243.8131 245.2062 272.9782 220.5560 -1.3952 243.9547 245.3499 273.0848 221.3125 -1.3944 244.0787 245.4731 273.2064 222.1815 -1.3959 244.1868 245.5827 273.3257 222.9173 -1.3960 244.3110 245.7071 273.4061 223.7760 -1.3982 244.4284 245.8266 273.5395 224.5323 -1.4015 244.5184 245.9199 273.6555 225.3705 -1.4004 244.6165 246.0169 273.7619 226.1575 -1.4080 244.7308 246.1388 273.8511 226.9753 -1.4049 244.8591 246.2640 273.9427 227.7725 -1.4100 244.9766 246.3866 274.0351 228.5698 -1.4093 245.0613 246.4706 274.1614 229.3978 -1.4083 245.1873 246.5956 274.2923 230.1745 -1.4081 245.3083 246.7164 274.3929 231.0230 -1.4080 245.3908 246.7988 274.5131 231.7895 -1.4049 245.4961 246.9010 274.6081 232.6175 -1.4053 245.6119 247.0172 274.7166 233.3840 -1.4045 245.7291 247.1336 274.7828 234.2120 -1.4007 245.8173 247.2180 274.8571 234.9990 -1.4009 245.9285 247.3294 274.9468 235.7963 -1.4060 246.0627 247.4687 275.0242 236.6140 -1.4047 246.1885 247.5932 275.1254 237.4010 -1.4081 246.3034 247.7116 275.2293 238.2195 -1.4167 246.4130 247.8298 275.3372 238.9965 -1.4154 246.5266 247.9419 275.4269 239.8450 -1.4130 246.6413 248.0543 275.5299 240.5705 -1.4152 246.7364 248.1516 275.6721 241.4395 -1.4124 246.8580 248.2704 275.8525 242.1958 -1.4132 246.9857 248.3989 275.9500 243.0135 -1.4117 247.1122 248.5239 276.0256 243.8108 -1.4093 247.1512 248.5605 276.0970 244.6080 -1.4079 247.2500 248.6578 276.1750 245.4258 -1.4088 247.3708 248.7796 276.2827 246.2028 -1.4100 247.4526 248.8626 276.3487 247.0520 -1.4129 247.5717 248.9846 276.4518 247.8083 -1.4162 247.6891 249.1052 276.5296 248.6363 -1.4148 247.8004 249.2153 276.6315 249.4335 -1.4152 247.9270 249.3422 276.7337 250.2205 -1.4118 248.0697 249.4815 276.8347 251.0588 -1.4114 248.1946 249.6060 276.9377 251.8150 -1.4151 248.2958 249.7110 277.0542 252.6738 -1.4178 248.4120 249.8298 277.1470 253.4403 -1.4105 248.5407 249.9512 277.2359 254.2580 -1.4055 248.6401 250.0457 277.3407 255.0245 -1.4018 248.7468 250.1486 277.4492 255.8528 -1.3924 248.8645 250.2568 277.5675 256.6508 -1.3954 248.9523 250.3477 277.6331 257.4480 -1.4001 249.0686 250.4687 277.7050 258.2658 -1.4067 249.1829 250.5896 277.8314 259.0425 -1.4093 249.2987 250.7081 277.9475 259.8910 -1.4133 249.4281 250.8414 278.0895 260.6575 -1.4108 249.5546 250.9654 278.2024 261.4855 -1.4096 249.7024 251.1120 278.3249 262.2828 -1.4139 249.8164 251.2303 278.4010 263.0800 -1.4171 249.9129 251.3300 278.4516 263.8978 -1.4172 250.0102 251.4274 278.5404 264.6745 -1.4188 250.1167 251.5355 278.6442 265.5230 -1.4163 250.2414 251.6578 278.7500 266.2895 -1.4168 250.3429 251.7597 278.8364 267.1185 -1.4162 250.4574 251.8736 278.9420 267.9158 -1.4140 250.5686 251.9825 279.0465 268.7130 -1.4115 250.6488 252.0603 279.1118 269.5308 -1.4084 250.7220 252.1304 279.1977 270.3075 -1.4089 250.8437 252.2526 279.2712 271.1560 -1.4143 250.9577 252.3720 279.3907 271.9225 -1.4157 251.0634 252.4791 279.4848 272.7505 -1.4150 251.1790 252.5939 279.6081 273.5273 -1.4125 251.2968 252.7093 279.6875 274.3450 -1.4135 251.4085 252.8220 279.7901 275.1428 -1.4148 251.5204 252.9352 279.8793 275.9405 -1.4202 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