DTA measure 11_meres Date: 20251118:1052 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.59 s Mass = 1094.200 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2605 -5.9379 221.2835 227.2215 276.9197 2.1088 -5.9413 221.5726 227.5139 276.9664 2.8745 -5.9459 221.8307 227.7766 276.9896 3.7018 -5.9509 222.0870 228.0379 276.9697 4.4885 -5.9535 222.3476 228.3011 276.9337 5.2848 -5.9599 222.6355 228.5954 276.8824 6.1125 -5.9684 222.9216 228.8901 276.8052 6.8783 -5.9725 223.1814 229.1540 276.7010 7.7260 -5.9761 223.4656 229.4418 276.5655 8.4920 -5.9786 223.7212 229.6998 276.4224 9.3193 -5.9814 223.9808 229.9623 276.2524 10.1158 -5.9810 224.2012 230.1821 276.0927 10.9025 -5.9852 224.4248 230.4100 275.9454 11.7398 -5.9931 224.6779 230.6710 275.6922 12.4955 -6.0001 224.9166 230.9167 275.5107 13.3230 -6.0061 225.2048 231.2108 275.2954 14.0888 -6.0109 225.4548 231.4658 275.1328 14.9573 -6.0198 225.7167 231.7365 274.9671 15.7128 -6.0259 225.9280 231.9539 274.8512 16.5400 -6.0288 226.2002 232.2289 274.7120 17.3368 -6.0352 226.4573 232.4925 274.6104 18.1333 -6.0442 226.7276 232.7718 274.5592 18.9608 -6.0464 226.9891 233.0355 274.5155 19.7165 -6.0492 227.2109 233.2601 274.5019 20.5845 -6.0552 227.4774 233.5326 274.5808 21.3508 -6.0616 227.7268 233.7884 274.6983 22.1780 -6.0669 228.0001 234.0670 274.8516 22.9643 -6.0716 228.2266 234.2982 275.0796 23.7715 -6.0729 228.4813 234.5542 275.3624 24.5883 -6.0750 228.7343 234.8093 275.6809 25.3645 -6.0819 228.9398 235.0217 276.0183 26.2125 -6.0908 229.1888 235.2796 276.4381 26.9885 -6.0954 229.4376 235.5330 276.8300 27.8058 -6.1021 229.6562 235.7583 277.2777 28.6125 -6.1108 229.9407 236.0514 277.7541 29.3988 -6.1157 230.1946 236.3102 278.2109 30.2365 -6.1204 230.4726 236.5929 278.6957 30.9920 -6.1236 230.7248 236.8484 279.1730 31.8398 -6.1269 230.9611 237.0880 279.6965 32.5855 -6.1273 231.1306 237.2579 280.1441 33.4330 -6.1375 231.3658 237.5033 280.6200 34.1990 -6.1427 231.6345 237.7772 281.0533 35.0265 -6.1490 231.8821 238.0311 281.4565 35.8125 -6.1527 232.0961 238.2489 281.8079 36.6093 -6.1566 232.3406 238.4972 282.1240 37.4368 -6.1626 232.6009 238.7635 282.4119 38.2025 -6.1673 232.8186 238.9859 282.6426 39.0505 -6.1693 233.0992 239.2685 282.8653 39.8163 -6.1729 233.3268 239.4998 283.0092 40.6435 -6.1727 233.5679 239.7407 283.0948 41.4403 -6.1722 233.8131 239.9853 283.1435 42.2265 -6.1775 234.0591 240.2365 283.1891 43.0643 -6.1829 234.2964 240.4793 283.1926 43.8200 -6.1890 234.5066 240.6956 283.1511 44.6778 -6.1923 234.7517 240.9439 283.1262 45.4440 -6.1949 234.9412 241.1361 283.0234 46.2713 -6.1971 235.1952 241.3923 282.9141 47.0678 -6.2020 235.4245 241.6265 282.8100 47.8545 -6.2051 235.6580 241.8630 282.6972 48.6918 -6.2095 235.9256 242.1352 282.5419 49.4580 -6.2108 236.1594 242.3702 282.3952 50.3160 -6.2119 236.4274 242.6393 282.2136 51.0715 -6.2156 236.6705 242.8861 282.0555 51.9093 -6.2238 236.9077 243.1315 281.8856 52.6955 -6.2252 237.1062 243.3314 281.7560 53.5025 -6.2308 237.3247 243.5554 281.6230 54.3198 -6.2370 237.5932 243.8302 281.5067 55.0958 -6.2386 237.8109 244.0495 281.4037 55.9438 -6.2427 238.0703 244.3130 281.2922 56.7095 -6.2472 238.2856 244.5328 281.2114 57.5370 -6.2502 238.5128 244.7630 281.1953 58.3440 -6.2595 238.7448 245.0043 281.1712 59.1300 -6.2668 238.9723 245.2390 281.2069 59.9575 -6.2725 239.2118 245.4843 281.3146 60.7235 -6.2789 239.4396 245.7185 281.4318 61.5813 -6.2833 239.6746 245.9579 281.6431 62.3475 -6.2856 239.8947 246.1803 281.8735 63.1645 -6.2889 240.1326 246.4215 282.1751 63.9608 -6.2946 240.3557 246.6503 282.4466 64.7578 -6.2998 240.5749 246.8747 282.7957 65.5748 -6.2998 240.7925 247.0923 283.2050 66.3510 -6.3024 241.0220 247.3244 283.5900 67.1683 -6.3058 241.2339 247.5397 284.0308 67.9338 -6.3086 241.4344 247.7430 284.4514 68.7920 -6.3130 241.6792 247.9922 284.9202 69.5478 -6.3185 241.8716 248.1901 285.3649 70.3748 -6.3188 242.1012 248.4201 285.8811 71.1715 -6.3242 242.3343 248.6585 286.3164 71.9683 -6.3296 242.5546 248.8842 286.7732 72.7955 -6.3334 242.7928 249.1262 287.1737 73.5513 -6.3321 243.0021 249.3343 287.5297 74.4195 -6.3329 243.2401 249.5730 287.8877 75.1753 -6.3332 243.4201 249.7534 288.1437 76.0028 -6.3312 243.6076 249.9387 288.4390 76.7990 -6.3326 243.8405 250.1731 288.7294 77.5960 -6.3402 244.0950 250.4352 288.9345 78.4233 -6.3445 244.3332 250.6777 289.0947 79.1790 -6.3452 244.5411 250.8863 289.2191 80.0168 -6.3525 244.7705 251.1231 289.3368 80.7720 -6.3574 245.0086 251.3660 289.3830 81.6303 -6.3595 245.2797 251.6393 289.4384 82.3963 -6.3613 245.4947 251.8560 289.4275 83.2338 -6.3674 245.6911 252.0585 289.3996 84.0203 -6.3718 245.9486 252.3204 289.3279 84.8168 -6.3751 246.1766 252.5517 289.2441 85.6440 -6.3764 246.4056 252.7820 289.1323 86.4100 -6.3775 246.5989 252.9763 289.0128 87.2680 -6.3857 246.8072 253.1929 288.8883 88.0340 -6.3923 247.0382 253.4305 288.7609 88.8615 -6.3965 247.2706 253.6671 288.6149 89.6578 -6.3999 247.4706 253.8706 288.4580 90.4545 -6.4035 247.6641 254.0676 288.3651 91.2718 -6.4070 247.8586 254.2656 288.2388 92.0475 -6.4080 248.0233 254.4312 288.1036 92.8955 -6.4084 248.2665 254.6749 287.9489 93.6615 -6.4115 248.4901 254.9016 287.8534 94.4888 -6.4171 248.7183 255.1354 287.8170 95.2855 -6.4228 248.9304 255.3533 287.8514 96.0718 -6.4273 249.1626 255.5899 287.8655 96.8683 -6.4279 249.3751 255.8030 287.8841 97.6548 -6.4287 249.5565 255.9851 287.9341 98.4820 -6.4315 249.7866 256.2181 288.0376 99.2478 -6.4339 250.0071 256.4410 288.1758 100.0958 -6.4378 250.2559 256.6937 288.3692 100.8615 -6.4429 250.4399 256.8828 288.6008 101.6888 -6.4471 250.6477 257.0948 288.8725 102.4858 -6.4491 250.8424 257.2915 289.1419 103.2820 -6.4542 251.0284 257.4826 289.4442 104.0688 -6.4572 251.2083 257.6656 289.7343 104.8755 -6.4618 251.4377 257.8995 290.0798 105.6925 -6.4685 251.6339 258.1024 290.4417 106.4690 -6.4753 251.8436 258.3188 290.8317 107.3165 -6.4769 252.0590 258.5359 291.2344 108.0620 -6.4804 252.2482 258.7286 291.6093 108.9100 -6.4848 252.4155 258.9003 292.0721 109.6755 -6.4856 252.5985 259.0842 292.4477 110.5030 -6.4871 252.7944 259.2815 292.9064 111.3100 -6.4913 252.9769 259.4682 293.3401 112.0960 -6.4918 253.2130 259.7048 293.6437 112.9238 -6.4949 253.4354 259.9302 293.9204 113.6895 -6.4998 253.6240 260.1238 294.1793 114.5475 -6.5056 253.8445 260.3501 294.4538 115.3135 -6.5064 254.0644 260.5708 294.6795 116.1305 -6.5094 254.2842 260.7937 294.8909 116.9373 -6.5133 254.4632 260.9765 295.0651 117.7340 -6.5166 254.6288 261.1454 295.1815 118.5613 -6.5208 254.8707 261.3916 295.2972 119.3170 -6.5220 255.0778 261.5998 295.3661 120.1855 -6.5248 255.3106 261.8354 295.3893 120.9203 -6.5269 255.5022 262.0292 295.3759 121.7785 -6.5295 255.6974 262.2269 295.3421 122.5343 -6.5347 255.8951 262.4299 295.3393 123.3718 -6.5407 256.1463 262.6870 295.3008 124.1583 -6.5417 256.3411 262.8828 295.2360 124.9548 -6.5437 256.5433 263.0871 295.1579 125.8130 -6.5422 256.7674 263.3096 295.0794 126.5585 -6.5417 256.9647 263.5065 295.0053 127.4060 -6.5463 257.1460 263.6923 294.9119 128.1720 -6.5497 257.3590 263.9087 294.8173 128.9995 -6.5520 257.5833 264.1353 294.6747 129.7958 -6.5556 257.7765 264.3321 294.5727 130.5925 -6.5583 257.9745 264.5328 294.4823 131.4098 -6.5617 258.1695 264.7312 294.4015 132.1855 -6.5669 258.3281 264.8950 294.3157 133.0338 -6.5703 258.5300 265.1003 294.3011 133.7995 -6.5739 258.7034 265.2773 294.2698 134.6268 -6.5747 258.8840 265.4587 294.2971 135.4235 -6.5782 259.1090 265.6872 294.3420 136.2200 -6.5796 259.2880 265.8676 294.4343 137.0373 -6.5850 259.4901 266.0751 294.5536 137.8135 -6.5914 259.6751 266.2665 294.6995 138.6610 -6.5980 259.8919 266.4899 294.9336 139.4273 -6.6044 260.0718 266.6762 295.1515 140.2545 -6.6083 260.2753 266.8836 295.3792 141.0513 -6.6123 260.4667 267.0790 295.6671 141.8480 -6.6158 260.6960 267.3118 295.9937 142.6650 -6.6181 260.8681 267.4862 296.3334 143.4413 -6.6184 261.0376 267.6560 296.6637 144.2890 -6.6201 261.2819 267.9021 297.0591 145.0548 -6.6243 261.5052 268.1295 297.4116 145.8825 -6.6234 261.7069 268.3303 297.7780 146.6788 -6.6247 261.8827 268.5074 298.1534 147.4755 -6.6274 262.0802 268.7076 298.5218 148.2928 -6.6282 262.2244 268.8526 298.9133 149.0685 -6.6309 262.3950 269.0260 299.2630 149.9165 -6.6319 262.6114 269.2433 299.6659 150.6928 -6.6338 262.7933 269.4271 299.9955 151.5098 -6.6355 262.9511 269.5865 300.2566 152.3168 -6.6379 263.1784 269.8163 300.5217 153.1030 -6.6434 263.3905 270.0338 300.7752 153.9305 -6.6442 263.5723 270.2165 300.9800 154.6965 -6.6437 263.7600 270.4037 301.1082 155.5645 -6.6453 263.9896 270.6349 301.2943 156.3203 -6.6543 264.1904 270.8448 301.3724 157.1478 -6.6572 264.3806 271.0378 301.4704 157.9440 -6.6605 264.5459 271.2064 301.5509 158.7510 -6.6641 264.7235 271.3877 301.5704 159.5683 -6.6700 264.9181 271.5881 301.6070 160.3338 -6.6749 265.1231 271.7981 301.5511 161.1920 -6.6804 265.3439 272.0242 301.5289 161.9683 -6.6837 265.5388 272.2225 301.4751 162.7853 -6.6861 265.7505 272.4366 301.3949 163.5823 -6.6892 265.9226 272.6118 301.3272 164.3785 -6.6914 266.1322 272.8236 301.2755 165.2063 -6.6933 266.3277 273.0211 301.1877 165.9720 -6.6941 266.5095 273.2036 301.1142 166.8198 -6.6965 266.7261 273.4226 301.0363 167.5963 -6.6975 266.9170 273.6145 300.9929 168.4233 -6.7010 267.1028 273.8038 300.9218 169.2200 -6.7071 267.2982 274.0053 300.8127 170.0065 -6.7117 267.4454 274.1571 300.7584 170.8440 -6.7140 267.6549 274.3689 300.7177 171.5998 -6.7201 267.8045 274.5247 300.6859 172.4680 -6.7220 267.9600 274.6819 300.6629 173.2238 -6.7237 268.1083 274.8320 300.7049 174.0615 -6.7269 268.3135 275.0404 300.7835 174.8475 -6.7375 268.5605 275.2980 300.8649 175.6443 -6.7402 268.7758 275.5161 300.9508 176.4718 -6.7403 268.9627 275.7029 301.1380 177.2478 -6.7427 269.1400 275.8827 301.3565 178.0650 -6.7511 269.3169 276.0680 301.5934 178.8308 -6.7596 269.5006 276.2602 301.8452 179.6888 -6.7630 269.6761 276.4391 302.1553 180.4653 -6.7634 269.8408 276.6043 302.4979 181.2820 -6.7655 270.0171 276.7826 302.8667 182.0788 -6.7732 270.1871 276.9603 303.2124 182.8755 -6.7783 270.3690 277.1474 303.5778 183.7025 -6.7802 270.5703 277.3506 303.9825 184.4688 -6.7784 270.7576 277.5360 304.3759 185.3268 -6.7827 270.9624 277.7450 304.7513 186.0925 -6.7819 271.1196 277.9015 305.0970 186.9200 -6.7812 271.3172 278.0983 305.4986 187.7165 -6.7884 271.4650 278.2534 305.8536 188.5133 -6.7915 271.6309 278.4224 306.1713 189.3100 -6.7934 271.7827 278.5760 306.4510 190.1063 -6.7966 271.9533 278.7499 306.7365 190.9343 -6.8022 272.1395 278.9417 306.9764 191.6895 -6.8042 272.3441 279.1483 307.1467 192.5478 -6.8074 272.5575 279.3649 307.3256 193.3035 -6.8139 272.7086 279.5225 307.4990 194.1308 -6.8168 272.8254 279.6422 307.6465 194.9275 -6.8142 273.0209 279.8351 307.7468 195.7240 -6.8169 273.2051 280.0219 307.8452 196.5410 -6.8197 273.3805 280.2002 307.8734 197.3173 -6.8170 273.5664 280.3833 307.8733 198.1343 -6.8157 273.7947 280.6103 307.8519 198.8900 -6.8182 273.9781 280.7963 307.8401 199.7585 -6.8226 274.1826 281.0052 307.7618 200.5138 -6.8237 274.3676 281.1913 307.6902 201.3310 -6.8262 274.5701 281.3964 307.6240 202.1380 -6.8268 274.7267 281.5535 307.5249 202.9240 -6.8291 274.9189 281.7480 307.4406 203.7515 -6.8305 275.1135 281.9440 307.4021 204.5175 -6.8354 275.2465 282.0819 307.3123 205.3548 -6.8374 275.4288 282.2662 307.2523 206.1105 -6.8342 275.6093 282.4435 307.2112 206.9688 -6.8347 275.7902 282.6249 307.1500 207.7345 -6.8387 275.9239 282.7625 307.0831 208.5620 -6.8424 276.1101 282.9524 307.0285 209.3585 -6.8446 276.3182 283.1628 307.0266 210.1450 -6.8452 276.4978 283.3430 307.0362 210.9828 -6.8507 276.6982 283.5489 307.0737 211.7380 -6.8551 276.8787 283.7338 307.1343 212.5658 -6.8602 277.0400 283.9002 307.2104 213.3315 -6.8673 277.2196 284.0869 307.3328 214.1898 -6.8721 277.4033 284.2754 307.4821 214.9558 -6.8766 277.5640 284.4406 307.6697 215.7728 -6.8805 277.7492 284.6297 307.8907 216.5798 -6.8816 277.9171 284.7988 308.1544 217.3660 -6.8807 278.0956 284.9763 308.4461 218.1933 -6.8854 278.2659 285.1513 308.7507 218.9595 -6.8870 278.4471 285.3341 309.0662 219.8173 -6.8899 278.6570 285.5470 309.4318 220.5833 -6.8910 278.8288 285.7198 309.8021 221.4005 -6.8946 279.0107 285.9052 310.1889 222.2070 -6.9010 279.1394 286.0404 310.5520 222.9935 -6.9089 279.2844 286.1934 310.9413 223.8210 -6.9177 279.4914 286.4091 311.3296 224.5865 -6.9181 279.6681 286.5862 311.6814 225.4550 -6.9175 279.8875 286.8050 312.0485 226.2108 -6.9244 280.0672 286.9916 312.3408 227.0378 -6.9252 280.2677 287.1929 312.6294 227.8345 -6.9263 280.4044 287.3306 312.9067 228.6313 -6.9295 280.5710 287.5006 313.1633 229.4585 -6.9361 280.7369 287.6729 313.3785 230.2143 -6.9409 280.8919 287.8328 313.5656 231.0825 -6.9408 281.0605 288.0013 313.7375 231.8380 -6.9410 281.2309 288.1719 313.8588 232.6658 -6.9495 281.4301 288.3796 313.9462 233.4620 -6.9527 281.6075 288.5602 314.0263 234.2690 -6.9546 281.7590 288.7136 314.0882 235.0555 -6.9587 281.9361 288.8948 314.1259 235.8520 -6.9582 282.1100 289.0682 314.1500 236.6795 -6.9600 282.2946 289.2546 314.1049 237.4453 -6.9650 282.4525 289.4175 314.0566 238.3035 -6.9657 282.6511 289.6168 314.0154 239.0695 -6.9680 282.8302 289.7982 313.9826 239.8965 -6.9695 283.0486 290.0180 313.9160 240.6933 -6.9703 283.2292 290.1994 313.8261 241.4900 -6.9741 283.4054 290.3794 313.7358 242.3070 -6.9780 283.5853 290.5633 313.6671 243.0835 -6.9813 283.7521 290.7334 313.5705 243.9413 -6.9907 283.9315 290.9222 313.4702 244.7075 -6.9941 284.0970 291.0911 313.4148 245.5245 -6.9980 284.2738 291.2718 313.3863 246.3313 -7.0005 284.4387 291.4392 313.3555 247.1280 -7.0034 284.6077 291.6111 313.3387 247.9553 -7.0088 284.7839 291.7927 313.3476 248.7108 -7.0106 284.9078 291.9185 313.3883 249.5793 -7.0141 285.0643 292.0785 313.4564 250.3450 -7.0167 285.2058 292.2225 313.5131 251.1723 -7.0162 285.3614 292.3776 313.6115 251.9590 -7.0223 285.5686 292.5910 313.7479 252.7655 -7.0250 285.7385 292.7635 313.9287 253.5930 -7.0312 285.9340 292.9651 314.1463 254.3590 -7.0365 286.0770 293.1135 314.3945 255.2065 -7.0415 286.2081 293.2495 314.6815 255.9520 -7.0436 286.3387 293.3823 314.9711 256.8103 -7.0454 286.5332 293.5786 315.3130 257.5655 -7.0497 286.6933 293.7430 315.6253 258.3933 -7.0514 286.8461 293.8975 316.0029 259.1898 -7.0532 287.0086 294.0619 316.3828 259.9763 -7.0551 287.1785 294.2336 316.7419 260.8038 -7.0615 287.3413 294.4029 317.1314 261.5693 -7.0634 287.5151 294.5785 317.4847 262.4175 -7.0648 287.7266 294.7914 317.8645 263.1833 -7.0653 287.8915 294.9568 318.2048 264.0108 -7.0681 288.0458 295.1140 318.5557 264.7768 -7.0742 288.1888 295.2630 318.8887 265.5938 -7.0815 288.3549 295.4364 319.1748 266.4008 -7.0864 288.5178 295.6042 319.4193 267.1870 -7.0884 288.6763 295.7648 319.6261 268.0143 -7.0889 288.8517 295.9406 319.8236 268.7805 -7.0888 288.9884 296.0772 319.9781 269.6280 -7.0883 289.1581 296.2464 320.1162 270.3940 -7.0922 289.3464 296.4386 320.2279 271.2215 -7.0896 289.5366 296.6262 320.3197 272.0178 -7.0910 289.7077 296.7987 320.3570 272.8145 -7.0959 289.8775 296.9735 320.3974 273.6318 -7.1014 290.0558 297.1571 320.4019 274.4075 -7.1088 290.2462 297.3550 320.4092 275.2558 -7.1112 290.4252 297.5363 320.3925 276.0215 -7.1151 290.5805 297.6956 320.3624 276.8488 -7.1187 290.7487 297.8674 320.2799 277.6248 -7.1165 290.9242 298.0407 320.2011 278.4420 -7.1231 291.0819 298.2050 320.1199 279.2385 -7.1258 291.2940 298.4198 320.0229 280.0353 -7.1317 291.4642 298.5959 319.9054 280.8625 -7.1349 291.6518 298.7868 319.8221 281.6283 -7.1384 291.7834 298.9219 319.7243 282.4763 -7.1395 291.9196 299.0591 319.6448 283.2523 -7.1426 292.0877 299.2303 319.5776 284.0695 -7.1466 292.2553 299.4019 319.5523 284.8355 -7.1480 292.4004 299.5484 319.5636 285.6628 -7.1502 292.6088 299.7590 319.5601 286.4598 -7.1470 292.7923 299.9393 319.5723 287.2560 -7.1504 292.9499 300.1003 319.5898 288.0735 -7.1500 293.1125 300.2625 319.6980 288.8495 -7.1520 293.2467 300.3986 319.8367 289.6973 -7.1591 293.4165 300.5756 320.0054 290.4635 -7.1606 293.5613 300.7219 320.2002 291.2905 -7.1661 293.7566 300.9226 320.4645 292.0873 -7.1712 293.9375 301.1086 320.7004 292.8840 -7.1762 294.0898 301.2660 320.9503 293.7110 -7.1814 294.2731 301.4545 321.2558 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