DTA measure 21_meres Date: 20251118:1122 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.68 s Mass = 1094.200 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3578 -10.4158 447.9540 458.3698 433.5888 3.9613 -10.4168 448.0086 458.4254 433.9109 5.5696 -10.4191 448.0573 458.4764 434.2452 7.1730 -10.4199 448.0776 458.4975 434.4865 8.7970 -10.4213 448.1418 458.5630 434.6356 10.4004 -10.4238 448.2147 458.6386 434.7097 12.0088 -10.4313 448.2423 458.6736 434.6471 13.6121 -10.4320 448.2615 458.6935 434.4985 15.2153 -10.4346 448.3020 458.7366 434.2488 16.8239 -10.4353 448.3175 458.7528 433.8853 18.4274 -10.4353 448.4139 458.8492 433.4804 20.0513 -10.4331 448.4290 458.8621 432.9551 21.6445 -10.4329 448.4529 458.8859 432.4517 23.2528 -10.4330 448.4740 458.9069 431.9147 24.8563 -10.4356 448.5145 458.9501 431.3778 26.4650 -10.4397 448.5571 458.9968 430.8172 28.0733 -10.4504 448.5713 459.0217 430.2821 29.6819 -10.4577 448.5792 459.0369 429.7827 31.2905 -10.4650 448.5920 459.0570 429.3380 32.9143 -10.4690 448.6067 459.0756 428.9440 34.5178 -10.4679 448.6303 459.0982 428.6238 36.1213 -10.4751 448.6280 459.1031 428.3274 37.7298 -10.4799 448.6024 459.0823 428.1098 39.3383 -10.4806 448.6185 459.0992 428.0234 40.9469 -10.4833 448.5803 459.0636 428.0309 42.5504 -10.4923 448.5707 459.0630 428.0692 44.1741 -10.4996 448.5702 459.0698 428.1113 45.7778 -10.5005 448.5097 459.0101 428.1943 47.3914 -10.4981 448.4827 458.9808 428.2786 48.9948 -10.5071 448.4658 458.9729 428.3058 50.5725 -10.5092 448.4749 458.9841 428.3146 52.1809 -10.5151 448.4754 458.9905 428.2777 53.7794 -10.5179 448.4500 458.9678 428.1748 55.3776 -10.5137 448.3817 458.8954 428.0239 56.9860 -10.5160 448.3720 458.8880 427.8156 58.5895 -10.5242 448.3738 458.8979 427.5884 60.1879 -10.5264 448.2611 458.7875 427.2640 61.7963 -10.5282 448.1254 458.6535 426.9293 63.3998 -10.5335 448.1446 458.6782 426.6120 65.0081 -10.5446 448.1203 458.6648 426.2192 66.5961 -10.5450 448.1309 458.6759 425.8161 68.2048 -10.5496 448.0800 458.6296 425.4109 69.8079 -10.5535 447.9939 458.5474 425.0414 71.4268 -10.5586 447.9385 458.4971 424.6290 73.0354 -10.5645 447.8972 458.4616 424.2998 74.6386 -10.5707 447.8531 458.4239 423.9661 76.2473 -10.5788 447.8116 458.3905 423.6599 77.8508 -10.5862 447.7323 458.3185 423.4315 79.4591 -10.5921 447.6935 458.2857 423.2397 81.0626 -10.5976 447.6496 458.2472 423.0667 82.6764 -10.6105 447.6068 458.2173 422.9402 84.2796 -10.6159 447.5411 458.1570 422.8553 85.8985 -10.6244 447.4448 458.0692 422.7889 87.5071 -10.6381 447.3651 458.0032 422.7486 89.1155 -10.6458 447.2453 457.8911 422.6914 90.7241 -10.6547 447.1611 457.8158 422.5998 92.3275 -10.6598 447.0896 457.7494 422.5214 93.9410 -10.6689 446.9752 457.6441 422.3635 95.5445 -10.6816 446.8686 457.5502 422.2077 97.1684 -10.6864 446.8310 457.5174 422.0693 98.7718 -10.6939 446.7847 457.4786 421.9223 100.3854 -10.7042 446.7033 457.4075 421.7056 101.9886 -10.7079 446.6142 457.3221 421.5184 103.5869 -10.7080 446.5311 457.2391 421.2663 105.1903 -10.7159 446.4259 457.1418 420.9760 106.8193 -10.7250 446.2855 457.0105 420.6766 108.4226 -10.7303 446.2244 456.9547 420.3459 110.0363 -10.7363 446.0893 456.8257 420.0297 111.6396 -10.7415 446.0055 456.7470 419.6827 113.2431 -10.7445 445.8850 456.6295 419.3477 114.8413 -10.7507 445.8293 456.5800 419.0620 116.4448 -10.7567 445.7258 456.4825 418.7779 118.0584 -10.7657 445.6136 456.3793 418.5239 119.6514 -10.7693 445.5302 456.2995 418.2837 121.2498 -10.7717 445.4085 456.1802 418.0755 122.8530 -10.7750 445.2806 456.0556 417.9042 124.4564 -10.7784 445.1968 455.9752 417.6813 126.0600 -10.7871 445.0855 455.8726 417.5137 127.6684 -10.7952 444.9239 455.7191 417.4082 129.2564 -10.8025 444.8084 455.6109 417.3108 130.8650 -10.8093 444.6673 455.4766 417.1917 132.4836 -10.8145 444.5645 455.3790 417.0921 134.0871 -10.8188 444.4928 455.3116 416.9489 135.6958 -10.8269 444.3715 455.1984 416.8095 137.2989 -10.8329 444.2525 455.0854 416.6892 138.8923 -10.8382 444.1178 454.9560 416.5210 140.5163 -10.8387 443.9794 454.8180 416.3201 142.1041 -10.8414 443.8596 454.7009 416.1463 143.7078 -10.8412 443.7218 454.5629 415.9302 145.3164 -10.8477 443.5889 454.4366 415.6672 146.9403 -10.8504 443.4990 454.3494 415.3974 148.5488 -10.8541 443.3757 454.2298 415.1642 150.1419 -10.8587 443.2534 454.1121 414.9300 151.7503 -10.8586 443.0998 453.9583 414.6502 153.3538 -10.8652 442.9519 453.8170 414.3727 154.9624 -10.8667 442.8542 453.7209 414.1005 156.5656 -10.8751 442.7335 453.6086 413.8378 158.1793 -10.8774 442.6246 453.5021 413.5142 159.7929 -10.8740 442.4764 453.3505 413.2250 161.3911 -10.8751 442.3503 453.2254 413.0044 162.9998 -10.8786 442.1470 453.0256 412.7899 164.6083 -10.8831 442.0147 452.8978 412.6063 166.2166 -10.8858 441.8272 452.7130 412.4303 167.8253 -10.8865 441.7089 452.5954 412.2493 169.4335 -10.8919 441.5531 452.4450 412.0593 171.0421 -10.8898 441.4528 452.3426 411.8464 172.6555 -10.8887 441.3030 452.1917 411.6498 174.2488 -10.8925 441.1328 452.0253 411.4572 175.8523 -10.8969 440.9348 451.8317 411.2742 177.4605 -10.8944 440.7733 451.6677 411.1960 179.0743 -10.8952 440.6412 451.5364 411.0312 180.6776 -10.8915 440.5050 451.3966 410.8798 182.2708 -10.8875 440.3873 451.2748 410.7318 183.8691 -10.8921 440.2702 451.1622 410.5558 185.4776 -10.8884 440.1031 450.9915 410.3609 187.0759 -10.8892 439.9599 450.8492 410.1543 188.6794 -10.8901 439.8132 450.7033 409.9269 190.2878 -10.8981 439.6570 450.5550 409.6633 191.9065 -10.8946 439.4994 450.3940 409.3596 193.5151 -10.8930 439.3361 450.2291 409.1242 195.1183 -10.8955 439.1594 450.0550 408.8359 196.7218 -10.8893 438.9615 449.8507 408.5861 198.3303 -10.8834 438.8033 449.6867 408.3729 199.9336 -10.8871 438.6936 449.5807 408.1741 201.5421 -10.8900 438.5543 449.4443 408.0012 203.1608 -10.8915 438.4199 449.3114 407.7398 204.7694 -10.8861 438.2211 449.1072 407.4975 206.3726 -10.8820 438.0130 448.8950 407.3231 207.9863 -10.8842 437.8738 448.7580 407.1017 209.5898 -10.8849 437.7444 448.6292 406.8998 211.1933 -10.8843 437.5546 448.4389 406.7174 212.8068 -10.8810 437.4190 448.3000 406.4954 214.4256 -10.8737 437.2240 448.0977 406.3029 216.0340 -10.8741 437.0673 447.9414 406.1111 217.6374 -10.8734 436.8675 447.7410 405.8950 219.2511 -10.8733 436.6727 447.5460 405.7059 220.8543 -10.8695 436.5096 447.3792 405.5128 222.4680 -10.8645 436.3305 447.1950 405.3185 224.0663 -10.8613 436.1704 447.0318 405.0850 225.6696 -10.8578 436.0187 446.8764 404.8958 227.2783 -10.8542 435.8847 446.7388 404.6447 228.9021 -10.8523 435.7015 446.5538 404.4243 230.5106 -10.8532 435.5465 446.3997 404.2261 232.1193 -10.8556 435.3550 446.2106 404.0504 233.7329 -10.8514 435.1867 446.0381 403.8451 235.3361 -10.8521 435.0421 445.8941 403.5661 236.9551 -10.8485 434.8617 445.7102 403.3507 238.5480 -10.8459 434.6812 445.5271 403.0900 240.1565 -10.8447 434.4892 445.3340 402.8750 241.7753 -10.8399 434.3067 445.1465 402.6569 243.3785 -10.8414 434.1486 444.9900 402.4396 244.9665 -10.8400 433.9814 444.8214 402.2406 246.5646 -10.8343 433.7919 444.6262 402.0387 248.1681 -10.8311 433.6055 444.4367 401.8312 249.7713 -10.8285 433.4082 444.2367 401.6244 251.3645 -10.8285 433.2348 444.0633 401.4313 252.9680 -10.8272 433.0307 443.8579 401.2101 254.5660 -10.8246 432.8618 443.6864 401.0058 256.1900 -10.8176 432.7043 443.5219 400.7825 257.7934 -10.8184 432.5093 443.3278 400.6103 259.3865 -10.8129 432.3284 443.1413 400.4380 260.9900 -10.8131 432.1402 442.9532 400.2470 262.5934 -10.8099 431.9620 442.7719 400.0685 264.2019 -10.8002 431.8027 442.6029 399.8794 265.8053 -10.8014 431.6476 442.4490 399.6706 267.4136 -10.8022 431.4638 442.2660 399.4646 269.0325 -10.7921 431.2921 442.0842 399.2859 270.6461 -10.7905 431.1112 441.9018 399.1232 272.2340 -10.7893 430.9149 441.7042 398.8962 273.8426 -10.7885 430.7302 441.5188 398.6839 275.4460 -10.7913 430.5575 441.3488 398.4752 277.0596 -10.7880 430.3601 441.1481 398.2547 278.6631 -10.7906 430.1663 440.9568 397.9982 280.2663 -10.7848 429.9739 440.7587 397.7694 281.8903 -10.7814 429.7679 440.5493 397.4661 283.4935 -10.7802 429.6205 440.4007 397.2165 285.1020 -10.7794 429.4223 440.2017 396.9696 286.7055 -10.7743 429.2362 440.0105 396.6705 288.3191 -10.7705 429.0322 439.8027 396.4709 289.9225 -10.7620 428.8386 439.6006 396.2499 291.5310 -10.7582 428.6057 439.3638 396.0561 293.1495 -10.7536 428.4125 439.1662 395.8643 294.7428 -10.7484 428.2764 439.0248 395.6543 296.3666 -10.7435 428.1167 438.8602 395.4436 297.9750 -10.7396 427.8858 438.6255 395.2207 299.5836 -10.7355 427.6986 438.4341 395.0509 301.1869 -10.7270 427.5246 438.2516 394.9099 302.8006 -10.7252 427.2591 437.9842 394.7277 304.4090 -10.7279 427.0815 437.8094 394.5463 306.0175 -10.7235 426.8793 437.6028 394.3912 307.6313 -10.7210 426.7027 437.4237 394.1681 309.2140 -10.7205 426.4956 437.2160 394.0287 310.8175 -10.7192 426.2698 436.9890 393.8899 312.4159 -10.7170 426.1162 436.8332 393.7174 314.0190 -10.7103 425.9428 436.6531 393.5067 315.6276 -10.7084 425.7179 436.4262 393.2671 317.2260 -10.7036 425.5323 436.2359 392.9939 318.8291 -10.6996 425.3527 436.0523 392.7381 320.4531 -10.6943 425.1587 435.8530 392.4726 322.0513 -10.6887 424.9903 435.6791 392.2215 323.6598 -10.6855 424.7947 435.4802 391.9392 325.2630 -10.6821 424.5972 435.2794 391.6977 326.8664 -10.6792 424.4045 435.0837 391.5044 328.4750 -10.6798 424.1952 434.8749 391.3013 330.0834 -10.6735 423.9735 434.6471 391.0768 331.7073 -10.6639 423.7589 434.4227 390.8398 333.3108 -10.6602 423.5510 434.2112 390.6031 334.9190 -10.6608 423.3632 434.0240 390.4348 336.5073 -10.6577 423.2146 433.8723 390.2513 338.1156 -10.6496 423.0393 433.6889 390.0737 339.7190 -10.6502 422.8304 433.4806 389.8475 341.3226 -10.6459 422.6022 433.2481 389.6856 342.9361 -10.6436 422.3861 433.0297 389.5116 344.5549 -10.6395 422.1394 432.7790 389.3304 346.1635 -10.6379 421.9462 432.5841 389.1026 347.7669 -10.6311 421.8312 432.4623 388.8809 349.3754 -10.6241 421.6204 432.2445 388.6747 350.9840 -10.6161 421.4108 432.0269 388.4345 352.5771 -10.6087 421.2143 431.8230 388.2236 354.1856 -10.6074 421.0368 431.6443 388.0234 355.7941 -10.6014 420.8243 431.4257 387.7981 357.4128 -10.6031 420.5836 431.1867 387.5717 359.0214 -10.6030 420.4142 431.0172 387.3387 360.6298 -10.5952 420.2202 430.8154 387.1028 362.2383 -10.5893 420.0049 430.5942 386.8673 363.8315 -10.5923 419.7726 430.3649 386.6617 365.4398 -10.5895 419.5316 430.1211 386.4628 367.0484 -10.5840 419.3596 429.9435 386.2572 368.6568 -10.5736 419.1984 429.7720 386.0213 370.2755 -10.5660 418.9955 429.5615 385.8051 371.8739 -10.5621 418.8061 429.3682 385.5761 373.4721 -10.5582 418.6101 429.1683 385.3674 375.0755 -10.5556 418.3877 428.9433 385.1517 376.6739 -10.5478 418.1991 428.7469 384.9421 378.2824 -10.5403 417.9844 428.5247 384.7181 379.8703 -10.5357 417.7424 428.2782 384.4922 381.4686 -10.5301 417.5272 428.0572 384.2969 383.0924 -10.5314 417.3068 427.8381 384.0988 384.6959 -10.5312 417.1168 427.6480 383.9451 386.3045 -10.5235 416.9198 427.4433 383.7584 387.9078 -10.5208 416.6864 427.2072 383.5825 389.5111 -10.5099 416.4704 426.9803 383.3968 391.1198 -10.5053 416.2909 426.7962 383.1899 392.7231 -10.5027 416.0793 426.5820 382.9586 394.3471 -10.4995 415.8591 426.3587 382.6956 395.9506 -10.4930 415.6794 426.1724 382.4747 397.5590 -10.4912 415.4781 425.9693 382.2858 399.1676 -10.4859 415.2749 425.7608 382.0659 400.7606 -10.4809 415.0398 425.5207 381.8875 402.3691 -10.4780 414.8212 425.2992 381.6992 403.9778 -10.4735 414.6420 425.1154 381.5081 405.5811 -10.4716 414.5140 424.9856 381.2884 407.2050 -10.4639 414.3040 424.7679 381.1177 408.8136 -10.4567 414.0996 424.5563 380.8807 410.4219 -10.4520 413.9252 424.3772 380.6693 412.0305 -10.4496 413.7255 424.1751 380.4088 413.6339 -10.4443 413.4825 423.9268 380.1635 415.2423 -10.4429 413.2882 423.7311 379.9569 416.8765 -10.4432 413.0447 423.4880 379.7591 418.4848 -10.4393 412.8281 423.2673 379.5503 420.0934 -10.4324 412.6250 423.0574 379.3167 421.7019 -10.4266 412.4126 422.8392 379.0902 423.3051 -10.4230 412.2134 422.6364 378.8677 424.9189 -10.4182 412.0219 422.4401 378.6415 426.5223 -10.4174 411.7877 422.2051 378.4170 428.1513 -10.4079 411.5646 421.9725 378.1973 429.7548 -10.4049 411.3645 421.7694 378.0318 431.3684 -10.4013 411.1410 421.5422 377.8099 432.9718 -10.4005 410.9138 421.3143 377.6352 434.5753 -10.3910 410.6712 421.0621 377.4345 436.1633 -10.3831 410.4643 420.8475 377.2167 437.7615 -10.3812 410.2857 420.6669 376.9337 439.3701 -10.3812 410.1003 420.4814 376.7416 440.9836 -10.3752 409.8630 420.2382 376.5310 442.5870 -10.3693 409.6850 420.0543 376.3131 444.1954 -10.3618 409.5096 419.8714 376.0904 445.7988 -10.3602 409.3248 419.6850 375.8844 447.3818 -10.3536 409.1309 419.4845 375.7132 448.9901 -10.3560 408.9043 419.2604 375.5468 450.5935 -10.3479 408.6636 419.0114 375.3686 452.2021 -10.3377 408.4347 418.7724 375.1772 453.8206 -10.3283 408.2350 418.5633 374.9668 455.4293 -10.3214 408.0293 418.3507 374.7804 457.0326 -10.3227 407.8517 418.1745 374.5623 458.6461 -10.3211 407.6309 417.9521 374.3507 460.2495 -10.3125 407.4021 417.7145 374.1182 461.8426 -10.3076 407.1765 417.4840 373.8793 463.4511 -10.3016 406.9796 417.2812 373.6314 465.0545 -10.2946 406.7923 417.0869 373.4227 466.6784 -10.2870 406.5582 416.8451 373.1564 468.2870 -10.2832 406.3547 416.6379 372.9650 469.8954 -10.2729 406.1542 416.4272 372.7394 471.4988 -10.2688 405.9371 416.2059 372.5360 473.1074 -10.2688 405.7241 415.9930 372.3437 474.7159 -10.2687 405.5021 415.7709 372.1167 476.3244 -10.2622 405.2979 415.5600 371.8950 477.9431 -10.2573 405.1320 415.3894 371.6795 479.5566 -10.2450 404.9635 415.2085 371.4587 481.1601 -10.2370 404.7067 414.9437 371.2638 482.7738 -10.2357 404.4737 414.7094 371.0852 484.3771 -10.2277 404.2323 414.4601 370.8792 485.9856 -10.2222 404.0478 414.2700 370.6401 487.5789 -10.2139 403.8796 414.0934 370.4213 489.1924 -10.2068 403.6762 413.8831 370.2086 490.8109 -10.2070 403.4296 413.6367 369.9831 492.4245 -10.1944 403.2200 413.4145 369.7497 494.0280 -10.1865 403.0183 413.2048 369.5198 495.6365 -10.1804 402.8308 413.0112 369.3335 497.2450 -10.1714 402.6396 412.8110 369.1431 498.8536 -10.1673 402.3767 412.5440 368.9344 500.4516 -10.1633 402.1719 412.3352 368.7351 502.0398 -10.1524 401.9740 412.1265 368.5367 503.6585 -10.1447 401.7527 411.8974 368.3364 505.2619 -10.1407 401.5203 411.6610 368.1304 506.8653 -10.1374 401.3139 411.4513 367.9274 508.4736 -10.1346 401.1186 411.2532 367.7267 510.0618 -10.1329 400.9052 411.0382 367.5554 511.6704 -10.1300 400.6757 410.8057 367.3589 513.2735 -10.1308 400.4265 410.5573 367.1353 514.8821 -10.1273 400.2324 410.3596 366.9097 516.5009 -10.1206 400.0406 410.1612 366.7017 518.1044 -10.1159 399.7989 409.9148 366.4611 519.7130 -10.1040 399.5652 409.6692 366.2135 521.3216 -10.0926 399.3998 409.4924 365.9840 522.9300 -10.0809 399.2059 409.2868 365.8089 524.5335 -10.0780 399.0007 409.0787 365.5765 526.1421 -10.0695 398.7866 408.8562 365.3790 527.7608 -10.0619 398.5923 408.6542 365.1010 529.3745 -10.0517 398.3803 408.4320 364.8186 530.9780 -10.0452 398.1985 408.2436 364.5996 532.5710 -10.0577 397.9836 408.0413 364.4284 534.1745 -10.0685 397.7650 407.8335 364.2583 535.7830 -10.0773 397.5576 407.6349 364.0635 537.3914 -10.0837 397.3670 407.4507 363.8332 539.0051 -10.0858 397.1131 407.1989 363.6011 540.6236 -10.0819 396.8786 406.9605 363.3446 542.2323 -10.0760 396.6524 406.7284 363.1465 543.8406 -10.0736 396.4967 406.5702 362.9755 545.4439 -10.0737 396.2816 406.3553 362.8334 547.0525 -10.0694 396.0111 406.0805 362.6474 548.6560 -10.0645 395.7756 405.8401 362.4457 550.2645 -10.0611 395.5850 405.6461 362.2405 551.8884 -10.0602 395.4005 405.4607 362.0575 553.4968 -10.0520 395.2034 405.2553 361.8608 555.1053 -10.0427 394.9890 405.0317 361.6693 556.7138 -10.0382 394.8283 404.8665 361.4645 558.3170 -10.0331 394.5933 404.6264 361.2568 559.9256 -10.0267 394.3810 404.4077 360.9914 561.5340 -10.0206 394.1807 404.2012 360.7517 563.1528 -10.0210 393.9435 403.9645 360.5792 564.7560 -10.0161 393.7201 403.7362 360.3340 566.3543 -10.0133 393.4922 403.5055 360.0984 567.9578 -10.0092 393.2776 403.2868 359.8911 569.5559 -10.0007 393.0732 403.0739 359.6668 571.1593 -9.8205 393.0132 402.8337 359.4445 572.7678 -9.4309 393.2485 402.6794 359.2000 574.3864 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