DTA measure 1lassu Date: 2025318:1149 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1238.03 s Mass = 924.800 mg data_number = 1540 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1958 -2.2133 261.2273 263.4406 262.1053 1.9220 -2.2125 261.2465 263.4589 262.0617 2.7823 -2.2120 261.2731 263.4851 261.9991 3.5500 -2.2113 261.2911 263.5024 261.9404 4.3793 -2.2097 261.3071 263.5168 261.8735 5.1675 -2.2087 261.3214 263.5301 261.8062 5.9660 -2.2067 261.3400 263.5468 261.7362 6.7953 -2.2050 261.3626 263.5676 261.6592 7.5525 -2.2046 261.3823 263.5868 261.5847 8.4130 -2.2028 261.4039 263.6067 261.4963 9.1808 -2.2007 261.4213 263.6220 261.4165 10.0100 -2.1988 261.4454 263.6442 261.3217 10.7980 -2.1965 261.4680 263.6645 261.2311 11.5965 -2.1944 261.4890 263.6834 261.1364 12.4260 -2.1917 261.5172 263.7089 261.0339 13.1830 -2.1892 261.5406 263.7298 260.9402 14.0228 -2.1859 261.5653 263.7511 260.8414 14.7798 -2.1826 261.5904 263.7730 260.7435 15.6403 -2.1790 261.6204 263.7995 260.6284 16.4078 -2.1752 261.6407 263.8159 260.5215 17.2373 -2.1711 261.6643 263.8354 260.3998 18.0253 -2.1673 261.6914 263.8587 260.2856 18.8235 -2.1637 261.7169 263.8806 260.1623 19.6530 -2.1598 261.7433 263.9031 260.0352 20.4100 -2.1563 261.7685 263.9249 259.9117 21.2703 -2.1521 261.8002 263.9523 259.7728 22.0378 -2.1485 261.8262 263.9746 259.6482 22.8673 -2.1451 261.8507 263.9958 259.5129 23.6553 -2.1414 261.8745 264.0159 259.3786 24.4640 -2.1372 261.9039 264.0411 259.2437 25.2830 -2.1334 261.9296 264.0630 259.1024 26.0400 -2.1290 261.9530 264.0820 258.9749 26.9003 -2.1241 261.9815 264.1056 258.8289 27.6573 -2.1195 262.0064 264.1259 258.6979 28.4760 -2.1136 262.0269 264.1405 258.5539 29.2743 -2.1085 262.0573 264.1658 258.4120 30.0728 -2.1043 262.0954 264.1997 258.2684 30.9020 -2.0990 262.1262 264.2253 258.1137 31.6593 -2.0937 262.1487 264.2424 257.9731 32.5090 -2.0884 262.1765 264.2649 257.8255 33.2870 -2.0831 262.2020 264.2851 257.6817 34.1060 -2.0779 262.2338 264.3117 257.5235 34.8733 -2.0725 262.2695 264.3419 257.3770 35.6923 -2.0675 262.3019 264.3695 257.2196 36.5010 -2.0620 262.3308 264.3927 257.0661 37.2893 -2.0563 262.3539 264.4102 256.9174 38.1080 -2.0509 262.3784 264.4293 256.7589 38.8855 -2.0450 262.4046 264.4496 256.6106 39.7355 -2.0387 262.4265 264.4652 256.4471 40.5030 -2.0329 262.4464 264.4793 256.2986 41.3320 -2.0267 262.4676 264.4943 256.1368 42.1303 -2.0200 262.4912 264.5112 255.9788 42.9183 -2.0141 262.5122 264.5263 255.8220 43.7580 -2.0075 262.5352 264.5428 255.6520 44.5148 -2.0013 262.5633 264.5646 255.5015 45.3648 -1.9946 262.5867 264.5813 255.3270 46.1425 -1.9883 262.6070 264.5952 255.1741 46.9618 -1.9819 262.6290 264.6108 255.0114 47.7600 -1.9749 262.6460 264.6208 254.8565 48.5583 -1.9677 262.6647 264.6324 254.7015 49.3875 -1.9611 262.6824 264.6436 254.5406 50.1448 -1.9550 262.7037 264.6587 254.3976 51.0050 -1.9472 262.7338 264.6810 254.2380 51.7413 -1.9404 262.7557 264.6961 254.0975 52.6015 -1.9334 262.7743 264.7077 253.9310 53.3690 -1.9273 262.7937 264.7210 253.7857 54.1880 -1.9212 262.8151 264.7363 253.6348 54.9863 -1.9144 262.8329 264.7473 253.4883 55.7848 -1.9081 262.8509 264.7590 253.3470 56.6140 -1.9013 262.8724 264.7737 253.2042 57.3710 -1.8958 262.8929 264.7887 253.0783 58.2210 -1.8894 262.9106 264.7999 252.9390 58.9988 -1.8831 262.9306 264.8138 252.8115 59.8178 -1.8768 262.9478 264.8247 252.6806 60.6160 -1.8704 262.9606 264.8310 252.5632 61.4040 -1.8638 262.9772 264.8410 252.4478 62.2230 -1.8576 262.9920 264.8496 252.3298 62.9903 -1.8516 263.0035 264.8551 252.2212 63.8093 -1.8450 263.0139 264.8589 252.1123 64.5870 -1.8391 263.0301 264.8692 252.0159 65.4368 -1.8323 263.0462 264.8785 251.9197 66.1938 -1.8268 263.0628 264.8895 251.8341 67.0335 -1.8199 263.0849 264.9048 251.7468 67.8215 -1.8140 263.0992 264.9132 251.6775 68.6198 -1.8074 263.1110 264.9184 251.6103 69.4388 -1.8016 263.1283 264.9300 251.5451 70.2163 -1.7964 263.1390 264.9355 251.4899 71.0353 -1.7906 263.1458 264.9364 251.4463 71.8025 -1.7856 263.1538 264.9394 251.4132 72.6628 -1.7806 263.1639 264.9444 251.3846 73.4198 -1.7755 263.1714 264.9468 251.3630 74.2493 -1.7696 263.1799 264.9495 251.3538 75.0478 -1.7643 263.1898 264.9541 251.3583 75.8460 -1.7593 263.1999 264.9593 251.3654 76.6648 -1.7542 263.2076 264.9618 251.3770 77.4425 -1.7499 263.2144 264.9643 251.3953 78.2928 -1.7450 263.2249 264.9698 251.4278 79.0498 -1.7404 263.2301 264.9705 251.4655 79.8893 -1.7358 263.2384 264.9743 251.5121 80.6460 -1.7312 263.2463 264.9775 251.5667 81.4855 -1.7269 263.2580 264.9849 251.6379 82.2735 -1.7227 263.2601 264.9828 251.7096 83.0720 -1.7184 263.2619 264.9803 251.7906 83.8908 -1.7147 263.2723 264.9870 251.8905 84.6683 -1.7110 263.2789 264.9899 251.9949 85.5183 -1.7064 263.2857 264.9921 252.1211 86.2855 -1.7037 263.2940 264.9977 252.2371 87.1148 -1.7005 263.3034 265.0039 252.3748 87.9028 -1.6972 263.3077 265.0048 252.5157 88.7115 -1.6949 263.3131 265.0081 252.6684 89.5305 -1.6927 263.3229 265.0157 252.8334 90.2978 -1.6909 263.3279 265.0188 252.9989 91.1478 -1.6887 263.3336 265.0223 253.1857 91.8840 -1.6871 263.3380 265.0251 253.3570 92.7443 -1.6835 263.3452 265.0287 253.5614 93.5010 -1.6813 263.3524 265.0336 253.7539 94.3305 -1.6801 263.3582 265.0383 253.9691 95.1185 -1.6780 263.3647 265.0427 254.1811 95.9068 -1.6766 263.3731 265.0497 254.3980 96.7360 -1.6754 263.3714 265.0468 254.6383 97.5030 -1.6727 263.3770 265.0497 254.8609 98.3633 -1.6717 263.3845 265.0562 255.1271 99.1205 -1.6706 263.3948 265.0655 255.3642 99.9398 -1.6697 263.4076 265.0773 255.6265 100.7380 -1.6691 263.4159 265.0850 255.8885 101.5365 -1.6687 263.4204 265.0892 256.1552 102.3658 -1.6686 263.4295 265.0981 256.4320 103.1228 -1.6687 263.4384 265.1071 256.6882 103.9830 -1.6685 263.4428 265.1112 256.9886 104.7503 -1.6684 263.4485 265.1169 257.2559 105.5695 -1.6692 263.4572 265.1265 257.5419 106.3680 -1.6699 263.4712 265.1411 257.8300 107.1665 -1.6708 263.4811 265.1519 258.1193 107.9960 -1.6712 263.4969 265.1682 258.4191 108.7528 -1.6726 263.5090 265.1816 258.6985 109.6233 -1.6745 263.5195 265.1940 259.0154 110.3805 -1.6761 263.5299 265.2061 259.2971 111.2100 -1.6772 263.5473 265.2245 259.6055 112.0083 -1.6779 263.5647 265.2426 259.9027 112.7960 -1.6790 263.5810 265.2600 260.1944 113.6358 -1.6802 263.5994 265.2796 260.5094 114.3930 -1.6822 263.6193 265.3015 260.7873 115.2223 -1.6850 263.6389 265.3239 261.0902 115.9895 -1.6869 263.6567 265.3436 261.3655 116.8498 -1.6894 263.6810 265.3704 261.6723 117.6068 -1.6918 263.7009 265.3927 261.9370 118.4463 -1.6936 263.7227 265.4163 262.2308 119.2343 -1.6963 263.7440 265.4403 262.5041 120.0325 -1.6992 263.7636 265.4627 262.7757 120.8620 -1.7023 263.7854 265.4877 263.0562 121.6293 -1.7046 263.8083 265.5129 263.3157 122.4793 -1.7077 263.8312 265.5389 263.5951 123.2468 -1.7099 263.8550 265.5649 263.8437 124.0658 -1.7133 263.8814 265.5947 264.1033 124.8333 -1.7167 263.9056 265.6223 264.3405 125.6520 -1.7201 263.9373 265.6574 264.5925 126.4503 -1.7237 263.9707 265.6944 264.8276 127.2383 -1.7274 264.0009 265.7283 265.0563 128.0573 -1.7310 264.0311 265.7622 265.2873 128.8353 -1.7343 264.0590 265.7933 265.5014 129.6850 -1.7381 264.0908 265.8289 265.7275 130.4523 -1.7418 264.1237 265.8655 265.9341 131.2713 -1.7456 264.1590 265.9047 266.1515 132.0490 -1.7490 264.1890 265.9380 266.3433 132.8678 -1.7528 264.2188 265.9716 266.5383 133.6558 -1.7561 264.2520 266.0081 266.7144 134.4643 -1.7600 264.2873 266.0472 266.8972 135.2833 -1.7638 264.3205 266.0842 267.0714 136.0510 -1.7669 264.3469 266.1138 267.2266 136.9010 -1.7707 264.3887 266.1595 267.3968 137.6790 -1.7744 264.4257 266.2001 267.5433 138.4978 -1.7777 264.4610 266.2388 267.6936 139.2860 -1.7812 264.5019 266.2832 267.8320 140.0950 -1.7849 264.5394 266.3243 267.9676 140.9140 -1.7880 264.5797 266.3677 268.1014 141.6813 -1.7911 264.6154 266.4064 268.2206 142.5008 -1.7945 264.6554 266.4499 268.3416 143.2783 -1.7978 264.6948 266.4926 268.4504 144.1283 -1.8006 264.7416 266.5422 268.5660 144.9160 -1.8036 264.7827 266.5863 268.6674 145.7248 -1.8066 264.8197 266.6263 268.7641 146.5130 -1.8094 264.8585 266.6679 268.8548 147.3215 -1.8118 264.9077 266.7196 268.9441 148.1408 -1.8145 264.9593 266.7739 269.0267 148.9080 -1.8178 265.0087 266.8265 269.0979 149.7583 -1.8198 265.0618 266.8816 269.1659 150.5360 -1.8232 265.1087 266.9319 269.2266 151.3548 -1.8256 265.1576 266.9832 269.2932 152.1428 -1.8272 265.2029 267.0301 269.3476 152.9518 -1.8295 265.2493 267.0788 269.4013 153.7708 -1.8326 265.2969 267.1295 269.4450 154.5380 -1.8345 265.3430 267.1775 269.4799 155.3883 -1.8369 265.3911 267.2281 269.5167 156.1450 -1.8388 265.4363 267.2751 269.5497 156.9743 -1.8407 265.4914 267.3321 269.5806 157.7623 -1.8423 265.5397 267.3820 269.6031 158.5605 -1.8439 265.5919 267.4358 269.6218 159.3900 -1.8463 265.6432 267.4894 269.6373 160.1470 -1.8480 265.6898 267.5378 269.6496 161.0073 -1.8493 265.7454 267.5947 269.6608 161.7643 -1.8499 265.7947 267.6447 269.6629 162.5935 -1.8506 265.8549 267.7055 269.6667 163.3920 -1.8520 265.9139 267.7659 269.6688 164.1800 -1.8531 265.9711 267.8242 269.6683 165.0093 -1.8540 266.0280 267.8820 269.6556 165.7870 -1.8546 266.0775 267.9321 269.6422 166.5853 -1.8554 266.1281 267.9835 269.6323 167.4043 -1.8554 266.1811 268.0365 269.6153 168.1928 -1.8557 266.2355 268.0912 269.5988 169.0013 -1.8562 266.2943 268.1505 269.5840 169.8203 -1.8568 266.3449 268.2017 269.5630 170.5878 -1.8568 266.3927 268.2495 269.5417 171.4378 -1.8573 266.4525 268.3098 269.5199 172.2463 -1.8575 266.5076 268.3651 269.4986 173.0343 -1.8581 266.5626 268.4207 269.4780 173.8538 -1.8592 266.6155 268.4747 269.4536 174.6313 -1.8596 266.6656 268.5252 269.4311 175.4813 -1.8585 266.7232 268.5817 269.4067 176.2385 -1.8579 266.7754 268.6333 269.3829 177.0783 -1.8571 266.8327 268.6899 269.3534 177.8455 -1.8569 266.8811 268.7380 269.3272 178.7058 -1.8563 266.9487 268.8050 269.3036 179.4628 -1.8556 267.0003 268.8559 269.2785 180.3028 -1.8546 267.0569 268.9115 269.2522 181.0908 -1.8540 267.1128 268.9668 269.2331 181.8890 -1.8531 267.1677 269.0208 269.2079 182.7078 -1.8525 267.2290 269.0815 269.1833 183.4858 -1.8518 267.2856 269.1374 269.1614 184.3358 -1.8496 267.3464 269.1960 269.1439 185.1133 -1.8488 267.3987 269.2475 269.1258 185.9323 -1.8474 267.4527 269.3001 269.1107 186.6890 -1.8458 267.5074 269.3532 269.0952 187.5183 -1.8454 267.5726 269.4180 269.0823 188.3168 -1.8440 267.6294 269.4733 269.0766 189.1050 -1.8423 267.6864 269.5287 269.0720 189.9343 -1.8414 267.7456 269.5870 269.0681 190.6918 -1.8402 267.7962 269.6364 269.0698 191.5520 -1.8382 267.8548 269.6930 269.0688 192.2778 -1.8369 267.9063 269.7431 269.0727 193.1383 -1.8348 267.9684 269.8032 269.0844 193.9058 -1.8333 268.0209 269.8542 269.0973 194.7248 -1.8315 268.0758 269.9073 269.1131 195.5230 -1.8303 268.1313 269.9616 269.1373 196.3110 -1.8295 268.1862 270.0157 269.1607 197.1508 -1.8289 268.2443 270.0732 269.1893 197.9078 -1.8284 268.2928 270.1212 269.2199 198.7578 -1.8268 268.3487 270.1755 269.2564 199.5353 -1.8252 268.4000 270.2252 269.2974 200.3543 -1.8238 268.4562 270.2800 269.3449 201.1530 -1.8228 268.5087 270.3315 269.3967 201.9408 -1.8219 268.5605 270.3824 269.4544 202.7495 -1.8205 268.6146 270.4352 269.5156 203.5375 -1.8188 268.6648 270.4837 269.5797 204.3568 -1.8173 268.7180 270.5353 269.6512 205.1343 -1.8163 268.7704 270.5867 269.7235 205.9840 -1.8154 268.8324 270.6478 269.8136 206.7513 -1.8146 268.8871 270.7017 269.8979 207.5703 -1.8139 268.9469 270.7609 269.9908 208.3793 -1.8129 269.0082 270.8211 270.0890 209.1673 -1.8122 269.0671 270.8793 270.1946 210.0070 -1.8112 269.1289 270.9402 270.3090 210.7638 -1.8110 269.1821 270.9931 270.4131 211.6138 -1.8105 269.2412 271.0517 270.5333 212.3918 -1.8099 269.2922 271.1021 270.6547 213.2108 -1.8094 269.3488 271.1582 270.7887 213.9780 -1.8082 269.3997 271.2080 270.9131 214.7968 -1.8080 269.4559 271.2639 271.0486 215.6363 -1.8079 269.5194 271.3272 271.1960 216.3933 -1.8085 269.5726 271.3811 271.3308 217.2123 -1.8081 269.6294 271.4375 271.4852 217.9903 -1.8082 269.6805 271.4887 271.6333 218.8400 -1.8089 269.7435 271.5523 271.8025 219.6073 -1.8096 269.7971 271.6067 271.9589 220.4263 -1.8091 269.8494 271.6586 272.1313 221.2143 -1.8097 269.9004 271.7101 272.3027 222.0228 -1.8105 269.9553 271.7658 272.4839 222.8420 -1.8108 270.0138 271.8247 272.6637 223.6093 -1.8120 270.0697 271.8817 272.8357 224.4593 -1.8123 270.1332 271.9455 273.0307 225.2160 -1.8127 270.1882 272.0009 273.2098 226.0560 -1.8129 270.2502 272.0631 273.4154 226.8440 -1.8134 270.3064 272.1199 273.6048 227.6423 -1.8138 270.3600 272.1738 273.7990 228.4613 -1.8140 270.4216 272.2357 274.0028 229.2388 -1.8149 270.4783 272.2932 274.1973 230.0578 -1.8161 270.5393 272.3554 274.4055 230.8250 -1.8171 270.5949 272.4119 274.6020 231.6853 -1.8192 270.6567 272.4759 274.8246 232.4423 -1.8202 270.7154 272.5356 275.0192 233.2715 -1.8214 270.7788 272.6002 275.2369 234.0698 -1.8220 270.8385 272.6606 275.4464 234.8683 -1.8236 270.8955 272.7191 275.6559 235.6873 -1.8243 270.9563 272.7807 275.8674 236.4545 -1.8255 271.0210 272.8465 276.0627 237.3153 -1.8273 271.0953 272.9226 276.2828 238.0720 -1.8295 271.1596 272.9892 276.4841 238.9018 -1.8324 271.2214 273.0539 276.6995 239.7000 -1.8346 271.2803 273.1149 276.9076 240.4983 -1.8361 271.3448 273.1809 277.1116 241.3175 -1.8386 271.4085 273.2470 277.3198 242.0850 -1.8408 271.4680 273.3088 277.5182 242.9453 -1.8427 271.5382 273.3809 277.7356 243.7025 -1.8445 271.5987 273.4432 277.9287 244.5418 -1.8466 271.6706 273.5172 278.1422 245.3298 -1.8488 271.7368 273.5855 278.3418 246.1283 -1.8508 271.8021 273.6530 278.5349 246.9578 -1.8534 271.8688 273.7222 278.7335 247.7250 -1.8552 271.9346 273.7899 278.9123 248.5748 -1.8578 272.0073 273.8651 279.1103 249.3523 -1.8601 272.0760 273.9361 279.2893 250.1715 -1.8622 272.1465 274.0086 279.4739 250.9598 -1.8638 272.2165 274.0803 279.6472 251.7583 -1.8660 272.2865 274.1524 279.8258 252.5773 -1.8683 272.3551 274.2234 280.0107 253.3550 -1.8707 272.4268 274.2975 280.1760 254.2050 -1.8732 272.5028 274.3760 280.3487 254.9620 -1.8761 272.5723 274.4484 280.4991 255.7913 -1.8789 272.6456 274.5245 280.6621 256.5793 -1.8815 272.7182 274.5997 280.8154 257.3775 -1.8837 272.7929 274.6766 280.9677 258.1763 -1.8869 272.8667 274.7536 281.1150 258.9640 -1.8898 272.9409 274.8307 281.2550 259.7933 -1.8923 273.0219 274.9142 281.4004 260.5608 -1.8953 273.0962 274.9914 281.5422 261.4210 -1.8975 273.1819 275.0794 281.6915 262.1780 -1.9001 273.2579 275.1579 281.8161 263.0075 -1.9028 273.3407 275.2435 281.9508 263.8058 -1.9052 273.4234 275.3286 282.0751 264.5938 -1.9079 273.4999 275.4078 282.1914 265.4230 -1.9107 273.5809 275.4916 282.3118 266.1908 -1.9134 273.6549 275.5684 282.4184 267.0510 -1.9166 273.7337 275.6503 282.5327 267.7768 -1.9185 273.8120 275.7304 282.6269 268.6370 -1.9206 273.8998 275.8204 282.7408 269.4043 -1.9220 273.9776 275.8996 282.8340 270.2338 -1.9242 274.0606 275.9848 282.9325 271.0323 -1.9264 274.1406 276.0670 283.0256 271.8200 -1.9283 274.2216 276.1498 283.1136 272.6493 -1.9306 274.3087 276.2392 283.2050 273.4168 -1.9325 274.3836 276.3161 283.2827 274.2770 -1.9335 274.4758 276.4092 283.3624 275.0448 -1.9347 274.5599 276.4946 283.4339 275.8740 -1.9365 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