DTA measure 2gyors Date: 2025318:1126 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1399.76 s Mass = 924.800 mg data_number = 1741 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2683 -5.1781 421.0680 426.2461 424.1496 2.0670 -5.1815 421.1863 426.3677 424.0877 2.8550 -5.1843 421.3033 426.4876 424.0177 3.6848 -5.1875 421.4260 426.6136 423.9374 4.4418 -5.1907 421.5307 426.7213 423.8559 5.3023 -5.1939 421.6491 426.8430 423.7541 6.0593 -5.1971 421.7546 426.9517 423.6593 6.8890 -5.1989 421.8713 427.0703 423.5532 7.6873 -5.2022 421.9777 427.1799 423.4435 8.4758 -5.2054 422.0898 427.2952 423.3285 9.3050 -5.2080 422.2060 427.4140 423.2044 10.0723 -5.2100 422.3159 427.5260 423.0835 10.9330 -5.2123 422.4361 427.6484 422.9437 11.6588 -5.2137 422.5363 427.7500 422.8254 12.5195 -5.2154 422.6532 427.8686 422.6695 13.2868 -5.2170 422.7530 427.9700 422.5291 14.1058 -5.2189 422.8642 428.0831 422.3728 14.9043 -5.2198 422.9698 428.1896 422.2163 15.7028 -5.2211 423.0734 428.2945 422.0499 16.5320 -5.2225 423.1793 428.4018 421.8724 17.2893 -5.2231 423.2797 428.5027 421.7083 18.1495 -5.2237 423.3843 428.6081 421.5202 18.9170 -5.2236 423.4816 428.7052 421.3449 19.7360 -5.2238 423.5838 428.8077 421.1550 20.5138 -5.2239 423.6782 428.9021 420.9706 21.3330 -5.2243 423.7806 429.0049 420.7789 22.1313 -5.2243 423.8778 429.1021 420.5884 22.9298 -5.2237 423.9690 429.1928 420.3923 23.7593 -5.2235 424.0696 429.2932 420.1801 24.5163 -5.2230 424.1584 429.3814 419.9850 25.3870 -5.2222 424.2585 429.4806 419.7588 26.1440 -5.2216 424.3432 429.5648 419.5585 26.9735 -5.2207 424.4337 429.6543 419.3359 27.7413 -5.2197 424.5188 429.7385 419.1320 28.5600 -5.2186 424.6089 429.8276 418.9153 29.3585 -5.2178 424.6934 429.9112 418.7001 30.1570 -5.2166 424.7765 429.9931 418.4855 30.9863 -5.2153 424.8612 430.0765 418.2591 31.7538 -5.2142 424.9385 430.1527 418.0481 32.6140 -5.2127 425.0279 430.2406 417.8086 33.3713 -5.2109 425.1021 430.3130 417.5993 34.1903 -5.2099 425.1826 430.3925 417.3686 34.9890 -5.2084 425.2594 430.4678 417.1492 35.7878 -5.2071 425.3365 430.5436 416.9230 36.6170 -5.2058 425.4197 430.6255 416.6879 37.3740 -5.2037 425.4869 430.6906 416.4720 38.2240 -5.2012 425.5615 430.7627 416.2310 38.9710 -5.2003 425.6246 430.8249 416.0223 39.8210 -5.1986 425.6984 430.8969 415.7888 40.5885 -5.1971 425.7698 430.9670 415.5744 41.4078 -5.1961 425.8444 431.0404 415.3494 42.2163 -5.1939 425.9145 431.1085 415.1266 43.0045 -5.1915 425.9813 431.1728 414.9075 43.8238 -5.1897 426.0468 431.2366 414.6815 44.6013 -5.1877 426.1045 431.2922 414.4722 45.4513 -5.1855 426.1667 431.3523 414.2459 46.2190 -5.1844 426.2208 431.4053 414.0427 47.0378 -5.1825 426.2796 431.4621 413.8226 47.8465 -5.1804 426.3365 431.5169 413.6171 48.6348 -5.1784 426.3909 431.5693 413.4186 49.4538 -5.1768 426.4497 431.6265 413.2087 50.2313 -5.1754 426.4964 431.6718 413.0121 51.0818 -5.1737 426.5498 431.7234 412.8010 51.8593 -5.1714 426.5994 431.7708 412.6077 52.6783 -5.1694 426.6487 431.8180 412.4055 53.4768 -5.1681 426.6926 431.8607 412.2131 54.2648 -5.1665 426.7287 431.8952 412.0266 55.1048 -5.1653 426.7689 431.9342 411.8249 55.8618 -5.1644 426.8074 431.9719 411.6501 56.7220 -5.1625 426.8504 432.0129 411.4516 57.4895 -5.1612 426.8836 432.0448 411.2820 58.3088 -5.1596 426.9244 432.0840 411.1094 59.0863 -5.1581 426.9621 432.1202 410.9457 59.9058 -5.1569 426.9982 432.1551 410.7782 60.7040 -5.1560 427.0310 432.1871 410.6138 61.5025 -5.1554 427.0653 432.2207 410.4485 62.3320 -5.1543 427.0985 432.2527 410.2860 63.0888 -5.1533 427.1276 432.2809 410.1438 63.9390 -5.1524 427.1639 432.3164 409.9893 64.7168 -5.1511 427.1951 432.3462 409.8513 65.5360 -5.1509 427.2267 432.3776 409.7148 66.3345 -5.1501 427.2528 432.4029 409.5850 67.1228 -5.1494 427.2748 432.4242 409.4537 67.9418 -5.1493 427.2998 432.4491 409.3206 68.7090 -5.1487 427.3217 432.4705 409.2108 69.5593 -5.1490 427.3427 432.4917 409.0872 70.3163 -5.1489 427.3608 432.5097 408.9795 71.1563 -5.1487 427.3792 432.5279 408.8635 71.9440 -5.1488 427.3964 432.5452 408.7598 72.7428 -5.1487 427.4079 432.5567 408.6615 73.5618 -5.1483 427.4234 432.5717 408.5670 74.3395 -5.1484 427.4359 432.5843 408.4842 75.1588 -5.1476 427.4439 432.5915 408.3958 75.9260 -5.1482 427.4498 432.5979 408.3132 76.7868 -5.1486 427.4628 432.6114 408.2274 77.5438 -5.1486 427.4710 432.6196 408.1514 78.3730 -5.1487 427.4765 432.6252 408.0721 79.1715 -5.1491 427.4845 432.6336 408.0056 79.9700 -5.1497 427.4907 432.6404 407.9379 80.7890 -5.1506 427.4969 432.6474 407.8791 81.5565 -5.1518 427.4970 432.6488 407.8240 82.4168 -5.1524 427.4982 432.6506 407.7617 83.1638 -5.1531 427.5008 432.6539 407.7100 84.0240 -5.1536 427.5057 432.6593 407.6601 84.7915 -5.1544 427.5055 432.6599 407.6140 85.6108 -5.1552 427.5085 432.6637 407.5684 86.4193 -5.1567 427.5012 432.6579 407.5271 87.2075 -5.1582 427.4967 432.6548 407.4901 88.0268 -5.1593 427.4942 432.6535 407.4616 88.8043 -5.1609 427.4927 432.6537 407.4292 89.6543 -5.1630 427.4906 432.6536 407.3986 90.4218 -5.1647 427.4822 432.6469 407.3692 91.2408 -5.1665 427.4785 432.6450 407.3397 92.0498 -5.1684 427.4698 432.6382 407.3160 92.8380 -5.1703 427.4642 432.6345 407.2952 93.6570 -5.1715 427.4584 432.6299 407.2700 94.4353 -5.1732 427.4502 432.6234 407.2427 95.2850 -5.1744 427.4383 432.6128 407.2137 96.0528 -5.1759 427.4306 432.6066 407.1942 96.8720 -5.1786 427.4238 432.6025 407.1743 97.6603 -5.1810 427.4110 432.5920 407.1603 98.4590 -5.1835 427.3991 432.5827 407.1367 99.2778 -5.1859 427.3872 432.5731 407.1188 100.0450 -5.1888 427.3775 432.5662 407.0939 100.9058 -5.1915 427.3638 432.5553 407.0708 101.6628 -5.1941 427.3542 432.5483 407.0510 102.4923 -5.1968 427.3460 432.5428 407.0277 103.2803 -5.1992 427.3369 432.5361 407.0080 104.0785 -5.2013 427.3258 432.5271 406.9885 104.8770 -5.2041 427.3142 432.5184 406.9682 105.6650 -5.2067 427.3016 432.5084 406.9416 106.4948 -5.2087 427.2860 432.4947 406.9133 107.2620 -5.2112 427.2760 432.4872 406.8827 108.1225 -5.2148 427.2643 432.4790 406.8544 108.8798 -5.2171 427.2546 432.4717 406.8325 109.7090 -5.2193 427.2448 432.4642 406.8051 110.5075 -5.2218 427.2348 432.4566 406.7753 111.2958 -5.2238 427.2174 432.4412 406.7411 112.1250 -5.2260 427.1989 432.4248 406.7031 112.8925 -5.2287 427.1802 432.4089 406.6647 113.7218 -5.2313 427.1636 432.3949 406.6228 114.4790 -5.2340 427.1535 432.3875 406.5837 115.3395 -5.2362 427.1417 432.3779 406.5432 116.1068 -5.2383 427.1253 432.3636 406.5023 116.9260 -5.2403 427.1124 432.3526 406.4556 117.7243 -5.2431 427.1017 432.3448 406.4026 118.5230 -5.2454 427.0867 432.3321 406.3504 119.3523 -5.2475 427.0692 432.3167 406.2921 120.1098 -5.2497 427.0512 432.3009 406.2439 120.9700 -5.2515 427.0284 432.2799 406.1801 121.7378 -5.2529 427.0110 432.2640 406.1238 122.5568 -5.2543 426.9911 432.2454 406.0631 123.3550 -5.2560 426.9743 432.2303 405.9990 124.1538 -5.2575 426.9531 432.2106 405.9290 124.9830 -5.2596 426.9305 432.1900 405.8539 125.7400 -5.2613 426.9082 432.1694 405.7832 126.6005 -5.2639 426.8798 432.1437 405.7052 127.3678 -5.2660 426.8552 432.1211 405.6314 128.1870 -5.2681 426.8331 432.1012 405.5475 128.9855 -5.2698 426.8084 432.0783 405.4640 129.7840 -5.2721 426.7872 432.0592 405.3901 130.6135 -5.2732 426.7647 432.0379 405.3064 131.3708 -5.2749 426.7371 432.0120 405.2260 132.2208 -5.2768 426.7109 431.9878 405.1306 132.9880 -5.2788 426.6865 431.9653 405.0369 133.8073 -5.2806 426.6614 431.9420 404.9365 134.6163 -5.2820 426.6407 431.9226 404.8385 135.4043 -5.2832 426.6193 431.9025 404.7472 136.2230 -5.2849 426.5865 431.8714 404.6455 136.9908 -5.2865 426.5580 431.8445 404.5415 137.8408 -5.2888 426.5292 431.8179 404.4246 138.5878 -5.2903 426.5059 431.7962 404.3169 139.4378 -5.2917 426.4735 431.7652 404.1969 140.1948 -5.2921 426.4450 431.7371 404.0860 141.0348 -5.2933 426.4101 431.7034 403.9637 141.8540 -5.2948 426.3775 431.6723 403.8471 142.6213 -5.2959 426.3500 431.6459 403.7352 143.4408 -5.2967 426.3200 431.6167 403.6133 144.2183 -5.2978 426.2921 431.5899 403.4930 145.0683 -5.2982 426.2648 431.5630 403.3593 145.8258 -5.2991 426.2360 431.5351 403.2403 146.6653 -5.2994 426.2029 431.5024 403.1062 147.4538 -5.2999 426.1678 431.4676 402.9806 148.2520 -5.3000 426.1371 431.4371 402.8482 149.0713 -5.3003 426.0983 431.3986 402.7110 149.8490 -5.3006 426.0670 431.3676 402.5805 150.6988 -5.3011 426.0332 431.3343 402.4341 151.4560 -5.3017 426.0037 431.3054 402.3057 152.2958 -5.3018 425.9717 431.2735 402.1633 153.0840 -5.3018 425.9405 431.2422 402.0222 153.8928 -5.3021 425.8988 431.2009 401.8822 154.7120 -5.3018 425.8571 431.1590 401.7395 155.4898 -5.3009 425.8210 431.1219 401.6034 156.3398 -5.3010 425.7860 431.0870 401.4538 157.1070 -5.3012 425.7518 431.0530 401.3183 157.9263 -5.3012 425.7159 431.0171 401.1720 158.7350 -5.3013 425.6816 430.9829 401.0287 159.5230 -5.3011 425.6461 430.9472 400.8844 160.3420 -5.3005 425.6044 430.9050 400.7335 161.1198 -5.3000 425.5669 430.8668 400.5886 161.9598 -5.2988 425.5221 430.8209 400.4306 162.6960 -5.2980 425.4818 430.7799 400.2926 163.5460 -5.2971 425.4384 430.7355 400.1342 164.3138 -5.2957 425.3962 430.6919 399.9923 165.1325 -5.2955 425.3535 430.6490 399.8397 165.9313 -5.2946 425.3089 430.6035 399.6934 166.7190 -5.2933 425.2661 430.5594 399.5454 167.5488 -5.2927 425.2224 430.5151 399.3911 168.3058 -5.2913 425.1818 430.4731 399.2545 169.1663 -5.2896 425.1302 430.4198 399.0910 169.9338 -5.2896 425.0799 430.3695 398.9460 170.7528 -5.2897 425.0281 430.3178 398.7937 171.5305 -5.2896 424.9758 430.2654 398.6450 172.3498 -5.2883 424.9155 430.2038 398.4889 173.1480 -5.2877 424.8649 430.1526 398.3436 173.9363 -5.2871 424.8161 430.1032 398.1983 174.7760 -5.2858 424.7658 430.0516 398.0441 175.5328 -5.2846 424.7175 430.0021 397.9063 176.3830 -5.2839 424.6654 429.9492 397.7487 177.1608 -5.2836 424.6177 429.9013 397.6103 177.9800 -5.2836 424.5663 429.8499 397.4612 178.7783 -5.2826 424.5126 429.7952 397.3178 179.5668 -5.2819 424.4581 429.7400 397.1758 180.4063 -5.2806 424.4074 429.6880 397.0292 181.1635 -5.2797 424.3608 429.6405 396.8994 182.0240 -5.2785 424.3034 429.5819 396.7500 182.7913 -5.2773 424.2523 429.5295 396.6204 183.6100 -5.2758 424.1974 429.4732 396.4830 184.4083 -5.2748 424.1402 429.4150 396.3469 185.2070 -5.2732 424.0844 429.3576 396.2109 186.0363 -5.2720 424.0275 429.2995 396.0716 186.7938 -5.2715 423.9734 429.2449 395.9393 187.6540 -5.2700 423.9124 429.1824 395.7967 188.4213 -5.2686 423.8575 429.1260 395.6688 189.2510 -5.2673 423.7930 429.0603 395.5353 190.0493 -5.2651 423.7279 428.9929 395.4098 190.8370 -5.2632 423.6708 428.9339 395.2861 191.6358 -5.2619 423.6114 428.8733 395.1654 192.4340 -5.2614 423.5465 428.8079 395.0380 193.2635 -5.2603 423.4815 428.7418 394.9073 194.0208 -5.2585 423.4196 428.6781 394.7933 194.8708 -5.2567 423.3528 428.6096 394.6711 195.6380 -5.2555 423.2916 428.5471 394.5588 196.4573 -5.2549 423.2252 428.4801 394.4407 197.2450 -5.2531 423.1674 428.4205 394.3344 198.0433 -5.2517 423.1059 428.3577 394.2352 198.8628 -5.2504 423.0439 428.2943 394.1197 199.6403 -5.2496 422.9855 428.2351 394.0128 200.4903 -5.2481 422.9159 428.1640 393.8970 201.2475 -5.2465 422.8511 428.0976 393.7967 202.0770 -5.2441 422.7818 428.0259 393.6842 202.8750 -5.2431 422.7111 427.9542 393.5808 203.6738 -5.2422 422.6433 427.8855 393.4788 204.4930 -5.2416 422.5794 427.8210 393.3750 205.2605 -5.2413 422.5161 427.7574 393.2829 206.1208 -5.2404 422.4468 427.6872 393.1744 206.8780 -5.2399 422.3848 427.6247 393.0874 207.7073 -5.2386 422.3149 427.5535 392.9866 208.5060 -5.2374 422.2454 427.4828 392.8909 209.3043 -5.2368 422.1791 427.4159 392.7972 210.1233 -5.2360 422.1128 427.3487 392.7013 210.8910 -5.2352 422.0509 427.2861 392.6138 211.7515 -5.2334 421.9756 427.2090 392.5134 212.5088 -5.2326 421.9055 427.1380 392.4260 213.3483 -5.2317 421.8309 427.0626 392.3271 214.1365 -5.2303 421.7593 426.9896 392.2363 214.9350 -5.2296 421.6877 426.9173 392.1538 215.7538 -5.2289 421.6119 426.8408 392.0642 216.5318 -5.2275 421.5392 426.7667 391.9789 217.3818 -5.2264 421.4572 426.6836 391.8873 218.1390 -5.2254 421.3888 426.6142 391.8082 218.9790 -5.2239 421.3103 426.5342 391.7237 219.7670 -5.2229 421.2350 426.4580 391.6457 220.5658 -5.2225 421.1616 426.3840 391.5640 221.3848 -5.2222 421.0846 426.3068 391.4759 222.1628 -5.2221 421.0150 426.2371 391.3951 223.0128 -5.2208 420.9406 426.1615 391.3179 223.7903 -5.2198 420.8698 426.0896 391.2451 224.6098 -5.2181 420.7902 426.0084 391.1629 225.3978 -5.2166 420.7138 425.9304 391.0855 226.1960 -5.2157 420.6362 425.8518 391.0082 227.0153 -5.2154 420.5595 425.7748 390.9334 227.7830 -5.2143 420.4867 425.7011 390.8593 228.6433 -5.2129 420.4096 425.6225 390.7733 229.3695 -5.2118 420.3381 425.5498 390.7071 230.2298 -5.2112 420.2530 425.4642 390.6244 230.9868 -5.2102 420.1787 425.3889 390.5525 231.8060 -5.2096 420.1015 425.3110 390.4768 232.6048 -5.2100 420.0221 425.2321 390.4044 233.4030 -5.2092 419.9488 425.1580 390.3315 234.2323 -5.2087 419.8708 425.0795 390.2540 234.9893 -5.2086 419.7974 425.0060 390.1837 235.8500 -5.2086 419.7166 424.9252 390.0991 236.5863 -5.2085 419.6425 424.8510 390.0292 237.4360 -5.2079 419.5558 424.7637 389.9525 238.2140 -5.2072 419.4760 424.6832 389.8825 239.0330 -5.2069 419.3933 424.6003 389.8017 239.8313 -5.2061 419.3124 424.5184 389.7223 240.6198 -5.2053 419.2361 424.4415 389.6464 241.4593 -5.2042 419.1556 424.3598 389.5684 242.2163 -5.2031 419.0795 424.2826 389.5005 243.0668 -5.2027 418.9951 424.1978 389.4201 243.8443 -5.2019 418.9225 424.1244 389.3440 244.6633 -5.2010 418.8430 424.0440 389.2705 245.4618 -5.2007 418.7592 423.9599 389.1980 246.2600 -5.1999 418.6785 423.8784 389.1165 247.0898 -5.1995 418.5956 423.7952 389.0363 247.8468 -5.1979 418.5193 423.7172 388.9643 248.6863 -5.1966 418.4368 423.6334 388.8839 249.4438 -5.1955 418.3610 423.5565 388.8108 250.3040 -5.1949 418.2722 423.4671 388.7214 251.0713 -5.1940 418.1937 423.3878 388.6398 251.8908 -5.1934 418.1166 423.3101 388.5504 252.6888 -5.1925 418.0395 423.2319 388.4650 253.4870 -5.1918 417.9598 423.1516 388.3787 254.3163 -5.1917 417.8824 423.0741 388.2966 255.0738 -5.1907 417.8051 422.9959 388.2138 255.9345 -5.1906 417.7188 422.9095 388.1231 256.6915 -5.1906 417.6393 422.8300 388.0374 257.5208 -5.1896 417.5544 422.7440 387.9429 258.2885 -5.1878 417.4798 422.6676 387.8579 259.1383 -5.1864 417.3979 422.5843 387.7619 259.9058 -5.1853 417.3233 422.5087 387.6735 260.7353 -5.1843 417.2396 422.4239 387.5817 261.5233 -5.1841 417.1567 422.3408 387.4906 262.3113 -5.1835 417.0729 422.2565 387.3973 263.1408 -5.1826 416.9879 422.1706 387.2999 263.9080 -5.1819 416.9141 422.0960 387.2055 264.7685 -5.1812 416.8246 422.0058 387.1031 265.4948 -5.1799 416.7513 421.9312 387.0168 266.3448 -5.1785 416.6678 421.8463 386.9134 267.1228 -5.1777 416.5917 421.7695 386.8224 267.9418 -5.1773 416.5102 421.6874 386.7205 268.7403 -5.1759 416.4266 421.6025 386.6222 269.5283 -5.1748 416.3437 421.5185 386.5249 270.3680 -5.1741 416.2600 421.4341 386.4167 271.1250 -5.1732 416.1840 421.3573 386.3280 271.9750 -5.1723 416.0947 421.2670 386.2191 272.7530 -5.1709 416.0167 421.1875 386.1205 273.5720 -5.1690 415.9350 421.1040 386.0149 274.3703 -5.1674 415.8533 421.0206 385.9094 275.1588 -5.1661 415.7711 420.9372 385.8036 275.9983 -5.1641 415.6850 420.8491 385.6948 276.7553 -5.1631 415.6057 420.7688 385.5914 277.6160 -5.1607 415.5185 420.6792 385.4724 278.3833 -5.1597 415.4416 420.6013 385.3761 279.2023 -5.1583 415.3611 420.5194 385.2667 280.0010 -5.1570 415.2806 420.4376 385.1589 280.7990 -5.1555 415.1990 420.3545 385.0458 281.6283 -5.1543 415.1109 420.2652 384.9275 282.3960 -5.1533 415.0287 420.1820 384.8198 283.2563 -5.1516 414.9378 420.0894 384.7034 284.0133 -5.1497 414.8592 420.0089 384.5932 284.8425 -5.1474 414.7750 419.9224 384.4731 285.6413 -5.1456 414.6975 419.8431 384.3646 286.4293 -5.1440 414.6156 419.7596 384.2562 287.2590 -5.1425 414.5222 419.6647 384.1457 288.0263 -5.1417 414.4434 419.5852 384.0365 288.8868 -5.1405 414.3543 419.4948 383.9087 289.6438 -5.1384 414.2744 419.4129 383.7989 290.4630 -5.1356 414.1901 419.3257 383.6859 291.2613 -5.1338 414.1048 419.2386 383.5773 292.0498 -5.1326 414.0195 419.1521 383.4648 292.8688 -5.1313 413.9382 419.0694 383.3478 293.6468 -5.1292 413.8606 418.9899 383.2363 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