DTA measure 1gyors Date: 2025325:1054 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 905.42 s Mass = 925.100 mg data_number = 1126 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3238 -0.1953 224.0132 224.2085 271.0233 2.0703 -0.1952 224.2765 224.4717 270.9052 2.9203 -0.1948 224.5787 224.7735 270.7703 3.6980 -0.1944 224.8554 225.0497 270.6428 4.5173 -0.1935 225.1448 225.3383 270.5046 5.3050 -0.1932 225.4218 225.6151 270.3679 6.1140 -0.1929 225.7122 225.9051 270.2296 6.9330 -0.1924 226.0031 226.1955 270.0850 7.7108 -0.1909 226.2681 226.4590 269.9410 8.5608 -0.1889 226.5641 226.7530 269.7811 9.3280 -0.1874 226.8299 227.0173 269.6367 10.1473 -0.1854 227.1143 227.2997 269.4844 10.9560 -0.1842 227.3941 227.5782 269.3390 11.7543 -0.1829 227.6706 227.8535 269.1918 12.5528 -0.1806 227.9443 228.1248 269.0452 13.3408 -0.1785 228.2169 228.3954 268.9021 14.1598 -0.1759 228.4901 228.6660 268.7465 14.9273 -0.1727 228.7472 228.9199 268.5996 15.7773 -0.1705 229.0287 229.1991 268.4404 16.5240 -0.1695 229.2794 229.4489 268.3002 17.3738 -0.1676 229.5675 229.7351 268.1487 18.1310 -0.1657 229.8177 229.9834 268.0112 18.9603 -0.1640 230.0914 230.2554 267.8629 19.7483 -0.1617 230.3544 230.5161 267.7178 20.5470 -0.1597 230.6218 230.7815 267.5737 21.3763 -0.1580 230.8987 231.0567 267.4313 22.1540 -0.1558 231.1487 231.3044 267.3043 22.9733 -0.1534 231.4086 231.5619 267.1721 23.7405 -0.1521 231.6483 231.8004 267.0551 24.6008 -0.1504 231.9250 232.0754 266.9271 25.3580 -0.1481 232.1670 232.3151 266.8204 26.1873 -0.1465 232.4271 232.5735 266.7081 26.9858 -0.1447 232.6802 232.8249 266.6080 27.7840 -0.1424 232.9276 233.0700 266.5062 28.6033 -0.1408 233.1841 233.3249 266.4136 29.3600 -0.1391 233.4172 233.5563 266.3333 30.2210 -0.1373 233.6791 233.8164 266.2496 30.9880 -0.1353 233.9092 234.0445 266.1847 31.8173 -0.1333 234.1644 234.2977 266.1222 32.6055 -0.1312 234.4104 234.5416 266.0743 33.4040 -0.1299 234.6503 234.7802 266.0266 34.2333 -0.1283 234.8985 235.0269 265.9903 34.9900 -0.1269 235.1263 235.2531 265.9635 35.8193 -0.1248 235.3760 235.5008 265.9461 36.6178 -0.1234 235.6107 235.7341 265.9404 37.4470 -0.1221 235.8526 235.9747 265.9517 38.2353 -0.1209 236.0831 236.2040 265.9717 39.0335 -0.1200 236.3130 236.4331 265.9991 39.8320 -0.1196 236.5456 236.6652 266.0374 40.6200 -0.1184 236.7713 236.8897 266.0862 41.4498 -0.1174 237.0072 237.1246 266.1529 42.2170 -0.1168 237.2247 237.3415 266.2225 43.0773 -0.1160 237.4691 237.5850 266.3085 43.8448 -0.1155 237.6852 237.8008 266.3912 44.6743 -0.1159 237.9209 238.0368 266.4987 45.4623 -0.1158 238.1376 238.2534 266.6173 46.2605 -0.1157 238.3635 238.4792 266.7451 47.0900 -0.1164 238.5949 238.7113 266.8858 47.8470 -0.1167 238.8015 238.9182 267.0252 48.7073 -0.1180 239.0378 239.1558 267.1916 49.4745 -0.1188 239.2466 239.3654 267.3578 50.3040 -0.1193 239.4715 239.5909 267.5526 51.0918 -0.1203 239.6898 239.8101 267.7420 51.8900 -0.1218 239.9065 240.0282 267.9454 52.7508 -0.1234 240.1352 240.2586 268.1747 53.4768 -0.1250 240.3274 240.4524 268.3786 54.3373 -0.1275 240.5538 240.6813 268.6299 55.1358 -0.1305 240.7658 240.8963 268.8724 55.9340 -0.1343 240.9769 241.1111 269.1261 56.7528 -0.1376 241.1929 241.3306 269.3974 57.5205 -0.1405 241.3995 241.5401 269.6649 58.3808 -0.1443 241.6294 241.7737 269.9621 59.1378 -0.1477 241.8256 241.9734 270.2323 59.9773 -0.1511 242.0453 242.1964 270.5407 60.7650 -0.1551 242.2481 242.4032 270.8411 61.5633 -0.1592 242.4551 242.6143 271.1482 62.3823 -0.1641 242.6702 242.8343 271.4707 63.1603 -0.1686 242.8687 243.0373 271.7812 64.0103 -0.1747 243.0891 243.2638 272.1259 64.7880 -0.1799 243.2866 243.4665 272.4506 65.6068 -0.1849 243.4981 243.6830 272.7919 66.3948 -0.1902 243.6956 243.8858 273.1270 67.2033 -0.1960 243.9037 244.0997 273.4748 68.0225 -0.2018 244.1101 244.3120 273.8314 68.8003 -0.2076 244.3046 244.5122 274.1717 69.6190 -0.2141 244.5151 244.7293 274.5367 70.3863 -0.2214 244.7114 244.9328 274.8752 71.2468 -0.2279 244.9356 245.1635 275.2617 72.0140 -0.2347 245.1319 245.3667 275.6051 72.8333 -0.2421 245.3401 245.5822 275.9730 73.6420 -0.2489 245.5490 245.7979 276.3341 74.4300 -0.2568 245.7513 246.0080 276.6846 75.2490 -0.2644 245.9618 246.2262 277.0530 76.0163 -0.2717 246.1551 246.4268 277.3979 76.8665 -0.2799 246.3731 246.6531 277.7737 77.6238 -0.2878 246.5651 246.8529 278.1063 78.4530 -0.2962 246.7757 247.0719 278.4703 79.2098 -0.3027 246.9673 247.2700 278.8006 80.0288 -0.3113 247.1797 247.4911 279.1574 80.8273 -0.3192 247.3811 247.7003 279.4961 81.6258 -0.3278 247.5822 247.9099 279.8276 82.4550 -0.3374 247.7935 248.1309 280.1646 83.2123 -0.3463 247.9831 248.3294 280.4721 84.0620 -0.3559 248.2004 248.5563 280.8079 84.8293 -0.3654 248.3925 248.7579 281.1043 85.6483 -0.3752 248.5986 248.9738 281.4256 86.4573 -0.3843 248.8021 249.1864 281.7344 87.2453 -0.3930 249.0023 249.3953 282.0283 88.0330 -0.4019 249.2037 249.6056 282.3079 88.8313 -0.4108 249.4119 249.8227 282.5835 89.6505 -0.4197 249.6160 250.0357 282.8636 90.4283 -0.4289 249.8153 250.2442 283.1217 91.2783 -0.4395 250.0307 250.4702 283.3961 92.0353 -0.4489 250.2199 250.6688 283.6323 92.8750 -0.4588 250.4306 250.8894 283.8857 93.6320 -0.4683 250.6250 251.0934 284.1056 94.5028 -0.4784 250.8447 251.3231 284.3572 95.2288 -0.4871 251.0268 251.5140 284.5570 96.0890 -0.4969 251.2480 251.7450 284.7878 96.8565 -0.5060 251.4436 251.9495 284.9898 97.6758 -0.5153 251.6441 252.1594 285.1972 98.4740 -0.5248 251.8485 252.3733 285.3852 99.2720 -0.5342 252.0526 252.5868 285.5678 100.1015 -0.5433 252.2660 252.8093 285.7473 100.8588 -0.5518 252.4542 253.0060 285.9061 101.7190 -0.5619 252.6725 253.2344 286.0748 102.4863 -0.5708 252.8657 253.4366 286.2184 103.3050 -0.5805 253.0766 253.6571 286.3666 104.0725 -0.5894 253.2751 253.8645 286.4958 104.8918 -0.5982 253.4929 254.0911 286.6243 105.7003 -0.6072 253.7000 254.3073 286.7489 106.4883 -0.6153 253.8968 254.5121 286.8657 107.3073 -0.6241 254.1108 254.7349 286.9807 108.0850 -0.6322 254.3187 254.9509 287.0796 108.9350 -0.6409 254.5383 255.1793 287.1734 109.7023 -0.6490 254.7344 255.3833 287.2561 110.5215 -0.6576 254.9431 255.6007 287.3414 111.3303 -0.6651 255.1508 255.8159 287.4199 112.1183 -0.6732 255.3528 256.0260 287.4908 112.9370 -0.6814 255.5585 256.2399 287.5541 113.7148 -0.6886 255.7556 256.4442 287.6106 114.5650 -0.6964 255.9716 256.6680 287.6638 115.3323 -0.7035 256.1688 256.8723 287.7100 116.1518 -0.7116 256.3749 257.0865 287.7504 116.9603 -0.7182 256.5828 257.3010 287.7832 117.7483 -0.7252 256.7788 257.5040 287.8098 118.5673 -0.7321 256.9833 257.7154 287.8355 119.3453 -0.7386 257.1792 257.9177 287.8573 120.1950 -0.7463 257.3939 258.1402 287.8791 120.9728 -0.7529 257.5886 258.3415 287.8931 121.7918 -0.7591 257.7977 258.5568 287.8990 122.5593 -0.7649 257.9898 258.7547 287.9059 123.3783 -0.7712 258.1933 258.9645 287.9088 124.1870 -0.7775 258.3957 259.1732 287.9016 124.9753 -0.7831 258.5974 259.3805 287.8985 125.7940 -0.7890 258.8018 259.5908 287.8871 126.5718 -0.7946 258.9978 259.7924 287.8753 127.4218 -0.8001 259.2110 260.0111 287.8540 128.1893 -0.8047 259.3983 260.2030 287.8376 129.0083 -0.8095 259.6008 260.4103 287.8156 129.8170 -0.8152 259.8006 260.6158 287.7889 130.6050 -0.8198 259.9925 260.8122 287.7658 131.4240 -0.8247 260.1945 261.0193 287.7425 132.2018 -0.8296 260.3857 261.2153 287.7166 133.0518 -0.8343 260.5929 261.4272 287.6883 133.8190 -0.8381 260.7827 261.6208 287.6613 134.6383 -0.8418 260.9783 261.8202 287.6334 135.4780 -0.8467 261.1838 262.0305 287.6055 136.2350 -0.8503 261.3637 262.2139 287.5747 137.0955 -0.8543 261.5687 262.4231 287.5446 137.8318 -0.8578 261.7427 262.6005 287.5203 138.6818 -0.8623 261.9412 262.8035 287.4956 139.4490 -0.8667 262.1232 262.9898 287.4723 140.2678 -0.8711 262.3185 263.1896 287.4432 141.0560 -0.8746 262.5076 263.3821 287.4176 141.8543 -0.8783 262.6990 263.5773 287.3935 142.6733 -0.8818 262.8906 263.7724 287.3726 143.4405 -0.8853 263.0687 263.9539 287.3533 144.3010 -0.8888 263.2683 264.1571 287.3386 145.0375 -0.8917 263.4388 264.3305 287.3240 145.8978 -0.8953 263.6396 264.5349 287.3098 146.6548 -0.8984 263.8151 264.7135 287.3046 147.4843 -0.9025 264.0064 264.9089 287.3082 148.2723 -0.9056 264.1896 265.0953 287.3099 149.0600 -0.9086 264.3787 265.2873 287.3135 149.8893 -0.9114 264.5652 265.4767 287.3172 150.6570 -0.9135 264.7392 265.6526 287.3280 151.5173 -0.9162 264.9387 265.8549 287.3438 152.2743 -0.9181 265.1079 266.0260 287.3644 153.0930 -0.9212 265.2968 266.2179 287.3919 153.8913 -0.9239 265.4742 266.3980 287.4240 154.6900 -0.9265 265.6531 266.5796 287.4624 155.5193 -0.9289 265.8388 266.7677 287.5094 156.2763 -0.9312 266.0050 266.9362 287.5589 157.1365 -0.9338 266.1974 267.1312 287.6231 157.9038 -0.9366 266.3646 267.3012 287.6864 158.7228 -0.9390 266.5412 267.4802 287.7541 159.5213 -0.9425 266.7103 267.6528 287.8293 160.3195 -0.9452 266.8826 267.8278 287.9095 161.1488 -0.9480 267.0635 268.0115 287.9981 161.9058 -0.9514 267.2295 268.1809 288.0845 162.7660 -0.9557 267.4115 268.3672 288.1917 163.5335 -0.9584 267.5719 268.5303 288.2887 164.3528 -0.9627 267.7434 268.7060 288.4060 165.1510 -0.9657 267.9153 268.8809 288.5269 165.9493 -0.9687 268.0895 269.0581 288.6528 166.7785 -0.9725 268.2671 269.2395 288.7965 167.5355 -0.9760 268.4269 269.4029 288.9290 168.3960 -0.9797 268.6044 269.5841 289.0830 169.1633 -0.9833 268.7594 269.7426 289.2295 169.9820 -0.9873 268.9286 269.9159 289.3893 170.7805 -0.9908 269.0924 270.0832 289.5482 171.5790 -0.9947 269.2580 270.2527 289.7188 172.4083 -0.9984 269.4347 270.4331 289.9127 173.1653 -1.0021 269.5879 270.5900 290.0852 174.0360 -1.0064 269.7703 270.7766 290.2937 174.7928 -1.0108 269.9304 270.9413 290.4795 175.6220 -1.0163 270.1071 271.1234 290.6889 176.4203 -1.0217 270.2760 271.2977 290.8916 177.2083 -1.0257 270.4370 271.4627 291.0974 178.0378 -1.0298 270.6094 271.6392 291.3251 178.8050 -1.0342 270.7674 271.8017 291.5352 179.6653 -1.0391 270.9431 271.9823 291.7759 180.4223 -1.0435 271.0969 272.1404 291.9903 181.2620 -1.0482 271.2686 272.3168 292.2318 182.0190 -1.0525 271.4255 272.4781 292.4607 182.8483 -1.0583 271.5951 272.6533 292.7090 183.6465 -1.0631 271.7555 272.8186 292.9551 184.4348 -1.0680 271.9111 272.9792 293.1966 185.2640 -1.0743 272.0838 273.1580 293.4569 186.0310 -1.0798 272.2426 273.3224 293.6950 186.8913 -1.0862 272.4215 273.5077 293.9596 187.6483 -1.0919 272.5773 273.6692 294.1981 188.4775 -1.0986 272.7445 273.8431 294.4693 189.2763 -1.1048 272.9078 274.0125 294.7302 190.0745 -1.1117 273.0687 274.1804 294.9904 190.9038 -1.1184 273.2398 274.3582 295.2629 191.6610 -1.1248 273.3962 274.5210 295.5130 192.5318 -1.1318 273.5697 274.7014 295.7974 193.2888 -1.1374 273.7189 274.8563 296.0444 194.1180 -1.1441 273.8891 275.0332 296.3172 194.8855 -1.1500 274.0504 275.2003 296.5669 195.7150 -1.1571 274.2247 275.3818 296.8362 196.5028 -1.1637 274.3941 275.5578 297.0921 197.3113 -1.1707 274.5668 275.7375 297.3572 198.1303 -1.1774 274.7356 275.9129 297.6240 198.9080 -1.1836 274.8944 276.0780 297.8708 199.7575 -1.1910 275.0713 276.2623 298.1449 200.5148 -1.1982 275.2273 276.4255 298.3852 201.3543 -1.2064 275.3980 276.6044 298.6452 202.1423 -1.2132 275.5668 276.7800 298.8890 202.9408 -1.2204 275.7360 276.9564 299.1364 203.7288 -1.2276 275.8964 277.1240 299.3736 204.5168 -1.2349 276.0581 277.2930 299.6098 205.3463 -1.2421 276.2292 277.4713 299.8537 206.1135 -1.2492 276.3901 277.6393 300.0719 206.9635 -1.2564 276.5677 277.8241 300.3164 207.7310 -1.2632 276.7253 277.9885 300.5347 208.5500 -1.2714 276.8920 278.1634 300.7608 209.3483 -1.2789 277.0618 278.3407 300.9744 210.1363 -1.2868 277.2263 278.5131 301.1829 210.9243 -1.2938 277.3860 278.6798 301.3874 211.7333 -1.3011 277.5518 278.8529 301.5964 212.5418 -1.3082 277.7249 279.0330 301.7996 213.3193 -1.3148 277.8930 279.2078 301.9880 214.1698 -1.3222 278.0641 279.3864 302.1945 214.9268 -1.3287 278.2195 279.5481 302.3704 215.7663 -1.3359 278.3869 279.7228 302.5602 216.5548 -1.3418 278.5537 279.8956 302.7333 217.3530 -1.3491 278.7189 280.0680 302.9046 218.1408 -1.3558 278.8837 280.2395 303.0715 218.9390 -1.3622 279.0511 280.4133 303.2314 219.7688 -1.3697 279.2287 280.5984 303.3894 220.5258 -1.3760 279.3923 280.7684 303.5312 221.3860 -1.3827 279.5770 280.9597 303.6915 222.1428 -1.3889 279.7359 281.1248 303.8258 222.9725 -1.3954 279.9100 281.3054 303.9703 223.7708 -1.4014 280.0758 281.4772 304.1038 224.5588 -1.4084 280.2418 281.6502 304.2274 225.3880 -1.4150 280.4195 281.8345 304.3520 226.1553 -1.4203 280.5805 282.0007 304.4695 227.0158 -1.4265 280.7661 282.1926 304.5949 227.7728 -1.4322 280.9265 282.3587 304.7013 228.6123 -1.4380 281.1013 282.5393 304.8088 229.3693 -1.4437 281.2586 282.7023 304.9056 230.1888 -1.4502 281.4346 282.8848 305.0094 230.9870 -1.4550 281.6028 283.0578 305.1046 231.7853 -1.4599 281.7715 283.2313 305.1954 232.6150 -1.4661 281.9421 283.4082 305.2853 233.3718 -1.4716 282.0989 283.5705 305.3637 234.2320 -1.4773 282.2808 283.7582 305.4485 234.9993 -1.4831 282.4485 283.9316 305.5193 235.8183 -1.4882 282.6194 284.1076 305.5936 236.6170 -1.4925 282.7858 284.2783 305.6601 237.4150 -1.4974 282.9518 284.4493 305.7242 238.2448 -1.5021 283.1222 284.6243 305.7895 239.0018 -1.5068 283.2785 284.7853 305.8467 239.8620 -1.5126 283.4553 284.9679 305.9030 240.6295 -1.5170 283.6143 285.1312 305.9497 241.4488 -1.5210 283.7906 285.3116 305.9987 242.2470 -1.5254 283.9591 285.4846 306.0441 243.0455 -1.5297 284.1232 285.6529 306.0898 243.8748 -1.5342 284.3007 285.8349 306.1321 244.6318 -1.5382 284.4647 286.0030 306.1672 245.4920 -1.5418 284.6450 286.1868 306.2063 246.2595 -1.5453 284.8051 286.3504 306.2382 247.0888 -1.5491 284.9742 286.5233 306.2734 247.8873 -1.5530 285.1395 286.6924 306.3035 248.6750 -1.5564 285.3047 286.8611 306.3367 249.5043 -1.5608 285.4755 287.0363 306.3768 250.2720 -1.5643 285.6338 287.1981 306.4057 251.1323 -1.5682 285.8131 287.3814 306.4383 251.8998 -1.5718 285.9686 287.5404 306.4697 252.7290 -1.5755 286.1365 287.7120 306.4947 253.5168 -1.5787 286.2981 287.8768 306.5170 254.3150 -1.5816 286.4635 288.0450 306.5443 255.1445 -1.5847 286.6340 288.2186 306.5765 255.9018 -1.5873 286.7904 288.3777 306.6044 256.7620 -1.5912 286.9670 288.5582 306.6361 257.5085 -1.5939 287.1193 288.7132 306.6663 258.3690 -1.5971 287.2953 288.8924 306.6986 259.1465 -1.6004 287.4517 289.0521 306.7299 259.9655 -1.6033 287.6149 289.2182 306.7671 260.7430 -1.6059 287.7772 289.3832 306.8067 261.5623 -1.6089 287.9412 289.5501 306.8486 262.3500 -1.6117 288.0957 289.7074 306.8827 263.1588 -1.6142 288.2604 289.8746 306.9205 263.9778 -1.6164 288.4232 290.0396 306.9642 264.7553 -1.6190 288.5764 290.1954 307.0115 265.6050 -1.6212 288.7481 290.3692 307.0719 266.3723 -1.6232 288.9007 290.5239 307.1232 267.1918 -1.6252 289.0572 290.6824 307.1778 267.9590 -1.6276 289.2072 290.8348 307.2315 268.8193 -1.6303 289.3771 291.0075 307.2964 269.5763 -1.6332 289.5246 291.1578 307.3555 270.3950 -1.6357 289.6868 291.3225 307.4243 271.1933 -1.6373 289.8383 291.4756 307.4948 271.9920 -1.6395 289.9907 291.6303 307.5711 272.8213 -1.6426 290.1549 291.7975 307.6465 273.5783 -1.6456 290.3008 291.9464 307.7248 274.4280 -1.6484 290.4628 292.1112 307.8194 275.1953 -1.6503 290.6129 292.2632 307.9061 276.0143 -1.6529 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