DTA measure 2gyors Date: 2025325:1124 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.39 s Mass = 925.100 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4666 -5.1794 426.1325 431.3119 429.8372 4.0479 -5.1840 426.3705 431.5545 429.6303 5.6550 -5.1873 426.6107 431.7980 429.4000 7.2778 -5.1903 426.8526 432.0429 429.1273 8.8849 -5.1915 427.0831 432.2746 428.8328 10.4869 -5.1930 427.3158 432.5088 428.5249 12.0994 -5.1949 427.5465 432.7414 428.1927 13.7016 -5.1960 427.7720 432.9680 427.8413 15.3089 -5.1964 427.9938 433.1902 427.4743 16.9161 -5.1957 428.2090 433.4047 427.0977 18.5390 -5.1956 428.4262 433.6218 426.6981 20.1465 -5.1955 428.6395 433.8350 426.2814 21.7485 -5.1944 428.8423 434.0367 425.8539 23.3610 -5.1925 429.0365 434.2290 425.4231 24.9681 -5.1915 429.2310 434.4225 424.9744 26.5754 -5.1900 429.4202 434.6102 424.5194 28.1825 -5.1876 429.6149 434.8025 424.0585 29.8053 -5.1846 429.8052 434.9899 423.5992 31.4128 -5.1821 429.9723 435.1544 423.1375 33.0201 -5.1794 430.1364 435.3158 422.6714 34.6221 -5.1765 430.3000 435.4766 422.2135 36.2346 -5.1733 430.4581 435.6314 421.7446 37.8369 -5.1704 430.6071 435.7775 421.2766 39.4443 -5.1679 430.7562 435.9241 420.8189 41.0514 -5.1648 430.8908 436.0556 420.3552 42.6586 -5.1627 431.0232 436.1859 419.9050 44.2658 -5.1606 431.1487 436.3093 419.4572 45.8678 -5.1577 431.2657 436.4234 419.0238 47.4803 -5.1546 431.3759 436.5304 418.6023 49.0875 -5.1535 431.4818 436.6354 418.1963 50.6841 -5.1500 431.5783 436.7283 417.8006 52.2913 -5.1485 431.6720 436.8205 417.4191 53.8724 -5.1478 431.7569 436.9047 417.0566 55.4849 -5.1480 431.8451 436.9931 416.7073 57.0973 -5.1487 431.9369 437.0855 416.3669 58.6838 -5.1485 432.0078 437.1563 416.0553 60.2805 -5.1487 432.0706 437.2193 415.7590 61.8930 -5.1505 432.1322 437.2828 415.4786 63.4898 -5.1516 432.1920 437.3436 415.2121 65.0971 -5.1540 432.2470 437.4009 414.9554 66.7044 -5.1555 432.2875 437.4429 414.7256 68.3218 -5.1568 432.3309 437.4877 414.5107 69.9291 -5.1600 432.3706 437.5306 414.3177 71.5208 -5.1631 432.4006 437.5637 414.1438 73.1229 -5.1663 432.4313 437.5976 413.9860 74.7353 -5.1700 432.4617 437.6317 413.8398 76.3374 -5.1740 432.4800 437.6540 413.7171 77.9498 -5.1782 432.4889 437.6670 413.6033 79.5519 -5.1829 432.5020 437.6849 413.5076 81.1744 -5.1886 432.5123 437.7009 413.4159 82.7661 -5.1941 432.5208 437.7149 413.3435 84.3680 -5.2003 432.5276 437.7279 413.2799 85.9806 -5.2069 432.5329 437.7398 413.2185 87.5825 -5.2135 432.5306 437.7441 413.1733 89.1948 -5.2199 432.5223 437.7422 413.1347 90.7970 -5.2265 432.5072 437.7337 413.0982 92.4044 -5.2332 432.4950 437.7282 413.0616 94.0270 -5.2405 432.4870 437.7275 413.0349 95.6291 -5.2476 432.4690 437.7166 413.0113 97.2416 -5.2553 432.4570 437.7122 412.9774 98.8438 -5.2634 432.4427 437.7061 412.9502 100.4561 -5.2718 432.4184 437.6902 412.9190 102.0584 -5.2801 432.3996 437.6798 412.8911 103.6656 -5.2879 432.3769 437.6647 412.8541 105.2936 -5.2957 432.3567 437.6524 412.8082 106.9009 -5.3035 432.3284 437.6319 412.7561 108.5030 -5.3109 432.3048 437.6157 412.6944 110.1153 -5.3186 432.2786 437.5972 412.6315 111.7275 -5.3256 432.2453 437.5709 412.5626 113.3295 -5.3340 432.2116 437.5456 412.4864 114.9213 -5.3413 432.1819 437.5232 412.3972 116.5234 -5.3479 432.1521 437.5000 412.3021 118.1355 -5.3544 432.1146 437.4690 412.1973 119.7274 -5.3613 432.0913 437.4526 412.0787 121.3344 -5.3692 432.0657 437.4349 411.9378 122.9315 -5.3764 432.0296 437.4060 411.7883 124.5440 -5.3827 431.9869 437.3696 411.6342 126.1406 -5.3881 431.9465 437.3346 411.4673 127.7373 -5.3928 431.9049 437.2977 411.2915 129.3393 -5.3974 431.8642 437.2616 411.1037 130.9413 -5.4019 431.8178 437.2197 410.9065 132.5641 -5.4068 431.7639 437.1707 410.6948 134.1711 -5.4112 431.7152 437.1263 410.4757 135.7733 -5.4148 431.6603 437.0751 410.2537 137.3855 -5.4192 431.6019 437.0211 410.0091 138.9721 -5.4218 431.5502 436.9721 409.7649 140.5848 -5.4240 431.4964 436.9204 409.5186 142.1868 -5.4275 431.4399 436.8674 409.2612 143.7939 -5.4299 431.3888 436.8187 408.9962 145.4166 -5.4325 431.3309 436.7634 408.7155 147.0290 -5.4350 431.2687 436.7037 408.4342 148.6311 -5.4374 431.1993 436.6367 408.1514 150.2279 -5.4395 431.1364 436.5760 407.8683 151.8299 -5.4414 431.0633 436.5048 407.5770 153.4423 -5.4432 431.0020 436.4452 407.2671 155.0496 -5.4452 430.9264 436.3716 406.9655 156.6568 -5.4461 430.8488 436.2949 406.6616 158.2795 -5.4457 430.7750 436.2208 406.3536 159.8919 -5.4464 430.6989 436.1453 406.0523 161.4990 -5.4465 430.6161 436.0626 405.7502 163.1010 -5.4472 430.5302 435.9774 405.4495 164.7134 -5.4476 430.4456 435.8932 405.1469 166.3206 -5.4472 430.3558 435.8030 404.8401 167.9278 -5.4470 430.2646 435.7117 404.5318 169.5504 -5.4467 430.1701 435.6167 404.2274 171.1524 -5.4462 430.0757 435.5219 403.9303 172.7649 -5.4453 429.9813 435.4266 403.6425 174.3671 -5.4447 429.8811 435.3258 403.3543 175.9794 -5.4441 429.7851 435.2292 403.0603 177.5763 -5.4426 429.6785 435.1212 402.7741 179.1784 -5.4419 429.5717 435.0136 402.4842 180.7855 -5.4418 429.4697 434.9115 402.1978 182.3774 -5.4407 429.3584 434.7990 401.9247 183.9848 -5.4399 429.2419 434.6818 401.6660 185.5815 -5.4382 429.1249 434.5631 401.4076 187.1834 -5.4360 428.9992 434.4353 401.1478 188.7905 -5.4342 428.8822 434.3164 400.9005 190.3925 -5.4329 428.7591 434.1920 400.6619 192.0049 -5.4315 428.6358 434.0674 400.4182 193.6174 -5.4298 428.5098 433.9396 400.1824 195.2246 -5.4291 428.3813 433.8105 399.9566 196.8266 -5.4277 428.2508 433.6785 399.7405 198.4288 -5.4266 428.1163 433.5430 399.5268 200.0409 -5.4247 427.9854 433.4101 399.3207 201.6274 -5.4238 427.8608 433.2847 399.1249 203.2344 -5.4229 427.7283 433.1512 398.9297 204.8415 -5.4217 427.5945 433.0161 398.7390 206.4594 -5.4209 427.4540 432.8749 398.5512 208.0718 -5.4200 427.3163 432.7364 398.3741 209.6738 -5.4179 427.1779 432.5958 398.2017 211.2861 -5.4171 427.0399 432.4570 398.0254 212.8884 -5.4170 426.8993 432.3163 397.8642 214.4954 -5.4159 426.7596 432.1755 397.7003 216.0924 -5.4169 426.6170 432.0340 397.5440 217.6998 -5.4167 426.4734 431.8901 397.3969 219.3173 -5.4158 426.3277 431.7435 397.2469 220.9298 -5.4155 426.1720 431.5875 397.0870 222.5318 -5.4145 426.0204 431.4349 396.9435 224.1443 -5.4147 425.8730 431.2877 396.7992 225.7564 -5.4154 425.7235 431.1388 396.6563 227.3844 -5.4149 425.5665 430.9815 396.5170 228.9605 -5.4146 425.4160 430.8306 396.3816 230.5731 -5.4140 425.2631 430.6771 396.2403 232.1803 -5.4133 425.1150 430.5283 396.0911 233.7874 -5.4134 424.9697 430.3832 395.9402 235.3995 -5.4127 424.8184 430.2311 395.7956 237.0224 -5.4120 424.6646 430.0766 395.6518 238.6296 -5.4116 424.5125 429.9241 395.5035 240.2419 -5.4109 424.3626 429.7735 395.3541 241.8438 -5.4096 424.2082 429.6178 395.2052 243.4303 -5.4093 424.0548 429.4641 395.0475 245.0428 -5.4096 423.8970 429.3066 394.8906 246.6399 -5.4088 423.7464 429.1552 394.7345 248.2210 -5.4083 423.5902 428.9985 394.5721 249.8593 -5.4085 423.4297 428.8382 394.3962 251.4664 -5.4082 423.2690 428.6772 394.2293 253.0479 -5.4074 423.1135 428.5209 394.0619 254.6600 -5.4061 422.9483 428.3544 393.8847 256.2568 -5.4050 422.7922 428.1972 393.7070 257.8694 -5.4036 422.6288 428.0323 393.5190 259.4714 -5.4019 422.4703 427.8722 393.3281 261.0838 -5.4000 422.3054 427.7054 393.1410 262.7015 -5.3990 422.1504 427.5494 392.9531 264.3083 -5.3976 421.9967 427.3943 392.7527 265.9155 -5.3965 421.8508 427.2473 392.5434 267.5175 -5.3944 421.6980 427.0924 392.3328 269.1300 -5.3923 421.5393 426.9316 392.1234 270.7168 -5.3895 421.3885 426.7780 391.9212 272.3448 -5.3868 421.2218 426.6086 391.6981 273.9315 -5.3849 421.0699 426.4548 391.4812 275.5544 -5.3823 420.9051 426.2874 391.2567 277.1616 -5.3789 420.7394 426.1183 391.0252 278.7741 -5.3755 420.5753 425.9508 390.7889 280.3608 -5.3728 420.4148 425.7876 390.5583 281.9731 -5.3708 420.2457 425.6165 390.3223 283.5854 -5.3684 420.0744 425.4429 390.0836 285.1873 -5.3653 419.9060 425.2714 389.8483 286.7996 -5.3609 419.7341 425.0950 389.6104 288.4066 -5.3562 419.5708 424.9269 389.3639 290.0139 -5.3510 419.4156 424.7666 389.1157 291.6209 -5.3460 419.2551 424.6011 388.8713 293.2333 -5.3418 419.0852 424.4271 388.6222 294.8351 -5.3384 418.9171 424.2555 388.3699 296.4474 -5.3341 418.7419 424.0759 388.1190 298.0546 -5.3293 418.5709 423.9002 387.8741 299.6619 -5.3249 418.3991 423.7240 387.6289 301.2896 -5.3207 418.2236 423.5442 387.3790 302.8815 -5.3173 418.0539 423.3711 387.1282 304.4886 -5.3135 417.8793 423.1928 386.8787 306.0905 -5.3092 417.7100 423.0192 386.6381 307.6875 -5.3050 417.5382 422.8432 386.3937 309.2896 -5.3011 417.3593 422.6604 386.1446 310.8918 -5.2966 417.1858 422.4824 385.9013 312.4989 -5.2919 417.0064 422.2983 385.6579 314.1114 -5.2866 416.8344 422.1210 385.4168 315.7083 -5.2819 416.6533 421.9352 385.1814 317.3100 -5.2767 416.4592 421.7359 384.9405 318.9173 -5.2714 416.2776 421.5489 384.7072 320.5196 -5.2660 416.0926 421.3586 384.4798 322.1316 -5.2611 415.9077 421.1688 384.2548 323.7338 -5.2562 415.7268 420.9830 384.0309 325.3406 -5.2514 415.5405 420.7919 383.8057 326.9634 -5.2478 415.3548 420.6026 383.5803 328.5703 -5.2440 415.1675 420.4116 383.3602 330.1774 -5.2407 414.9867 420.2274 383.1416 331.7793 -5.2368 414.8021 420.0389 382.9174 333.3916 -5.2324 414.6141 419.8464 382.7043 334.9939 -5.2276 414.4257 419.6533 382.4954 336.6064 -5.2235 414.2344 419.4579 382.2871 338.1983 -5.2200 414.0543 419.2742 382.0920 339.8209 -5.2160 413.8657 419.0817 381.8838 341.4331 -5.2124 413.6721 418.8846 381.6788 343.0404 -5.2089 413.4870 418.6959 381.4827 344.6528 -5.2045 413.2961 418.5006 381.2791 346.2445 -5.2002 413.1067 418.3069 381.0825 347.8518 -5.1962 412.9129 418.1091 380.8873 349.4589 -5.1918 412.7216 417.9135 380.6943 351.0663 -5.1886 412.5286 417.7171 380.4984 352.6838 -5.1852 412.3343 417.5195 380.3137 354.2963 -5.1806 412.1400 417.3207 380.1243 355.8883 -5.1761 411.9532 417.1292 379.9405 357.4954 -5.1709 411.7635 416.9343 379.7592 359.1076 -5.1664 411.5700 416.7364 379.5818 360.7149 -5.1620 411.3762 416.5382 379.4021 362.3223 -5.1580 411.1721 416.3301 379.2240 363.9295 -5.1533 410.9797 416.1331 379.0398 365.5211 -5.1499 410.7939 415.9438 378.8608 367.1491 -5.1459 410.5957 415.7416 378.6737 368.7509 -5.1422 410.4028 415.5450 378.4970 370.3530 -5.1377 410.2131 415.3508 378.3139 371.9604 -5.1342 410.0238 415.1580 378.1244 373.5624 -5.1289 409.8381 414.9670 377.9386 375.1435 -5.1240 409.6515 414.7754 377.7575 376.7510 -5.1198 409.4615 414.5813 377.5749 378.3584 -5.1153 409.2751 414.3903 377.3883 379.9706 -5.1114 409.0832 414.1946 377.1982 381.5778 -5.1063 408.8911 413.9975 377.0159 383.1798 -5.1011 408.7030 413.8041 376.8267 384.7820 -5.0959 408.5132 413.6091 376.6372 386.3943 -5.0913 408.3170 413.4083 376.4549 387.9911 -5.0873 408.1320 413.2193 376.2697 389.5985 -5.0825 407.9412 413.0236 376.0775 391.1899 -5.0778 407.7496 412.8274 375.8890 392.8124 -5.0742 407.5533 412.6274 375.6958 394.4298 -5.0701 407.3522 412.4224 375.4962 396.0268 -5.0652 407.1561 412.2213 375.3059 397.6235 -5.0605 406.9634 412.0239 375.1109 399.2511 -5.0572 406.7676 411.8248 374.9099 400.8379 -5.0535 406.5795 411.6330 374.7063 402.4503 -5.0488 406.3930 411.4418 374.5060 404.0730 -5.0447 406.1926 411.2373 374.3063 405.6800 -5.0405 405.9949 411.0354 374.1033 407.2871 -5.0353 405.7997 410.8350 373.8943 408.8998 -5.0293 405.6089 410.6382 373.6904 410.4918 -5.0240 405.4244 410.4485 373.4809 412.0993 -5.0199 405.2431 410.2630 373.2744 413.7061 -5.0149 405.0511 410.0660 373.0630 415.3135 -5.0103 404.8610 409.8712 372.8568 416.9313 -5.0050 404.6631 409.6681 372.6431 418.5435 -4.9999 404.4684 409.4683 372.4271 420.1560 -4.9954 404.2762 409.2716 372.2080 421.7684 -4.9901 404.0837 409.0738 371.9861 423.3705 -4.9845 403.8883 408.8727 371.7704 424.9830 -4.9792 403.6893 408.6684 371.5472 426.5850 -4.9731 403.4999 408.4730 371.3254 428.2079 -4.9676 403.3070 408.2747 371.1081 429.8154 -4.9626 403.1160 408.0786 370.8903 431.4174 -4.9573 402.9177 407.8750 370.6723 433.0300 -4.9519 402.7202 407.6721 370.4521 434.6165 -4.9472 402.5270 407.4743 370.2310 436.2134 -4.9422 402.3368 407.2790 370.0055 437.8259 -4.9370 402.1429 407.0799 369.7798 439.4224 -4.9316 401.9500 406.8816 369.5573 441.0399 -4.9252 401.7432 406.6684 369.3291 442.6420 -4.9193 401.5487 406.4680 369.1010 444.2494 -4.9142 401.3543 406.2685 368.8703 445.8461 -4.9082 401.1612 406.0694 368.6471 447.4585 -4.9013 400.9617 405.8630 368.4320 449.0453 -4.8954 400.7633 405.6587 368.2195 450.6578 -4.8896 400.5722 405.4618 367.9866 452.2595 -4.8848 400.3726 405.2574 367.7570 453.8824 -4.8791 400.1728 405.0519 367.5256 455.4896 -4.8723 399.9778 404.8501 367.2955 457.0915 -4.8664 399.7826 404.6490 367.0713 458.7040 -4.8601 399.5834 404.4435 366.8450 460.3063 -4.8543 399.3836 404.2379 366.6260 461.9186 -4.8487 399.1832 404.0318 366.4004 463.5205 -4.8422 398.9886 403.8309 366.1772 465.1434 -4.8369 398.7847 403.6216 365.9475 466.7506 -4.8308 398.5875 403.4183 365.7322 468.3526 -4.8253 398.3833 403.2086 365.5110 469.9651 -4.8195 398.1820 403.0015 365.2874 471.5673 -4.8133 397.9820 402.7953 365.0718 473.1798 -4.8066 397.7797 402.5864 364.8558 474.7819 -4.8016 397.5813 402.3829 364.6399 476.4046 -4.7962 397.3777 402.1739 364.4252 478.0120 -4.7903 397.1760 401.9663 364.2174 479.6143 -4.7854 396.9802 401.7656 364.0060 481.2268 -4.7806 396.7856 401.5662 363.7950 482.8288 -4.7759 396.5837 401.3595 363.5799 484.4413 -4.7695 396.3886 401.1581 363.3699 486.0536 -4.7633 396.1851 400.9484 363.1567 487.6764 -4.7576 395.9797 400.7373 362.9470 489.2786 -4.7514 395.7711 400.5226 362.7410 490.8909 -4.7464 395.5628 400.3092 362.5347 492.4984 -4.7412 395.3581 400.0993 362.3267 494.1056 -4.7353 395.1559 399.8912 362.1262 495.7129 -4.7302 394.9557 399.6859 361.9226 497.3200 -4.7240 394.7508 399.4749 361.7214 498.9428 -4.7179 394.5507 399.2686 361.5090 500.5398 -4.7132 394.3529 399.0661 361.3073 502.1524 -4.7078 394.1505 398.8582 361.1117 503.7335 -4.7016 393.9513 398.6530 360.9231 505.3354 -4.6965 393.7519 398.4484 360.7170 506.9478 -4.6920 393.5518 398.2438 360.5214 508.5446 -4.6864 393.3440 398.0304 360.3249 510.1521 -4.6811 393.1364 397.8176 360.1211 511.7694 -4.6759 392.9343 397.6102 359.9174 513.3818 -4.6718 392.7288 397.4006 359.7235 514.9736 -4.6672 392.5282 397.1954 359.5334 516.5808 -4.6611 392.3315 396.9926 359.3322 518.1879 -4.6554 392.1314 396.7868 359.1343 519.7899 -4.6493 391.9267 396.5760 358.9405 521.4021 -4.6442 391.7263 396.3705 358.7459 523.0044 -4.6387 391.5209 396.1596 358.5537 524.6273 -4.6337 391.3139 395.9477 358.3527 526.2189 -4.6290 391.1162 395.7453 358.1679 527.8261 -4.6236 390.9143 395.5379 357.9794 529.4334 -4.6190 390.7109 395.3299 357.7910 531.0356 -4.6131 390.5039 395.1170 357.6016 532.6480 -4.6073 390.3000 394.9073 357.4109 534.2501 -4.6023 390.0995 394.7017 357.2218 535.8574 -4.5977 389.9025 394.5002 357.0285 537.4800 -4.5929 389.7018 394.2947 356.8269 539.0925 -4.5887 389.4941 394.0828 356.6228 540.6996 -4.5848 389.2876 393.8724 356.4248 542.3066 -4.5790 389.0879 393.6669 356.2292 543.9139 -4.5739 388.8856 393.4595 356.0357 545.5108 -4.5687 388.6836 393.2523 355.8331 547.1179 -4.5637 388.4861 393.0497 355.6339 548.7251 -4.5593 388.2869 392.8462 355.4319 550.3478 -4.5551 388.0818 392.6369 355.2288 551.9549 -4.5499 387.8820 392.4319 355.0272 553.5673 -4.5445 387.6746 392.2192 354.8272 555.1795 -4.5388 387.4752 392.0140 354.6163 556.7815 -4.5333 387.2792 391.8125 354.4056 558.3939 -4.5279 387.0836 391.6115 354.1939 559.9905 -4.5234 386.8797 391.4032 353.9878 561.5928 -4.5187 386.6762 391.1949 353.7850 563.2154 -4.5147 386.4704 390.9851 353.5797 564.8123 -4.5108 386.2639 390.7747 353.3705 566.4144 -4.5039 386.0585 390.5625 353.1561 568.0268 -4.4991 385.8524 390.3515 352.9458 569.6236 -4.4938 385.6436 390.1374 352.7403 571.2099 -4.4885 385.4479 389.9364 352.5321 572.8171 -4.4841 385.2541 389.7382 352.3213 574.4241 -4.4787 385.0545 389.5332 352.1213 576.0468 -4.4730 384.8517 389.3246 351.9106 577.6439 -4.4676 384.6508 389.1184 351.7057 579.2560 -4.4626 384.4541 388.9167 351.4928 580.8581 -4.4571 384.2594 388.7165 351.2805 582.4654 -4.4529 384.0608 388.5137 351.0726 584.0725 -4.4479 383.8560 388.3039 350.8614 585.6796 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