DTA measure 2meas1 Date: 202634:90 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.29 s Mass = 1172.100 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1898 -3.9411 189.4166 193.3577 247.1201 1.9863 -3.9315 189.6442 193.5757 247.1032 2.7833 -3.9172 189.8886 193.8058 247.0226 3.6010 -3.9038 190.1195 194.0234 246.9199 4.3668 -3.8923 190.3315 194.2238 246.8546 5.2253 -3.8817 190.5986 194.4803 246.7922 5.9918 -3.8753 190.8231 194.6984 246.7338 6.8088 -3.8708 191.0889 194.9597 246.6977 7.6058 -3.8652 191.2907 195.1559 246.6257 8.4030 -3.8611 191.5423 195.4034 246.5719 9.2203 -3.8495 191.7473 195.5968 246.4952 9.9965 -3.8363 191.9527 195.7890 246.4229 10.8450 -3.8272 192.1502 195.9774 246.3369 11.6108 -3.8170 192.3429 196.1599 246.2909 12.4385 -3.8102 192.5688 196.3790 246.2713 13.2050 -3.8059 192.7781 196.5839 246.2300 14.0325 -3.7960 193.0174 196.8135 246.1835 14.8190 -3.7876 193.2636 197.0512 246.1447 15.6265 -3.7762 193.5244 197.3006 246.0842 16.4435 -3.7657 193.7565 197.5222 246.0364 17.2098 -3.7507 193.9433 197.6939 245.9891 18.0685 -3.7374 194.1577 197.8950 245.9313 18.8343 -3.7268 194.3840 198.1109 245.8853 19.6620 -3.7162 194.5920 198.3082 245.8493 20.4490 -3.7062 194.7735 198.4797 245.8206 21.2558 -3.6943 194.9729 198.6672 245.8295 22.0733 -3.6828 195.2251 198.9079 245.8444 22.8398 -3.6724 195.4550 199.1274 245.8861 23.6978 -3.6668 195.6861 199.3529 245.8892 24.4640 -3.6596 195.8902 199.5499 245.8992 25.2920 -3.6514 196.1205 199.7719 245.8787 26.0783 -3.6390 196.3106 199.9496 245.8837 26.8855 -3.6258 196.5057 200.1315 245.9054 27.7033 -3.6168 196.7451 200.3619 245.9570 28.4690 -3.6061 196.9215 200.5276 246.0034 29.3275 -3.5953 197.1606 200.7559 246.0427 30.0940 -3.5816 197.3459 200.9274 246.0844 30.9213 -3.5659 197.5601 201.1260 246.1384 31.7080 -3.5566 197.7402 201.2967 246.1755 32.5155 -3.5446 197.9613 201.5059 246.2554 33.3325 -3.5351 198.2110 201.7461 246.3538 34.0988 -3.5242 198.4209 201.9452 246.4165 34.9575 -3.5113 198.6522 202.1634 246.5197 35.7235 -3.5025 198.8544 202.3569 246.6080 36.5510 -3.4923 199.0704 202.5627 246.7172 37.3380 -3.4855 199.2463 202.7319 246.8253 38.1450 -3.4785 199.4421 202.9206 246.9429 38.9725 -3.4682 199.6588 203.1271 247.0746 39.7390 -3.4575 199.8739 203.3314 247.1550 40.5870 -3.4449 200.0611 203.5061 247.2657 41.3633 -3.4336 200.2620 203.6955 247.3787 42.1810 -3.4211 200.5150 203.9361 247.5141 42.9778 -3.4113 200.7254 204.1368 247.6503 43.7745 -3.4000 200.9252 204.3253 247.7947 44.6128 -3.3840 201.0972 204.4812 247.9354 45.3685 -3.3735 201.2457 204.6192 248.0987 46.2268 -3.3673 201.4598 204.8271 248.3018 46.9933 -3.3589 201.6680 205.0269 248.4510 47.8213 -3.3529 201.8813 205.2342 248.6398 48.6175 -3.3426 202.0585 205.4011 248.7873 49.4045 -3.3309 202.2652 205.5961 248.9123 50.2428 -3.3218 202.4514 205.7731 249.0607 50.9980 -3.3102 202.6211 205.9313 249.2010 51.8568 -3.3039 202.8307 206.1346 249.3612 52.6233 -3.2948 203.0318 206.3265 249.5296 53.4503 -3.2853 203.2467 206.5320 249.6796 54.2475 -3.2810 203.4377 206.7187 249.8626 55.0345 -3.2691 203.6324 206.9015 250.0722 55.8718 -3.2634 203.8401 207.1035 250.2638 56.6280 -3.2600 204.0190 207.2790 250.4704 57.4868 -3.2462 204.2610 207.5072 250.6826 58.2523 -3.2414 204.4485 207.6899 250.8336 59.0700 -3.2360 204.6505 207.8864 251.0069 59.8570 -3.2269 204.8370 208.0639 251.1851 60.6535 -3.2196 204.9998 208.2194 251.3707 61.4710 -3.2141 205.2108 208.4249 251.5709 62.2375 -3.1997 205.3894 208.5891 251.7815 63.0858 -3.1922 205.5788 208.7710 251.9772 63.8515 -3.1848 205.7718 208.9566 252.1848 64.6795 -3.1745 205.9891 209.1636 252.4026 65.4353 -3.1666 206.1840 209.3506 252.5820 66.2628 -3.1596 206.3929 209.5525 252.7719 67.0600 -3.1534 206.5866 209.7399 252.9371 67.8465 -3.1471 206.7866 209.9337 253.0935 68.6740 -3.1347 206.9673 210.1020 253.3069 69.4405 -3.1260 207.1458 210.2718 253.5111 70.2988 -3.1223 207.3729 210.4952 253.6793 71.0545 -3.1206 207.5241 210.6447 253.8560 71.8825 -3.1144 207.7043 210.8187 254.0618 72.6793 -3.1081 207.8820 210.9900 254.2539 73.4760 -3.1011 208.0500 211.1510 254.4539 74.2630 -3.0973 208.2280 211.3253 254.6580 75.0700 -3.0912 208.4179 211.5091 254.8260 75.8873 -3.0848 208.6190 211.7038 255.0041 76.6538 -3.0796 208.7703 211.8499 255.1521 77.5125 -3.0686 208.9693 212.0379 255.3109 78.2780 -3.0656 209.1507 212.2163 255.4785 79.1060 -3.0617 209.3911 212.4527 255.6853 79.8930 -3.0553 209.5622 212.6175 255.8715 80.6998 -3.0484 209.7421 212.7905 256.0270 81.4865 -3.0442 209.9396 212.9837 256.1823 82.2838 -3.0373 210.1309 213.1683 256.3518 83.1110 -3.0320 210.3030 213.3351 256.4865 83.8773 -3.0282 210.4809 213.5092 256.6282 84.7360 -3.0219 210.6786 213.7005 256.8455 85.4915 -3.0160 210.8631 213.8791 257.0033 86.3295 -3.0126 211.0225 214.0351 257.1736 87.1165 -3.0085 211.1888 214.1973 257.3409 87.9130 -3.0038 211.3864 214.3902 257.5404 88.7408 -2.9989 211.5948 214.5937 257.7052 89.5073 -2.9957 211.7705 214.7662 257.8672 90.3653 -2.9910 211.9602 214.9512 258.0381 91.1008 -2.9870 212.1306 215.1175 258.1635 91.9595 -2.9835 212.3265 215.3100 258.2640 92.7250 -2.9855 212.4613 215.4468 258.3964 93.5530 -2.9812 212.6591 215.6403 258.5510 94.3400 -2.9747 212.8401 215.8148 258.6739 95.1468 -2.9687 213.0236 215.9923 258.7783 95.9745 -2.9657 213.2225 216.1883 258.9106 96.7410 -2.9601 213.3878 216.3479 259.0679 97.5885 -2.9525 213.5604 216.5130 259.1708 98.3345 -2.9457 213.7509 216.6966 259.2609 99.1830 -2.9469 213.8922 216.8391 259.3850 99.9485 -2.9421 214.0742 217.0163 259.5077 100.7765 -2.9357 214.2841 217.2197 259.6469 101.5738 -2.9288 214.4980 217.4268 259.7849 102.3703 -2.9269 214.6813 217.6082 259.9376 103.1980 -2.9222 214.8502 217.7724 260.0797 103.9645 -2.9169 215.0421 217.9590 260.1830 104.8225 -2.9143 215.1995 218.1138 260.3643 105.5888 -2.9106 215.3918 218.3023 260.4870 106.4065 -2.9033 215.5758 218.4791 260.5856 107.2133 -2.8954 215.7781 218.6734 260.6856 108.0000 -2.8911 215.9497 218.8407 260.8237 108.8280 -2.8875 216.1668 219.0543 260.9280 109.5940 -2.8856 216.3499 219.2355 261.0602 110.4523 -2.8834 216.5384 219.4218 261.2023 111.2188 -2.8756 216.7123 219.5879 261.3151 112.0360 -2.8684 216.8999 219.7683 261.4266 112.8430 -2.8695 217.0576 219.9271 261.5598 113.6300 -2.8731 217.2194 220.0926 261.6689 114.4578 -2.8713 217.3781 220.2494 261.7639 115.2235 -2.8634 217.5455 220.4089 261.8552 116.0823 -2.8552 217.7452 220.6004 261.9728 116.8488 -2.8445 217.9351 220.7796 262.0921 117.6758 -2.8387 218.1242 220.9629 262.2000 118.4730 -2.8319 218.3047 221.1367 262.3249 119.2703 -2.8303 218.4472 221.2775 262.4434 120.0973 -2.8273 218.6419 221.4692 262.5449 120.8638 -2.8254 218.8342 221.6595 262.6674 121.6915 -2.8236 219.0348 221.8584 262.8187 122.4470 -2.8204 219.2408 222.0613 262.9350 123.2955 -2.8127 219.4208 222.2335 263.0492 124.0720 -2.8109 219.5505 222.3614 263.1677 124.8890 -2.8108 219.7142 222.5250 263.2868 125.6760 -2.8079 219.9233 222.7312 263.3828 126.4835 -2.8016 220.1087 222.9102 263.4991 127.3003 -2.7948 220.2375 223.0324 263.5773 128.0565 -2.7867 220.3960 223.1827 263.7035 128.9153 -2.7841 220.5693 223.3535 263.8246 129.6808 -2.7870 220.7360 223.5229 263.9344 130.4985 -2.7817 220.9161 223.6978 264.0534 131.2958 -2.7748 221.0965 223.8713 264.1780 132.0923 -2.7774 221.2717 224.0491 264.2633 132.8790 -2.7706 221.4534 224.2241 264.3384 133.6865 -2.7636 221.6247 224.3884 264.4619 134.5038 -2.7593 221.7657 224.5250 264.5463 135.2698 -2.7530 221.9071 224.6601 264.6810 136.1285 -2.7505 222.0964 224.8468 264.7765 136.8945 -2.7500 222.2676 225.0177 264.9149 137.7220 -2.7475 222.4308 225.1784 265.0551 138.5090 -2.7449 222.6188 225.3637 265.1503 139.3055 -2.7390 222.7828 225.5218 265.3228 140.1333 -2.7342 222.9774 225.7116 265.4746 140.8895 -2.7297 223.1476 225.8773 265.5901 141.7580 -2.7239 223.3468 226.0707 265.7062 142.5138 -2.7181 223.5156 226.2337 265.8134 143.3418 -2.7110 223.7047 226.4157 265.9283 144.1388 -2.7055 223.8678 226.5733 266.0630 144.9353 -2.7059 224.0223 226.7281 266.1708 145.7633 -2.7003 224.1807 226.8810 266.3088 146.5190 -2.6996 224.3253 227.0249 266.4329 147.3875 -2.6952 224.5188 227.2140 266.5546 148.1438 -2.6914 224.6681 227.3595 266.6540 148.9715 -2.6860 224.8440 227.5300 266.7916 149.7680 -2.6827 225.0087 227.6914 266.9253 150.5653 -2.6767 225.1364 227.8131 267.0559 151.3933 -2.6714 225.3287 228.0001 267.1944 152.1485 -2.6675 225.5147 228.1822 267.2690 153.0175 -2.6611 225.7139 228.3750 267.3861 153.7738 -2.6555 225.8967 228.5522 267.5248 154.6113 -2.6518 226.0338 228.6857 267.6872 155.3980 -2.6450 226.2088 228.8538 267.8122 156.1953 -2.6399 226.3718 229.0117 267.9658 157.0230 -2.6390 226.5809 229.2199 268.1285 157.7785 -2.6396 226.7700 229.4096 268.2314 158.6475 -2.6343 226.9475 229.5818 268.3912 159.4035 -2.6350 227.0643 229.6993 268.4907 160.2308 -2.6334 227.2201 229.8535 268.5940 161.0280 -2.6265 227.4082 230.0347 268.7498 161.8253 -2.6256 227.5884 230.2139 268.8833 162.6528 -2.6266 227.7410 230.3676 269.0513 163.4085 -2.6232 227.8835 230.5067 269.1802 164.2775 -2.6189 228.0875 230.7065 269.3347 165.0333 -2.6150 228.2668 230.8818 269.4415 165.8608 -2.6142 228.4201 231.0343 269.5845 166.6580 -2.6134 228.5666 231.1800 269.7498 167.4653 -2.6109 228.7625 231.3734 269.8462 168.2823 -2.6073 228.9270 231.5343 270.0020 169.0488 -2.6083 229.0647 231.6730 270.1464 169.9075 -2.6010 229.2593 231.8603 270.2698 170.6733 -2.5970 229.4641 232.0611 270.3891 171.5010 -2.5957 229.6546 232.2503 270.5234 172.2880 -2.5963 229.8053 232.4017 270.6819 173.0950 -2.5920 229.9562 232.5481 270.8315 173.9123 -2.5865 230.1114 232.6979 270.9829 174.6788 -2.5881 230.2596 232.8477 271.1030 175.5370 -2.5883 230.4345 233.0228 271.2494 176.3030 -2.5807 230.5737 233.1544 271.3741 177.1310 -2.5754 230.7323 233.3077 271.5559 177.9180 -2.5709 230.9025 233.4735 271.7142 178.7245 -2.5657 231.0891 233.6548 271.8307 179.5423 -2.5640 231.2586 233.8226 271.9441 180.3190 -2.5594 231.4067 233.9662 272.0768 181.1665 -2.5548 231.5846 234.1393 272.2272 181.9125 -2.5523 231.7070 234.2592 272.3554 182.7610 -2.5473 231.9272 234.4746 272.5001 183.5265 -2.5474 232.1155 234.6629 272.5982 184.3545 -2.5463 232.2952 234.8415 272.7410 185.1515 -2.5471 232.4726 235.0196 272.8825 185.9378 -2.5435 232.6438 235.1873 272.9981 186.7658 -2.5418 232.8001 235.3419 273.1385 187.5218 -2.5345 232.9202 235.4548 273.2492 188.3695 -2.5313 233.0695 235.6008 273.3584 189.1463 -2.5281 233.2464 235.7745 273.4685 189.9640 -2.5246 233.3975 235.9221 273.6134 190.7500 -2.5219 233.5714 236.0933 273.7378 191.5473 -2.5186 233.7367 236.2553 273.8786 192.3650 -2.5145 233.8751 236.3897 273.9952 193.1305 -2.5103 233.9988 236.5091 274.1349 193.9893 -2.5097 234.1778 236.6875 274.2766 194.7250 -2.5036 234.3071 236.8107 274.4202 195.5725 -2.5041 234.4729 236.9770 274.5718 196.3390 -2.5007 234.6408 237.1415 274.6765 197.1670 -2.4978 234.8290 237.3268 274.8292 197.9533 -2.4971 234.9539 237.4510 274.9873 198.7605 -2.4931 235.1225 237.6156 275.1112 199.5783 -2.4891 235.3061 237.7951 275.2289 200.3343 -2.4885 235.4696 237.9581 275.3338 201.2025 -2.4881 235.6018 238.0899 275.4663 201.9588 -2.4908 235.7666 238.2575 275.6154 202.7865 -2.4904 235.9326 238.4230 275.7460 203.5523 -2.4873 236.0954 238.5827 275.8689 204.3803 -2.4850 236.2669 238.7519 276.0092 205.1670 -2.4888 236.4140 238.9028 276.1214 205.9635 -2.4897 236.5830 239.0727 276.2517 206.7915 -2.4864 236.7751 239.2616 276.3946 207.5578 -2.4866 236.9674 239.4540 276.5162 208.4158 -2.4854 237.1578 239.6432 276.6430 209.1823 -2.4846 237.3199 239.8045 276.7842 210.0098 -2.4775 237.4819 239.9593 276.9316 210.8065 -2.4626 237.6204 240.0830 277.0811 211.5935 -2.4489 237.7556 240.2045 277.2411 212.4005 -2.4458 237.8715 240.3173 277.3507 213.1870 -2.4446 238.0169 240.4614 277.4382 214.0150 -2.4410 238.1953 240.6364 277.5705 214.7810 -2.4431 238.3654 240.8086 277.6829 215.6393 -2.4427 238.5281 240.9708 277.8053 216.4058 -2.4419 238.6396 241.0815 277.9231 217.2233 -2.4450 238.7581 241.2031 278.0704 218.0300 -2.4474 238.9519 241.3992 278.2320 218.8170 -2.4463 239.1369 241.5832 278.3534 219.6448 -2.4445 239.3289 241.7734 278.4690 220.4105 -2.4467 239.4860 241.9327 278.5884 221.2693 -2.4435 239.6404 242.0839 278.7222 222.0358 -2.4391 239.7721 242.2111 278.8462 222.8525 -2.4364 239.9053 242.3418 279.0066 223.6600 -2.4397 240.0269 242.4667 279.1540 224.4470 -2.4387 240.1775 242.6162 279.2726 225.2740 -2.4345 240.3620 242.7965 279.3833 226.0405 -2.4306 240.5024 242.9330 279.5079 226.8993 -2.4286 240.6969 243.1254 279.6281 227.6653 -2.4237 240.8653 243.2890 279.7453 228.4825 -2.4168 241.0556 243.4723 279.8773 229.2900 -2.4181 241.2386 243.6567 279.9890 230.0763 -2.4187 241.3744 243.7931 280.1035 230.9040 -2.4203 241.5523 243.9726 280.2118 231.6705 -2.4212 241.6833 244.1045 280.3174 232.5288 -2.4185 241.8326 244.2511 280.4508 233.2948 -2.4164 241.9478 244.3643 280.5724 234.1125 -2.4133 242.1016 244.5149 280.6805 234.9195 -2.4105 242.2544 244.6649 280.8118 235.7060 -2.4070 242.4201 244.8271 280.9183 236.5340 -2.4066 242.6028 245.0095 281.0445 237.3003 -2.4072 242.7494 245.1566 281.1488 238.1583 -2.3980 242.9231 245.3211 281.2659 238.9248 -2.4000 243.0864 245.4864 281.3662 239.7425 -2.3990 243.2736 245.6727 281.4910 240.5490 -2.3936 243.3865 245.7801 281.6088 241.3360 -2.3871 243.5312 245.9182 281.7581 242.1640 -2.3817 243.6581 246.0398 281.9107 242.9298 -2.3784 243.7860 246.1644 282.0643 243.7883 -2.3752 243.9875 246.3627 282.1894 244.5548 -2.3721 244.1580 246.5301 282.3160 245.3720 -2.3741 244.3374 246.7115 282.4329 246.1790 -2.3725 244.4881 246.8606 282.5357 246.9660 -2.3688 244.5971 246.9660 282.6318 247.8038 -2.3618 244.7325 247.0943 282.7370 248.5595 -2.3574 244.8939 247.2513 282.8895 249.4183 -2.3570 245.0680 247.4249 283.0505 250.1740 -2.3542 245.1928 247.5469 283.1823 251.0015 -2.3549 245.3361 247.6909 283.3075 251.7988 -2.3551 245.5032 247.8583 283.4189 252.5855 -2.3527 245.6814 248.0340 283.5936 253.4128 -2.3513 245.8420 248.1933 283.7200 254.1895 -2.3421 246.0105 248.3525 283.8772 255.0380 -2.3385 246.1480 248.4865 284.0110 255.7625 -2.3356 246.3191 248.6547 284.0914 256.6315 -2.3324 246.5019 248.8343 284.2682 257.3878 -2.3292 246.6550 248.9842 284.3899 258.2045 -2.3211 246.8381 249.1592 284.5186 259.0120 -2.3189 246.9614 249.2802 284.6859 259.7988 -2.3196 247.0970 249.4166 284.8332 260.6158 -2.3216 247.2366 249.5582 284.9863 261.3925 -2.3183 247.3896 249.7079 285.1199 262.2408 -2.3151 247.5662 249.8813 285.2754 263.0065 -2.3153 247.6987 250.0140 285.4074 263.8345 -2.3132 247.8608 250.1740 285.5766 264.6215 -2.3092 248.0246 250.3338 285.7031 265.4178 -2.3085 248.1871 250.4957 285.8316 266.2458 -2.3082 248.3317 250.6399 285.9733 267.0123 -2.3035 248.4655 250.7690 286.1176 267.8703 -2.3012 248.6190 250.9202 286.2788 268.6263 -2.2991 248.7750 251.0741 286.4087 269.4645 -2.2968 248.9432 251.2400 286.5754 270.2513 -2.2969 249.1123 251.4092 286.6971 271.0375 -2.2932 249.2403 251.5335 286.8196 271.8758 -2.2921 249.4164 251.7085 286.9098 272.6315 -2.2918 249.5378 251.8296 287.0812 273.4590 -2.2900 249.7133 252.0034 287.2410 274.2255 -2.2848 249.8730 252.1579 287.3939 275.0840 -2.2834 250.0032 252.2866 287.5702 275.8498 -2.2825 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