DTA measure 3gyorsfutes Date: 2025923:1123 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.72 s Mass = 1115.900 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3938 -13.0771 435.1807 448.2578 433.7574 3.9971 -13.0935 435.2784 448.3719 433.9745 5.5955 -13.1134 435.3461 448.4594 434.0806 7.1988 -13.1337 435.4035 448.5372 434.1074 8.8021 -13.1512 435.4878 448.6390 433.9794 10.4004 -13.1639 435.5918 448.7557 433.7309 12.0039 -13.1723 435.7104 448.8828 433.3666 13.6074 -13.1762 435.7721 448.9483 432.8996 15.2005 -13.1865 435.8330 449.0195 432.4315 16.8038 -13.1932 435.9234 449.1166 431.8179 18.4226 -13.2018 436.0281 449.2299 431.2101 20.0311 -13.2121 436.0818 449.2939 430.5660 21.6345 -13.2196 436.1587 449.3783 430.0013 23.2431 -13.2220 436.2443 449.4663 429.4470 24.8309 -13.2255 436.2878 449.5133 428.9034 26.4395 -13.2387 436.2894 449.5281 428.4570 28.0481 -13.2445 436.2532 449.4977 428.0476 29.6565 -13.2487 436.3065 449.5552 427.7149 31.2754 -13.2519 436.3552 449.6071 427.5045 32.8789 -13.2579 436.3663 449.6242 427.4206 34.4873 -13.2630 436.3641 449.6271 427.3597 36.0908 -13.2706 436.3530 449.6236 427.3647 37.6991 -13.2864 436.3467 449.6332 427.4576 39.3076 -13.2953 436.3267 449.6220 427.5625 40.9163 -13.3044 436.3541 449.6585 427.6822 42.5351 -13.3147 436.3661 449.6808 427.7794 44.1486 -13.3241 436.4174 449.7415 427.8537 45.7521 -13.3341 436.4363 449.7704 427.8992 47.3606 -13.3512 436.4802 449.8314 427.8784 48.9641 -13.3626 436.4904 449.8530 427.7601 50.5728 -13.3678 436.4672 449.8351 427.5769 52.1814 -13.3763 436.4538 449.8300 427.3003 53.7999 -13.3831 436.4357 449.8189 426.9019 55.4136 -13.3857 436.4272 449.8129 426.5119 57.0014 -13.3909 436.3971 449.7880 426.1318 58.6150 -13.3984 436.3963 449.7947 425.7127 60.2186 -13.4066 436.4010 449.8076 425.3107 61.8320 -13.4133 436.4224 449.8357 424.8726 63.4355 -13.4176 436.3977 449.8153 424.4446 65.0489 -13.4244 436.3508 449.7752 424.0947 66.6678 -13.4350 436.3371 449.7721 423.7436 68.2764 -13.4394 436.2787 449.7181 423.4160 69.8744 -13.4479 436.2355 449.6833 423.1369 71.4779 -13.4552 436.2140 449.6692 422.9409 73.0659 -13.4646 436.1957 449.6603 422.8290 74.6693 -13.4740 436.1245 449.5985 422.7232 76.2728 -13.4820 436.0875 449.5695 422.6311 77.8761 -13.4888 436.0481 449.5369 422.5221 79.4795 -13.4888 435.9955 449.4843 422.4856 81.0880 -13.4940 435.9681 449.4621 422.3960 82.6861 -13.5030 435.9312 449.4343 422.3342 84.2948 -13.5084 435.7715 449.2799 422.2928 85.8983 -13.5192 435.6696 449.1888 422.2354 87.5015 -13.5247 435.6097 449.1344 422.1128 89.1101 -13.5311 435.6183 449.1494 421.9557 90.7135 -13.5362 435.5615 449.0976 421.7940 92.3373 -13.5402 435.5246 449.0648 421.5886 93.9254 -13.5448 435.4461 448.9909 421.3489 95.5390 -13.5518 435.4183 448.9702 421.0427 97.1475 -13.5526 435.4100 448.9625 420.7483 98.7408 -13.5572 435.3210 448.8781 420.4504 100.3441 -13.5605 435.2399 448.8004 420.1597 101.9526 -13.5620 435.1838 448.7458 419.8013 103.5563 -13.5685 435.0983 448.6669 419.4622 105.1598 -13.5744 434.9914 448.5658 419.1331 106.7835 -13.5796 434.9201 448.4996 418.8429 108.3871 -13.5854 434.8386 448.4240 418.5183 110.0008 -13.5880 434.7508 448.3388 418.2226 111.6040 -13.5853 434.6855 448.2708 417.9655 113.2126 -13.5850 434.6270 448.2120 417.7411 114.8161 -13.5842 434.5041 448.0883 417.5736 116.4245 -13.5889 434.3835 447.9724 417.4141 118.0435 -13.5975 434.2516 447.8491 417.2963 119.6470 -13.6023 434.1438 447.7461 417.1635 121.2555 -13.6087 434.0614 447.6701 417.0725 122.8640 -13.6161 433.9683 447.5844 416.9430 124.4726 -13.6131 433.8804 447.4935 416.8850 126.0811 -13.6141 433.7866 447.4007 416.8050 127.6896 -13.6216 433.6983 447.3199 416.7181 129.3136 -13.6282 433.6199 447.2482 416.6077 130.9066 -13.6297 433.4245 447.0542 416.3928 132.5101 -13.6269 433.2694 446.8962 416.1725 134.1135 -13.6314 433.1879 446.8193 415.9587 135.7119 -13.6379 433.0872 446.7251 415.7255 137.3151 -13.6344 432.9897 446.6242 415.4811 138.9186 -13.6399 432.8901 446.5300 415.1985 140.5219 -13.6372 432.7858 446.4230 414.9058 142.1254 -13.6338 432.6931 446.3270 414.5754 143.7340 -13.6382 432.5721 446.2103 414.2549 145.3373 -13.6364 432.4838 446.1201 413.9681 146.9510 -13.6334 432.3610 445.9944 413.6758 148.5543 -13.6341 432.2139 445.8481 413.3908 150.1474 -13.6392 432.1096 445.7488 413.1390 151.7663 -13.6405 431.9803 445.6208 412.9459 153.3748 -13.6490 431.8693 445.5183 412.7117 154.9936 -13.6509 431.7258 445.3767 412.5038 156.5766 -13.6494 431.5762 445.2256 412.3420 158.2106 -13.6545 431.4570 445.1115 412.1900 159.8141 -13.6472 431.3427 444.9900 412.0064 161.4226 -13.6416 431.2651 444.9067 411.8564 163.0311 -13.6401 431.1304 444.7705 411.7138 164.6241 -13.6369 431.0041 444.6411 411.5628 166.2431 -13.6370 430.8703 444.5073 411.4069 167.8466 -13.6405 430.7287 444.3692 411.2396 169.4603 -13.6434 430.5858 444.2291 411.0553 171.0636 -13.6459 430.4516 444.0975 410.9167 172.6723 -13.6412 430.2850 443.9262 410.7131 174.2756 -13.6418 430.1164 443.7582 410.5184 175.8894 -13.6370 429.9812 443.6182 410.3300 177.4928 -13.6351 429.8260 443.4612 410.1097 179.1064 -13.6290 429.6964 443.3254 409.8730 180.7098 -13.6298 429.5561 443.1858 409.6370 182.3234 -13.6255 429.4421 443.0676 409.4288 183.9115 -13.6204 429.2816 442.9020 409.1845 185.5201 -13.6156 429.1770 442.7926 408.9392 187.1441 -13.6129 429.0515 442.6644 408.6408 188.7474 -13.6104 428.9050 442.5154 408.4059 190.3560 -13.6032 428.7365 442.3397 408.1378 191.9646 -13.6050 428.5380 442.1430 407.8775 193.5730 -13.6034 428.3694 441.9728 407.6399 195.1816 -13.6025 428.2078 441.8103 407.4183 196.7903 -13.6035 428.0827 441.6862 407.1990 198.4089 -13.6041 427.9793 441.5834 407.0296 200.0175 -13.6010 427.8374 441.4383 406.8570 201.6211 -13.5986 427.7279 441.3265 406.6731 203.2295 -13.5909 427.5741 441.1650 406.5074 204.8226 -13.5843 427.3966 440.9808 406.3112 206.4311 -13.5794 427.2282 440.8076 406.0856 208.0395 -13.5766 427.0222 440.5989 405.8915 209.6481 -13.5719 426.8663 440.4382 405.7356 211.2669 -13.5682 426.7090 440.2772 405.5014 212.8600 -13.5683 426.5109 440.0791 405.3064 214.4379 -13.5667 426.3918 439.9585 405.1523 216.0259 -13.5675 426.2185 439.7860 404.9137 217.6243 -13.5643 426.0294 439.5937 404.7320 219.2226 -13.5599 425.8740 439.4339 404.5218 220.8261 -13.5547 425.7165 439.2711 404.2922 222.4243 -13.5471 425.5911 439.1382 404.0653 224.0483 -13.5395 425.4506 438.9901 403.8581 225.6518 -13.5331 425.2520 438.7850 403.6516 227.2601 -13.5267 425.0637 438.5904 403.3990 228.8483 -13.5245 424.9248 438.4493 403.1667 230.4565 -13.5216 424.7485 438.2701 402.9358 232.0599 -13.5145 424.5618 438.0764 402.7307 233.6685 -13.5095 424.3918 437.9014 402.4897 235.2769 -13.5058 424.1826 437.6885 402.2510 236.8958 -13.5003 423.9902 437.4905 402.0346 238.5095 -13.4921 423.8202 437.3123 401.8400 240.1128 -13.4863 423.6450 437.1314 401.6917 241.7265 -13.4883 423.5108 436.9992 401.4761 243.3298 -13.4851 423.3058 436.7909 401.2679 244.9333 -13.4805 423.1205 436.6009 401.0635 246.5316 -13.4763 422.9770 436.4533 400.8581 248.1198 -13.4777 422.8081 436.2858 400.6580 249.7384 -13.4773 422.6414 436.1187 400.4365 251.3419 -13.4701 422.4873 435.9574 400.2395 252.9505 -13.4644 422.2824 435.7468 400.0257 254.5538 -13.4618 422.1045 435.5663 399.7919 256.1573 -13.4581 421.9679 435.4260 399.6099 257.7658 -13.4489 421.7892 435.2382 399.3835 259.3690 -13.4396 421.6017 435.0414 399.1716 260.9981 -13.4351 421.4070 434.8420 398.9466 262.6015 -13.4268 421.2357 434.6625 398.7283 264.2151 -13.4217 421.0446 434.4663 398.4971 265.8186 -13.4147 420.8537 434.2683 398.2957 267.4271 -13.4122 420.6667 434.0790 398.1165 269.0305 -13.4053 420.4842 433.8894 397.9214 270.6391 -13.3960 420.3619 433.7579 397.7833 272.2579 -13.3894 420.2178 433.6071 397.5803 273.8715 -13.3867 420.0266 433.4133 397.3686 275.4751 -13.3904 419.8278 433.2182 397.1026 277.0579 -13.3827 419.6223 433.0050 396.9095 278.6664 -13.3727 419.4041 432.7768 396.6963 280.2699 -13.3684 419.1736 432.5420 396.4864 281.8681 -13.3600 419.0370 432.3970 396.2230 283.4766 -13.3482 418.8960 432.2441 395.9740 285.0648 -13.3399 418.6810 432.0209 395.8088 286.6886 -13.3324 418.5253 431.8577 395.5930 288.2920 -13.3257 418.3652 431.6909 395.3756 289.9006 -13.3162 418.2024 431.5185 395.1765 291.5141 -13.3100 418.0228 431.3328 394.9802 293.1023 -13.3082 417.8451 431.1532 394.7820 294.7109 -13.3059 417.6245 430.9304 394.5689 296.3191 -13.3054 417.4442 430.7496 394.3168 297.9278 -13.2940 417.2556 430.5497 394.0647 299.5361 -13.2888 417.0925 430.3813 393.8105 301.1446 -13.2820 416.8949 430.1769 393.5764 302.7533 -13.2719 416.7107 429.9826 393.3474 304.3615 -13.2679 416.4951 429.7630 393.1488 305.9701 -13.2593 416.2843 429.5436 392.9111 307.5784 -13.2479 416.1025 429.3505 392.7328 309.1818 -13.2505 415.8844 429.1349 392.5805 310.7646 -13.2442 415.6860 428.9301 392.4280 312.3680 -13.2342 415.4628 428.6970 392.2283 313.9714 -13.2268 415.2525 428.4792 392.0334 315.5901 -13.2220 415.0690 428.2910 391.8655 317.1935 -13.2114 414.8991 428.1105 391.7237 318.7970 -13.2046 414.7503 427.9549 391.4686 320.4004 -13.1968 414.6276 427.8244 391.2355 322.0089 -13.1938 414.4828 427.6766 391.0409 323.6124 -13.1853 414.2734 427.4587 390.8487 325.2209 -13.1777 414.0175 427.1953 390.6542 326.8396 -13.1723 413.7945 426.9669 390.4275 328.4483 -13.1684 413.5826 426.7509 390.2378 330.0568 -13.1616 413.4025 426.5641 390.0370 331.6654 -13.1529 413.2320 426.3849 389.8003 333.2739 -13.1454 413.0353 426.1807 389.5425 334.8824 -13.1368 412.8646 426.0015 389.3113 336.4858 -13.1307 412.6754 425.8061 389.0545 338.1149 -13.1192 412.4921 425.6114 388.8260 339.7183 -13.1121 412.3022 425.4143 388.6358 341.3216 -13.1049 412.1043 425.2091 388.4134 342.9099 -13.0982 411.8999 424.9981 388.1677 344.5131 -13.0935 411.6733 424.7668 387.9690 346.1114 -13.0838 411.5014 424.5852 387.7574 347.7200 -13.0716 411.3245 424.3961 387.5483 349.3181 -13.0629 411.1615 424.2243 387.3431 350.9420 -13.0561 410.9665 424.0226 387.1118 352.5455 -13.0480 410.7924 423.8403 386.8703 354.1489 -13.0438 410.5455 423.5893 386.6454 355.7574 -13.0413 410.3606 423.4019 386.4665 357.3609 -13.0354 410.1748 423.2102 386.2908 358.9693 -13.0294 409.9469 422.9763 386.1243 360.5779 -13.0196 409.7559 422.7755 385.9316 362.2019 -13.0072 409.5818 422.5891 385.7254 363.8051 -13.0017 409.4129 422.4146 385.5905 365.4139 -12.9960 409.1827 422.1787 385.3900 367.0174 -12.9888 408.9807 421.9695 385.1549 368.6310 -12.9816 408.7998 421.7814 384.9448 370.2343 -12.9721 408.5936 421.5658 384.6990 371.8480 -12.9641 408.4070 421.3712 384.4786 373.4666 -12.9564 408.2099 421.1663 384.2155 375.0650 -12.9517 408.0379 420.9896 383.9875 376.6736 -12.9439 407.8243 420.7682 383.7656 378.2564 -12.9389 407.6367 420.5756 383.5238 379.8599 -12.9346 407.4216 420.3562 383.3088 381.4685 -12.9268 407.2154 420.1421 383.1110 383.0718 -12.9214 407.0162 419.9375 382.8632 384.6805 -12.9094 406.7922 419.7016 382.6564 386.2993 -12.9054 406.5902 419.4956 382.4486 387.9079 -12.9047 406.4058 419.3105 382.2281 389.5163 -12.9020 406.2635 419.1656 381.9789 391.1095 -12.8935 406.0778 418.9713 381.7654 392.7128 -12.8842 405.8914 418.7756 381.5995 394.3265 -12.8713 405.6829 418.5542 381.4186 395.9299 -12.8621 405.5130 418.3751 381.1968 397.5435 -12.8514 405.2902 418.1416 380.9887 399.1624 -12.8413 405.0481 417.8894 380.8009 400.7710 -12.8318 404.7873 417.6192 380.6257 402.3641 -12.8289 404.5727 417.4016 380.4222 403.9779 -12.8190 404.4128 417.2318 380.2397 405.5814 -12.8148 404.2493 417.0641 380.0340 407.1794 -12.8064 404.0840 416.8903 379.8586 408.7880 -12.7955 403.8612 416.6567 379.6531 410.3916 -12.7869 403.6470 416.4339 379.4490 412.0053 -12.7864 403.4514 416.2378 379.2204 413.6138 -12.7761 403.2272 416.0033 378.9835 415.2173 -12.7693 403.0362 415.8055 378.7852 416.8258 -12.7633 402.8488 415.6122 378.6129 418.4188 -12.7555 402.6233 415.3788 378.4230 420.0274 -12.7480 402.4135 415.1614 378.1704 421.6306 -12.7375 402.2173 414.9548 377.8945 423.2393 -12.7330 402.0023 414.7353 377.7021 424.8633 -12.7245 401.8203 414.5448 377.5387 426.4768 -12.7142 401.5942 414.3084 377.3389 428.0803 -12.7049 401.4250 414.1300 377.0892 429.6940 -12.6936 401.2014 413.8950 376.8084 431.2973 -12.6786 401.0249 413.7035 376.5640 432.9059 -12.6692 400.8462 413.5154 376.3147 434.5094 -12.6658 400.6295 413.2953 376.0610 436.1383 -12.6604 400.4246 413.0851 375.8295 437.7418 -12.6497 400.2540 412.9037 375.5793 439.3401 -12.6417 400.0981 412.7398 375.3671 440.9485 -12.6404 399.8980 412.5384 375.1701 442.5519 -12.6367 399.6490 412.2857 374.9744 444.1553 -12.6325 399.4606 412.0931 374.8021 445.7586 -12.6296 399.2451 411.8747 374.6289 447.3620 -12.6236 399.0316 411.6552 374.4327 448.9705 -12.6116 398.7838 411.3954 374.2482 450.5740 -12.5993 398.5913 411.1906 374.0945 452.1980 -12.5950 398.3649 410.9600 373.8665 453.8013 -12.5845 398.1852 410.7698 373.6706 455.4048 -12.5753 398.0156 410.5909 373.4434 457.0134 -12.5658 397.8146 410.3804 373.2535 458.6374 -12.5502 397.5498 410.1001 373.0711 460.2458 -12.5416 397.3339 409.8756 372.8446 461.8493 -12.5353 397.1252 409.6605 372.6305 463.4580 -12.5296 396.9875 409.5171 372.4211 465.0613 -12.5210 396.8178 409.3388 372.1648 466.6699 -12.5158 396.6248 409.1406 371.9534 468.2785 -12.5086 396.4270 408.9356 371.7181 469.9023 -12.4965 396.1941 408.6906 371.5143 471.5006 -12.4918 396.0037 408.4955 371.3009 473.0888 -12.4852 395.8307 408.3159 371.0978 474.6971 -12.4747 395.5802 408.0549 370.9024 476.3006 -12.4660 395.3525 407.8185 370.7008 477.9093 -12.4565 395.1641 407.6206 370.4779 479.5125 -12.4502 394.9220 407.3722 370.2970 481.1160 -12.4418 394.7619 407.2038 370.0962 482.7451 -12.4337 394.5195 406.9531 369.8882 484.3484 -12.4278 394.3230 406.7507 369.6631 485.9570 -12.4222 394.1538 406.5760 369.4378 487.5605 -12.4110 393.9537 406.3646 369.1848 489.1689 -12.4011 393.8066 406.2077 368.9374 490.7775 -12.3927 393.5638 405.9565 368.7336 492.3861 -12.3924 393.3316 405.7240 368.5179 494.0048 -12.3920 393.1509 405.5430 368.3237 495.6134 -12.3820 392.9731 405.3551 368.1482 497.2170 -12.3775 392.7405 405.1181 367.9071 498.8305 -12.3735 392.5362 404.9097 367.6972 500.4339 -12.3708 392.3743 404.7452 367.4594 502.0374 -12.3630 392.1468 404.5099 367.2467 503.6409 -12.3543 391.8943 404.2486 367.0279 505.2596 -12.3445 391.7085 404.0529 366.8123 506.8426 -12.3312 391.5513 403.8826 366.6180 508.4511 -12.3243 391.3492 403.6735 366.4058 510.0545 -12.3129 391.1519 403.4648 366.2298 511.6631 -12.3003 390.9579 403.2582 366.0165 513.2665 -12.2935 390.7576 403.0511 365.7574 514.8750 -12.2850 390.5158 402.8009 365.5351 516.4785 -12.2756 390.2625 402.5381 365.3273 518.0870 -12.2703 390.0685 402.3388 365.1388 519.6955 -12.2636 389.8915 402.1551 364.9113 521.3041 -12.2510 389.7019 401.9529 364.7097 522.9125 -12.2368 389.4879 401.7247 364.5651 524.5159 -12.2284 389.2503 401.4787 364.3788 526.1246 -12.2201 389.0397 401.2598 364.1693 527.7331 -12.2121 388.8258 401.0379 363.9259 529.3416 -12.2070 388.6442 400.8512 363.7048 530.9656 -12.2009 388.4221 400.6230 363.4947 532.5741 -12.1926 388.2315 400.4242 363.2482 534.1775 -12.1869 388.0312 400.2182 363.0251 535.7759 -12.1812 387.7920 399.9732 362.8228 537.3740 -12.1723 387.6237 399.7960 362.6207 538.9724 -12.1699 387.4262 399.5961 362.4538 540.5656 -12.1632 387.1918 399.3550 362.2612 542.1689 -12.1546 386.9741 399.1288 362.0748 543.7774 -12.1489 386.8190 398.9679 361.8542 545.3860 -12.1431 386.6205 398.7636 361.5559 546.9893 -12.1351 386.4056 398.5407 361.3294 548.6133 -12.1228 386.1826 398.3053 361.1356 550.2168 -12.1142 385.9902 398.1045 360.9607 551.8149 -12.1097 385.7765 397.8863 360.7479 553.4183 -12.1006 385.5612 397.6618 360.4983 555.0268 -12.0910 385.3848 397.4758 360.2801 556.6301 -12.0814 385.1752 397.2566 360.0825 558.2388 -12.0734 384.9533 397.0267 359.8584 559.8523 -12.0684 384.7626 396.8309 359.6641 561.4761 -12.0647 384.5444 396.6091 359.4299 563.0848 -12.0627 384.3335 396.3962 359.2494 564.6933 -12.0524 384.1566 396.2091 359.0612 566.2865 -12.0441 383.9206 395.9647 358.8746 567.8848 -12.0350 383.7197 395.7547 358.6612 569.4829 -12.0230 383.5219 395.5449 358.4654 571.0864 -12.0124 383.3510 395.3633 358.2716 572.6899 -12.0034 383.1629 395.1663 358.0418 574.3085 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