DTA measure 2lassu Date: 2026428:1159 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.70 s Mass = 960.600 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3405 -0.9896 212.1930 213.1827 196.8305 3.9504 -0.9852 212.1415 213.1267 196.8400 5.5560 -0.9820 212.0902 213.0722 196.8403 7.1660 -0.9669 212.0382 213.0051 196.8427 8.7766 -0.9697 211.9920 212.9617 196.8472 10.3816 -0.9681 211.9506 212.9187 196.8571 11.9918 -0.9622 211.9088 212.8710 196.8591 13.5921 -0.9626 211.8630 212.8256 196.8712 15.1918 -0.9660 211.8130 212.7790 196.8877 16.7818 -0.9680 211.7591 212.7271 196.9091 18.3869 -0.9688 211.7015 212.6704 196.9463 19.9968 -0.9687 211.6490 212.6177 196.9815 21.6128 -0.9687 211.6028 212.5715 197.0314 23.2175 -0.9668 211.5544 212.5211 197.0881 24.8279 -0.9652 211.5046 212.4698 197.1517 26.4178 -0.9629 211.4690 212.4319 197.2321 28.0276 -0.9603 211.4248 212.3851 197.3055 29.6331 -0.9594 211.3853 212.3447 197.3912 31.2381 -0.9582 211.3415 212.2997 197.4816 32.8485 -0.9568 211.2998 212.2567 197.5859 34.4691 -0.9549 211.2518 212.2067 197.6964 36.0794 -0.9539 211.2185 212.1724 197.8033 37.6848 -0.9527 211.1805 212.1332 197.9392 39.2949 -0.9504 211.1414 212.0917 198.0601 40.9004 -0.9486 211.1019 212.0505 198.1808 42.5103 -0.9472 211.0501 211.9973 198.3185 44.1160 -0.9454 211.0015 211.9469 198.4568 45.7003 -0.9440 210.9539 211.8979 198.5903 47.3161 -0.9423 210.9142 211.8565 198.7292 48.9210 -0.9434 210.8849 211.8283 198.8842 50.5265 -0.9440 210.8474 211.7914 199.0433 52.1264 -0.9447 210.8050 211.7497 199.1969 53.7315 -0.9460 210.7767 211.7227 199.3577 55.3369 -0.9448 210.7582 211.7030 199.5212 56.9468 -0.9420 210.7145 211.6564 199.6911 58.5679 -0.9401 210.6846 211.6247 199.8642 60.1726 -0.9385 210.6511 211.5896 200.0515 61.7829 -0.9364 210.6159 211.5522 200.2305 63.3883 -0.9350 210.5970 211.5320 200.4018 64.9981 -0.9325 210.5721 211.5045 200.5752 66.5885 -0.9323 210.5416 211.4739 200.7506 68.1984 -0.9324 210.5157 211.4481 200.9428 69.8036 -0.9308 210.4783 211.4091 201.1205 71.4396 -0.9311 210.4486 211.3796 201.3045 73.0344 -0.9306 210.4401 211.3707 201.4836 74.6399 -0.9300 210.4198 211.3497 201.6642 76.2498 -0.9295 210.4092 211.3387 201.8559 77.8551 -0.9285 210.3850 211.3134 202.0472 79.4551 -0.9270 210.3684 211.2954 202.2574 81.0605 -0.9257 210.3502 211.2759 202.4378 82.6759 -0.9245 210.3270 211.2515 202.6216 84.2810 -0.9237 210.3121 211.2357 202.8087 85.8915 -0.9229 210.2994 211.2223 202.9903 87.4963 -0.9226 210.2784 211.2010 203.1735 89.1068 -0.9218 210.2724 211.1943 203.3736 90.7068 -0.9206 210.2620 211.1826 203.5659 92.3119 -0.9188 210.2525 211.1713 203.7527 93.9378 -0.9172 210.2522 211.1694 203.9292 95.5425 -0.9159 210.2533 211.1692 204.1213 97.1533 -0.9137 210.2456 211.1594 204.2981 98.7581 -0.9124 210.2494 211.1618 204.4816 100.3533 -0.9106 210.2483 211.1589 204.6387 101.9584 -0.9089 210.2375 211.1464 204.8206 103.5635 -0.9094 210.2462 211.1557 205.0030 105.1740 -0.9094 210.2599 211.1693 205.1773 106.7943 -0.9096 210.2633 211.1728 205.3537 108.4050 -0.9097 210.2869 211.1966 205.5385 110.0098 -0.9076 210.2858 211.1934 205.7229 111.5894 -0.9047 210.2902 211.1948 205.9139 113.1998 -0.9047 210.3100 211.2147 206.1077 114.7996 -0.9031 210.3306 211.2338 206.3009 116.4000 -0.9010 210.3394 211.2403 206.4879 118.0099 -0.9007 210.3432 211.2439 206.6840 119.6310 -0.9001 210.3572 211.2573 206.8785 121.2306 -0.8978 210.3750 211.2727 207.0775 122.8258 -0.8928 210.3999 211.2927 207.2742 124.4309 -0.8907 210.4226 211.3133 207.4634 126.0409 -0.8896 210.4428 211.3323 207.6521 127.6465 -0.8883 210.4654 211.3537 207.8468 129.2564 -0.8857 210.4885 211.3742 208.0413 130.8619 -0.8812 210.5096 211.3908 208.2352 132.4823 -0.8772 210.5311 211.4083 208.4220 134.0824 -0.8757 210.5610 211.4367 208.5949 135.6876 -0.8766 210.5940 211.4705 208.7669 137.2979 -0.8762 210.6236 211.4998 208.9424 138.9033 -0.8759 210.6637 211.5396 209.1303 140.5131 -0.8728 210.7059 211.5787 209.3003 142.1188 -0.8706 210.7368 211.6074 209.4905 143.7134 -0.8687 210.7744 211.6432 209.6836 145.3338 -0.8671 210.8179 211.6851 209.8803 146.9341 -0.8623 210.8538 211.7161 210.0676 148.5390 -0.8609 210.8895 211.7504 210.2647 150.1498 -0.8585 210.9383 211.7968 210.4638 151.7545 -0.8576 210.9770 211.8346 210.6629 153.3645 -0.8533 211.0217 211.8750 210.8627 154.9700 -0.8507 211.0647 211.9154 211.0739 156.5595 -0.8485 211.1162 211.9647 211.2840 158.1855 -0.8451 211.1737 212.0188 211.4885 159.8059 -0.8418 211.2124 212.0543 211.6960 161.4159 -0.8389 211.2619 212.1008 211.8984 163.0215 -0.8370 211.3169 212.1540 212.0895 164.6314 -0.8318 211.3615 212.1934 212.2791 166.2213 -0.8303 211.4177 212.2479 212.4657 167.8573 -0.8302 211.4818 212.3120 212.6537 169.4673 -0.8284 211.5434 212.3718 212.8447 171.0729 -0.8234 211.5992 212.4226 213.0375 172.6725 -0.8218 211.6567 212.4785 213.2207 174.2730 -0.8198 211.7173 212.5371 213.4038 175.8676 -0.8194 211.7788 212.5982 213.5949 177.4781 -0.8164 211.8430 212.6594 213.7672 179.0781 -0.8139 211.8977 212.7117 213.9488 180.6880 -0.8121 211.9577 212.7698 214.1347 182.2730 -0.8084 212.0249 212.8334 214.3118 183.8985 -0.8055 212.1008 212.9063 214.4989 185.5035 -0.8017 212.1975 212.9992 214.6766 187.1090 -0.7991 212.2648 213.0638 214.8578 188.7039 -0.7940 212.3372 213.1312 215.0345 190.3093 -0.7896 212.4148 213.2044 215.2078 191.9191 -0.7877 212.4964 213.2841 215.4006 193.5249 -0.7856 212.5567 213.3422 215.5963 195.1348 -0.7831 212.6252 213.4083 215.7983 196.7558 -0.7789 212.6963 213.4752 216.0042 198.3453 -0.7756 212.7679 213.5436 216.2032 199.9561 -0.7738 212.8519 213.6257 216.4143 201.5609 -0.7706 212.9376 213.7082 216.6175 203.1716 -0.7682 213.0164 213.7846 216.8220 204.7765 -0.7658 213.1025 213.8683 217.0209 206.3871 -0.7624 213.2025 213.9649 217.2248 207.9870 -0.7607 213.2893 214.0500 217.4254 209.5868 -0.7591 213.3647 214.1238 217.6225 211.1924 -0.7550 213.4468 214.2018 217.8267 212.7971 -0.7507 213.5364 214.2871 218.0289 214.4029 -0.7480 213.6327 214.3807 218.2220 216.0076 -0.7460 213.7136 214.4597 218.4257 217.6130 -0.7419 213.8168 214.5587 218.6179 219.2181 -0.7384 213.9059 214.6442 218.8092 220.8283 -0.7356 213.9965 214.7321 219.0012 222.4491 -0.7319 214.0861 214.8179 219.1883 224.0436 -0.7280 214.1787 214.9067 219.3748 225.6486 -0.7229 214.2791 215.0019 219.5774 227.2593 -0.7195 214.3763 215.0957 219.7768 228.8640 -0.7173 214.4717 215.1891 219.9567 230.4696 -0.7157 214.5670 215.2827 220.1421 232.0848 -0.7138 214.6717 215.3855 220.3341 233.6901 -0.7088 214.7714 215.4802 220.5156 235.3158 -0.7060 214.8848 215.5908 220.7177 236.9205 -0.7025 214.9976 215.7000 220.8991 238.5310 -0.6996 215.1006 215.8002 221.0836 240.1259 -0.6961 215.2079 215.9039 221.2729 241.7260 -0.6911 215.3208 216.0119 221.4690 243.3210 -0.6877 215.4382 216.1259 221.6609 244.9211 -0.6840 215.5502 216.2341 221.8622 246.5264 -0.6811 215.6545 216.3356 222.0737 248.1569 -0.6755 215.7549 216.4305 222.2820 249.7625 -0.6725 215.8689 216.5415 222.5116 251.3724 -0.6660 215.9876 216.6536 222.7304 252.9776 -0.6632 216.1063 216.7695 222.9450 254.5880 -0.6609 216.2148 216.8757 223.1644 256.1929 -0.6589 216.3372 216.9961 223.3911 257.7985 -0.6554 216.4647 217.1201 223.6041 259.4084 -0.6522 216.5838 217.2360 223.8269 261.0294 -0.6495 216.6911 217.3407 224.0437 262.6394 -0.6462 216.8094 217.4556 224.2582 264.2446 -0.6415 216.9279 217.5694 224.4662 265.8550 -0.6405 217.0526 217.6931 224.6810 267.4603 -0.6379 217.1690 217.8069 224.8893 269.0655 -0.6335 217.2924 217.9259 225.0946 270.6703 -0.6307 217.4333 218.0640 225.2980 272.2605 -0.6274 217.5481 218.1755 225.5099 273.8756 -0.6254 217.6699 218.2953 225.7112 275.4806 -0.6231 217.7905 218.4137 225.9090 277.0810 -0.6192 217.9238 218.5430 226.1047 278.6755 -0.6155 218.0500 218.6655 226.3092 280.2810 -0.6111 218.1806 218.7917 226.5071 281.8911 -0.6078 218.3154 218.9232 226.7024 283.4966 -0.6066 218.4458 219.0525 226.9021 285.1068 -0.6054 218.5779 219.1833 227.1177 286.6964 -0.6037 218.6955 219.2992 227.3139 288.3173 -0.5984 218.8388 219.4372 227.5071 289.9271 -0.5937 218.9771 219.5708 227.7157 291.5328 -0.5899 219.1246 219.7146 227.9304 293.1428 -0.5875 219.2689 219.8563 228.1433 294.7480 -0.5846 219.4142 219.9987 228.3335 296.3584 -0.5797 219.5390 220.1187 228.5279 297.9529 -0.5786 219.6727 220.2513 228.7167 299.5534 -0.5749 219.8134 220.3882 228.9092 301.1941 -0.5722 219.9511 220.5233 229.1136 302.7789 -0.5677 220.0865 220.6543 229.3071 304.3739 -0.5650 220.2317 220.7966 229.5002 305.9841 -0.5640 220.3824 220.9464 229.6956 307.5844 -0.5601 220.5306 221.0907 229.8946 309.1789 -0.5538 220.6699 221.2237 230.0834 310.7846 -0.5512 220.8154 221.3665 230.2794 312.3894 -0.5484 220.9590 221.5074 230.4649 314.0156 -0.5470 221.1014 221.6484 230.6586 315.6153 -0.5440 221.2633 221.8073 230.8494 317.2209 -0.5410 221.4093 221.9503 231.0264 318.8206 -0.5365 221.5611 222.0976 231.2032 320.4259 -0.5334 221.7030 222.2364 231.3850 322.0363 -0.5289 221.8525 222.3814 231.5745 323.6414 -0.5254 222.0133 222.5387 231.7654 325.2519 -0.5228 222.1773 222.7000 231.9650 326.8725 -0.5204 222.3349 222.8553 232.1441 328.4829 -0.5160 222.4914 223.0074 232.3209 330.0879 -0.5134 222.6415 223.1550 232.5177 331.6934 -0.5105 222.7948 223.3053 232.7267 333.3033 -0.5075 222.9566 223.4641 232.9290 334.9088 -0.5051 223.1054 223.6105 233.1461 336.5138 -0.5026 223.2682 223.7708 233.3740 338.1138 -0.5006 223.4151 223.9157 233.5751 339.7140 -0.4994 223.5663 224.0657 233.7883 341.3188 -0.4978 223.7240 224.2219 233.9982 342.9244 -0.4936 223.8801 224.3737 234.2068 344.5293 -0.4897 224.0316 224.5213 234.4221 346.1344 -0.4872 224.1811 224.6683 234.6440 347.7398 -0.4850 224.3402 224.8252 234.8601 349.3445 -0.4829 224.5072 224.9900 235.0716 350.9706 -0.4814 224.6706 225.1520 235.2921 352.5755 -0.4789 224.8349 225.3137 235.5154 354.1858 -0.4764 224.9952 225.4716 235.7338 355.7911 -0.4735 225.1525 225.6261 235.9406 357.4010 -0.4727 225.3186 225.7913 236.1512 359.0068 -0.4702 225.4896 225.9598 236.3572 360.6115 -0.4683 225.6558 226.1240 236.5752 362.2374 -0.4663 225.8289 226.2952 236.7743 363.8425 -0.4650 225.9852 226.4503 236.9678 365.4529 -0.4623 226.1592 226.6215 237.1699 367.0581 -0.4616 226.3302 226.7918 237.3673 368.6375 -0.4618 226.4960 226.9578 237.5612 370.2481 -0.4584 226.6698 227.1282 237.7737 371.8426 -0.4576 226.8353 227.2929 237.9679 373.4483 -0.4561 226.9966 227.4526 238.1643 375.0685 -0.4551 227.1682 227.6233 238.3723 376.6580 -0.4543 227.3343 227.7886 238.5731 378.2636 -0.4536 227.5142 227.9678 238.7761 379.8736 -0.4530 227.6889 228.1420 238.9861 381.4793 -0.4518 227.8662 228.3180 239.1836 383.0891 -0.4500 228.0417 228.4917 239.3848 384.6944 -0.4483 228.2102 228.6585 239.5794 386.2894 -0.4466 228.3775 228.8241 239.7689 387.8941 -0.4457 228.5391 228.9848 239.9623 389.5153 -0.4439 228.7138 229.1576 240.1701 391.1149 -0.4418 228.8948 229.3365 240.3786 392.7203 -0.4410 229.0630 229.5040 240.5692 394.3305 -0.4405 229.2400 229.6805 240.7575 395.9354 -0.4389 229.4032 229.8421 240.9507 397.5461 -0.4387 229.5852 230.0239 241.1475 399.1509 -0.4366 229.7603 230.1969 241.3517 400.7458 -0.4372 229.9421 230.3793 241.5437 402.3511 -0.4355 230.1210 230.5564 241.7403 403.9509 -0.4345 230.3000 230.7345 241.9352 405.5668 -0.4326 230.4901 230.9227 242.1341 407.1766 -0.4328 230.6675 231.1003 242.3271 408.7773 -0.4333 230.8398 231.2731 242.5232 410.3820 -0.4329 231.0174 231.4502 242.7111 411.9876 -0.4324 231.2023 231.6347 242.9027 413.5976 -0.4299 231.4031 231.8330 243.0892 415.2029 -0.4301 231.5880 232.0181 243.2817 416.8081 -0.4292 231.7651 232.1942 243.4897 418.4134 -0.4281 231.9397 232.3678 243.7096 420.0238 -0.4280 232.1124 232.5404 243.9303 421.6290 -0.4267 232.2950 232.7217 244.1515 423.2394 -0.4257 232.4948 232.9204 244.3928 424.8441 -0.4256 232.6858 233.1114 244.6201 426.4653 -0.4237 232.8833 233.3070 244.8476 428.0751 -0.4211 233.0760 233.4971 245.0858 429.6808 -0.4219 233.2589 233.6808 245.3127 431.2908 -0.4236 233.4373 233.8609 245.5449 432.8909 -0.4243 233.6149 234.0392 245.7736 434.4910 -0.4249 233.8181 234.2430 246.0013 436.0958 -0.4244 233.9977 234.4221 246.2373 437.7166 -0.4238 234.1759 234.5997 246.4774 439.3216 -0.4263 234.3629 234.7891 246.7139 440.9168 -0.4262 234.5478 234.9740 246.9491 442.5219 -0.4253 234.7221 235.1474 247.1812 444.1320 -0.4273 234.9262 235.3535 247.4069 445.7375 -0.4287 235.1236 235.5522 247.6216 447.3474 -0.4279 235.3152 235.7431 247.8471 448.9530 -0.4275 235.5013 235.9287 248.0678 450.5733 -0.4253 235.6798 236.1051 248.2975 452.1839 -0.4251 235.8491 236.2741 248.5306 453.7889 -0.4254 236.0369 236.4622 248.7410 455.3993 -0.4251 236.2216 236.6467 248.9454 457.0045 -0.4244 236.4166 236.8410 249.1544 458.6148 -0.4221 236.6083 237.0304 249.3455 460.2201 -0.4252 236.8136 237.2388 249.5316 461.8403 -0.4276 237.0118 237.4394 249.7202 463.4511 -0.4292 237.1944 237.6236 249.9038 465.0559 -0.4277 237.3841 237.8118 250.0662 466.6560 -0.4265 237.5944 238.0209 250.2368 468.2561 -0.4275 237.7969 238.2244 250.3961 469.8610 -0.4298 237.9963 238.4261 250.5582 471.4666 -0.4304 238.1999 238.6303 250.7216 473.0868 -0.4318 238.4061 238.8379 250.8833 474.6918 -0.4325 238.5966 239.0290 251.0576 476.2973 -0.4320 238.8045 239.2365 251.2389 477.9020 -0.4325 239.0072 239.4398 251.4305 479.5075 -0.4328 239.2002 239.6330 251.6174 481.1176 -0.4329 239.3970 239.8299 251.8089 482.7226 -0.4326 239.5853 240.0179 252.0011 484.3486 -0.4332 239.7802 240.2134 252.2059 485.9589 -0.4346 239.9742 240.4088 252.3983 487.5694 -0.4348 240.1682 240.6030 252.6073 489.1741 -0.4357 240.3619 240.7975 252.8137 490.7850 -0.4372 240.5642 241.0014 253.0252 492.3898 -0.4371 240.7711 241.2082 253.2320 493.9955 -0.4378 240.9608 241.3986 253.4417 495.6209 -0.4388 241.1601 241.5989 253.6613 497.2214 -0.4415 241.3590 241.8004 253.8656 498.8056 -0.4411 241.5590 242.0001 254.0555 500.4108 -0.4418 241.7490 242.1908 254.2482 502.0059 -0.4441 241.9518 242.3958 254.4467 503.6158 -0.4464 242.1582 242.6047 254.6469 505.2265 -0.4460 242.3596 242.8056 254.8435 506.8314 -0.4468 242.5656 243.0124 255.0489 508.4568 -0.4485 242.7794 243.2280 255.2478 510.0573 -0.4491 242.9721 243.4212 255.4431 511.6620 -0.4495 243.1722 243.6217 255.6317 513.2726 -0.4495 243.3731 243.8226 255.8479 514.8776 -0.4500 243.5648 244.0148 256.0410 516.4880 -0.4497 243.7734 244.2231 256.2314 518.0933 -0.4527 243.9745 244.4272 256.4128 519.7189 -0.4547 244.1740 244.6287 256.6049 521.3243 -0.4549 244.3786 244.8335 256.8050 522.9291 -0.4553 244.5793 245.0346 257.0051 524.5399 -0.4593 244.7797 245.2390 257.2084 526.1446 -0.4630 244.9932 245.4563 257.4240 527.7606 -0.4652 245.2165 245.6817 257.6465 529.3449 -0.4685 245.4143 245.8828 257.8610 530.9454 -0.4716 245.6219 246.0935 258.0790 532.5656 -0.4735 245.8222 246.2957 258.3129 534.1708 -0.4749 246.0447 246.5196 258.5455 535.7608 -0.4755 246.2411 246.7166 258.7701 537.3659 -0.4768 246.4390 246.9158 259.0068 538.9713 -0.4758 246.6356 247.1114 259.2358 540.5811 -0.4767 246.8307 247.3075 259.4757 542.1866 -0.4763 247.0261 247.5024 259.7069 543.7968 -0.4766 247.2389 247.7155 259.9463 545.4170 -0.4779 247.4504 247.9284 260.1840 547.0073 -0.4791 247.6565 248.1356 260.4238 548.6171 -0.4810 247.8673 248.3483 260.6647 550.2228 -0.4834 248.0712 248.5547 260.8905 551.8379 -0.4845 248.2835 248.7680 261.1093 553.4428 -0.4876 248.4840 248.9716 261.3388 555.0535 -0.4898 248.6792 249.1690 261.5649 556.6583 -0.4924 248.8766 249.3691 261.7990 558.2845 -0.4952 249.0852 249.5804 262.0336 559.8893 -0.4982 249.2981 249.7963 262.2518 561.4793 -0.5006 249.5100 250.0106 262.4698 563.0844 -0.5022 249.7117 250.2139 262.6736 564.6793 -0.5029 249.9208 250.4237 262.8735 566.2846 -0.5068 250.1321 250.6389 263.0646 567.8895 -0.5095 250.3447 250.8542 263.2497 569.4951 -0.5116 250.5490 251.0606 263.4355 571.1154 -0.5141 250.7658 251.2799 263.6308 572.7108 -0.5166 250.9728 251.4895 263.8103 574.3155 -0.5184 251.1786 251.6970 263.9813 575.9258 -0.5212 251.3952 251.9163 264.1590 577.5311 -0.5224 251.6081 252.1305 264.3355 579.1410 -0.5227 251.8205 252.3432 264.5199 580.7465 -0.5253 252.0319 252.5572 264.6884 582.3515 -0.5276 252.2351 252.7628 264.8608 583.9769 -0.5320 252.4620 252.9940 265.0453 585.5825 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