DTA measure 3gyors Date: 2026428:1124 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.86 s Mass = 960.600 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3541 -4.3109 424.7572 429.0681 406.2487 3.9638 -4.3217 424.7722 429.0939 406.2872 5.5834 -4.3337 424.7699 429.1036 406.3243 7.1928 -4.3452 424.7618 429.1069 406.3677 8.8021 -4.3546 424.7555 429.1102 406.3925 10.4064 -4.3644 424.7570 429.1214 406.3910 12.0108 -4.3729 424.7643 429.1372 406.3888 13.5995 -4.3825 424.7719 429.1545 406.3674 15.2039 -4.3910 424.7752 429.1662 406.3342 16.8080 -4.3998 424.7640 429.1638 406.2721 18.4126 -4.4072 424.7643 429.1715 406.1965 20.0216 -4.4156 424.7488 429.1643 406.1156 21.6264 -4.4236 424.7327 429.1562 405.9976 23.2354 -4.4313 424.7340 429.1653 405.8728 24.8400 -4.4385 424.7279 429.1664 405.7492 26.4288 -4.4444 424.7198 429.1642 405.6260 28.0383 -4.4499 424.7117 429.1616 405.4909 29.6425 -4.4564 424.7001 429.1565 405.3344 31.2519 -4.4613 424.6888 429.1502 405.1582 32.8769 -4.4662 424.6766 429.1428 404.9957 34.4860 -4.4711 424.6668 429.1379 404.8287 36.0959 -4.4767 424.6584 429.1350 404.6496 37.7049 -4.4824 424.6382 429.1206 404.4729 39.3095 -4.4865 424.6252 429.1117 404.2856 40.9190 -4.4909 424.6097 429.1006 404.0993 42.5231 -4.4938 424.5932 429.0870 403.8998 44.1429 -4.4983 424.5615 429.0597 403.7119 45.7368 -4.5033 424.5410 429.0443 403.5133 47.3360 -4.5071 424.5199 429.0271 403.3191 48.9401 -4.5107 424.5156 429.0263 403.1131 50.5444 -4.5122 424.4836 428.9958 402.9042 52.1486 -4.5144 424.4553 428.9697 402.6989 53.7583 -4.5179 424.4142 428.9322 402.4873 55.3623 -4.5227 424.3714 428.8942 402.2838 56.9873 -4.5261 424.3297 428.8558 402.0770 58.5913 -4.5293 424.2985 428.8278 401.8701 60.1960 -4.5319 424.2705 428.8025 401.6442 61.8050 -4.5337 424.2268 428.7606 401.4383 63.4096 -4.5354 424.1771 428.7126 401.2366 65.0238 -4.5365 424.1373 428.6738 401.0250 66.6284 -4.5376 424.0996 428.6372 400.8173 68.2528 -4.5392 424.0616 428.6009 400.6104 69.8574 -4.5398 424.0228 428.5626 400.4126 71.4719 -4.5419 423.9790 428.5209 400.2170 73.0761 -4.5422 423.9420 428.4843 400.0241 74.6855 -4.5447 423.8841 428.4288 399.8283 76.2898 -4.5456 423.8297 428.3753 399.6393 77.8840 -4.5482 423.7749 428.3232 399.4467 79.5034 -4.5501 423.7103 428.2604 399.2570 81.0925 -4.5506 423.6610 428.2116 399.0776 82.6914 -4.5514 423.5910 428.1424 398.8966 84.3013 -4.5534 423.5290 428.0824 398.7244 85.9050 -4.5554 423.4672 428.0226 398.5438 87.5098 -4.5581 423.4055 427.9636 398.3575 89.1135 -4.5608 423.3304 427.8913 398.1922 90.7231 -4.5619 423.2689 427.8307 398.0178 92.3271 -4.5626 423.1926 427.7552 397.8496 93.9318 -4.5639 423.1134 427.6773 397.6788 95.5459 -4.5665 423.0397 427.6063 397.5198 97.1506 -4.5680 422.9597 427.5276 397.3523 98.7595 -4.5675 422.8780 427.4456 397.1826 100.3643 -4.5665 422.7991 427.3657 397.0076 101.9731 -4.5679 422.7069 427.2748 396.8231 103.5676 -4.5682 422.6310 427.1992 396.6572 105.1765 -4.5692 422.5554 427.1246 396.4720 106.7864 -4.5683 422.4779 427.0462 396.2910 108.4108 -4.5689 422.3813 426.9503 396.0953 109.9949 -4.5696 422.2961 426.8656 395.8973 111.5939 -4.5697 422.2063 426.7760 395.7001 113.2034 -4.5711 422.1152 426.6863 395.5160 114.8028 -4.5710 422.0399 426.6109 395.3339 116.4068 -4.5721 421.9606 426.5328 395.1480 118.0166 -4.5723 421.8714 426.4437 394.9655 119.6204 -4.5725 421.7729 426.3454 394.7713 121.2149 -4.5727 421.6665 426.2392 394.5992 122.8341 -4.5735 421.5770 426.1506 394.4190 124.4439 -4.5724 421.4923 426.0648 394.2392 126.0476 -4.5725 421.3951 425.9676 394.0461 127.6524 -4.5745 421.2879 425.8623 393.8660 129.2614 -4.5728 421.1932 425.7661 393.6886 130.8660 -4.5711 421.0881 425.6593 393.5076 132.4804 -4.5729 420.9864 425.5593 393.3198 134.1001 -4.5733 420.8776 425.4509 393.1230 135.7094 -4.5728 420.7775 425.3503 392.9213 137.3138 -4.5726 420.6648 425.2374 392.7315 138.9284 -4.5725 420.5554 425.1279 392.5367 140.5325 -4.5712 420.4629 425.0340 392.3397 142.1268 -4.5720 420.3526 424.9246 392.1366 143.7359 -4.5725 420.2339 424.8064 391.9325 145.3509 -4.5720 420.1317 424.7038 391.7244 146.9393 -4.5715 420.0277 424.5992 391.5351 148.5491 -4.5707 419.9103 424.4810 391.3246 150.1529 -4.5699 419.7942 424.3641 391.1222 151.7628 -4.5697 419.6664 424.2361 390.9239 153.3671 -4.5685 419.5520 424.1206 390.7205 154.9764 -4.5655 419.4462 424.0116 390.5182 156.5810 -4.5645 419.3317 423.8962 390.3182 158.2003 -4.5633 419.2182 423.7815 390.1261 159.8101 -4.5604 419.0914 423.6518 389.9470 161.4143 -4.5591 418.9717 423.5308 389.7547 163.0238 -4.5581 418.8501 423.4082 389.5660 164.6331 -4.5561 418.7167 423.2728 389.3654 166.2425 -4.5546 418.5949 423.1495 389.1685 167.8469 -4.5539 418.4806 423.0345 388.9714 169.4766 -4.5544 418.3519 422.9063 388.7793 171.0808 -4.5526 418.2293 422.7819 388.5896 172.6954 -4.5511 418.0980 422.6490 388.3975 174.2893 -4.5504 417.9662 422.5166 388.2210 175.8936 -4.5493 417.8272 422.3765 388.0449 177.4823 -4.5487 417.6875 422.2362 387.8654 179.0868 -4.5479 417.5700 422.1179 387.6987 180.6908 -4.5457 417.4378 421.9835 387.5125 182.3106 -4.5434 417.3050 421.8484 387.3300 183.8994 -4.5415 417.1729 421.7144 387.1398 185.5089 -4.5395 417.0418 421.5813 386.9420 187.1131 -4.5376 416.9000 421.4376 386.7469 188.7174 -4.5344 416.7650 421.2994 386.5587 190.3269 -4.5323 416.6303 421.1627 386.3560 191.9310 -4.5303 416.5009 421.0312 386.1648 193.5406 -4.5293 416.3687 420.8980 385.9650 195.1446 -4.5276 416.2286 420.7562 385.7631 196.7545 -4.5247 416.0833 420.6080 385.5609 198.3584 -4.5226 415.9379 420.4604 385.3726 199.9681 -4.5197 415.7966 420.3163 385.1691 201.5773 -4.5192 415.6594 420.1786 384.9782 203.1869 -4.5181 415.5223 420.0404 384.7776 204.7913 -4.5164 415.3803 419.8967 384.5777 206.3749 -4.5148 415.2359 419.7507 384.3719 207.9793 -4.5122 415.0847 419.5968 384.1764 209.5988 -4.5112 414.9465 419.4577 383.9926 211.1980 -4.5096 414.8013 419.3109 383.7971 212.8073 -4.5071 414.6643 419.1713 383.5965 214.4119 -4.5059 414.5182 419.0241 383.4058 216.0004 -4.5046 414.3804 418.8850 383.2265 217.6103 -4.5028 414.2283 418.7310 383.0375 219.2143 -4.4993 414.0946 418.5938 382.8438 220.8239 -4.4962 413.9412 418.4374 382.6555 222.4433 -4.4929 413.7861 418.2790 382.4661 224.0529 -4.4899 413.6322 418.1221 382.2893 225.6568 -4.4879 413.4827 417.9706 382.0985 227.2614 -4.4856 413.3237 417.8093 381.9123 228.8756 -4.4819 413.1728 417.6547 381.7232 230.4750 -4.4794 413.0186 417.4979 381.5231 232.0841 -4.4773 412.8696 417.3469 381.3294 233.6938 -4.4760 412.7049 417.1809 381.1220 235.3133 -4.4741 412.5426 417.0167 380.9207 236.9228 -4.4708 412.3849 416.8557 380.7304 238.5270 -4.4667 412.2304 416.6971 380.5323 240.1261 -4.4629 412.0937 416.5566 380.3415 241.7256 -4.4596 411.9509 416.4105 380.1446 243.3295 -4.4578 411.7988 416.2566 379.9345 244.9343 -4.4544 411.6406 416.0950 379.7328 246.5585 -4.4498 411.4842 415.9340 379.5236 248.1633 -4.4475 411.3263 415.7738 379.3300 249.7671 -4.4433 411.1696 415.6129 379.1253 251.3769 -4.4389 411.0068 415.4457 378.9191 252.9806 -4.4368 410.8384 415.2752 378.7175 254.5905 -4.4341 410.6769 415.1110 378.5248 256.1946 -4.4321 410.5140 414.9460 378.3284 257.8195 -4.4294 410.3556 414.7849 378.1319 259.4293 -4.4248 410.1951 414.6199 377.9292 261.0229 -4.4224 410.0268 414.4492 377.7308 262.6430 -4.4191 409.8585 414.2776 377.5325 264.2471 -4.4171 409.7057 414.1227 377.3464 265.8618 -4.4146 409.5480 413.9625 377.1613 267.4508 -4.4135 409.3834 413.7968 376.9923 269.0600 -4.4106 409.2251 413.6357 376.7998 270.6748 -4.4064 409.0622 413.4686 376.6114 272.2736 -4.4037 408.9113 413.3150 376.4216 273.8680 -4.3997 408.7436 413.1433 376.2346 275.4668 -4.3965 408.5692 412.9656 376.0634 277.0766 -4.3925 408.4007 412.7932 375.8766 278.6805 -4.3880 408.2271 412.6151 375.7094 280.2851 -4.3844 408.0576 412.4420 375.5321 281.8841 -4.3798 407.8995 412.2793 375.3441 283.4988 -4.3756 407.7332 412.1088 375.1501 285.0873 -4.3726 407.5786 411.9512 374.9540 286.7071 -4.3698 407.4072 411.7770 374.7582 288.3161 -4.3673 407.2339 411.6013 374.5592 289.9209 -4.3646 407.0546 411.4192 374.3515 291.5248 -4.3621 406.8918 411.2539 374.1567 293.1294 -4.3594 406.7169 411.0762 373.9481 294.7388 -4.3553 406.5364 410.8917 373.7437 296.3430 -4.3508 406.3736 410.7244 373.5390 297.9523 -4.3468 406.2103 410.5571 373.3422 299.5720 -4.3448 406.0261 410.3709 373.1410 301.1660 -4.3411 405.8638 410.2049 372.9375 302.7651 -4.3368 405.6942 410.0311 372.7491 304.3693 -4.3338 405.5255 409.8593 372.5650 305.9736 -4.3283 405.3554 409.6836 372.3641 307.5728 -4.3239 405.1848 409.5087 372.1576 309.1770 -4.3207 405.0156 409.3362 371.9493 310.7865 -4.3185 404.8411 409.1596 371.7420 312.3753 -4.3150 404.6694 408.9844 371.5452 314.0001 -4.3102 404.4908 408.8010 371.3636 315.6043 -4.3061 404.3182 408.6244 371.1721 317.2086 -4.3024 404.1443 408.4467 370.9698 318.8179 -4.2996 403.9650 408.2646 370.7749 320.4226 -4.2963 403.7969 408.0932 370.5891 322.0366 -4.2930 403.6191 407.9121 370.3898 323.6414 -4.2890 403.4468 407.7358 370.1940 325.2659 -4.2844 403.2661 407.5505 370.0024 326.8704 -4.2810 403.0996 407.3805 369.8116 328.4800 -4.2762 402.9230 407.1992 369.6194 330.0840 -4.2724 402.7444 407.0168 369.4352 331.6885 -4.2676 402.5718 406.8394 369.2575 333.2976 -4.2636 402.3944 406.6580 369.0766 334.8971 -4.2616 402.2370 406.4986 368.8935 336.4960 -4.2587 402.0650 406.3237 368.6947 338.1058 -4.2536 401.8962 406.1498 368.4969 339.7046 -4.2478 401.7203 405.9680 368.2880 341.3143 -4.2435 401.5322 405.7757 368.0795 342.9183 -4.2391 401.3541 405.5932 367.8689 344.5228 -4.2354 401.1601 405.3955 367.6598 346.1321 -4.2318 400.9767 405.2085 367.4611 347.7364 -4.2282 400.8086 405.0367 367.2475 349.3610 -4.2229 400.6249 404.8478 367.0358 350.9654 -4.2191 400.4434 404.6625 366.8234 352.5750 -4.2155 400.2633 404.4788 366.6131 354.1841 -4.2112 400.0867 404.2979 366.3996 355.7990 -4.2055 399.9040 404.1095 366.1897 357.4029 -4.2023 399.7327 403.9350 365.9865 359.0126 -4.1985 399.5588 403.7573 365.7840 360.6319 -4.1945 399.3708 403.5653 365.5693 362.2418 -4.1913 399.1782 403.3694 365.3678 363.8460 -4.1854 399.0005 403.1859 365.1626 365.4554 -4.1800 398.8181 402.9981 364.9604 367.0598 -4.1761 398.6328 402.8090 364.7457 368.6434 -4.1724 398.4566 402.6290 364.5558 370.2479 -4.1676 398.2763 402.4439 364.3678 371.8519 -4.1640 398.0996 402.2636 364.1657 373.4615 -4.1587 397.9216 402.0803 363.9679 375.0501 -4.1550 397.7306 401.8856 363.7724 376.6701 -4.1521 397.5561 401.7082 363.5653 378.2791 -4.1465 397.3665 401.5130 363.3688 379.8839 -4.1420 397.1755 401.3175 363.1756 381.4929 -4.1385 396.9938 401.1323 362.9709 383.0873 -4.1333 396.8210 400.9543 362.7871 384.6961 -4.1298 396.6385 400.7683 362.5971 386.3009 -4.1268 396.4479 400.5747 362.3834 387.9098 -4.1205 396.2706 400.3911 362.1980 389.5299 -4.1154 396.0935 400.2089 362.0064 391.1389 -4.1129 395.9066 400.0195 361.8108 392.7333 -4.1094 395.7234 399.8329 361.6187 394.3375 -4.1046 395.5327 399.6373 361.4161 395.9469 -4.0981 395.3457 399.4438 361.2306 397.5511 -4.0922 395.1534 399.2456 361.0461 399.1554 -4.0886 394.9630 399.0516 360.8501 400.7546 -4.0855 394.7920 398.8774 360.6481 402.3690 -4.0827 394.5967 398.6794 360.4600 403.9738 -4.0792 394.4015 398.4808 360.2745 405.5776 -4.0744 394.2157 398.2901 360.0803 407.1823 -4.0716 394.0363 398.1079 359.8837 408.7914 -4.0674 393.8495 397.9168 359.6852 410.3959 -4.0632 393.6677 397.7308 359.4931 412.0050 -4.0580 393.4852 397.5431 359.2890 413.6249 -4.0549 393.2985 397.3534 359.0830 415.2289 -4.0515 393.1214 397.1729 358.8947 416.8231 -4.0480 392.9291 396.9771 358.6899 418.4274 -4.0435 392.7379 396.7815 358.4703 420.0368 -4.0392 392.5538 396.5930 358.2628 421.6413 -4.0342 392.3788 396.4130 358.0607 423.2658 -4.0296 392.2055 396.2351 357.8629 424.8705 -4.0257 392.0080 396.0337 357.6608 426.4848 -4.0218 391.8134 395.8352 357.4482 428.0893 -4.0189 391.6249 395.6439 357.2449 429.6938 -4.0141 391.4250 395.4392 357.0415 431.3029 -4.0091 391.2322 395.2413 356.8346 432.9024 -4.0023 391.0498 395.0521 356.6293 434.5114 -3.9986 390.8659 394.8645 356.4279 436.1108 -3.9956 390.6764 394.6720 356.2304 437.7301 -3.9916 390.4860 394.4776 356.0426 439.3349 -3.9870 390.2930 394.2800 355.8477 440.9386 -3.9830 390.1150 394.0980 355.6573 442.5434 -3.9805 389.9313 393.9118 355.4593 444.1531 -3.9766 389.7379 393.7145 355.2699 445.7570 -3.9705 389.5431 393.5136 355.0592 447.3719 -3.9659 389.3504 393.3164 354.8500 448.9911 -3.9611 389.1602 393.1213 354.6447 450.6010 -3.9574 388.9738 392.9312 354.4633 452.2049 -3.9550 388.7821 392.7370 354.2726 453.8146 -3.9517 388.5923 392.5441 354.0788 455.4236 -3.9477 388.4046 392.3523 353.8844 457.0334 -3.9427 388.2119 392.1546 353.6905 458.6375 -3.9377 388.0193 391.9571 353.5101 460.2573 -3.9343 387.8296 391.7638 353.3269 461.8665 -3.9305 387.6304 391.5609 353.1296 463.4709 -3.9264 387.4438 391.3702 352.9375 465.0755 -3.9215 387.2632 391.1847 352.7489 466.6743 -3.9187 387.0687 390.9875 352.5575 468.2789 -3.9145 386.8676 390.7821 352.3623 469.8725 -3.9111 386.6704 390.5815 352.1720 471.4875 -3.9060 386.4954 390.4015 351.9810 473.0915 -3.9010 386.3063 390.2072 351.7927 474.7011 -3.8960 386.1131 390.0091 351.5973 476.3053 -3.8916 385.9290 389.8206 351.3838 477.9148 -3.8871 385.7296 389.6167 351.1686 479.5194 -3.8801 385.5336 389.4137 350.9615 481.1284 -3.8736 385.3462 389.2198 350.7570 482.7380 -3.8681 385.1628 389.0308 350.5603 484.3625 -3.8642 384.9726 388.8369 350.3436 485.9673 -3.8614 384.7797 388.6411 350.1200 487.5710 -3.8567 384.5810 388.4377 349.9083 489.1809 -3.8518 384.4029 388.2547 349.7017 490.7850 -3.8481 384.2065 388.0545 349.4827 492.3945 -3.8441 384.0086 387.8527 349.2707 494.0294 -3.8394 383.8213 387.6607 349.0575 495.6338 -3.8342 383.6318 387.4659 348.8445 497.2379 -3.8300 383.4338 387.2638 348.6405 498.8218 -3.8259 383.2388 387.0647 348.4439 500.4314 -3.8206 383.0382 386.8589 348.2424 502.0303 -3.8162 382.8442 386.6605 348.0361 503.6349 -3.8131 382.6704 386.4835 347.8287 505.2439 -3.8082 382.4816 386.2898 347.6228 506.8640 -3.8006 382.3047 386.1053 347.4286 508.4731 -3.7963 382.1196 385.9159 347.2314 510.0776 -3.7916 381.9150 385.7066 347.0282 511.6818 -3.7862 381.7030 385.4892 346.8205 513.2913 -3.7811 381.5031 385.2842 346.6152 514.8955 -3.7762 381.3080 385.0842 346.4039 516.5049 -3.7715 381.1194 384.8908 346.2217 518.1298 -3.7670 380.9223 384.6893 346.0281 519.7390 -3.7643 380.7286 384.4929 345.8282 521.3488 -3.7609 380.5250 384.2859 345.6347 522.9578 -3.7559 380.3268 384.0827 345.4478 524.5625 -3.7521 380.1473 383.8994 345.2485 526.1714 -3.7501 379.9565 383.7066 345.0453 527.7710 -3.7461 379.7622 383.5083 344.8540 529.3853 -3.7414 379.5751 383.3164 344.6465 530.9898 -3.7358 379.3906 383.1264 344.4490 532.5938 -3.7297 379.1842 382.9139 344.2520 534.1983 -3.7267 378.9913 382.7180 344.0647 535.7925 -3.7230 378.7978 382.5208 343.8796 537.3965 -3.7195 378.6118 382.3313 343.6894 539.0060 -3.7152 378.4256 382.1408 343.5038 540.6101 -3.7116 378.2219 381.9335 343.3175 542.2298 -3.7076 378.0160 381.7236 343.1210 543.8391 -3.7019 377.8210 381.5230 342.9223 545.4438 -3.6967 377.6322 381.3289 342.7278 547.0528 -3.6907 377.4390 381.1297 342.5281 548.6575 -3.6865 377.2493 380.9358 342.3345 550.2668 -3.6806 377.0490 380.7296 342.1375 551.8711 -3.6734 376.8549 380.5284 341.9346 553.4909 -3.6670 376.6654 380.3324 341.7162 555.1001 -3.6612 376.4519 380.1131 341.5060 556.7048 -3.6562 376.2497 379.9060 341.2928 558.3138 -3.6506 376.0576 379.7082 341.0801 559.9185 -3.6459 375.8695 379.5154 340.8653 561.5224 -3.6418 375.6703 379.3121 340.6494 563.1270 -3.6387 375.4732 379.1119 340.4270 564.7158 -3.6344 375.2844 378.9188 340.2163 566.3355 -3.6313 375.1016 378.7328 340.0036 567.9398 -3.6254 374.9157 378.5411 339.8017 569.5440 -3.6209 374.7259 378.3468 339.6090 571.1536 -3.6168 374.5309 378.1477 339.3924 572.7423 -3.6109 374.3260 377.9369 339.1939 574.3519 -3.6078 374.1254 377.7332 338.9779 575.9559 -3.6043 373.9274 377.5317 338.7561 577.5655 -3.6008 373.7387 377.3395 338.5456 579.1849 -3.5991 373.5452 377.1443 338.3193 580.7896 -3.5943 373.3466 376.9410 338.1190 582.3985 -3.5876 373.1430 376.7306 337.9024 584.0031 -3.5835 372.9452 376.5287 337.6978 585.6121 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