DTA measure 11.meres Date: 2025930:1450 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.31 s Mass = 1111.5 mg data_number = 1265 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2308 -0.2090 251.2590 251.4681 273.9085 2.0280 -0.2054 251.4047 251.6100 273.7317 2.8458 -0.1989 251.5784 251.7773 273.5778 3.6223 -0.1961 251.7458 251.9419 273.4493 4.4700 -0.1888 251.9470 252.1358 273.3040 5.2365 -0.1825 252.1142 252.2966 273.2362 6.0645 -0.1712 252.3130 252.4842 273.1575 6.8618 -0.1658 252.4862 252.6520 273.0957 7.6590 -0.1600 252.6224 252.7824 273.0652 8.4758 -0.1547 252.8008 252.9555 273.0701 9.2525 -0.1487 252.9502 253.0989 273.1159 10.1010 -0.1420 253.1352 253.2773 273.2148 10.8675 -0.1365 253.2935 253.4300 273.3538 11.6955 -0.1307 253.4652 253.5959 273.5374 12.4920 -0.1226 253.6240 253.7466 273.7330 13.2890 -0.1172 253.7887 253.9059 273.9561 14.1068 -0.1147 253.9706 254.0853 274.2230 14.8835 -0.1126 254.1251 254.2377 274.5180 15.7318 -0.1087 254.3129 254.4216 274.8956 16.4975 -0.1048 254.4437 254.5485 275.2712 17.3255 -0.0986 254.5904 254.6890 275.6831 18.1228 -0.0966 254.7637 254.8603 276.1148 18.9200 -0.0916 254.9555 255.0470 276.5609 19.7378 -0.0879 255.0861 255.1740 277.0149 20.5143 -0.0917 255.2461 255.3377 277.4008 21.3620 -0.0921 255.3979 255.4900 277.8907 22.1285 -0.0875 255.5598 255.6474 278.2921 22.9565 -0.0806 255.7298 255.8103 278.7485 23.7230 -0.0742 255.9148 255.9889 279.1263 24.5408 -0.0663 256.1181 256.1844 279.4764 25.3378 -0.0636 256.2979 256.3615 279.7720 26.1240 -0.0583 256.4717 256.5300 280.0724 26.9418 -0.0533 256.6103 256.6636 280.3787 27.7185 -0.0517 256.7607 256.8124 280.6149 28.5670 -0.0482 256.9501 256.9983 280.8534 29.3228 -0.0477 257.1203 257.1680 281.0363 30.1503 -0.0484 257.3069 257.3553 281.2041 30.9475 -0.0469 257.4831 257.5301 281.2973 31.7345 -0.0444 257.6300 257.6745 281.3743 32.5625 -0.0421 257.8069 257.8490 281.4491 33.3285 -0.0385 257.9720 258.0105 281.4702 34.1765 -0.0396 258.1279 258.1675 281.4525 34.9533 -0.0390 258.2955 258.3345 281.4282 35.7710 -0.0394 258.4549 258.4943 281.3656 36.5683 -0.0380 258.6136 258.6516 281.2888 37.3648 -0.0361 258.7888 258.8249 281.2136 38.1823 -0.0361 258.9311 258.9671 281.1110 38.9488 -0.0338 259.1029 259.1367 281.0140 39.7768 -0.0337 259.2601 259.2937 280.8708 40.5430 -0.0312 259.4085 259.4397 280.7472 41.3908 -0.0293 259.5778 259.6071 280.5886 42.1880 -0.0259 259.7088 259.7347 280.4472 42.9853 -0.0300 259.8561 259.8862 280.3014 43.8133 -0.0261 260.0359 260.0620 280.2213 44.5693 -0.0213 260.2058 260.2272 280.1527 45.4375 -0.0172 260.3814 260.3987 280.0809 46.1630 -0.0164 260.5102 260.5266 280.0013 47.0218 -0.0163 260.6948 260.7110 279.8910 47.7883 -0.0172 260.8413 260.8585 279.8390 48.6163 -0.0166 260.9728 260.9894 279.8378 49.4125 -0.0118 261.1356 261.1474 279.8864 50.1995 -0.0098 261.3407 261.3506 279.9771 51.0378 -0.0087 261.5172 261.5259 280.0926 51.7940 -0.0060 261.6490 261.6550 280.2332 52.6528 -0.0034 261.8376 261.8410 280.4371 53.4183 -0.0006 261.9865 261.9871 280.6301 54.2463 0.0032 262.1406 262.1373 280.8983 55.0435 0.0035 262.2750 262.2714 281.1954 55.8305 0.0057 262.4200 262.4143 281.5220 56.6688 0.0085 262.5562 262.5477 281.9097 57.4240 0.0139 262.7196 262.7058 282.2757 58.2930 0.0158 262.9382 262.9224 282.7365 59.0493 0.0224 263.1103 263.0879 283.1116 59.8875 0.0235 263.2563 263.2327 283.5738 60.6745 0.0227 263.4064 263.3836 283.9963 61.4710 0.0262 263.5641 263.5378 284.4120 62.2988 0.0270 263.7363 263.7093 284.8609 63.0755 0.0291 263.8744 263.8453 285.2840 63.9240 0.0333 264.0358 264.0025 285.7184 64.6905 0.0344 264.2060 264.1715 286.0959 65.5178 0.0322 264.3847 264.3526 286.4805 66.2840 0.0267 264.5474 264.5206 286.8025 67.1120 0.0224 264.7364 264.7141 287.0807 67.8990 0.0220 264.8811 264.8591 287.3086 68.7065 0.0201 265.0408 265.0207 287.5079 69.5338 0.0154 265.1981 265.1828 287.7010 70.3000 0.0177 265.3457 265.3279 287.8287 71.1485 0.0251 265.4916 265.4665 287.9553 71.9253 0.0242 265.6298 265.6056 287.9930 72.7430 0.0221 265.7953 265.7733 288.0036 73.5088 0.0220 265.9526 265.9306 288.0579 74.3365 0.0232 266.0820 266.0588 288.0760 75.1338 0.0233 266.2477 266.2243 288.0681 75.9310 0.0234 266.4221 266.3987 288.0138 76.7488 0.0252 266.5947 266.5695 287.9202 77.5255 0.0251 266.7512 266.7261 287.8369 78.3733 0.0274 266.9179 266.8905 287.7274 79.1395 0.0307 267.0819 267.0512 287.6290 79.9675 0.0308 267.2619 267.2310 287.5209 80.7648 0.0292 267.4363 267.4071 287.3976 81.5620 0.0293 267.5865 267.5572 287.2354 82.3790 0.0301 267.7762 267.7461 287.0780 83.1555 0.0292 267.9218 267.8926 286.9338 84.0040 0.0305 268.1134 268.0829 286.7864 84.7705 0.0265 268.2824 268.2558 286.6757 85.5985 0.0286 268.4435 268.4149 286.6091 86.3958 0.0281 268.6169 268.5887 286.5632 87.1925 0.0293 268.7969 268.7677 286.5268 88.0098 0.0265 268.9455 268.9190 286.5310 88.7865 0.0241 269.0443 269.0201 286.5314 89.6350 0.0290 269.1944 269.1654 286.5958 90.3913 0.0303 269.3381 269.3078 286.6573 91.2295 0.0339 269.5237 269.4898 286.8231 92.0160 0.0392 269.6744 269.6353 287.0014 92.8025 0.0419 269.8381 269.7962 287.1996 93.6305 0.0436 269.9832 269.9396 287.4348 94.3970 0.0501 270.1692 270.1191 287.6869 95.2455 0.0483 270.3639 270.3156 288.0189 96.0215 0.0470 270.5015 270.4544 288.3168 96.8390 0.0437 270.6704 270.6266 288.6437 97.6055 0.0443 270.8338 270.7895 288.9845 98.4335 0.0407 270.9934 270.9527 289.3774 99.2308 0.0401 271.1762 271.1360 289.8116 100.0168 0.0393 271.3409 271.3016 290.2428 100.8448 0.0388 271.4860 271.4472 290.7153 101.6113 0.0398 271.6073 271.5675 291.1419 102.4700 0.0391 271.7460 271.7070 291.5838 103.2263 0.0377 271.9044 271.8667 291.9471 104.0638 0.0344 272.0835 272.0491 292.3375 104.8505 0.0307 272.2178 272.1871 292.6663 105.6478 0.0272 272.3299 272.3028 292.9960 106.4758 0.0195 272.5056 272.4861 293.3296 107.2423 0.0147 272.6943 272.6796 293.5940 108.0908 0.0173 272.8654 272.8482 293.8268 108.8563 0.0184 273.0165 272.9981 294.0185 109.6843 0.0174 273.1523 273.1349 294.1880 110.4815 0.0142 273.2929 273.2787 294.2872 111.2685 0.0106 273.4465 273.4359 294.4062 112.1063 0.0074 273.6258 273.6184 294.5029 112.8620 0.0028 273.7644 273.7617 294.5532 113.7208 -0.0028 273.9381 273.9410 294.5716 114.4873 -0.0029 274.0904 274.0933 294.5943 115.3153 -0.0063 274.2752 274.2815 294.5583 116.1123 -0.0077 274.4488 274.4565 294.5005 116.8985 -0.0059 274.6082 274.6141 294.4160 117.7060 -0.0080 274.7555 274.7634 294.3048 118.4930 -0.0083 274.8869 274.8952 294.2032 119.3210 -0.0040 275.0296 275.0336 294.0893 120.0873 -0.0040 275.1754 275.1794 293.9631 120.9453 -0.0065 275.3207 275.3272 293.8446 121.7118 -0.0112 275.4974 275.5085 293.7192 122.5295 -0.0131 275.6787 275.6918 293.6068 123.3370 -0.0107 275.8156 275.8263 293.4748 124.1240 -0.0099 275.9901 276.0000 293.3851 124.9510 -0.0133 276.1169 276.1301 293.2942 125.7175 -0.0144 276.2437 276.2581 293.2216 126.5763 -0.0132 276.3993 276.4125 293.1815 127.3428 -0.0151 276.5232 276.5382 293.1527 128.1605 -0.0125 276.7171 276.7297 293.1768 128.9675 -0.0160 276.8433 276.8592 293.2098 129.7540 -0.0166 276.9985 277.0151 293.2748 130.5820 -0.0140 277.1108 277.1248 293.3586 131.3485 -0.0130 277.2500 277.2629 293.4848 132.1868 -0.0103 277.4128 277.4230 293.6759 132.9430 -0.0114 277.5761 277.5875 293.8978 133.8010 -0.0124 277.7571 277.7695 294.1679 134.5673 -0.0111 277.9279 277.9390 294.4440 135.3953 -0.0084 278.1213 278.1297 294.7916 136.1925 -0.0098 278.2442 278.2540 295.1787 136.9795 -0.0099 278.3952 278.4051 295.5473 137.8175 -0.0105 278.5818 278.5923 295.9478 138.5730 -0.0100 278.7353 278.7453 296.3185 139.4318 -0.0091 278.8715 278.8807 296.7475 140.1983 -0.0104 279.0387 279.0491 297.1540 141.0365 -0.0124 279.2093 279.2217 297.5713 141.8235 -0.0148 279.3653 279.3801 297.9567 142.6203 -0.0194 279.5034 279.5228 298.3454 143.4478 -0.0218 279.6766 279.6984 298.7519 144.2143 -0.0217 279.8128 279.8345 299.0974 145.0730 -0.0239 279.9788 280.0027 299.4400 145.8395 -0.0285 280.1210 280.1495 299.6939 146.6668 -0.0349 280.2673 280.3022 299.9877 147.4638 -0.0401 280.4176 280.4576 300.2170 148.2610 -0.0389 280.5675 280.6064 300.3905 149.0480 -0.0341 280.7051 280.7392 300.5755 149.8555 -0.0329 280.8851 280.9181 300.7255 150.6833 -0.0358 281.0416 281.0774 300.8597 151.4490 -0.0382 281.1842 281.2223 300.9297 152.2975 -0.0400 281.3404 281.3804 300.9914 153.0640 -0.0385 281.4689 281.5073 301.0298 153.8818 -0.0361 281.6590 281.6951 301.0153 154.6790 -0.0407 281.7669 281.8076 300.9971 155.4653 -0.0453 281.9043 281.9496 300.9711 156.2828 -0.0477 282.0918 282.1394 300.9092 157.0595 -0.0496 282.2746 282.3242 300.8041 157.9080 -0.0506 282.4261 282.4767 300.7016 158.6643 -0.0531 282.5632 282.6163 300.6089 159.5023 -0.0514 282.7148 282.7662 300.5127 160.2885 -0.0607 282.8718 282.9325 300.4018 161.0755 -0.0609 283.0400 283.1009 300.2725 161.9138 -0.0571 283.1915 283.2486 300.1616 162.6700 -0.0575 283.3603 283.4178 300.0801 163.5185 -0.0549 283.5434 283.5983 299.9893 164.2643 -0.0547 283.7149 283.7696 299.8968 165.1120 -0.0567 283.8609 283.9175 299.8073 165.8785 -0.0571 284.0124 284.0695 299.7660 166.7065 -0.0565 284.1436 284.2001 299.7273 167.4935 -0.0550 284.2989 284.3539 299.6986 168.2908 -0.0596 284.4210 284.4807 299.7241 169.1178 -0.0617 284.5596 284.6212 299.8375 169.8843 -0.0605 284.6770 284.7376 299.9432 170.7430 -0.0577 284.8350 284.8927 300.0959 171.4993 -0.0586 284.9695 285.0281 300.2458 172.3375 -0.0597 285.1230 285.1827 300.4517 173.1238 -0.0587 285.2875 285.3462 300.6944 173.9208 -0.0608 285.4602 285.5210 300.9734 174.7488 -0.0612 285.6444 285.7055 301.2724 175.5153 -0.0614 285.7883 285.8497 301.5737 176.3433 -0.0581 285.9299 285.9880 301.9500 177.0993 -0.0586 286.0535 286.1121 302.3474 177.9675 -0.0586 286.1998 286.2584 302.7873 178.7238 -0.0577 286.3501 286.4078 303.1697 179.5518 -0.0608 286.5053 286.5661 303.6032 180.3490 -0.0669 286.6719 286.7388 303.9688 181.1463 -0.0706 286.8203 286.8909 304.3869 181.9743 -0.0711 286.9925 287.0636 304.8020 182.7303 -0.0742 287.1766 287.2509 305.1746 183.5678 -0.0780 287.3408 287.4188 305.5697 184.3240 -0.0776 287.4889 287.5665 305.9110 185.1828 -0.0805 287.6277 287.7082 306.2314 185.9493 -0.0828 287.7784 287.8612 306.4945 186.7770 -0.0863 287.9343 288.0206 306.7546 187.5735 -0.0876 288.1052 288.1928 306.9942 188.3605 -0.0897 288.2602 288.3500 307.2013 189.1988 -0.0958 288.4297 288.5255 307.3487 189.9550 -0.0985 288.5464 288.6450 307.4410 190.8138 -0.0993 288.7142 288.8135 307.5299 191.5793 -0.1036 288.8981 289.0017 307.6085 192.4073 -0.1104 289.0746 289.1850 307.6443 193.2045 -0.1113 289.2376 289.3489 307.6307 193.9915 -0.1114 289.3637 289.4751 307.5745 194.8295 -0.1120 289.4973 289.6092 307.4973 195.5850 -0.1106 289.6260 289.7367 307.4291 196.4438 -0.1111 289.7646 289.8757 307.3279 197.2103 -0.1122 289.9481 290.0603 307.2507 198.0383 -0.1117 290.1227 290.2344 307.1461 198.8355 -0.1108 290.2672 290.3781 307.0162 199.6225 -0.1070 290.4121 290.5191 306.8643 200.4598 -0.1095 290.5572 290.6667 306.7233 201.2160 -0.1110 290.7123 290.8233 306.6177 202.0850 -0.1102 290.8613 290.9715 306.4986 202.8413 -0.1095 290.9722 291.0817 306.3857 203.6795 -0.1121 291.1113 291.2234 306.3110 204.4665 -0.1143 291.2833 291.3976 306.2576 205.2733 -0.1169 291.4516 291.5685 306.1804 206.0908 -0.1182 291.6318 291.7500 306.1401 206.8675 -0.1201 291.7834 291.9035 306.1332 207.7160 -0.1199 291.9302 292.0501 306.1698 208.4825 -0.1173 292.0673 292.1846 306.2322 209.3105 -0.1184 292.2018 292.3202 306.3411 210.0868 -0.1213 292.3527 292.4739 306.5019 210.9040 -0.1219 292.5548 292.6766 306.6959 211.7013 -0.1180 292.7230 292.8410 306.9486 212.4985 -0.1147 292.8786 292.9933 307.2262 213.3265 -0.1151 293.0087 293.1238 307.5617 214.0928 -0.1142 293.1385 293.2527 307.8884 214.9405 -0.1179 293.3066 293.4246 308.2828 215.7173 -0.1207 293.4684 293.5891 308.6656 216.5350 -0.1224 293.6464 293.7689 309.0668 217.3220 -0.1199 293.7968 293.9168 309.4741 218.1193 -0.1215 293.9346 294.0561 309.8703 218.9365 -0.1249 294.0686 294.1935 310.3144 219.7025 -0.1295 294.2214 294.3509 310.7119 220.5613 -0.1308 294.3853 294.5161 311.1239 221.2868 -0.1325 294.4867 294.6192 311.4625 222.1455 -0.1340 294.6855 294.8195 311.8453 222.9018 -0.1341 294.8240 294.9581 312.1797 223.7295 -0.1378 294.9982 295.1360 312.4971 224.5260 -0.1433 295.1587 295.3020 312.7685 225.3130 -0.1440 295.3193 295.4632 313.0117 226.1410 -0.1480 295.4707 295.6187 313.2537 226.9075 -0.1546 295.5889 295.7435 313.4724 227.7355 -0.1553 295.7452 295.9005 313.6344 228.5013 -0.1541 295.9091 296.0632 313.7664 229.3495 -0.1545 296.0678 296.2223 313.8547 230.1263 -0.1588 296.1995 296.3584 313.8884 230.9440 -0.1614 296.3744 296.5359 313.9224 231.7310 -0.1634 296.5572 296.7207 313.9795 232.5375 -0.1614 296.7047 296.8661 313.9942 233.3553 -0.1622 296.8505 297.0127 313.9563 234.1218 -0.1645 296.9844 297.1489 313.9082 234.9805 -0.1689 297.1453 297.3142 313.8813 235.7160 -0.1759 297.2636 297.4395 313.7735 236.5740 -0.1761 297.4469 297.6231 313.6423 237.3303 -0.1763 297.6311 297.8074 313.5392 238.1685 -0.1753 297.8239 297.9992 313.4341 238.9555 -0.1728 297.9738 298.1466 313.2856 239.7525 -0.1731 298.1298 298.3029 313.1490 240.5798 -0.1753 298.2652 298.4406 313.0097 241.3463 -0.1768 298.4063 298.5831 312.9042 242.2050 -0.1788 298.5691 298.7479 312.7909 242.9613 -0.1768 298.7233 298.9000 312.7099 243.7995 -0.1786 298.8714 299.0500 312.6453 244.5558 -0.1774 299.0172 299.1946 312.6280 245.3828 -0.1756 299.1637 299.3392 312.6242 246.2108 -0.1775 299.3060 299.4835 312.6455 246.9773 -0.1782 299.4643 299.6426 312.7142 247.8053 -0.1821 299.6020 299.7841 312.8079 248.5615 -0.1826 299.7281 299.9106 312.9196 249.4305 -0.1853 299.9053 300.0906 313.0886 250.1868 -0.1832 300.0429 300.2261 313.2641 251.0138 -0.1867 300.1948 300.3816 313.5105 251.8110 -0.1899 300.3424 300.5324 313.7817 252.6083 -0.1896 300.4965 300.6860 314.0851 253.4363 -0.1859 300.6573 300.8432 314.4177 254.1925 -0.1831 300.8046 300.9876 314.7693 255.0613 -0.1854 300.9839 301.1693 315.1978 255.8270 -0.1846 301.1452 301.3298 315.5805 256.6550 -0.1867 301.2922 301.4789 316.0214 257.4420 -0.1885 301.4076 301.5961 316.4567 258.2495 -0.1857 301.5788 301.7645 316.8786 259.0673 -0.1838 301.7557 301.9395 317.3085 259.8330 -0.1840 301.8945 302.0785 317.6838 260.6915 -0.1896 302.0454 302.2350 318.0802 261.4580 -0.1974 302.2044 302.4018 318.4503 262.2860 -0.2024 302.3775 302.5799 318.8452 263.0730 -0.2035 302.4934 302.6970 319.1771 263.8803 -0.2067 302.6204 302.8271 319.4768 264.7075 -0.2043 302.8137 303.0180 319.7264 265.4740 -0.2077 302.9768 303.1844 319.9181 266.3225 -0.2139 303.1351 303.3490 320.1116 267.0685 -0.2176 303.2575 303.4751 320.2354 267.9170 -0.2193 303.3824 303.6017 320.3274 268.6828 -0.2221 303.5326 303.7547 320.4225 269.5105 -0.2277 303.7121 303.9399 320.4678 270.3180 -0.2288 303.8956 304.1244 320.4892 271.1050 -0.2315 304.0225 304.2539 320.4823 271.9330 -0.2353 304.1825 304.4178 320.4647 272.6993 -0.2379 304.3053 304.5432 320.3993 273.5675 -0.2376 304.4669 304.7044 320.3295 274.3238 -0.2384 304.5913 304.8297 320.2397 275.1518 -0.2362 304.7819 305.0182 320.1223 275.9490 -0.2383 304.9345 305.1728 319.9811 276.7463 -0.2394 305.0783 305.3177 319.8487 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