DTA measure 1lassu Date: 2025930:1554 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.74 s Mass = 1111.5 mg data_number = 1070 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5306 0.0681 242.3642 242.2961 225.8307 4.1451 0.0803 242.3772 242.2968 225.4787 5.7345 0.0931 242.4141 242.3210 225.1917 7.3385 0.1078 242.4730 242.3651 224.8984 8.9379 0.1169 242.4759 242.3590 224.6224 10.5476 0.1295 242.5351 242.4056 224.3129 12.1515 0.1414 242.5352 242.3938 224.0222 13.7614 0.1526 242.5788 242.4262 223.7372 15.3508 0.1618 242.5957 242.4338 223.4625 16.9548 0.1702 242.6160 242.4458 223.2012 18.5798 0.1840 242.6162 242.4322 222.8872 20.1845 0.1950 242.6332 242.4382 222.6064 21.7936 0.2069 242.6336 242.4267 222.3610 23.4033 0.2129 242.6473 242.4344 222.0814 25.0129 0.2216 242.6146 242.3930 221.8101 26.6015 0.2251 242.6111 242.3860 221.5104 28.2165 0.2289 242.5976 242.3687 221.2729 29.8205 0.2401 242.5658 242.3258 221.0493 31.4455 0.2524 242.5539 242.3015 220.8253 33.0503 0.2580 242.5666 242.3086 220.5946 34.6543 0.2630 242.5574 242.2944 220.3454 36.2588 0.2686 242.5211 242.2526 220.0776 37.8635 0.2703 242.5147 242.2443 219.8727 39.4628 0.2680 242.4872 242.2192 219.6634 41.0669 0.2718 242.4713 242.1995 219.4679 42.6870 0.2811 242.4296 242.1486 219.3717 44.2861 0.2896 242.4330 242.1434 219.3466 45.8955 0.2941 242.4436 242.1495 219.4364 47.5003 0.3023 242.3801 242.0778 219.5600 49.0941 0.3065 242.3563 242.0498 219.7713 50.6985 0.3114 242.3627 242.0513 220.0933 52.3084 0.3163 242.3427 242.0264 220.4839 53.9121 0.3170 242.3368 242.0198 220.8938 55.5323 0.3196 242.3040 241.9844 221.4512 57.1421 0.3221 242.2688 241.9467 222.0465 58.7515 0.3214 242.1898 241.8684 222.5962 60.3609 0.3212 242.1221 241.8009 223.1739 61.9656 0.3219 242.0734 241.7515 223.7144 63.5750 0.3238 242.0434 241.7196 224.1866 65.1793 0.3256 242.0281 241.7025 224.5852 66.8045 0.3187 242.0130 241.6943 224.9788 68.4041 0.3153 241.9764 241.6611 225.2835 69.9928 0.3127 241.9460 241.6333 225.4904 71.6024 0.3022 241.9173 241.6152 225.6773 73.1969 0.3009 241.9009 241.6000 225.7606 74.8006 0.2968 241.8776 241.5807 225.8323 76.4105 0.2888 241.8699 241.5811 225.8929 77.9999 0.2836 241.8429 241.5592 225.8884 79.6041 0.2817 241.7869 241.5052 225.8881 81.2135 0.2761 241.7752 241.4991 225.8675 82.8183 0.2764 241.7669 241.4906 225.8672 84.4435 0.2732 241.7029 241.4297 225.8207 86.0483 0.2620 241.6405 241.3785 225.7803 87.6370 0.2621 241.6333 241.3712 225.7727 89.2619 0.2593 241.6228 241.3635 225.7443 90.8665 0.2598 241.6209 241.3611 225.8020 92.4704 0.2571 241.6396 241.3824 225.8805 94.0803 0.2489 241.6221 241.3732 226.0555 95.6846 0.2444 241.6162 241.3718 226.2870 97.3041 0.2444 241.6006 241.3562 226.6156 98.9038 0.2393 241.5446 241.3053 226.9389 100.5028 0.2344 241.4964 241.2620 227.2854 102.1225 0.2349 241.4820 241.2471 227.6851 103.7221 0.2328 241.4873 241.2545 228.0937 105.3264 0.2268 241.5031 241.2763 228.5292 106.9204 0.2174 241.4865 241.2691 228.9592 108.5354 0.2098 241.4298 241.2200 229.3888 110.1289 0.2052 241.3523 241.1471 229.8360 111.7336 0.1962 241.3827 241.1864 230.2091 113.3435 0.1870 241.3982 241.2111 230.5203 114.9473 0.1833 241.3920 241.2086 230.7720 116.5725 0.1727 241.3939 241.2212 230.9991 118.1773 0.1611 241.4172 241.2561 231.1684 119.7813 0.1563 241.4514 241.2951 231.2979 121.3755 0.1533 241.4469 241.2935 231.3542 122.9803 0.1511 241.4530 241.3019 231.4663 124.5893 0.1418 241.4968 241.3550 231.5333 126.1939 0.1450 241.4781 241.3330 231.5502 127.8038 0.1419 241.4453 241.3033 231.5425 129.4233 0.1405 241.4327 241.2922 231.5635 131.0276 0.1371 241.4498 241.3127 231.5746 132.6375 0.1356 241.4417 241.3061 231.6436 134.2365 0.1341 241.4752 241.3411 231.6682 135.8358 0.1277 241.4632 241.3355 231.7497 137.4405 0.1207 241.4752 241.3545 231.9086 139.0293 0.1204 241.4567 241.3362 232.1246 140.6388 0.1181 241.4795 241.3613 232.4096 142.2589 0.1147 241.5376 241.4229 232.7501 143.8630 0.1064 241.5286 241.4222 233.0941 145.4725 0.1047 241.5301 241.4253 233.4300 147.0771 0.1001 241.5043 241.4042 233.7722 148.6861 0.0920 241.5021 241.4100 234.1834 150.2909 0.0834 241.4975 241.4141 234.5918 151.8854 0.0833 241.5297 241.4465 234.9547 153.4891 0.0805 241.5757 241.4953 235.3414 155.1093 0.0702 241.5861 241.5159 235.6352 156.7191 0.0625 241.6417 241.5792 235.8635 158.3280 0.0552 241.6922 241.6370 236.1362 159.9379 0.0493 241.7100 241.6607 236.3361 161.5421 0.0474 241.7048 241.6574 236.5198 163.1515 0.0444 241.7209 241.6764 236.6605 164.7563 0.0421 241.7785 241.7363 236.7668 166.3703 0.0422 241.8156 241.7734 236.8739 167.9750 0.0369 241.8446 241.8076 236.9058 169.5798 0.0347 241.8744 241.8398 236.9801 171.1784 0.0331 241.9204 241.8873 237.0656 172.7729 0.0266 241.9625 241.9359 237.0852 174.3775 0.0234 242.0235 242.0001 237.1760 175.9865 0.0156 242.0587 242.0432 237.3241 177.5913 0.0162 242.1300 242.1138 237.4531 179.2163 0.0152 242.1766 242.1614 237.5987 180.8049 0.0127 242.2427 242.2300 237.7711 182.4199 0.0077 242.2810 242.2734 237.9947 184.0246 0.0074 242.3589 242.3515 238.2143 185.6284 0.0035 242.3880 242.3844 238.5149 187.2383 0.0003 242.4425 242.4423 238.8000 188.8428 0.0013 242.4653 242.4640 239.1427 190.4570 -0.0025 242.5152 242.5176 239.5029 192.0618 -0.0032 242.5912 242.5945 239.8745 193.6709 -0.0059 242.6859 242.6918 240.2028 195.2754 -0.0116 242.7275 242.7391 240.5416 196.8801 -0.0134 242.7632 242.7766 240.8773 198.4639 -0.0157 242.8175 242.8332 241.1948 200.0579 -0.0206 242.8877 242.9083 241.4617 201.6626 -0.0261 242.9353 242.9615 241.6797 203.2980 -0.0264 242.9868 243.0132 241.8876 204.9174 -0.0283 243.0560 243.0842 242.0847 206.5323 -0.0334 243.1103 243.1437 242.2626 208.1370 -0.0376 243.1707 243.2083 242.3518 209.7409 -0.0408 243.2405 243.2813 242.4437 211.3353 -0.0375 243.3295 243.3669 242.5122 212.9400 -0.0393 243.4065 243.4458 242.6150 214.5493 -0.0455 243.5012 243.5467 242.7235 216.1690 -0.0512 243.6162 243.6674 242.8288 217.7789 -0.0504 243.6924 243.7428 242.8983 219.3834 -0.0464 243.7490 243.7953 242.9904 220.9874 -0.0476 243.8330 243.8806 243.1219 222.5973 -0.0482 243.9169 243.9651 243.2638 224.2013 -0.0522 243.9660 244.0183 243.4488 225.8058 -0.0540 244.0226 244.0766 243.6927 227.4208 -0.0548 244.1195 244.1743 243.9407 229.0195 -0.0563 244.1850 244.2413 244.2199 230.6344 -0.0589 244.2848 244.3437 244.5321 232.2389 -0.0585 244.3790 244.4375 244.9293 233.8429 -0.0577 244.4884 244.5461 245.3042 235.4425 -0.0636 244.5302 244.5938 245.6446 237.0473 -0.0634 244.5732 244.6365 246.0051 238.6510 -0.0635 244.7056 244.7691 246.3810 240.2609 -0.0616 244.8770 244.9386 246.6917 241.8805 -0.0569 244.9929 245.0498 246.9260 243.4745 -0.0546 245.0666 245.1213 247.1248 245.0793 -0.0577 245.1523 245.2100 247.3092 246.6834 -0.0615 245.2442 245.3057 247.4828 248.2929 -0.0644 245.3488 245.4132 247.6678 249.8976 -0.0684 245.4735 245.5419 247.8425 251.5071 -0.0696 245.6254 245.6950 247.9797 253.1113 -0.0702 245.7317 245.8020 248.0560 254.7365 -0.0698 245.8355 245.9053 248.0791 256.3413 -0.0647 245.9404 246.0051 248.1571 257.9553 -0.0682 246.0453 246.1136 248.2394 259.5600 -0.0700 246.1106 246.1806 248.3922 261.1596 -0.0709 246.1885 246.2594 248.5234 262.7641 -0.0683 246.3334 246.4017 248.6858 264.3476 -0.0728 246.4607 246.5336 248.8353 265.9524 -0.0741 246.5516 246.6257 249.0254 267.5725 -0.0711 246.6610 246.7321 249.2499 269.1713 -0.0694 246.7880 246.8575 249.4587 270.7759 -0.0644 246.9111 246.9755 249.7511 272.3858 -0.0625 247.0055 247.0680 250.0453 273.9895 -0.0600 247.1267 247.1866 250.3329 275.5994 -0.0556 247.2370 247.2926 250.6658 277.1939 -0.0556 247.3414 247.3970 251.0136 278.8030 -0.0601 247.4115 247.4717 251.4079 280.4229 -0.0620 247.5613 247.6234 251.7528 282.0225 -0.0595 247.6952 247.7548 252.0673 283.6368 -0.0586 247.8275 247.8861 252.3696 285.2464 -0.0580 247.9913 248.0493 252.6040 286.8563 -0.0529 248.1277 248.1806 252.8415 288.4653 -0.0543 248.2355 248.2898 253.0438 290.0699 -0.0551 248.3491 248.4042 253.1933 291.6793 -0.0568 248.4804 248.5372 253.3465 293.2989 -0.0568 248.6234 248.6802 253.4948 294.8985 -0.0602 248.7338 248.7940 253.5766 296.4926 -0.0631 248.8504 248.9135 253.6413 298.0916 -0.0605 249.0181 249.0786 253.7344 299.6913 -0.0569 249.1394 249.1963 253.8045 301.3011 -0.0578 249.2965 249.3543 253.9208 302.9100 -0.0564 249.4435 249.4999 254.0166 304.5353 -0.0574 249.6264 249.6838 254.1327 306.1451 -0.0574 249.7713 249.8287 254.2615 307.7541 -0.0564 249.9400 249.9964 254.4259 309.3434 -0.0530 250.0868 250.1398 254.6916 310.9580 -0.0483 250.2427 250.2910 254.9655 312.5621 -0.0496 250.3648 250.4144 255.2551 314.1720 -0.0478 250.4933 250.5411 255.5692 315.7765 -0.0475 250.5857 250.6332 255.8977 317.4881 -0.0523 250.7421 250.7944 256.2367 319.2518 -0.0556 250.9175 250.9732 256.6361 320.8615 -0.0517 251.0551 251.1068 256.9704 322.4705 -0.0544 251.2045 251.2589 257.3449 324.0599 -0.0575 251.3680 251.4255 257.6966 325.6696 -0.0596 251.5300 251.5897 257.9452 327.2735 -0.0570 251.6932 251.7502 258.1781 328.8680 -0.0625 251.8243 251.8868 258.4115 330.4779 -0.0673 251.9557 252.0230 258.6415 332.0615 -0.0661 252.1505 252.2167 258.7975 333.6813 -0.0663 252.2728 252.3391 258.9089 335.2911 -0.0680 252.4280 252.4960 259.0288 336.8951 -0.0610 252.6013 252.6622 259.0829 338.5048 -0.0633 252.7517 252.8150 259.1493 340.1095 -0.0664 252.9037 252.9701 259.1927 341.7184 -0.0664 253.0812 253.1477 259.2740 343.3231 -0.0621 253.2517 253.3138 259.3769 344.9279 -0.0572 253.3976 253.4548 259.4558 346.5474 -0.0592 253.5359 253.5951 259.6142 348.1620 -0.0627 253.7082 253.7709 259.7938 349.7668 -0.0591 253.8961 253.9552 260.0432 351.3764 -0.0555 254.0811 254.1366 260.2723 352.9855 -0.0488 254.2373 254.2861 260.5523 354.5954 -0.0452 254.3873 254.4325 260.8711 356.1993 -0.0465 254.5406 254.5871 261.2163 357.7936 -0.0462 254.6972 254.7434 261.5289 359.4083 -0.0425 254.8538 254.8964 261.8593 361.0124 -0.0376 255.0228 255.0604 262.2223 362.6120 -0.0370 255.1974 255.2344 262.5626 364.2160 -0.0387 255.3247 255.3634 262.8625 365.8205 -0.0383 255.5072 255.5455 263.1705 367.4148 -0.0413 255.6664 255.7077 263.4522 369.0188 -0.0436 255.8147 255.8583 263.7127 370.6235 -0.0439 256.0025 256.0464 263.9254 372.2485 -0.0434 256.1628 256.2062 264.0946 373.8423 -0.0403 256.3489 256.3893 264.2457 375.4521 -0.0448 256.5390 256.5838 264.4006 377.0560 -0.0519 256.7400 256.7919 264.4900 378.6658 -0.0472 256.9390 256.9862 264.5574 380.2705 -0.0445 257.1431 257.1876 264.6246 381.8794 -0.0431 257.2865 257.3296 264.6614 383.4893 -0.0405 257.4518 257.4923 264.7445 385.1144 -0.0378 257.5894 257.6272 264.8240 386.7029 -0.0345 257.7449 257.7793 264.9450 388.3076 -0.0321 257.9181 257.9502 265.0955 389.9171 -0.0290 258.0888 258.1178 265.2957 391.5161 -0.0254 258.2928 258.3181 265.4760 393.1158 -0.0282 258.4940 258.5222 265.7753 394.7200 -0.0302 258.6629 258.6932 266.0871 396.3243 -0.0327 258.8683 258.9010 266.3831 397.9393 -0.0335 259.0537 259.0873 266.7636 399.5383 -0.0315 259.2475 259.2790 267.1157 401.1426 -0.0317 259.3945 259.4262 267.5012 402.7523 -0.0290 259.5536 259.5826 267.8586 404.3563 -0.0208 259.7647 259.7855 268.1906 405.9661 -0.0173 259.9731 259.9903 268.5500 407.5705 -0.0203 260.1502 260.1705 268.8645 409.1798 -0.0276 260.3247 260.3523 269.1097 410.7999 -0.0304 260.4903 260.5206 269.3150 412.4094 -0.0269 260.6616 260.6886 269.4456 414.0186 -0.0273 260.8610 260.8884 269.6064 415.6234 -0.0298 261.0549 261.0847 269.7743 417.2330 -0.0260 261.2677 261.2937 269.8918 418.8216 -0.0222 261.4304 261.4526 269.9918 420.4469 -0.0215 261.6029 261.6244 270.0441 422.0670 -0.0201 261.8001 261.8202 270.0923 423.6554 -0.0224 262.0132 262.0356 270.1253 425.2601 -0.0202 262.2146 262.2348 270.1949 426.8596 -0.0219 262.4093 262.4312 270.2716 428.4635 -0.0226 262.5824 262.6049 270.3601 430.0683 -0.0244 262.7926 262.8170 270.4952 431.6725 -0.0239 263.0128 263.0367 270.6691 433.2819 -0.0203 263.2171 263.2374 270.9012 434.9020 -0.0222 263.4400 263.4622 271.2292 436.4958 -0.0246 263.6803 263.7049 271.5595 438.1003 -0.0212 263.8950 263.9162 271.9283 439.7050 -0.0183 264.0482 264.0665 272.3529 441.3145 -0.0198 264.2109 264.2307 272.7376 442.9186 -0.0177 264.3497 264.3673 273.0908 444.5285 -0.0165 264.5396 264.5561 273.4830 446.1331 -0.0179 264.8139 264.8318 273.8620 447.7575 -0.0176 265.0292 265.0467 274.1996 449.3623 -0.0180 265.1633 265.1813 274.5211 450.9670 -0.0186 265.3597 265.3783 274.7274 452.5760 -0.0234 265.5611 265.5845 274.8973 454.1806 -0.0241 265.8043 265.8284 275.0285 455.7854 -0.0302 266.0079 266.0381 275.1286 457.3891 -0.0323 266.2280 266.2604 275.1965 459.0041 -0.0343 266.4259 266.4602 275.3085 460.6134 -0.0328 266.6526 266.6854 275.3496 462.2178 -0.0404 266.8205 266.8610 275.4239 463.8174 -0.0385 266.9658 267.0043 275.4651 465.4266 -0.0389 267.2327 267.2716 275.4988 467.0310 -0.0316 267.4393 267.4709 275.5727 468.6409 -0.0274 267.6236 267.6509 275.7258 470.2503 -0.0276 267.8501 267.8777 275.8314 471.8596 -0.0240 268.0539 268.0779 275.9744 473.4644 -0.0182 268.2346 268.2527 276.2168 475.0743 -0.0163 268.4493 268.4656 276.4892 476.6789 -0.0174 268.6497 268.6671 276.7986 478.2828 -0.0174 268.8660 268.8833 277.1406 479.9080 -0.0201 269.0430 269.0631 277.5390 481.5179 -0.0178 269.2428 269.2607 277.9646 483.1270 -0.0183 269.4395 269.4578 278.3889 484.7315 -0.0192 269.6183 269.6375 278.7334 486.3464 -0.0184 269.8436 269.8621 279.1018 487.9503 -0.0257 270.0959 270.1217 279.4765 489.5448 -0.0314 270.3131 270.3445 279.8104 491.1388 -0.0346 270.5140 270.5486 280.1211 492.7379 -0.0361 270.6989 270.7350 280.3426 494.3631 -0.0350 270.8991 270.9341 280.4787 495.9671 -0.0317 271.1346 271.1663 280.6096 497.5716 -0.0330 271.3654 271.3984 280.7133 499.1815 -0.0350 271.5614 271.5964 280.7620 500.7860 -0.0366 271.7462 271.7828 280.8039 502.3951 -0.0350 271.9253 271.9603 280.8416 503.9999 -0.0360 272.1687 272.2047 280.8847 505.6098 -0.0401 272.3630 272.4031 280.9218 507.2290 -0.0408 272.5944 272.6352 280.9914 508.8439 -0.0428 272.7947 272.8375 281.0793 510.4486 -0.0501 273.0763 273.1264 281.1555 512.0524 -0.0451 273.2950 273.3401 281.2758 513.6623 -0.0433 273.5254 273.5687 281.4538 515.2670 -0.0457 273.6965 273.7422 281.7049 516.8768 -0.0447 273.8617 273.9064 282.0100 518.4960 -0.0490 274.0679 274.1170 282.3368 520.0803 -0.0528 274.2603 274.3131 282.7171 521.6850 -0.0541 274.4820 274.5361 283.0827 523.2891 -0.0508 274.6885 274.7393 283.5111 524.8884 -0.0544 274.9373 274.9917 283.9680 526.4983 -0.0548 275.1490 275.2038 284.4227 528.1029 -0.0560 275.3683 275.4243 284.8262 529.7119 -0.0585 275.6004 275.6589 285.1849 531.3166 -0.0590 275.8306 275.8896 285.4926 532.9265 -0.0686 276.0238 276.0924 285.7171 534.5305 -0.0777 276.2432 276.3209 285.8929 536.1350 -0.0773 276.4803 276.5575 286.0565 537.7449 -0.0760 276.6997 276.7757 286.1312 539.3489 -0.0775 276.9288 277.0063 286.1537 540.9585 -0.0804 277.1217 277.2021 286.2131 542.5633 -0.0796 277.3117 277.3913 286.2170 544.1881 -0.0858 277.5540 277.6398 286.2126 545.7923 -0.0847 277.7646 277.8494 286.2379 547.3970 -0.0825 278.0067 278.0892 286.2125 549.0119 -0.0801 278.2209 278.3010 286.2781 550.6158 -0.0801 278.4124 278.4925 286.3706 552.2205 -0.0766 278.6465 278.7231 286.5218 553.8195 -0.0799 278.8112 278.8911 286.6776 555.4341 -0.0818 279.0432 279.1250 286.9431 557.0440 -0.0881 279.2732 279.3612 287.2558 558.6479 -0.0906 279.5341 279.6248 287.6531 560.2474 -0.0868 279.7652 279.8520 288.0821 561.8470 -0.0889 279.9901 280.0790 288.5311 563.4510 -0.0935 280.2801 280.3737 289.0240 565.0606 -0.0954 280.4938 280.5893 289.5053 566.6654 -0.0945 280.7155 280.8100 289.9080 568.2906 -0.0940 280.9234 281.0173 290.2760 569.8995 -0.0981 281.1362 281.2342 290.6040 571.5094 -0.0965 281.3956 281.4921 290.9118 573.1141 -0.1040 281.6505 281.7545 291.1265 574.7284 -0.1072 281.8831 281.9903 291.2767 576.3329 -0.1144 282.0607 282.1752 291.3767 577.9428 -0.1145 282.2827 282.3972 291.4625 579.5629 -0.1120 282.4549 282.5669 291.4745 581.1666 -0.1196 282.6589 282.7785 291.4674 582.7765 -0.1201 282.9081 283.0282 291.4180 584.3813 -0.1208 283.1292 283.2500 291.3735 585.9699 -0.1215 283.3323 283.4537 291.3889 587.5693 -0.1206 283.5407 283.6612 291.4342 589.1740 -0.1236 283.7317 283.8553 291.4687 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