DTA measure 21.meres Date: 2025930:1520 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.58 s Mass = 1111.5 mg data_number = 1023 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3851 -2.5775 461.3619 463.9395 434.5407 3.9894 -2.5857 461.3911 463.9768 434.8267 5.5986 -2.5877 461.4079 463.9956 435.0092 7.2030 -2.5919 461.4147 464.0066 435.1001 8.8123 -2.6019 461.4870 464.0888 435.1116 10.4371 -2.6100 461.5407 464.1507 435.0451 12.0465 -2.6181 461.5699 464.1880 434.8365 13.6508 -2.6221 461.6050 464.2271 434.5135 15.2601 -2.6267 461.6713 464.2980 434.1410 16.8695 -2.6277 461.7376 464.3653 433.6790 18.4740 -2.6285 461.7543 464.3828 433.1400 20.0626 -2.6360 461.7692 464.4051 432.5794 21.6776 -2.6363 461.8014 464.4378 431.9969 23.2814 -2.6443 461.8051 464.4494 431.4080 24.9065 -2.6413 461.8237 464.4649 430.8313 26.5155 -2.6402 461.8251 464.4653 430.2918 28.1254 -2.6395 461.8715 464.5110 429.7866 29.7291 -2.6398 461.9088 464.5486 429.3308 31.3390 -2.6386 461.9429 464.5816 428.9354 32.9479 -2.6362 461.9407 464.5769 428.6795 34.5578 -2.6343 461.9529 464.5871 428.4472 36.1619 -2.6301 461.9324 464.5625 428.2998 37.7765 -2.6322 461.9012 464.5335 428.2478 39.3806 -2.6366 461.9006 464.5372 428.2821 40.9850 -2.6431 461.8667 464.5098 428.3551 42.5945 -2.6467 461.8815 464.5282 428.4112 44.1884 -2.6430 461.8612 464.5042 428.5370 45.7828 -2.6485 461.8465 464.4950 428.6249 47.3764 -2.6471 461.8076 464.4547 428.7101 48.9658 -2.6549 461.7636 464.4185 428.7047 50.5800 -2.6581 461.7186 464.3767 428.6297 52.1794 -2.6605 461.6780 464.3385 428.4968 53.7890 -2.6667 461.6744 464.3412 428.3924 55.3879 -2.6721 461.6525 464.3246 428.2164 56.9926 -2.6797 461.5582 464.2379 427.9446 58.6016 -2.6784 461.5141 464.1925 427.5554 60.2063 -2.6771 461.4875 464.1645 427.1460 61.8003 -2.6790 461.4521 464.1311 426.8028 63.4199 -2.6750 461.4015 464.0765 426.3886 65.0243 -2.6735 461.3948 464.0683 425.9357 66.6335 -2.6717 461.3666 464.0382 425.4675 68.2379 -2.6702 461.3087 463.9789 425.0250 69.8471 -2.6762 461.3212 463.9975 424.6174 71.4569 -2.6753 461.3115 463.9868 424.2625 73.0710 -2.6741 461.2477 463.9218 423.9649 74.6911 -2.6694 461.2012 463.8706 423.7309 76.3000 -2.6693 461.1504 463.8197 423.5191 77.9099 -2.6671 461.0673 463.7344 423.3516 79.5189 -2.6631 461.0554 463.7185 423.2246 81.1235 -2.6599 460.9926 463.6525 423.1168 82.7325 -2.6547 460.9349 463.5896 423.0670 84.3269 -2.6509 460.8207 463.4716 423.0309 85.9361 -2.6509 460.7360 463.3869 423.0069 87.5559 -2.6524 460.6338 463.2862 422.9784 89.1603 -2.6561 460.5797 463.2357 422.9525 90.7695 -2.6536 460.5226 463.1762 422.8672 92.3739 -2.6578 460.4345 463.0923 422.7675 93.9831 -2.6585 460.3553 463.0139 422.6065 95.5879 -2.6631 460.3135 462.9766 422.4261 97.1968 -2.6663 460.2647 462.9310 422.2502 98.8169 -2.6710 460.1555 462.8265 421.9996 100.4210 -2.6663 460.1134 462.7797 421.7263 102.0305 -2.6691 459.9830 462.6521 421.4634 103.6403 -2.6768 459.8997 462.5765 421.1605 105.2493 -2.6713 459.7896 462.4609 420.8022 106.8591 -2.6653 459.6847 462.3501 420.4913 108.4528 -2.6613 459.6062 462.2675 420.1567 110.0574 -2.6598 459.5411 462.2010 419.8424 111.6304 -2.6601 459.4707 462.1308 419.4901 113.2400 -2.6595 459.3715 462.0311 419.1669 114.8440 -2.6597 459.2969 461.9566 418.8216 116.4436 -2.6562 459.2213 461.8775 418.5422 118.0425 -2.6523 459.1637 461.8160 418.3062 119.6521 -2.6508 459.0451 461.6959 418.1238 121.2564 -2.6537 458.9109 461.5647 417.9734 122.8555 -2.6527 458.7650 461.4177 417.8501 124.4801 -2.6458 458.6267 461.2725 417.7438 126.0845 -2.6431 458.5450 461.1881 417.5871 127.6941 -2.6375 458.4157 461.0533 417.4663 129.2981 -2.6327 458.3067 460.9394 417.3578 130.8926 -2.6312 458.2020 460.8332 417.2780 132.4964 -2.6346 458.0574 460.6920 417.1830 134.1011 -2.6434 457.9312 460.5746 417.0837 135.7156 -2.6437 457.8106 460.4543 416.9281 137.3353 -2.6412 457.6939 460.3351 416.7407 138.9450 -2.6474 457.5849 460.2322 416.5284 140.5489 -2.6526 457.4814 460.1340 416.3251 142.1588 -2.6528 457.3909 460.0437 416.0822 143.7628 -2.6554 457.2761 459.9315 415.8373 145.3724 -2.6510 457.1747 459.8257 415.5544 146.9769 -2.6475 457.0313 459.6788 415.1818 148.6014 -2.6445 456.8928 459.5373 414.8949 150.2113 -2.6439 456.7659 459.4098 414.6581 151.7999 -2.6483 456.6697 459.3179 414.4433 153.4249 -2.6443 456.5435 459.1878 414.1927 155.0295 -2.6363 456.3862 459.0225 413.9471 156.6283 -2.6344 456.2386 458.8730 413.6828 158.2330 -2.6370 456.1197 458.7567 413.4156 159.8419 -2.6388 455.9304 458.5691 413.1727 161.4620 -2.6404 455.8031 458.4435 412.9589 163.0714 -2.6431 455.6728 458.3159 412.7585 164.6756 -2.6495 455.5211 458.1706 412.5606 166.2804 -2.6544 455.3546 458.0089 412.4261 167.8893 -2.6554 455.2412 457.8966 412.2512 169.4940 -2.6491 455.1015 457.7506 412.0455 171.1034 -2.6454 454.9727 457.6181 411.8112 172.7230 -2.6408 454.8683 457.5091 411.6499 174.3274 -2.6325 454.7168 457.3493 411.4858 175.9264 -2.6299 454.5721 457.2020 411.3624 177.5209 -2.6305 454.4008 457.0313 411.1828 179.1043 -2.6284 454.1991 456.8275 411.0504 180.6986 -2.6246 454.0653 456.6898 410.8635 182.3031 -2.6203 453.9360 456.5563 410.6671 183.9071 -2.6178 453.7869 456.4048 410.4317 185.5221 -2.6197 453.6552 456.2749 410.1658 187.1311 -2.6181 453.5272 456.1453 409.9796 188.7358 -2.6128 453.3659 455.9786 409.7617 190.3296 -2.6116 453.2406 455.8522 409.4867 191.9340 -2.6073 453.0866 455.6938 409.2188 193.5383 -2.6025 452.8834 455.4859 408.9759 195.1476 -2.6028 452.6902 455.2930 408.7406 196.7523 -2.6026 452.5268 455.1294 408.5230 198.3766 -2.6007 452.4023 455.0030 408.2994 199.9814 -2.5974 452.2474 454.8448 408.0950 201.5903 -2.5936 452.0903 454.6839 407.8914 203.1796 -2.5880 451.9126 454.5006 407.6865 204.7838 -2.5806 451.7387 454.3193 407.4982 206.3933 -2.5742 451.5970 454.1713 407.2907 207.9976 -2.5768 451.4460 454.0228 407.0723 209.6069 -2.5707 451.2997 453.8704 406.8702 211.2269 -2.5687 451.1315 453.7003 406.6353 212.8359 -2.5687 450.9444 453.5131 406.4528 214.4406 -2.5638 450.7266 453.2903 406.2699 216.0449 -2.5571 450.6156 453.1727 406.0811 217.6543 -2.5535 450.4847 453.0382 405.8839 219.2586 -2.5497 450.3135 452.8631 405.6652 220.8679 -2.5465 450.2026 452.7491 405.4877 222.4880 -2.5436 450.0357 452.5793 405.2952 224.0969 -2.5442 449.8521 452.3964 405.1261 225.7068 -2.5398 449.6620 452.2018 404.9180 227.3158 -2.5424 449.4673 452.0098 404.6621 228.9255 -2.5387 449.2941 451.8328 404.4444 230.5349 -2.5367 449.1539 451.6905 404.2081 232.1391 -2.5390 449.0160 451.5550 403.9823 233.7593 -2.5377 448.8432 451.3809 403.7095 235.3683 -2.5323 448.6537 451.1860 403.4874 236.9729 -2.5253 448.4719 450.9972 403.2562 238.5819 -2.5264 448.3046 450.8309 403.0549 240.1763 -2.5275 448.1298 450.6573 402.8562 241.7595 -2.5268 447.9510 450.4778 402.6322 243.3538 -2.5225 447.7318 450.2543 402.3881 244.9578 -2.5157 447.5542 450.0700 402.1718 246.5570 -2.5105 447.3610 449.8715 401.9741 248.1611 -2.5083 447.2241 449.7324 401.7886 249.7656 -2.5110 447.0636 449.5745 401.5374 251.3645 -2.5109 446.8662 449.3770 401.2930 252.9691 -2.5121 446.6847 449.1969 401.0663 254.5781 -2.5073 446.5156 449.0229 400.8525 256.1829 -2.5019 446.3055 448.8074 400.6488 257.7766 -2.4988 446.1102 448.6090 400.4730 259.3811 -2.4935 445.9470 448.4404 400.3147 261.0004 -2.4943 445.7339 448.2282 400.1208 262.6101 -2.4900 445.5361 448.0261 399.9626 264.2139 -2.4847 445.3617 447.8464 399.7662 265.8238 -2.4810 445.2323 447.7133 399.5854 267.4328 -2.4800 445.0922 447.5722 399.4168 269.0425 -2.4774 444.8523 447.3297 399.2291 270.6309 -2.4716 444.6640 447.1355 398.9992 272.2408 -2.4694 444.4814 446.9508 398.7803 273.8599 -2.4686 444.2917 446.7603 398.5771 275.4646 -2.4709 444.1527 446.6236 398.3369 277.0736 -2.4699 443.9766 446.4465 398.0877 278.6783 -2.4609 443.8087 446.2695 397.9227 280.2928 -2.4579 443.5962 446.0541 397.7219 281.8970 -2.4518 443.3937 445.8455 397.4863 283.5064 -2.4515 443.1862 445.6377 397.2516 285.1260 -2.4477 442.9519 445.3996 397.0491 286.7404 -2.4443 442.7700 445.2142 396.7866 288.3448 -2.4406 442.6121 445.0526 396.6053 289.9539 -2.4372 442.4067 444.8439 396.4339 291.5584 -2.4317 442.2045 444.6362 396.1788 293.1729 -2.4320 442.0111 444.4430 395.9045 294.7771 -2.4304 441.8508 444.2812 395.6584 296.3970 -2.4268 441.6443 444.0711 395.4424 298.0061 -2.4140 441.4276 443.8416 395.2672 299.6109 -2.4138 441.2485 443.6623 395.0674 301.2200 -2.4122 441.0683 443.4805 394.8706 302.8245 -2.4146 440.8571 443.2717 394.6730 304.4440 -2.4099 440.7081 443.1180 394.4367 306.0279 -2.4080 440.4835 442.8915 394.2263 307.6220 -2.4072 440.2295 442.6366 393.9909 309.2210 -2.4085 440.0587 442.4671 393.7627 310.8203 -2.4021 439.9064 442.3085 393.5473 312.4244 -2.3958 439.7205 442.1162 393.2953 314.0134 -2.3927 439.4638 441.8565 393.0475 315.6175 -2.3878 439.2586 441.6464 392.8626 317.2223 -2.3897 439.0959 441.4856 392.6552 318.8260 -2.3863 438.8889 441.2753 392.4326 320.4359 -2.3842 438.6763 441.0605 392.2573 322.0245 -2.3861 438.4846 440.8707 392.0898 323.6495 -2.3897 438.3064 440.6961 391.8837 325.2590 -2.3912 438.1495 440.5407 391.7151 326.8580 -2.3943 437.9671 440.3614 391.4922 328.4679 -2.3922 437.7495 440.1417 391.2974 330.0769 -2.3900 437.5671 439.9572 391.1053 331.6815 -2.3862 437.3354 439.7216 390.9263 333.2906 -2.3842 437.1224 439.5066 390.7652 334.8951 -2.3794 436.9464 439.3258 390.5826 336.5146 -2.3682 436.7514 439.1197 390.3851 338.1241 -2.3650 436.5617 438.9267 390.1809 339.7284 -2.3624 436.3395 438.7019 389.9616 341.3378 -2.3599 436.1476 438.5074 389.7318 342.9425 -2.3534 435.9679 438.3214 389.4618 344.5515 -2.3542 435.8080 438.1622 389.1868 346.1560 -2.3576 435.5930 437.9506 388.9989 347.7855 -2.3570 435.3470 437.7041 388.7898 349.3901 -2.3574 435.1550 437.5125 388.5040 350.9940 -2.3547 434.9398 437.2945 388.2700 352.6039 -2.3487 434.7241 437.0728 388.0172 354.2133 -2.3402 434.5240 436.8641 387.7832 355.8226 -2.3363 434.3440 436.6803 387.5829 357.4273 -2.3345 434.1419 436.4764 387.3781 359.0516 -2.3281 433.9465 436.2746 387.1656 360.6564 -2.3194 433.7570 436.0764 386.9517 362.2708 -2.3171 433.5380 435.8550 386.7517 363.8751 -2.3095 433.3469 435.6564 386.5204 365.4745 -2.3023 433.1328 435.4351 386.3177 367.0785 -2.2987 432.9754 435.2740 386.1513 368.6930 -2.2973 432.7556 435.0529 385.9800 370.2870 -2.2971 432.5491 434.8462 385.7999 371.8705 -2.2902 432.3420 434.6322 385.6238 373.4853 -2.2909 432.1470 434.4379 385.4212 375.0894 -2.2896 431.9811 434.2707 385.2157 376.6835 -2.2852 431.8051 434.0903 385.0185 378.2881 -2.2871 431.5767 433.8639 384.8078 379.8971 -2.2808 431.3378 433.6186 384.5756 381.4968 -2.2785 431.1314 433.4099 384.4097 383.1008 -2.2807 430.9074 433.1881 384.1822 384.7258 -2.2746 430.7098 432.9844 383.9295 386.3298 -2.2698 430.4901 432.7599 383.6940 387.9240 -2.2601 430.2691 432.5292 383.5079 389.5281 -2.2515 430.0934 432.3450 383.2816 391.1428 -2.2528 429.9029 432.1558 383.0560 392.7473 -2.2508 429.6856 431.9364 382.8060 394.3564 -2.2463 429.4590 431.7053 382.5947 395.9610 -2.2392 429.2262 431.4654 382.4186 397.5854 -2.2359 429.0447 431.2806 382.2181 399.1850 -2.2354 428.8660 431.1013 381.9483 400.7940 -2.2298 428.6720 430.9018 381.7392 402.3986 -2.2311 428.4624 430.6935 381.5302 404.0078 -2.2255 428.2868 430.5123 381.3383 405.6174 -2.2233 428.0806 430.3039 381.1533 407.2263 -2.2197 427.8897 430.1094 380.9227 408.8361 -2.2099 427.6688 429.8787 380.6918 410.4555 -2.2040 427.4486 429.6525 380.4606 412.0651 -2.1996 427.2252 429.4249 380.2721 413.6690 -2.1946 426.9889 429.1835 380.0442 415.2788 -2.1937 426.7381 428.9318 379.8702 416.8829 -2.1908 426.5529 428.7437 379.6802 418.4924 -2.1816 426.3259 428.5075 379.5188 420.0969 -2.1823 426.1118 428.2941 379.2956 421.7163 -2.1790 425.9277 428.1067 379.1129 423.3261 -2.1746 425.7530 427.9277 378.8735 424.9301 -2.1712 425.5439 427.7151 378.6514 426.5398 -2.1665 425.3334 427.4999 378.4603 428.1596 -2.1603 425.0872 427.2475 378.2433 429.7688 -2.1495 424.8910 427.0405 378.0287 431.3888 -2.1502 424.7140 426.8642 377.7650 433.0029 -2.1443 424.4962 426.6406 377.5290 434.5869 -2.1310 424.2813 426.4123 377.3457 436.1755 -2.1246 424.0592 426.1838 377.1311 437.7751 -2.1257 423.8266 425.9523 376.9116 439.3686 -2.1229 423.6489 425.7718 376.7538 440.9734 -2.1141 423.4521 425.5662 376.5686 442.5775 -2.1082 423.2480 425.3562 376.3579 444.1973 -2.1046 423.0744 425.1790 376.0976 445.8015 -2.0974 422.9113 425.0087 375.8822 447.4058 -2.0955 422.6668 424.7623 375.6618 449.0153 -2.0918 422.4423 424.5341 375.4513 450.6194 -2.0900 422.1857 424.2757 375.2394 452.2241 -2.0846 421.9810 424.0656 374.9861 453.8331 -2.0805 421.7792 423.8598 374.7441 455.4531 -2.0768 421.5542 423.6310 374.4776 457.0626 -2.0716 421.3439 423.4156 374.2725 458.6668 -2.0634 421.0983 423.1617 374.0399 460.2765 -2.0634 420.8639 422.9273 373.8252 461.8804 -2.0625 420.6488 422.7113 373.6567 463.4850 -2.0536 420.4457 422.4994 373.4938 465.0940 -2.0480 420.2458 422.2939 373.3198 466.7141 -2.0448 420.0256 422.0704 373.1162 468.3233 -2.0403 419.8534 421.8937 372.9554 469.9431 -2.0416 419.6515 421.6931 372.7511 471.5528 -2.0396 419.4579 421.4975 372.5527 473.1568 -2.0339 419.2709 421.3048 372.3313 474.7718 -2.0271 419.0059 421.0330 372.1282 476.3909 -2.0233 418.7652 420.7884 371.9402 477.9956 -2.0203 418.5899 420.6102 371.7200 479.5895 -2.0200 418.4028 420.4228 371.4881 481.1990 -2.0191 418.1936 420.2128 371.2223 482.8081 -2.0152 417.9715 419.9866 370.9899 484.4126 -2.0082 417.7218 419.7300 370.7490 486.0221 -2.0056 417.5061 419.5117 370.5150 487.6314 -2.0040 417.3110 419.3150 370.2769 489.2563 -2.0036 417.1570 419.1605 370.0418 490.8604 -2.0003 416.9822 418.9825 369.8432 492.4754 -1.9980 416.7641 418.7621 369.6531 494.0793 -1.9997 416.5085 418.5082 369.4312 495.6890 -1.9989 416.2759 418.2747 369.1813 497.2984 -1.9927 416.0025 417.9952 368.9855 498.9026 -1.9911 415.8154 417.8065 368.8171 500.5013 -1.9830 415.6295 417.6125 368.6087 502.1006 -1.9782 415.4152 417.3934 368.4558 503.6893 -1.9846 415.2119 417.1965 368.2697 505.2940 -1.9782 415.0174 416.9956 368.0611 506.8926 -1.9807 414.7665 416.7472 367.8454 508.4923 -1.9767 414.5581 416.5348 367.6455 510.1015 -1.9710 414.2850 416.2561 367.4559 511.7059 -1.9712 414.0802 416.0514 367.2998 513.3151 -1.9706 413.9128 415.8834 367.1148 514.9349 -1.9658 413.7087 415.6745 366.8990 516.5391 -1.9632 413.4595 415.4227 366.6846 518.1485 -1.9643 413.2554 415.2197 366.4521 519.7525 -1.9592 413.0528 415.0120 366.2206 521.3621 -1.9587 412.8017 414.7604 365.9678 522.9668 -1.9550 412.5783 414.5333 365.7335 524.5758 -1.9444 412.3526 414.2970 365.5043 526.1959 -1.9339 412.1554 414.0893 365.2882 527.8000 -1.9285 411.9417 413.8702 365.0805 529.4095 -1.9258 411.7236 413.6495 364.8417 531.0140 -1.9218 411.5281 413.4499 364.5994 532.6283 -1.9232 411.3327 413.2559 364.3843 534.2329 -1.9153 411.1434 413.0588 364.1587 535.8265 -1.9108 410.9190 412.8297 363.9485 537.4620 -1.9025 410.7588 412.6614 363.7229 539.0760 -1.9014 410.5776 412.4790 363.5510 540.6654 -1.8989 410.3821 412.2810 363.3016 542.2794 -1.8899 410.1578 412.0478 363.0518 543.8841 -1.8857 409.9383 411.8240 362.8171 545.4939 -1.8840 409.6811 411.5651 362.6042 547.1029 -1.8827 409.4462 411.3289 362.3762 548.7128 -1.8722 409.2705 411.1428 362.1796 550.3320 -1.8690 409.0588 410.9279 362.0078 551.9469 -1.8713 408.8215 410.6928 361.8216 553.5510 -1.8735 408.5540 410.4275 361.6458 555.1554 -1.8692 408.2985 410.1677 361.4513 556.7703 -1.8679 408.1119 409.9798 361.2929 558.3741 -1.8629 407.9000 409.7629 361.1109 559.9840 -1.8568 407.6536 409.5104 360.8954 561.6035 -1.8527 407.4187 409.2714 360.6867 563.2181 -1.8464 407.1901 409.0364 360.4488 564.7968 -1.8422 406.9830 408.8252 360.2335 566.3959 -1.8409 406.7699 408.6108 360.0358 567.9799 -1.8347 406.5588 408.3935 359.8009 569.5788 -1.8334 406.3505 408.1839 359.6019 571.1835 -1.8305 406.1539 407.9843 359.4452 572.7821 -1.8239 406.0016 407.8256 359.2767 574.3869 -1.8229 405.8179 407.6408 359.0444 576.0064 -1.8245 405.6191 407.4436 358.8280 577.6005 -1.8208 405.4157 407.2365 358.5892 579.2049 -1.8128 405.1952 407.0080 358.3146 580.8090 -1.8073 404.9894 406.7967 358.0999 582.4189 -1.7996 404.7500 406.5497 357.8801 584.0229 -1.7945 404.5424 406.3369 357.6307 585.6376 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