DTA measure 1gyors Date: 20241022:1513 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 922.77 s Mass = 959.700 mg data_number = 1148 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0965 -1.1418 265.0021 266.1440 264.6197 1.8885 -1.1399 264.9908 266.1307 264.6277 2.7105 -1.1419 264.9947 266.1366 264.6195 3.5025 -1.1420 265.0005 266.1425 264.6171 4.3255 -1.1370 264.9974 266.1344 264.6122 5.1173 -1.1384 264.9957 266.1341 264.6111 5.9103 -1.1392 265.0116 266.1508 264.6032 6.7325 -1.1405 264.9975 266.1380 264.6348 7.5238 -1.1438 264.9972 266.1410 264.6358 8.3458 -1.1388 264.9784 266.1172 264.6302 9.1380 -1.1356 265.0034 266.1390 264.6409 9.9295 -1.1386 264.9953 266.1339 264.6496 10.7520 -1.1379 264.9825 266.1204 264.6615 11.5438 -1.1366 264.9943 266.1310 264.7006 12.3665 -1.1389 265.0099 266.1487 264.7213 13.1590 -1.1397 265.0040 266.1437 264.7323 13.9505 -1.1407 264.9902 266.1309 264.7702 14.7708 -1.1406 264.9912 266.1318 264.8086 15.5603 -1.1389 265.0212 266.1601 264.8326 16.3780 -1.1377 264.9962 266.1339 264.8638 17.1665 -1.1439 264.9924 266.1363 264.9102 17.9550 -1.1455 264.9850 266.1305 264.9497 18.7743 -1.1419 265.0022 266.1441 265.0118 19.5633 -1.1397 265.0063 266.1459 265.0716 20.3830 -1.1387 265.0170 266.1557 265.1340 21.1718 -1.1396 264.9977 266.1373 265.2162 21.9610 -1.1396 265.0016 266.1412 265.2726 22.8108 -1.1389 265.0086 266.1476 265.3426 23.5708 -1.1403 265.0077 266.1480 265.4156 24.3915 -1.1408 265.0156 266.1563 265.5037 25.1833 -1.1448 265.0113 266.1561 265.5998 25.9750 -1.1441 265.0017 266.1458 265.6863 26.7973 -1.1450 265.0063 266.1512 265.7746 27.5890 -1.1521 265.0153 266.1674 265.8714 28.4123 -1.1471 265.0189 266.1660 265.9978 29.2080 -1.1412 265.0167 266.1580 266.1142 29.9995 -1.1428 265.0204 266.1632 266.2439 30.8220 -1.1432 265.0278 266.1710 266.3338 31.5838 -1.1466 265.0227 266.1693 266.4619 32.4360 -1.1520 265.0287 266.1807 266.6044 33.2283 -1.1540 265.0397 266.1937 266.7088 34.0198 -1.1544 265.0261 266.1805 266.8481 34.8423 -1.1573 265.0312 266.1885 266.9805 35.6035 -1.1652 265.0301 266.1952 267.1272 36.4560 -1.1676 265.0312 266.1988 267.2537 37.2480 -1.1705 265.0472 266.2177 267.3805 38.0395 -1.1713 265.0531 266.2244 267.5257 38.8620 -1.1763 265.0535 266.2298 267.6716 39.6538 -1.1868 265.0506 266.2374 267.8041 40.4765 -1.1915 265.0813 266.2728 267.9809 41.2690 -1.1860 265.0851 266.2711 268.1153 42.0605 -1.1917 265.0844 266.2761 268.2644 42.8830 -1.1998 265.0902 266.2900 268.4093 43.6745 -1.2070 265.1049 266.3120 268.5557 44.4968 -1.2098 265.0959 266.3057 268.7206 45.2888 -1.2115 265.0967 266.3082 268.8706 46.0815 -1.2079 265.1128 266.3208 269.0154 46.9035 -1.2142 265.1207 266.3349 269.1725 47.6648 -1.2172 265.1454 266.3626 269.3174 48.5130 -1.2099 265.1549 266.3648 269.4631 49.3010 -1.2164 265.1542 266.3706 269.6296 50.0890 -1.2205 265.1545 266.3750 269.7851 50.9083 -1.2183 265.1745 266.3929 269.9242 51.6670 -1.2148 265.1812 266.3960 270.0821 52.5168 -1.2230 265.1720 266.3949 270.2564 53.3053 -1.2241 265.1861 266.4102 270.3941 54.0948 -1.2286 265.2150 266.4436 270.5513 54.9143 -1.2370 265.2228 266.4598 270.6903 55.6748 -1.2373 265.2244 266.4616 270.8437 56.5260 -1.2364 265.2404 266.4768 271.0158 57.2878 -1.2380 265.2556 266.4936 271.1692 58.1098 -1.2418 265.2461 266.4878 271.3225 58.9320 -1.2434 265.2726 266.5160 271.4723 59.6935 -1.2493 265.2905 266.5398 271.6014 60.5460 -1.2511 265.3059 266.5570 271.7668 61.3078 -1.2561 265.3221 266.5782 271.9122 62.1300 -1.2609 265.3312 266.5921 272.0608 62.9520 -1.2649 265.3500 266.6149 272.1963 63.7135 -1.2613 265.3792 266.6405 272.3458 64.5660 -1.2732 265.3727 266.6459 272.5059 65.3278 -1.2785 265.3977 266.6763 272.6290 66.1498 -1.2802 265.4069 266.6871 272.7749 66.9425 -1.2840 265.4187 266.7027 272.9276 67.7365 -1.2893 265.4371 266.7265 273.0722 68.5893 -1.2876 265.4722 266.7597 273.2082 69.3515 -1.2934 265.4891 266.7826 273.3389 70.1738 -1.2992 265.5058 266.8050 273.4526 70.9658 -1.3050 265.5152 266.8202 273.5851 71.7575 -1.3086 265.5576 266.8662 273.7285 72.6095 -1.3090 265.5758 266.8848 273.8540 73.3715 -1.3148 265.5904 266.9052 273.9744 74.1935 -1.3184 265.5985 266.9169 274.1039 74.9855 -1.3231 265.6175 266.9406 274.2409 75.7775 -1.3267 265.6436 266.9703 274.3627 76.6295 -1.3303 265.6653 266.9956 274.5007 77.3915 -1.3342 265.6955 267.0298 274.6119 78.2135 -1.3349 265.7103 267.0452 274.7167 79.0358 -1.3397 265.7399 267.0796 274.8534 79.7968 -1.3445 265.7506 267.0951 274.9799 80.6450 -1.3442 265.7770 267.1213 275.0974 81.4030 -1.3491 265.7851 267.1342 275.2115 82.2210 -1.3520 265.8139 267.1659 275.3277 83.0390 -1.3557 265.8408 267.1965 275.4471 83.7970 -1.3556 265.8758 267.2314 275.5505 84.6460 -1.3624 265.9254 267.2877 275.6696 85.4340 -1.3648 265.9466 267.3114 275.7821 86.2235 -1.3674 265.9586 267.3261 275.9038 87.0430 -1.3707 265.9847 267.3554 276.0188 87.8020 -1.3702 265.9911 267.3613 276.1048 88.6525 -1.3768 266.0243 267.4012 276.2247 89.4438 -1.3796 266.0544 267.4340 276.3239 90.2355 -1.3828 266.0854 267.4682 276.4441 91.0580 -1.3857 266.1210 267.5067 276.5463 91.8195 -1.3867 266.1250 267.5117 276.6413 92.6718 -1.3914 266.1602 267.5516 276.7484 93.4635 -1.3961 266.1852 267.5812 276.8563 94.2555 -1.3973 266.2090 267.6063 276.9625 95.0775 -1.4022 266.2255 267.6277 277.0709 95.8395 -1.4063 266.2732 267.6795 277.1913 96.6915 -1.4081 266.3112 267.7193 277.3187 97.4835 -1.4124 266.3489 267.7613 277.4186 98.2755 -1.4118 266.4029 267.8147 277.5230 99.0975 -1.4165 266.4208 267.8372 277.6478 99.8595 -1.4203 266.4313 267.8516 277.7337 100.7115 -1.4220 266.4609 267.8829 277.8626 101.5035 -1.4241 266.5006 267.9248 277.9702 102.2955 -1.4287 266.5545 267.9832 278.0893 103.1175 -1.4333 266.5584 267.9916 278.1994 103.8795 -1.4356 266.5699 268.0055 278.3025 104.7315 -1.4378 266.6179 268.0557 278.4297 105.5235 -1.4409 266.6597 268.1005 278.5666 106.3155 -1.4434 266.6847 268.1280 278.6733 107.1375 -1.4471 266.7209 268.1680 278.7838 107.9008 -1.4479 266.7473 268.1952 278.9074 108.7575 -1.4531 266.7850 268.2382 279.0384 109.5490 -1.4602 266.8500 268.3102 279.1520 110.3415 -1.4629 266.8591 268.3219 279.2679 111.1643 -1.4673 266.8830 268.3503 279.4044 111.9243 -1.4684 266.9458 268.4142 279.5318 112.7725 -1.4696 266.9958 268.4653 279.6603 113.5303 -1.4713 267.0315 268.5028 279.7753 114.3490 -1.4741 267.0538 268.5279 279.9090 115.1678 -1.4744 267.0978 268.5722 280.0253 115.9258 -1.4789 267.1284 268.6073 280.1506 116.7740 -1.4851 267.1738 268.6589 280.2709 117.5320 -1.4890 267.2019 268.6908 280.4040 118.3513 -1.4918 267.2406 268.7324 280.5290 119.1713 -1.4931 267.2626 268.7556 280.6654 119.9310 -1.4982 267.3214 268.8196 280.7688 120.7815 -1.5008 267.3687 268.8695 280.9087 121.5435 -1.5074 267.3970 268.9044 281.0232 122.3655 -1.5114 267.4423 268.9537 281.1579 123.1875 -1.5159 267.4880 269.0038 281.2813 123.9500 -1.5149 267.5401 269.0550 281.4031 124.8025 -1.5185 267.5707 269.0892 281.5275 125.5645 -1.5233 267.6083 269.1316 281.6507 126.3865 -1.5256 267.6643 269.1899 281.7882 127.1785 -1.5283 267.6947 269.2230 281.9002 127.9705 -1.5318 267.7363 269.2681 282.0285 128.8223 -1.5342 267.7747 269.3089 282.1666 129.5845 -1.5350 267.8220 269.3570 282.2924 130.4065 -1.5399 267.8742 269.4141 282.4162 131.1985 -1.5416 267.9335 269.4751 282.5483 131.9903 -1.5448 267.9628 269.5076 282.6765 132.8125 -1.5486 268.0088 269.5574 282.8035 133.6043 -1.5532 268.0415 269.5946 282.9343 134.4268 -1.5585 268.0920 269.6505 283.0861 135.2190 -1.5587 268.1453 269.7039 283.2190 136.0105 -1.5621 268.1928 269.7549 283.3501 136.8330 -1.5652 268.2391 269.8044 283.4897 137.6248 -1.5680 268.2788 269.8468 283.6078 138.4475 -1.5721 268.3342 269.9063 283.7652 139.2400 -1.5764 268.3845 269.9608 283.9093 140.0315 -1.5809 268.4231 270.0040 284.0224 140.8845 -1.5812 268.4857 270.0670 284.1509 141.6468 -1.5869 268.5289 270.1158 284.2919 142.4688 -1.5912 268.5701 270.1613 284.4477 143.2608 -1.5934 268.6260 270.2194 284.6003 144.0500 -1.5925 268.6881 270.2806 284.7316 144.8980 -1.5959 268.7280 270.3238 284.8655 145.6563 -1.6029 268.7793 270.3823 284.9818 146.4740 -1.6071 268.8293 270.4364 285.1208 147.2628 -1.6104 268.8684 270.4789 285.2595 148.0520 -1.6136 268.9385 270.5520 285.3864 148.9023 -1.6163 269.0024 270.6187 285.5481 149.6635 -1.6201 269.0530 270.6731 285.6846 150.4830 -1.6250 269.1126 270.7376 285.8229 151.3018 -1.6264 269.1774 270.8038 285.9784 152.0623 -1.6306 269.2053 270.8359 286.1058 152.9123 -1.6350 269.2469 270.8819 286.2462 153.6740 -1.6397 269.3088 270.9485 286.3852 154.4958 -1.6403 269.3514 270.9917 286.5145 155.2880 -1.6443 269.4157 271.0600 286.6524 156.0795 -1.6460 269.4814 271.1274 286.7860 156.9320 -1.6515 269.5361 271.1876 286.9354 157.6938 -1.6529 269.5793 271.2322 287.0673 158.5158 -1.6564 269.6513 271.3077 287.1911 159.3138 -1.6607 269.7096 271.3702 287.3098 160.1130 -1.6622 269.7535 271.4157 287.4564 160.9350 -1.6673 269.8090 271.4763 287.6061 161.6965 -1.6692 269.8602 271.5294 287.7202 162.5490 -1.6757 269.9178 271.5935 287.8547 163.3410 -1.6768 269.9854 271.6622 287.9845 164.1328 -1.6779 270.0527 271.7307 288.1210 164.9550 -1.6830 270.1065 271.7896 288.2454 165.7468 -1.6888 270.1726 271.8614 288.3998 166.5688 -1.6904 270.2231 271.9135 288.5170 167.3610 -1.6932 270.3098 272.0030 288.6437 168.1525 -1.6967 270.3490 272.0457 288.7840 168.9750 -1.6969 270.4112 272.1081 288.9121 169.7665 -1.7006 270.4906 272.1912 289.0457 170.5895 -1.7052 270.5430 272.2482 289.1755 171.3818 -1.7067 270.5991 272.3058 289.2971 172.1735 -1.7083 270.6530 272.3613 289.4311 172.9958 -1.7132 270.7238 272.4370 289.5691 173.7875 -1.7170 270.7713 272.4884 289.6817 174.6105 -1.7202 270.8397 272.5598 289.8064 175.4025 -1.7250 270.9102 272.6352 289.9299 176.1945 -1.7279 270.9696 272.6975 290.0546 177.0143 -1.7299 271.0442 272.7741 290.1871 177.8020 -1.7333 271.1185 272.8518 290.3209 178.6200 -1.7353 271.1795 272.9148 290.4464 179.4080 -1.7392 271.2375 272.9766 290.5762 180.1970 -1.7410 271.2876 273.0286 290.6980 181.0163 -1.7491 271.3664 273.1154 290.8128 181.7750 -1.7520 271.4250 273.1771 290.9077 182.6235 -1.7533 271.4938 273.2471 291.0452 183.4123 -1.7553 271.5564 273.3116 291.1801 184.2010 -1.7575 271.6169 273.3744 291.2890 185.0203 -1.7602 271.6901 273.4503 291.4048 185.8105 -1.7654 271.7527 273.5181 291.5342 186.6328 -1.7684 271.8319 273.6003 291.6630 187.4248 -1.7744 271.9036 273.6780 291.7748 188.2165 -1.7781 271.9666 273.7446 291.8761 189.0390 -1.7829 272.0290 273.8119 292.0029 189.8005 -1.7838 272.1035 273.8873 292.1248 190.6530 -1.7832 272.1714 273.9546 292.2454 191.4448 -1.7903 272.2502 274.0405 292.3768 192.2365 -1.7944 272.3402 274.1346 292.4799 193.0588 -1.7972 272.3918 274.1890 292.5940 193.8205 -1.8017 272.4486 274.2503 292.7020 194.6728 -1.8043 272.5308 274.3351 292.8294 195.4348 -1.8040 272.5786 274.3826 292.9414 196.2568 -1.8043 272.6512 274.4555 293.0546 197.0788 -1.8047 272.7291 274.5337 293.1748 197.8405 -1.8079 272.8061 274.6140 293.2952 198.6928 -1.8167 272.8721 274.6888 293.4202 199.4845 -1.8186 272.9449 274.7634 293.5320 200.2765 -1.8201 273.0239 274.8440 293.6414 201.0985 -1.8263 273.0834 274.9097 293.7709 201.8605 -1.8303 273.1651 274.9954 293.8773 202.7125 -1.8314 273.2594 275.0908 293.9984 203.5045 -1.8323 273.3290 275.1612 294.1058 204.2975 -1.8374 273.3941 275.2316 294.2434 205.1198 -1.8410 273.4654 275.3064 294.3558 205.8825 -1.8470 273.5368 275.3838 294.4663 206.7345 -1.8460 273.6372 275.4832 294.6099 207.5265 -1.8496 273.7006 275.5503 294.7406 208.3193 -1.8542 273.7707 275.6249 294.8660 209.1388 -1.8542 273.8652 275.7194 294.9992 209.8970 -1.8603 273.9342 275.7945 295.1299 210.7453 -1.8631 273.9999 275.8631 295.2515 211.5330 -1.8639 274.0801 275.9441 295.3684 212.3210 -1.8621 274.1523 276.0145 295.4764 213.1393 -1.8676 274.2498 276.1174 295.6104 213.9280 -1.8706 274.3076 276.1782 295.7397 214.7460 -1.8769 274.3807 276.2576 295.8770 215.5355 -1.8786 274.4514 276.3300 296.0028 216.3263 -1.8804 274.5446 276.4250 296.1083 217.1765 -1.8836 274.6273 276.5109 296.2579 217.9385 -1.8876 274.6890 276.5766 296.3850 218.7615 -1.8872 274.7696 276.6568 296.5134 219.5548 -1.8929 274.8522 276.7452 296.6261 220.3465 -1.8989 274.9247 276.8237 296.7451 221.1700 -1.9031 275.0054 276.9085 296.8751 221.9625 -1.9043 275.0752 276.9795 296.9939 222.7845 -1.9065 275.1682 277.0746 297.1350 223.5765 -1.9078 275.2401 277.1479 297.2546 224.3685 -1.9084 275.3286 277.2369 297.3708 225.1905 -1.9136 275.4214 277.3350 297.4975 225.9825 -1.9169 275.4902 277.4071 297.6318 226.8045 -1.9185 275.5601 277.4786 297.7719 227.5965 -1.9222 275.6436 277.5658 297.9048 228.3885 -1.9255 275.7287 277.6542 298.0235 229.2405 -1.9263 275.8165 277.7428 298.1638 230.0025 -1.9314 275.9068 277.8382 298.2984 230.8245 -1.9360 276.0100 277.9460 298.4236 231.6165 -1.9385 276.0647 278.0032 298.5610 232.4085 -1.9388 276.1379 278.0767 298.6863 233.2605 -1.9400 276.2261 278.1661 298.8275 234.0225 -1.9440 276.3008 278.2448 298.9527 234.8450 -1.9475 276.3890 278.3365 299.1059 235.6375 -1.9501 276.4747 278.4248 299.2478 236.4300 -1.9516 276.5737 278.5252 299.3728 237.2825 -1.9564 276.6476 278.6040 299.5155 238.0448 -1.9600 276.7321 278.6921 299.6567 238.8675 -1.9624 276.8167 278.7791 299.7973 239.6600 -1.9682 276.8947 278.8629 299.9169 240.4523 -1.9702 276.9875 278.9577 300.0691 241.3015 -1.9717 277.0725 279.0442 300.2343 242.0593 -1.9745 277.1466 279.1211 300.3576 242.8773 -1.9811 277.2361 279.2173 300.4982 243.6655 -1.9819 277.3284 279.3103 300.6175 244.4530 -1.9871 277.4209 279.4080 300.7639 245.2715 -1.9909 277.5030 279.4939 300.9046 246.0600 -1.9918 277.5748 279.5666 301.0594 246.8795 -1.9952 277.6819 279.6771 301.2013 247.6698 -1.9982 277.7624 279.7607 301.3526 248.4600 -2.0004 277.8513 279.8517 301.4845 249.3095 -2.0009 277.9509 279.9518 301.6436 250.0715 -2.0082 278.0091 280.0173 301.7605 250.8935 -2.0112 278.1123 280.1235 301.9132 251.6855 -2.0145 278.2038 280.2183 302.0320 252.4775 -2.0167 278.2837 280.3005 302.1932 253.2995 -2.0204 278.3603 280.3807 302.3326 254.0615 -2.0247 278.4405 280.4652 302.4621 254.9135 -2.0295 278.5383 280.5678 302.5983 255.6755 -2.0337 278.6129 280.6466 302.7433 256.4975 -2.0365 278.7102 280.7467 302.8869 257.3195 -2.0421 278.8149 280.8569 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