DTA measure 2lassu Date: 20241022:1639 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1905.51 s Mass = 959.700 mg data_number = 1185 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4455 -4.6580 398.6060 403.2640 418.5841 4.0595 -4.6551 398.8203 403.4754 418.6448 5.6735 -4.6546 399.0651 403.7197 418.7010 7.2725 -4.6508 399.2851 403.9358 418.7197 8.8863 -4.6510 399.5269 404.1779 418.7536 10.5003 -4.6494 399.7425 404.3919 418.8185 12.1148 -4.6492 399.9817 404.6308 418.8282 13.7138 -4.6447 400.2058 404.8504 418.8364 15.3278 -4.6445 400.4290 405.0735 418.8316 16.9268 -4.6429 400.6374 405.2803 418.8196 18.5430 -4.6281 400.8649 405.4930 418.8141 20.1588 -4.6266 401.1027 405.7293 418.7825 21.7578 -4.6237 401.2997 405.9234 418.7202 23.3716 -4.6257 401.5084 406.1341 418.6520 24.9674 -4.6232 401.7242 406.3474 418.5631 26.5724 -4.6124 401.9364 406.5488 418.4717 28.1774 -4.6061 402.1411 406.7472 418.3686 29.7691 -4.6042 402.3309 406.9351 418.2593 31.3616 -4.5970 402.5511 407.1480 418.1321 32.9700 -4.5878 402.7532 407.3410 417.9871 34.5645 -4.5886 402.9556 407.5442 417.8661 36.1900 -4.5751 403.1440 407.7191 417.7332 37.7825 -4.5704 403.3381 407.9086 417.5893 39.3799 -4.5580 403.5282 408.0862 417.4664 40.9754 -4.5482 403.7113 408.2594 417.3229 42.5854 -4.5459 403.8977 408.4436 417.1875 44.1965 -4.5393 404.0853 408.6246 417.0524 45.8093 -4.5332 404.2641 408.7973 416.9270 47.4075 -4.5298 404.4267 408.9565 416.7942 49.0065 -4.5214 404.6100 409.1315 416.6684 50.6205 -4.5139 404.7870 409.3008 416.5143 52.2345 -4.5071 404.9564 409.4635 416.3964 53.8335 -4.4976 405.1350 409.6326 416.2733 55.4455 -4.4920 405.2959 409.7878 416.1337 57.0544 -4.4843 405.4499 409.9342 416.0238 58.6529 -4.4783 405.6191 410.0974 415.8930 60.2669 -4.4789 405.7716 410.2505 415.7820 61.8659 -4.4723 405.9207 410.3930 415.6823 63.4950 -4.4672 406.0727 410.5400 415.5638 65.0938 -4.4591 406.2239 410.6831 415.4476 66.7078 -4.4504 406.3655 410.8159 415.3295 68.3068 -4.4417 406.5131 410.9548 415.2132 69.9206 -4.4350 406.6461 411.0811 415.0976 71.5348 -4.4283 406.7934 411.2217 414.9709 73.1486 -4.4182 406.9320 411.3502 414.8443 74.7475 -4.4100 407.0727 411.4827 414.7416 76.3465 -4.4026 407.2008 411.6034 414.6023 77.9755 -4.3973 407.3215 411.7188 414.4776 79.5895 -4.3896 407.4417 411.8313 414.3383 81.1885 -4.3829 407.5784 411.9613 414.2252 82.7875 -4.3719 407.7013 412.0732 414.1106 84.4015 -4.3666 407.8199 412.1865 414.0093 86.0304 -4.3559 407.9389 412.2949 413.8645 87.6300 -4.3393 408.0598 412.3991 413.7494 89.2236 -4.3365 408.1562 412.4927 413.6570 90.8298 -4.3446 408.2589 412.6035 413.5463 92.4214 -4.3377 408.3652 412.7029 413.4349 94.0275 -4.3216 408.4631 412.7847 413.3389 95.6368 -4.3127 408.5634 412.8761 413.2140 97.2384 -4.3034 408.6671 412.9705 413.1176 98.8303 -4.2895 408.7696 413.0591 413.0213 100.4241 -4.2817 408.8656 413.1473 412.9208 102.0489 -4.2735 408.9432 413.2167 412.8020 103.6418 -4.2710 409.0388 413.3098 412.6767 105.2506 -4.2544 409.1265 413.3809 412.5723 106.8441 -4.2425 409.2109 413.4534 412.4320 108.4524 -4.2387 409.2971 413.5358 412.3133 110.0659 -4.2335 409.3841 413.6176 412.1918 111.6769 -4.2231 409.4659 413.6890 412.0713 113.2738 -4.2275 409.5271 413.7546 411.9392 114.8728 -4.2280 409.5876 413.8156 411.8393 116.4718 -4.2195 409.6773 413.8968 411.7184 118.1006 -4.2055 409.7404 413.9459 411.5973 119.6996 -4.1984 409.8122 414.0106 411.5032 121.3136 -4.1899 409.8618 414.0517 411.3717 122.9125 -4.1894 409.9449 414.1343 411.2568 124.5115 -4.1829 410.0074 414.1903 411.1396 126.1405 -4.1764 410.0596 414.2360 411.0143 127.7395 -4.1674 410.1226 414.2900 410.9246 129.3535 -4.1622 410.1684 414.3306 410.8238 130.9525 -4.1562 410.2296 414.3858 410.7171 132.5515 -4.1455 410.2706 414.4160 410.5984 134.1655 -4.1393 410.3365 414.4758 410.5081 135.7803 -4.1282 410.3780 414.5062 410.3937 137.3810 -4.1491 410.4247 414.5738 410.2718 138.9839 -4.1607 410.4756 414.6363 410.1459 140.5988 -4.1285 410.5185 414.6470 410.0325 142.2139 -4.1142 410.5440 414.6582 409.9146 143.8280 -4.1106 410.5971 414.7077 409.7898 145.4288 -4.1084 410.6309 414.7393 409.6566 147.0428 -4.1030 410.6666 414.7696 409.5287 148.6418 -4.0872 410.7033 414.7905 409.4086 150.2575 -4.0835 410.7401 414.8236 409.2804 151.8746 -4.0655 410.7588 414.8243 409.1620 153.4710 -4.0581 410.7825 414.8406 409.0355 155.0780 -4.0611 410.8055 414.8667 408.9013 156.6744 -4.0515 410.8254 414.8770 408.7913 158.2674 -4.0442 410.8486 414.8928 408.6728 159.8740 -4.0424 410.8761 414.9185 408.5608 161.4800 -4.0348 410.8906 414.9254 408.4400 163.0705 -4.0313 410.9135 414.9449 408.3339 164.6780 -4.0297 410.9255 414.9552 408.1969 166.2711 -4.0266 410.9456 414.9722 408.0866 167.8988 -4.0089 410.9532 414.9621 407.9707 169.4928 -4.0118 410.9478 414.9596 407.8737 171.0864 -4.0461 410.9703 415.0164 407.7492 172.6978 -4.0377 410.9797 415.0174 407.6297 174.2943 -4.0183 410.9714 414.9896 407.4917 175.9076 -4.0125 410.9732 414.9856 407.3623 177.5215 -4.0036 410.9832 414.9867 407.2522 179.1205 -3.9948 410.9953 414.9901 407.1088 180.7195 -3.9955 410.9916 414.9870 406.9814 182.3194 -3.9937 411.0065 415.0002 406.8481 183.9485 -3.9775 410.9904 414.9679 406.7188 185.5481 -3.9922 410.9789 414.9712 406.5955 187.1469 -3.9810 410.9693 414.9503 406.4659 188.7611 -3.9633 410.9675 414.9308 406.3371 190.3620 -3.9496 410.9646 414.9142 406.1943 191.9635 -3.9477 410.9528 414.9005 406.0669 193.5934 -3.9367 410.9270 414.8637 405.9452 195.1928 -3.9271 410.9286 414.8557 405.8173 196.7918 -3.9205 410.9055 414.8260 405.6947 198.4056 -3.9193 410.8803 414.7995 405.5490 200.0196 -3.9154 410.8681 414.7835 405.4410 201.6336 -3.9113 410.8480 414.7594 405.3208 203.2325 -3.9041 410.8266 414.7307 405.1947 204.8465 -3.8964 410.8030 414.6993 405.0648 206.4466 -3.8878 410.7907 414.6784 404.9590 208.0635 -3.8847 410.7618 414.6466 404.8388 209.6775 -3.8758 410.7457 414.6215 404.7158 211.2915 -3.8747 410.7046 414.5793 404.6138 212.8904 -3.8685 410.6894 414.5579 404.5066 214.4893 -3.8648 410.6520 414.5168 404.4018 216.1179 -3.8631 410.6261 414.4892 404.2803 217.7294 -3.8551 410.5988 414.4539 404.1805 219.3213 -3.8520 410.5663 414.4183 404.0709 220.9125 -3.8450 410.5164 414.3614 403.9588 222.5194 -3.8398 410.5010 414.3408 403.8392 224.1254 -3.8344 410.4648 414.2992 403.7332 225.7314 -3.8316 410.4433 414.2749 403.6078 227.3223 -3.8281 410.3799 414.2079 403.4886 228.9284 -3.8183 410.3490 414.1673 403.3631 230.5389 -3.8139 410.3205 414.1344 403.2292 232.1470 -3.8115 410.2702 414.0817 403.1070 233.7581 -3.8151 410.2379 414.0531 402.9843 235.3526 -3.8370 410.1785 414.0155 402.8375 236.9533 -3.8164 410.1573 413.9737 402.7062 238.5530 -3.8059 410.1244 413.9303 402.5787 240.1814 -3.8053 410.0609 413.8662 402.4398 241.7798 -3.8022 410.0124 413.8146 402.3314 243.3786 -3.7968 409.9708 413.7677 402.1767 244.9776 -3.7928 409.9184 413.7112 402.0588 246.5916 -3.7843 409.8631 413.6474 401.9281 248.2065 -3.7781 409.8014 413.5795 401.7958 249.8058 -3.7777 409.7580 413.5358 401.6625 251.4060 -3.7736 409.7165 413.4901 401.5366 253.0225 -3.7730 409.6483 413.4213 401.3956 254.6225 -3.7717 409.5943 413.3660 401.2755 256.2365 -3.7676 409.5627 413.3303 401.1531 257.8505 -3.7612 409.4980 413.2593 401.0270 259.4495 -3.7604 409.4446 413.2050 400.9135 261.0634 -3.7522 409.3799 413.1320 400.7912 262.6625 -3.7602 409.3326 413.0928 400.6679 264.2764 -3.7569 409.2564 413.0133 400.5368 265.8910 -3.7390 409.2028 412.9418 400.4118 267.4911 -3.7354 409.1477 412.8831 400.3086 269.0910 -3.7304 409.0903 412.8207 400.1940 270.7039 -3.7224 409.0158 412.7382 400.0776 272.3053 -3.7428 408.9676 412.7104 399.9620 273.9349 -3.7287 408.9062 412.6349 399.8312 275.5356 -3.7126 408.8373 412.5499 399.7217 277.1496 -3.7137 408.7752 412.4889 399.6063 278.7485 -3.7118 408.7140 412.4258 399.4941 280.3475 -3.7085 408.6436 412.3522 399.3800 281.9728 -3.7202 408.5670 412.2872 399.2612 283.5629 -3.6944 408.5111 412.2055 399.1355 285.1700 -3.6772 408.4284 412.1055 399.0056 286.7610 -3.6660 408.3531 412.0191 398.8999 288.3676 -3.6630 408.2855 411.9485 398.7584 289.9751 -3.6573 408.2220 411.8793 398.6209 291.5810 -3.6523 408.1447 411.7970 398.4761 293.1726 -3.6491 408.0842 411.7333 398.3446 294.7818 -3.6468 408.0141 411.6609 398.2255 296.3934 -3.6418 407.9461 411.5879 398.0855 298.0054 -3.6331 407.8782 411.5113 397.9564 299.6035 -3.6300 407.7925 411.4225 397.8262 301.2175 -3.6295 407.7245 411.3541 397.6979 302.8165 -3.6242 407.6341 411.2583 397.5532 304.4155 -3.6197 407.5607 411.1805 397.4195 306.0295 -3.6142 407.4834 411.0976 397.2844 307.6435 -3.6111 407.3990 411.0101 397.1570 309.2425 -3.6076 407.3233 410.9309 397.0252 310.8411 -3.5985 407.2446 410.8431 396.8770 312.4555 -3.5935 407.1709 410.7644 396.7480 314.0689 -3.5910 407.1098 410.7008 396.6315 315.6829 -3.5897 407.0086 410.5983 396.4658 317.2818 -3.5819 406.9174 410.4992 396.3620 318.8808 -3.5690 406.8466 410.4156 396.2398 320.4948 -3.5650 406.7734 410.3384 396.0997 322.1105 -3.5808 406.6915 410.2723 395.9678 323.7248 -3.5872 406.6006 410.1878 395.8387 325.3243 -3.5751 406.5109 410.0860 395.7276 326.9236 -3.5640 406.4217 409.9857 395.6110 328.5376 -3.5693 406.3343 409.9036 395.4631 330.1515 -3.5675 406.2525 409.8200 395.3545 331.7658 -3.5475 406.1699 409.7175 395.2303 333.3655 -3.5383 406.0806 409.6189 395.1146 334.9645 -3.5283 405.9931 409.5214 394.9959 336.5785 -3.5296 405.9061 409.4358 394.8728 338.1925 -3.5332 405.8371 409.3703 394.7640 339.8065 -3.5485 405.7268 409.2753 394.6321 341.4129 -3.5464 405.6440 409.1903 394.5175 343.0149 -3.5473 405.5515 409.0989 394.4071 344.6138 -3.5480 405.4715 409.0195 394.2885 346.2211 -3.5433 405.3733 408.9166 394.1936 347.8283 -3.5410 405.2716 408.8126 394.0741 349.4348 -3.5299 405.1870 408.7170 393.9558 351.0266 -3.5073 405.1049 408.6123 393.8324 352.6249 -3.5005 405.0176 408.5182 393.7139 354.2243 -3.4969 404.9098 408.4067 393.5736 355.8180 -3.4951 404.8216 408.3167 393.4578 357.4424 -3.4902 404.7230 408.2132 393.3360 359.0364 -3.4852 404.6395 408.1247 393.1880 360.6459 -3.4828 404.5361 408.0189 393.0565 362.2411 -3.4784 404.4490 407.9275 392.9298 363.8523 -3.4751 404.3454 407.8205 392.8043 365.4640 -3.4742 404.2447 407.7189 392.6613 367.0629 -3.4707 404.1673 407.6381 392.5494 368.6768 -3.4677 404.0694 407.5371 392.4108 370.2758 -3.4646 403.9677 407.4323 392.2706 371.8748 -3.4615 403.8785 407.3400 392.1420 373.4900 -3.4580 403.7871 407.2451 392.0101 375.1046 -3.4546 403.6889 407.1436 391.8482 376.7058 -3.4392 403.5710 407.0102 391.7372 378.3066 -3.4439 403.4904 406.9343 391.5897 379.9205 -3.4429 403.3921 406.8350 391.4647 381.5195 -3.4394 403.2861 406.7255 391.3336 383.1335 -3.4346 403.1911 406.6256 391.1868 384.7475 -3.4298 403.0911 406.5208 391.0644 386.3465 -3.4265 402.9922 406.4187 390.9438 387.9455 -3.4223 402.8957 406.3180 390.8162 389.5595 -3.4178 402.7898 406.2076 390.6832 391.1731 -3.4121 402.6883 406.1004 390.5506 392.7873 -3.4077 402.5872 405.9949 390.4198 394.3858 -3.4079 402.4866 405.8946 390.2976 395.9848 -3.4025 402.3821 405.7846 390.1651 397.5994 -3.4020 402.2877 405.6897 390.0412 399.2139 -3.3970 402.1775 405.5745 389.9312 400.8289 -3.3944 402.0719 405.4663 389.7796 402.4288 -3.3937 401.9697 405.3634 389.6540 404.0276 -3.3896 401.8791 405.2688 389.5360 405.6416 -3.3846 401.7667 405.1513 389.4226 407.2706 -3.3813 401.6649 405.0462 389.2945 408.8696 -3.3766 401.5433 404.9199 389.1754 410.4688 -3.3737 401.4391 404.8128 389.0476 412.0760 -3.3693 401.3456 404.7149 388.9314 413.6670 -3.3622 401.2410 404.6032 388.8116 415.2880 -3.3580 401.1464 404.5044 388.6783 416.8805 -3.3563 401.0370 404.3933 388.5738 418.4731 -3.3514 400.9301 404.2815 388.4437 420.0813 -3.3464 400.8323 404.1786 388.3246 421.6894 -3.3450 400.7203 404.0653 388.2012 423.2975 -3.3421 400.6118 403.9538 388.0705 424.8938 -3.3380 400.4976 403.8355 387.9599 426.5025 -3.3344 400.3860 403.7204 387.8416 428.0976 -3.3318 400.2865 403.6182 387.7229 429.7255 -3.3282 400.1624 403.4906 387.5985 431.3235 -3.3209 400.0837 403.4045 387.5025 432.9375 -3.3190 399.9813 403.3003 387.3682 434.5365 -3.3168 399.8492 403.1661 387.2457 436.1355 -3.3137 399.7596 403.0733 387.1083 437.7643 -3.3120 399.6523 402.9643 386.9758 439.3633 -3.3096 399.5296 402.8392 386.8573 440.9773 -3.3038 399.4343 402.7381 386.7120 442.5758 -3.2982 399.3181 402.6163 386.5660 444.1763 -3.2895 399.2278 402.5173 386.4350 445.8059 -3.2838 399.0991 402.3830 386.3051 447.4049 -3.2807 398.9848 402.2655 386.1870 449.0188 -3.2767 398.8747 402.1514 386.0379 450.6178 -3.2720 398.7738 402.0459 385.8877 452.2168 -3.2699 398.6734 401.9433 385.7466 453.8458 -3.2712 398.5520 401.8232 385.6105 455.4598 -3.2818 398.4415 401.7233 385.4646 457.0585 -3.2783 398.3281 401.6064 385.3120 458.6575 -3.2768 398.2255 401.5023 385.1709 460.2565 -3.2736 398.1102 401.3838 385.0327 461.8863 -3.2643 397.9998 401.2641 384.9055 463.4863 -3.2619 397.8875 401.1494 384.7556 465.1015 -3.2578 397.7818 401.0396 384.6287 466.7005 -3.2544 397.6519 400.9063 384.4887 468.2993 -3.2495 397.5394 400.7890 384.3348 469.9281 -3.2444 397.4395 400.6839 384.2058 471.5420 -3.2390 397.3287 400.5676 384.0722 473.1418 -3.2377 397.1975 400.4352 383.9230 474.7388 -3.2313 397.0922 400.3235 383.8071 476.3454 -3.2277 396.9894 400.2170 383.6813 477.9515 -3.2240 396.8682 400.0921 383.5522 479.5433 -3.2235 396.7380 399.9615 383.4179 481.1494 -3.2165 396.6252 399.8416 383.2875 482.7406 -3.2150 396.5264 399.7414 383.1500 484.3483 -3.2130 396.4129 399.6259 383.0241 485.9561 -3.2082 396.2954 399.5036 382.8994 487.5636 -3.2035 396.1866 399.3900 382.7513 489.1590 -3.2014 396.0582 399.2596 382.6236 490.7690 -3.1990 395.9259 399.1249 382.5031 492.3649 -3.1937 395.8306 399.0244 382.3727 493.9931 -3.1899 395.7037 398.8937 382.2518 495.5904 -3.1893 395.5979 398.7872 382.1102 497.1888 -3.1856 395.4921 398.6777 381.9987 498.8026 -3.1787 395.3733 398.5520 381.8602 500.4016 -3.1766 395.2491 398.4257 381.7391 502.0156 -3.1739 395.1297 398.3036 381.6083 503.6295 -3.1693 395.0141 398.1834 381.4752 505.2285 -3.1637 394.8978 398.0615 381.3619 506.8276 -3.1628 394.7861 397.9490 381.2288 508.4416 -3.1600 394.6655 397.8255 381.1056 510.0556 -3.1567 394.5425 397.6993 380.9923 511.6695 -3.1520 394.4263 397.5783 380.8829 513.2689 -3.1466 394.3059 397.4525 380.7437 514.8685 -3.1448 394.1891 397.3339 380.6110 516.4828 -3.1412 394.0693 397.2105 380.4894 518.0995 -3.1387 393.9575 397.0962 380.3686 519.7134 -3.1363 393.8402 396.9765 380.2359 521.3120 -3.1332 393.7279 396.8611 380.1181 522.9108 -3.1314 393.6075 396.7388 379.9956 524.5254 -3.1278 393.4816 396.6094 379.8771 526.1406 -3.1223 393.3708 396.4930 379.7666 527.7549 -3.1213 393.2557 396.3770 379.6304 529.3538 -3.1181 393.1301 396.2482 379.5257 530.9678 -3.1143 393.0062 396.1205 379.4059 532.5816 -3.1102 392.8908 396.0010 379.2758 534.1958 -3.1088 392.7808 395.8895 379.1574 535.7960 -3.1052 392.6623 395.7675 379.0391 537.4109 -3.1008 392.5451 395.6459 378.9311 539.0078 -3.0961 392.4266 395.5227 378.8073 540.5990 -3.0955 392.3034 395.3988 378.7021 542.2208 -3.1016 392.1995 395.3010 378.5891 543.8114 -3.1239 392.0580 395.1818 378.4744 545.4043 -3.1166 391.9568 395.0734 378.3600 547.0420 -3.0891 391.8409 394.9300 378.2380 548.6480 -3.0664 391.7253 394.7917 378.0933 550.2413 -3.0638 391.5991 394.6629 377.9723 551.8500 -3.0619 391.4771 394.5390 377.8416 553.4410 -3.0591 391.3710 394.4301 377.7036 555.0643 -3.0582 391.2385 394.2966 377.5644 556.6603 -3.0799 391.1214 394.2013 377.4403 558.2599 -3.0942 391.0051 394.0993 377.3077 559.8734 -3.0975 390.8886 393.9860 377.1645 561.4715 -3.0962 390.7667 393.8629 377.0269 563.1003 -3.0722 390.6554 393.7275 376.8864 564.6986 -3.0505 390.5295 393.5800 376.7332 566.3123 -3.0479 390.4128 393.4607 376.5887 567.9108 -3.0438 390.2926 393.3365 376.4568 569.5100 -3.0451 390.1659 393.2111 376.3120 571.1389 -3.0659 390.0426 393.1085 376.1489 572.7380 -3.0731 389.9164 392.9895 376.0187 574.3375 -3.0647 389.8062 392.8710 375.8872 575.9528 -3.0333 389.7005 392.7338 375.7456 577.6790 -3.0334 389.5434 392.5768 375.5876 579.3746 -3.0377 389.4177 392.4554 375.4580 580.9738 -3.0328 389.3077 392.3405 375.3145 582.5726 -3.0361 389.1788 392.2149 375.1762 584.2015 -3.0434 389.0647 392.1082 375.0221 585.8006 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