DTA measure 3gyors Date: 20241022:1542 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1647.91 s Mass = 959.700 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3508 -4.6886 398.2629 402.9515 418.4888 3.9656 -4.6834 398.5117 403.1950 418.5261 5.5809 -4.6835 398.7519 403.4354 418.5623 7.1809 -4.6800 398.9811 403.6611 418.5942 8.7808 -4.6785 399.2211 403.8996 418.6276 10.3926 -4.6734 399.4708 404.1442 418.6497 11.9991 -4.6687 399.7003 404.3691 418.6614 13.6050 -4.6671 399.9354 404.6025 418.6548 15.1960 -4.6624 400.1718 404.8341 418.6070 16.7915 -4.6589 400.3968 405.0557 418.5723 18.4000 -4.6560 400.6324 405.2883 418.4924 20.0219 -4.6498 400.8758 405.5256 418.4070 21.6151 -4.6433 401.1007 405.7440 418.3010 23.2228 -4.6388 401.3005 405.9394 418.1743 24.8165 -4.6348 401.5203 406.1552 418.0421 26.4408 -4.6283 401.7420 406.3703 417.8573 28.0378 -4.6207 401.9448 406.5656 417.6887 29.6360 -4.6150 402.1506 406.7657 417.5120 31.2496 -4.6063 402.3555 406.9618 417.3027 32.8485 -4.6032 402.5732 407.1764 417.1014 34.4475 -4.5974 402.7778 407.3752 416.8887 36.0765 -4.5842 402.9680 407.5522 416.6622 37.6755 -4.5752 403.1570 407.7322 416.4300 39.2745 -4.5650 403.3463 407.9113 416.2077 40.8735 -4.5551 403.5418 408.0970 415.9862 42.4875 -4.5490 403.7378 408.2867 415.7300 44.1015 -4.5529 403.9224 408.4753 415.5155 45.7154 -4.5389 404.0900 408.6289 415.2816 47.3139 -4.5174 404.2578 408.7753 415.0391 48.9130 -4.5007 404.4356 408.9363 414.8198 50.5128 -4.4851 404.6013 409.0864 414.6055 52.1439 -4.4834 404.7659 409.2493 414.3820 53.7429 -4.4699 404.9522 409.4221 414.1678 55.3568 -4.4643 405.1078 409.5721 413.9562 56.9558 -4.4675 405.2457 409.7132 413.7453 58.5570 -4.4636 405.3953 409.8589 413.5336 60.1866 -4.4499 405.5655 410.0154 413.3377 61.7863 -4.4245 405.7029 410.1273 413.1494 63.4006 -4.4079 405.8356 410.2436 412.9457 65.0000 -4.3960 405.9808 410.3768 412.7538 66.6009 -4.3788 406.1102 410.4890 412.5739 68.2305 -4.3732 406.2441 410.6173 412.3850 69.8295 -4.3647 406.3578 410.7225 412.1826 71.4438 -4.3523 406.4851 410.8374 412.0124 73.0439 -4.3456 406.6188 410.9643 411.8604 74.6393 -4.3349 406.7274 411.0623 411.6879 76.2438 -4.3249 406.8485 411.1735 411.5007 77.8516 -4.3142 406.9674 411.2816 411.3472 79.4578 -4.3035 407.0788 411.3823 411.1747 81.0490 -4.2908 407.1664 411.4572 411.0188 82.6403 -4.2782 407.2772 411.5554 410.8396 84.2626 -4.2847 407.3746 411.6593 410.6799 85.8698 -4.2964 407.4821 411.7785 410.4989 87.4610 -4.2887 407.5757 411.8643 410.3401 89.1591 -4.2757 407.6612 411.9370 410.1476 90.7833 -4.2502 407.7657 412.0159 409.9684 92.3934 -4.2225 407.8394 412.0619 409.7885 94.0070 -4.2139 407.9235 412.1374 409.5974 95.6058 -4.2105 408.0017 412.2122 409.4311 97.2048 -4.2032 408.0781 412.2813 409.2623 98.8038 -4.1925 408.1671 412.3596 409.0483 100.4179 -4.1822 408.2352 412.4174 408.8728 102.0319 -4.1739 408.2960 412.4699 408.6919 103.6308 -4.1633 408.3538 412.5171 408.5076 105.2298 -4.1551 408.4179 412.5729 408.3338 106.8436 -4.1493 408.4690 412.6183 408.1597 108.4426 -4.1390 408.5263 412.6653 407.9462 110.0716 -4.1285 408.5849 412.7135 407.7589 111.6706 -4.1183 408.6268 412.7450 407.5554 113.2695 -4.1095 408.6895 412.7990 407.3649 114.8685 -4.1010 408.7375 412.8385 407.1697 116.4825 -4.0842 408.7738 412.8581 406.9791 118.1115 -4.0661 408.8294 412.8955 406.7766 119.7116 -4.0514 408.8577 412.9091 406.5752 121.3115 -4.0408 408.9021 412.9429 406.3598 122.9255 -4.0296 408.9186 412.9482 406.2016 124.5250 -4.0160 408.9460 412.9620 405.9869 126.1541 -4.0060 408.9883 412.9943 405.7945 127.7529 -3.9996 409.0183 413.0178 405.5802 129.3530 -3.9873 409.0334 413.0206 405.4164 130.9683 -3.9794 409.0488 413.0282 405.2289 132.5829 -3.9692 409.0738 413.0430 405.0238 134.1969 -3.9581 409.0810 413.0391 404.8281 135.7958 -3.9507 409.1026 413.0533 404.6588 137.4099 -3.9340 409.0933 413.0273 404.4596 139.0034 -3.9198 409.1104 413.0302 404.2625 140.6076 -3.9092 409.1219 413.0311 404.0582 142.2143 -3.9015 409.1148 413.0163 403.8779 143.8210 -3.8919 409.1120 413.0038 403.6869 145.4120 -3.8859 409.1184 413.0044 403.4889 147.0050 -3.8919 409.0969 412.9888 403.2927 148.6118 -3.8849 409.0968 412.9818 403.0931 150.2283 -3.8744 409.1040 412.9784 402.8952 151.8255 -3.8559 409.0672 412.9231 402.7113 153.4360 -3.8441 409.0608 412.9049 402.5113 155.0321 -3.8369 409.0555 412.8924 402.3308 156.6304 -3.8275 409.0312 412.8588 402.1646 158.2285 -3.8238 409.0209 412.8447 401.9539 159.8468 -3.8137 408.9974 412.8111 401.7814 161.4585 -3.8031 408.9711 412.7743 401.5994 163.0575 -3.8032 408.9404 412.7436 401.4183 164.6715 -3.7999 408.9195 412.7194 401.2275 166.2705 -3.7881 408.8908 412.6788 401.0330 167.8695 -3.7794 408.8735 412.6529 400.8359 169.4985 -3.7703 408.8169 412.5871 400.6387 171.0974 -3.7631 408.8024 412.5656 400.4410 172.6965 -3.7525 408.7584 412.5109 400.2609 174.3101 -3.7411 408.7073 412.4484 400.0633 175.9090 -3.7348 408.6790 412.4138 399.8812 177.5229 -3.7286 408.6386 412.3671 399.6930 179.1369 -3.7209 408.5943 412.3152 399.5040 180.7358 -3.7147 408.5386 412.2533 399.3134 182.3348 -3.7075 408.4951 412.2026 399.1253 183.9488 -3.7018 408.4500 412.1518 398.9250 185.5629 -3.6901 408.3888 412.0789 398.7350 187.1778 -3.6815 408.3489 412.0305 398.5494 188.7766 -3.6742 408.3174 411.9916 398.3500 190.3756 -3.6649 408.2616 411.9265 398.1810 191.9896 -3.6598 408.1910 411.8508 397.9514 193.6185 -3.6562 408.1334 411.7896 397.7366 195.2185 -3.6464 408.0711 411.7174 397.5440 196.8183 -3.6405 408.0005 411.6410 397.3408 198.4325 -3.6338 407.9510 411.5848 397.1476 200.0465 -3.6233 407.8764 411.4997 396.9505 201.6548 -3.6152 407.8031 411.4184 396.7402 203.2643 -3.6077 407.7388 411.3465 396.5514 204.8556 -3.6012 407.6575 411.2587 396.3763 206.4458 -3.5934 407.6121 411.2055 396.1806 208.0529 -3.5849 407.5363 411.1212 395.9800 209.6604 -3.5772 407.4414 411.0186 395.7775 211.2670 -3.5693 407.3690 410.9382 395.5868 212.8589 -3.5643 407.3037 410.8680 395.4120 214.4666 -3.5556 407.2148 410.7704 395.2159 216.0620 -3.5463 407.1259 410.6722 395.0236 217.6738 -3.5375 407.0431 410.5806 394.8285 219.2831 -3.5294 406.9716 410.5010 394.6445 220.8798 -3.5211 406.8734 410.3945 394.4569 222.4761 -3.5150 406.7800 410.2950 394.2499 224.0749 -3.5092 406.7092 410.2184 394.0509 225.7039 -3.5058 406.6170 410.1228 393.8508 227.3029 -3.4956 406.5163 410.0119 393.6674 228.9018 -3.4882 406.4260 409.9142 393.4356 230.5158 -3.4784 406.3347 409.8131 393.2306 232.1209 -3.4735 406.2383 409.7118 393.0315 233.7216 -3.4668 406.1324 409.5992 392.8415 235.3359 -3.4579 406.0344 409.4923 392.6312 236.9498 -3.4481 405.9416 409.3898 392.4217 238.5486 -3.4425 405.8437 409.2862 392.2258 240.1475 -3.4381 405.7467 409.1848 392.0470 241.7465 -3.4264 405.6444 409.0708 391.8309 243.3755 -3.4205 405.5472 408.9677 391.6424 244.9758 -3.4119 405.4452 408.8572 391.4394 246.5935 -3.4035 405.3298 408.7333 391.2464 248.1925 -3.3997 405.2211 408.6208 391.0471 249.7915 -3.3917 405.1214 408.5131 390.8542 251.4200 -3.3828 405.0008 408.3836 390.6568 253.0191 -3.3782 404.8999 408.2780 390.4757 254.6328 -3.3716 404.8070 408.1787 390.2796 256.2318 -3.3566 404.6801 408.0367 390.0781 257.8308 -3.3512 404.5591 407.9102 389.8786 259.4599 -3.3506 404.4584 407.8090 389.6841 261.0613 -3.3457 404.3414 407.6872 389.4683 262.6798 -3.3396 404.2209 407.5605 389.2649 264.2786 -3.3315 404.1219 407.4534 389.0665 265.8776 -3.3274 403.9961 407.3236 388.8627 267.5039 -3.3209 403.8676 407.1885 388.6729 269.1094 -3.3151 403.7422 407.0572 388.4650 270.7010 -3.3096 403.6302 406.9398 388.2690 272.2926 -3.3056 403.5182 406.8238 388.0635 273.8990 -3.2982 403.3876 406.6858 387.8431 275.5068 -3.2934 403.2659 406.5594 387.6575 277.1135 -3.2854 403.1386 406.4240 387.4732 278.7063 -3.2780 403.0179 406.2959 387.2780 280.3141 -3.2723 402.9027 406.1749 387.0690 281.9233 -3.2658 402.7658 406.0316 386.8651 283.5340 -3.2596 402.6205 405.8802 386.6692 285.1301 -3.2536 402.5081 405.7617 386.4881 286.7429 -3.2480 402.3793 405.6273 386.2851 288.3415 -3.2452 402.2412 405.4864 386.1117 289.9405 -3.2395 402.1172 405.3567 385.9095 291.5545 -3.2307 401.9952 405.2259 385.7110 293.1685 -3.2209 401.8623 405.0832 385.5016 294.7675 -3.2187 401.7173 404.9359 385.3130 296.3665 -3.2122 401.5810 404.7932 385.1058 297.9655 -3.2093 401.4637 404.6730 384.8873 299.5795 -3.2044 401.3150 404.5195 384.6987 301.1933 -3.1966 401.1881 404.3848 384.4888 302.7919 -3.1998 401.0336 404.2334 384.2855 304.3909 -3.1962 400.9141 404.1103 384.0900 306.0048 -3.1883 400.7656 403.9539 383.8734 307.6038 -3.1816 400.6314 403.8131 383.6846 309.2330 -3.1787 400.4961 403.6748 383.4657 310.8316 -3.1703 400.3439 403.5141 383.2709 312.4308 -3.1637 400.1990 403.3627 383.0667 314.0448 -3.1599 400.0459 403.2058 382.8687 315.6436 -3.1552 399.9100 403.0652 382.6642 317.2575 -3.1471 399.7824 402.9295 382.4765 318.8715 -3.1396 399.6190 402.7586 382.2822 320.4705 -3.1308 399.4848 402.6157 382.0784 322.0851 -3.1239 399.3515 402.4754 381.8854 323.6878 -3.1162 399.1921 402.3084 381.6660 325.3105 -3.1102 399.0354 402.1456 381.4818 326.9095 -3.1064 398.9066 402.0131 381.2881 328.5248 -3.1032 398.7582 401.8614 381.0964 330.1240 -3.0914 398.6114 401.7028 380.8883 331.7186 -3.0822 398.4474 401.5296 380.6923 333.3389 -3.0798 398.3111 401.3910 380.4802 334.9301 -3.0762 398.1595 401.2357 380.2826 336.5368 -3.0762 397.9876 401.0638 380.0632 338.1284 -3.0730 397.8595 400.9325 379.8544 339.7343 -3.0705 397.7040 400.7745 379.6457 341.3414 -3.0674 397.5581 400.6255 379.4471 342.9496 -3.0613 397.3972 400.4585 379.2417 344.5415 -3.0550 397.2491 400.3041 379.0304 346.1501 -3.0486 397.1035 400.1521 378.8277 347.7615 -3.0466 396.9457 399.9922 378.6193 349.3734 -3.0399 396.7883 399.8282 378.4186 350.9718 -3.0328 396.6357 399.6685 378.2078 352.5708 -3.0257 396.4631 399.4888 378.0017 354.1855 -3.0149 396.3104 399.3253 377.8080 355.7889 -3.0086 396.1378 399.1463 377.5946 357.4029 -3.0038 395.9796 398.9834 377.3781 359.0019 -2.9996 395.8450 398.8446 377.1926 360.6156 -2.9933 395.6778 398.6711 376.9736 362.2146 -2.9912 395.5262 398.5174 376.7748 363.8138 -2.9841 395.3533 398.3375 376.5770 365.4371 -2.9767 395.2025 398.1792 376.3703 367.0401 -2.9696 395.0468 398.0163 376.1776 368.6545 -2.9633 394.8616 397.8249 375.9735 370.2535 -2.9604 394.7154 397.6758 375.7754 371.8525 -2.9548 394.5663 397.5211 375.5748 373.4515 -2.9478 394.3799 397.3278 375.3785 375.0698 -2.9440 394.2297 397.1737 375.1902 376.6895 -2.9347 394.0633 396.9980 374.9942 378.2885 -2.9298 393.8901 396.8198 374.7882 379.8874 -2.9248 393.7275 396.6523 374.6002 381.5010 -2.9216 393.5679 396.4896 374.4175 383.1004 -2.9213 393.4070 396.3283 374.2163 384.7308 -2.9140 393.2385 396.1525 374.0267 386.3299 -2.9065 393.0534 395.9599 373.8222 387.9298 -2.9018 392.8840 395.7857 373.6117 389.5443 -2.8965 392.7278 395.6243 373.4215 391.1444 -2.8912 392.5538 395.4451 373.2231 392.7594 -2.8852 392.3954 395.2806 373.0010 394.3736 -2.8765 392.2358 395.1123 372.7981 395.9670 -2.8730 392.0691 394.9421 372.6034 397.5580 -2.8693 391.8967 394.7661 372.3917 399.1648 -2.8647 391.7130 394.5778 372.1854 400.7861 -2.8621 391.5502 394.4123 371.9639 402.3775 -2.8566 391.3824 394.2390 371.7691 403.9709 -2.8535 391.2206 394.0741 371.5781 405.5799 -2.8486 391.0461 393.8947 371.3758 407.1885 -2.8424 390.8685 393.7109 371.1654 408.7969 -2.8381 390.7047 393.5428 370.9661 410.4068 -2.8344 390.5241 393.3585 370.7729 412.0029 -2.8278 390.3485 393.1763 370.5698 413.6006 -2.8207 390.1736 392.9943 370.3705 415.2296 -2.8147 390.0143 392.8290 370.1648 416.8285 -2.8128 389.8422 392.6550 369.9791 418.4425 -2.8082 389.6638 392.4720 369.7664 420.0415 -2.8009 389.5032 392.3042 369.5791 421.6449 -2.7984 389.3205 392.1189 369.3843 423.2605 -2.7905 389.1408 391.9313 369.1868 424.8745 -2.7871 388.9800 391.7671 368.9826 426.4735 -2.7836 388.8153 391.5989 368.7738 428.0874 -2.7773 388.6177 391.3950 368.5826 429.6881 -2.7707 388.4367 391.2074 368.3929 431.2878 -2.7656 388.2633 391.0288 368.1718 432.9170 -2.7621 388.0877 390.8497 367.9686 434.5158 -2.7576 387.9198 390.6774 367.7633 436.1298 -2.7512 387.7372 390.4884 367.5590 437.7739 -2.7487 387.5477 390.2964 367.3374 439.3729 -2.7439 387.3674 390.1113 367.1251 440.9868 -2.7388 387.2106 389.9494 366.9228 442.5856 -2.7306 387.0205 389.7511 366.7159 444.1996 -2.7278 386.8452 389.5730 366.5283 445.8136 -2.7192 386.6663 389.3854 366.3137 447.4285 -2.7121 386.4869 389.1990 366.1023 449.0275 -2.7078 386.3224 389.0302 365.8922 450.6269 -2.7030 386.1571 388.8602 365.6857 452.2421 -2.6981 385.9664 388.6645 365.4602 453.8565 -2.6959 385.7730 388.4689 365.2727 455.4705 -2.6893 385.5958 388.2851 365.0683 457.0698 -2.6839 385.4236 388.1076 364.8409 458.6688 -2.6809 385.2479 387.9289 364.6456 460.2763 -2.6747 385.0569 387.7316 364.4471 461.8836 -2.6685 384.8867 387.5552 364.2437 463.4896 -2.6634 384.7090 387.3723 364.0348 465.0806 -2.6579 384.5247 387.1826 363.8540 466.6726 -2.6543 384.3241 386.9784 363.6476 468.2800 -2.6486 384.1556 386.8042 363.4540 469.8885 -2.6458 383.9728 386.6185 363.2506 471.4976 -2.6434 383.7987 386.4422 363.0594 473.0921 -2.6374 383.6205 386.2578 362.8519 474.7035 -2.6336 383.4296 386.0631 362.6544 476.3008 -2.6262 383.2474 385.8736 362.4725 477.9286 -2.6199 383.0616 385.6815 362.2620 479.5265 -2.6141 382.8788 385.4929 362.0671 481.1248 -2.6107 382.7109 385.3216 361.8661 482.7238 -2.6045 382.5204 385.1249 361.6669 484.3378 -2.5997 382.3500 384.9497 361.4484 485.9519 -2.5935 382.1458 384.7393 361.2552 487.5659 -2.5915 381.9656 384.5571 361.0411 489.1648 -2.5855 381.7892 384.3747 360.8476 490.7636 -2.5813 381.6073 384.1886 360.6300 492.3776 -2.5762 381.4318 384.0079 360.4302 493.9916 -2.5724 381.2396 383.8121 360.2175 495.6055 -2.5707 381.0652 383.6359 360.0156 497.2049 -2.5668 380.8678 383.4346 359.7987 498.8045 -2.5652 380.6881 383.2533 359.5884 500.4185 -2.5616 380.5035 383.0651 359.3873 502.0475 -2.5537 380.3095 382.8632 359.1695 503.6465 -2.5507 380.1203 382.6710 358.9585 505.2454 -2.5441 379.9381 382.4822 358.7459 506.8594 -2.5391 379.7437 382.2828 358.5200 508.4586 -2.5364 379.5755 382.1119 358.3381 510.0920 -2.5312 379.3717 381.9029 358.1212 511.6909 -2.5287 379.1989 381.7276 357.9222 513.2908 -2.5215 379.0075 381.5290 357.7245 514.9053 -2.5175 378.8166 381.3341 357.5148 516.5199 -2.5107 378.6213 381.1320 357.3009 518.1350 -2.5044 378.4318 380.9362 357.0919 519.7356 -2.5007 378.2537 380.7544 356.8927 521.3500 -2.5005 378.0656 380.5661 356.6847 522.9496 -2.4950 377.8731 380.3681 356.4779 524.5609 -2.4850 377.6871 380.1721 356.2740 526.1670 -2.4801 377.5008 379.9809 356.0792 527.7584 -2.4792 377.3186 379.7978 355.8844 529.3655 -2.4733 377.1316 379.6049 355.6910 530.9575 -2.4701 376.9363 379.4065 355.4751 532.5800 -2.4638 376.7649 379.2287 355.2788 534.1731 -2.4612 376.5770 379.0382 355.0986 535.7821 -2.4581 376.3723 378.8304 354.8877 537.3754 -2.4521 376.1781 378.6302 354.6882 538.9860 -2.4503 376.0046 378.4549 354.4964 540.5985 -2.4461 375.8157 378.2618 354.2953 542.2110 -2.4395 375.6257 378.0652 354.0728 543.8095 -2.4375 375.4360 377.8735 353.8704 545.4086 -2.4316 375.2446 377.6762 353.6595 547.0225 -2.4264 375.0467 377.4731 353.4569 548.6365 -2.4217 374.8557 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