DTA measure 1Lassu Date: 2025311:124 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1615.16 s Mass = 923.900 mg data_number = 1004 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4928 -1.0995 219.8612 220.9606 208.7560 4.0905 -1.0988 219.8441 220.9429 208.7624 5.6779 -1.0977 219.8161 220.9138 208.7732 7.2911 -1.0973 219.8033 220.9006 208.7868 8.9045 -1.0963 219.7924 220.8887 208.8012 10.5125 -1.0962 219.7678 220.8640 208.8141 12.1000 -1.0955 219.7365 220.8320 208.8284 13.7029 -1.0930 219.7158 220.8089 208.8397 15.3161 -1.0907 219.6977 220.7884 208.8561 16.9190 -1.0899 219.6778 220.7677 208.8729 18.5274 -1.0891 219.6596 220.7487 208.8955 20.1353 -1.0869 219.6416 220.7285 208.9211 21.7536 -1.0859 219.6193 220.7052 208.9566 23.3515 -1.0858 219.5945 220.6803 208.9975 24.9595 -1.0855 219.5736 220.6590 209.0421 26.5675 -1.0855 219.5549 220.6404 209.1020 28.1809 -1.0853 219.5383 220.6237 209.1636 29.7839 -1.0845 219.5201 220.6046 209.2353 31.3916 -1.0839 219.4969 220.5808 209.3207 33.0050 -1.0836 219.4782 220.5618 209.4174 34.6029 -1.0827 219.4652 220.5480 209.5301 36.2161 -1.0809 219.4485 220.5294 209.6520 37.8189 -1.0805 219.4275 220.5081 209.7786 39.4219 -1.0799 219.4075 220.4874 209.9208 41.0196 -1.0803 219.3891 220.4694 210.0761 42.6279 -1.0805 219.3726 220.4531 210.2492 44.2309 -1.0805 219.3552 220.4357 210.4297 45.8436 -1.0809 219.3500 220.4309 210.6233 47.4311 -1.0807 219.3294 220.4101 210.8256 49.0549 -1.0818 219.3138 220.3956 211.0418 50.6628 -1.0820 219.3068 220.3888 211.2672 52.2658 -1.0828 219.3065 220.3892 211.4967 53.8688 -1.0829 219.3038 220.3867 211.7386 55.4821 -1.0835 219.2955 220.3789 211.9966 57.0850 -1.0859 219.2879 220.3738 212.2729 58.6929 -1.0863 219.2818 220.3681 212.5553 60.3165 -1.0872 219.2841 220.3713 212.8529 61.9194 -1.0887 219.2868 220.3755 213.1526 63.5329 -1.0907 219.2914 220.3821 213.4696 65.1358 -1.0932 219.2912 220.3845 213.7841 66.7489 -1.0958 219.2928 220.3887 214.1054 68.3466 -1.0980 219.2946 220.3926 214.4258 69.9445 -1.1011 219.3056 220.4067 214.7505 71.5679 -1.1053 219.3097 220.4151 215.0836 73.1708 -1.1094 219.3161 220.4255 215.4261 74.7738 -1.1128 219.3247 220.4376 215.7650 76.3714 -1.1152 219.3352 220.4504 216.0999 77.9849 -1.1185 219.3434 220.4619 216.4447 79.5723 -1.1214 219.3545 220.4759 216.7791 81.1858 -1.1256 219.3721 220.4977 217.1191 82.7885 -1.1293 219.3864 220.5157 217.4628 84.4121 -1.1331 219.4059 220.5390 217.7979 86.0203 -1.1371 219.4333 220.5705 218.1204 87.6231 -1.1402 219.4626 220.6029 218.4400 89.2364 -1.1433 219.4939 220.6372 218.7731 90.8239 -1.1469 219.5202 220.6671 219.0862 92.4371 -1.1508 219.5480 220.6989 219.3960 94.0400 -1.1537 219.5896 220.7432 219.6960 95.6533 -1.1570 219.6299 220.7869 219.9919 97.2768 -1.1609 219.6676 220.8285 220.2688 98.8846 -1.1647 219.7070 220.8716 220.5333 100.4876 -1.1681 219.7504 220.9184 220.7991 102.0904 -1.1719 219.7960 220.9679 221.0525 103.6829 -1.1753 219.8425 221.0179 221.2942 105.2860 -1.1787 219.8834 221.0621 221.5422 106.8836 -1.1821 219.9270 221.1091 221.7722 108.4918 -1.1844 219.9793 221.1637 221.9960 110.1154 -1.1880 220.0361 221.2241 222.2111 111.7129 -1.1908 220.0883 221.2792 222.4168 113.3261 -1.1927 220.1404 221.3331 222.6231 114.9240 -1.1943 220.2051 221.3995 222.8189 116.5371 -1.1969 220.2747 221.4715 223.0038 118.1404 -1.1998 220.3386 221.5385 223.1742 119.7536 -1.2022 220.4042 221.6065 223.3421 121.3723 -1.2037 220.4725 221.6762 223.5010 122.9803 -1.2043 220.5344 221.7387 223.6558 124.5881 -1.2056 220.5939 221.7996 223.8047 126.1910 -1.2067 220.6628 221.8695 223.9406 127.8041 -1.2067 220.7332 221.9399 224.0766 129.4070 -1.2076 220.8046 222.0122 224.2075 131.0204 -1.2086 220.8774 222.0860 224.3276 132.6234 -1.2083 220.9487 222.1570 224.4411 134.2314 -1.2078 221.0318 222.2397 224.5480 135.8291 -1.2084 221.1147 222.3231 224.6512 137.4321 -1.2094 221.1933 222.4027 224.7554 139.0249 -1.2096 221.2684 222.4780 224.8681 140.6278 -1.2097 221.3409 222.5506 224.9765 142.2308 -1.2087 221.4183 222.6271 225.0846 143.8388 -1.2082 221.5054 222.7135 225.1985 145.4468 -1.2083 221.5959 222.8041 225.3063 147.0394 -1.2079 221.6816 222.8894 225.4144 148.6626 -1.2062 221.7747 222.9808 225.5244 150.2656 -1.2041 221.8592 223.0633 225.6337 151.8789 -1.2028 221.9556 223.1583 225.7501 153.4818 -1.2015 222.0483 223.2498 225.8634 155.0899 -1.2003 222.1378 223.3382 225.9817 156.6983 -1.1988 222.2320 223.4308 226.1055 158.3061 -1.1976 222.3212 223.5188 226.2439 159.9298 -1.1967 222.4189 223.6155 226.3856 161.5326 -1.1952 222.5139 223.7091 226.5363 163.1458 -1.1930 222.6075 223.8005 226.6840 164.7431 -1.1902 222.6971 223.8873 226.8426 166.3461 -1.1894 222.7932 223.9826 227.0083 167.9438 -1.1879 222.8863 224.0741 227.1714 169.5520 -1.1865 222.9804 224.1669 227.3530 171.1546 -1.1853 223.0760 224.2613 227.5378 172.7729 -1.1838 223.1835 224.3674 227.7235 174.3813 -1.1821 223.2896 224.4717 227.9203 175.9841 -1.1812 223.3875 224.5686 228.1137 177.5818 -1.1804 223.4939 224.6742 228.3172 179.1846 -1.1790 223.5984 224.7774 228.5326 180.7926 -1.1789 223.6985 224.8774 228.7576 182.4009 -1.1787 223.8033 224.9820 228.9883 184.0245 -1.1778 223.9108 225.0886 229.2244 185.6329 -1.1771 224.0278 225.2049 229.4702 187.2409 -1.1757 224.1375 225.3132 229.7114 188.8488 -1.1751 224.2448 225.4200 229.9745 190.4621 -1.1749 224.3606 225.5355 230.2411 192.0649 -1.1748 224.4839 225.6587 230.5043 193.6623 -1.1759 224.5964 225.7723 230.7701 195.2706 -1.1769 224.7136 225.8905 231.0474 196.8939 -1.1773 224.8291 226.0065 231.3343 198.4864 -1.1788 224.9379 226.1166 231.6183 200.0843 -1.1783 225.0571 226.2354 231.9013 201.6870 -1.1790 225.1774 226.3564 232.1933 203.2951 -1.1793 225.3031 226.4824 232.4881 204.8983 -1.1801 225.4301 226.6102 232.7789 206.5011 -1.1806 225.5570 226.7376 233.0699 208.1090 -1.1811 225.6829 226.8640 233.3552 209.7120 -1.1811 225.8040 226.9851 233.6392 211.3046 -1.1829 225.9269 227.1098 233.9286 212.9281 -1.1840 226.0548 227.2388 234.2192 214.5311 -1.1854 226.1751 227.3605 234.5040 216.1445 -1.1867 226.3095 227.4962 234.7902 217.7474 -1.1885 226.4327 227.6212 235.0729 219.3605 -1.1893 226.5610 227.7503 235.3382 220.9634 -1.1893 226.6964 227.8857 235.6064 222.5714 -1.1902 226.8286 228.0189 235.8628 224.1950 -1.1918 226.9603 228.1520 236.1236 225.7980 -1.1934 227.0908 228.2842 236.3698 227.4113 -1.1949 227.2340 228.4289 236.6093 229.0140 -1.1966 227.3706 228.5672 236.8568 230.6121 -1.1995 227.5059 228.7054 237.0960 232.2254 -1.2008 227.6456 228.8464 237.3334 233.8071 -1.2019 227.7892 228.9911 237.5572 235.4101 -1.2026 227.9348 229.1374 237.7835 237.0334 -1.2037 228.0799 229.2835 238.0021 238.6364 -1.2048 228.2262 229.4310 238.2093 240.2493 -1.2054 228.3823 229.5877 238.4202 241.8471 -1.2072 228.5321 229.7393 238.6173 243.4603 -1.2079 228.6814 229.8893 238.8124 245.0631 -1.2106 228.8310 230.0416 239.0055 246.6764 -1.2113 228.9882 230.1995 239.1934 248.3000 -1.2109 229.1402 230.3511 239.3882 249.9026 -1.2106 229.2881 230.4987 239.5672 251.5159 -1.2107 229.4358 230.6465 239.7424 253.1189 -1.2120 229.5923 230.8043 239.9075 254.7269 -1.2126 229.7443 230.9568 240.0646 256.3351 -1.2126 229.8994 231.1120 240.2206 257.9434 -1.2128 230.0603 231.2730 240.3777 259.5411 -1.2126 230.2183 231.4308 240.5310 261.1644 -1.2125 230.3806 231.5932 240.6856 262.7674 -1.2122 230.5439 231.7561 240.8337 264.3650 -1.2116 230.7022 231.9138 240.9857 265.9680 -1.2113 230.8613 232.0727 241.1286 267.5554 -1.2108 231.0265 232.2373 241.2708 269.1581 -1.2095 231.1929 232.4023 241.4149 270.7611 -1.2092 231.3570 232.5662 241.5610 272.3744 -1.2091 231.5223 232.7314 241.7167 273.9774 -1.2085 231.6878 232.8963 241.8761 275.6006 -1.2088 231.8576 233.0665 242.0313 277.1931 -1.2088 232.0253 233.2341 242.1839 278.8011 -1.2099 232.1912 233.4011 242.3328 280.4094 -1.2094 232.3581 233.5675 242.4890 282.0124 -1.2090 232.5217 233.7307 242.6442 283.6258 -1.2087 232.6978 233.9065 242.8071 285.2286 -1.2077 232.8703 234.0781 242.9788 286.8368 -1.2070 233.0441 234.2511 243.1509 288.4606 -1.2071 233.2159 234.4229 243.3288 290.0686 -1.2054 233.3790 234.5844 243.5001 291.6766 -1.2042 233.5422 234.7464 243.6815 293.2796 -1.2043 233.7075 234.9118 243.8571 294.8620 -1.2037 233.8699 235.0737 244.0424 296.4751 -1.2030 234.0386 235.2416 244.2364 298.0779 -1.2029 234.2060 235.4089 244.4328 299.6759 -1.2026 234.3827 235.5854 244.6391 301.2889 -1.2027 234.5625 235.7652 244.8490 302.9019 -1.2023 234.7326 235.9350 245.0580 304.5045 -1.2014 234.9040 236.1054 245.2629 306.1128 -1.2005 235.0873 236.2878 245.4805 307.7154 -1.2012 235.2606 236.4619 245.6976 309.3286 -1.2001 235.4247 236.6248 245.9228 310.9316 -1.2009 235.5975 236.7984 246.1560 312.5551 -1.2013 235.7739 236.9752 246.3909 314.1633 -1.2023 235.9492 237.1515 246.6257 315.7711 -1.2034 236.1251 237.3285 246.8611 317.3791 -1.2037 236.3034 237.5071 247.1044 318.9821 -1.2040 236.4823 237.6863 247.3548 320.5954 -1.2047 236.6673 237.8720 247.5992 322.1983 -1.2057 236.8428 238.0485 247.8477 323.8216 -1.2068 237.0211 238.2279 248.1096 325.4295 -1.2075 237.2020 238.4095 248.3648 327.0374 -1.2089 237.3882 238.5970 248.6240 328.6195 -1.2094 237.5682 238.7776 248.8877 330.2223 -1.2099 237.7528 238.9628 249.1552 331.8306 -1.2110 237.9371 239.1481 249.4148 333.4336 -1.2122 238.1219 239.3341 249.6724 335.0366 -1.2145 238.3053 239.5198 249.9301 336.6291 -1.2157 238.4811 239.6968 250.1825 338.2528 -1.2181 238.6644 239.8825 250.4484 339.8554 -1.2211 238.8547 240.0758 250.7043 341.4685 -1.2230 239.0400 240.2630 250.9669 343.0714 -1.2250 239.2199 240.4450 251.2273 344.6690 -1.2267 239.4081 240.6347 251.4819 346.2719 -1.2292 239.6078 240.8370 251.7436 347.8854 -1.2305 239.7940 241.0245 251.9963 349.4934 -1.2318 239.9827 241.2146 252.2502 351.1171 -1.2344 240.1717 241.4061 252.4957 352.7045 -1.2363 240.3593 241.5956 252.7329 354.3179 -1.2392 240.5497 241.7889 252.9715 355.9209 -1.2412 240.7405 241.9816 253.2122 357.5495 -1.2428 240.9386 242.1814 253.4504 359.1474 -1.2446 241.1271 242.3717 253.6764 360.7296 -1.2455 241.3168 242.5624 253.9044 362.3379 -1.2467 241.5095 242.7563 254.1310 363.9564 -1.2465 241.7067 242.9532 254.3493 365.5594 -1.2467 241.9092 243.1559 254.5605 367.1671 -1.2477 242.0964 243.3441 254.7750 368.7701 -1.2497 242.2903 243.5399 254.9815 370.3729 -1.2513 242.4902 243.7414 255.1817 371.9860 -1.2525 242.6883 243.9408 255.3804 373.5888 -1.2533 242.8813 244.1347 255.5666 375.2121 -1.2548 243.0760 244.3308 255.7576 376.8200 -1.2549 243.2687 244.5237 255.9367 378.4228 -1.2559 243.4676 244.7235 256.1149 380.0361 -1.2571 243.6701 244.9272 256.2972 381.6391 -1.2580 243.8617 245.1197 256.4708 383.2524 -1.2590 244.0548 245.3138 256.6461 384.8553 -1.2604 244.2515 245.5119 256.8178 386.4789 -1.2624 244.4564 245.7188 256.9917 388.0870 -1.2625 244.6551 245.9176 257.1620 389.6899 -1.2631 244.8583 246.1214 257.3225 391.2825 -1.2637 245.0611 246.3248 257.4762 392.8855 -1.2639 245.2655 246.5294 257.6426 394.4883 -1.2653 245.4720 246.7373 257.8024 396.0863 -1.2662 245.6781 246.9443 257.9574 397.6891 -1.2674 245.8820 247.1494 258.1149 399.2870 -1.2679 246.0856 247.3535 258.2791 400.9054 -1.2687 246.2910 247.5597 258.4451 402.5134 -1.2701 246.5004 247.7705 258.6124 404.1215 -1.2705 246.7100 247.9804 258.7861 405.7244 -1.2712 246.9104 248.1816 258.9531 407.3376 -1.2711 247.1151 248.3862 259.1295 408.9401 -1.2711 247.3226 248.5937 259.3026 410.5534 -1.2722 247.5277 248.7999 259.4850 412.1716 -1.2732 247.7321 249.0052 259.6684 413.7796 -1.2738 247.9405 249.2143 259.8404 415.3880 -1.2738 248.1482 249.4220 260.0280 416.9910 -1.2753 248.3539 249.6292 260.2203 418.6043 -1.2755 248.5595 249.8350 260.4203 420.2070 -1.2769 248.7655 250.0424 260.6166 421.8201 -1.2778 248.9739 250.2516 260.8198 423.4178 -1.2790 249.1790 250.4580 261.0157 425.0156 -1.2796 249.3898 250.6694 261.2194 426.6239 -1.2808 249.5924 250.8732 261.4349 428.2319 -1.2818 249.7983 251.0801 261.6519 429.8293 -1.2838 249.9972 251.2811 261.8689 431.4426 -1.2856 250.1990 251.4846 262.0917 433.0404 -1.2867 250.4022 251.6889 262.3183 434.6485 -1.2887 250.6093 251.8981 262.5467 436.2721 -1.2910 250.8134 252.1044 262.7831 437.8799 -1.2924 251.0141 252.3065 263.0134 439.4828 -1.2943 251.2193 252.5136 263.2498 441.0959 -1.2953 251.4220 252.7173 263.4943 442.6988 -1.2972 251.6251 252.9223 263.7471 444.3070 -1.2997 251.8256 253.1253 263.9890 445.9203 -1.3019 252.0265 253.3283 264.2347 447.5280 -1.3036 252.2397 253.5433 264.4856 449.1361 -1.3048 252.4457 253.7505 264.7363 450.7440 -1.3061 252.6431 253.9492 264.9915 452.3524 -1.3072 252.8455 254.1527 265.2535 453.9604 -1.3084 253.0516 254.3600 265.5075 455.5738 -1.3093 253.2734 254.5827 265.7553 457.1714 -1.3118 253.4850 254.7968 266.0006 458.7744 -1.3142 253.6856 254.9997 266.2489 460.3978 -1.3166 253.9020 255.2186 266.5017 462.0006 -1.3177 254.1139 255.4316 266.7544 463.5985 -1.3188 254.3283 255.6471 267.0001 465.2116 -1.3205 254.5497 255.8702 267.2504 466.8145 -1.3237 254.7603 256.0840 267.4958 468.4175 -1.3258 254.9706 256.2963 267.7303 470.0256 -1.3275 255.1806 256.5081 267.9636 471.6491 -1.3307 255.3921 256.7228 268.2017 473.2520 -1.3332 255.6070 256.9402 268.4326 474.8655 -1.3344 255.8203 257.1547 268.6644 476.4681 -1.3355 256.0292 257.3647 268.8982 478.0814 -1.3373 256.2432 257.5805 269.1281 479.6843 -1.3396 256.4557 257.7953 269.3481 481.2921 -1.3416 256.6749 258.0165 269.5667 482.9158 -1.3433 256.8952 258.2384 269.7788 484.5186 -1.3445 257.1138 258.4583 269.9864 486.1318 -1.3463 257.3335 258.6797 270.2090 487.7348 -1.3486 257.5455 258.8941 270.4192 489.3324 -1.3512 257.7567 259.1078 270.6309 490.9456 -1.3547 257.9709 259.3256 270.8333 492.5431 -1.3573 258.1911 259.5483 271.0380 494.1356 -1.3611 258.4090 259.7701 271.2356 495.7591 -1.3635 258.6287 259.9922 271.4298 497.3566 -1.3656 258.8422 260.2078 271.6171 498.9699 -1.3679 259.0560 260.4239 271.8090 500.5725 -1.3697 259.2748 260.6445 271.9941 502.1806 -1.3717 259.4916 260.8632 272.1751 503.7785 -1.3737 259.7092 261.0829 272.3530 505.3814 -1.3747 259.9309 261.3056 272.5289 506.9945 -1.3762 260.1477 261.5239 272.7098 508.6129 -1.3794 260.3643 261.7437 272.8895 510.2208 -1.3820 260.5840 261.9660 273.0655 511.8291 -1.3842 260.8100 262.1943 273.2350 513.4320 -1.3867 261.0248 262.4115 273.4060 515.0451 -1.3883 261.2467 262.6350 273.5831 516.6533 -1.3907 261.4690 262.8597 273.7598 518.2666 -1.3924 261.6862 263.0786 273.9354 519.8901 -1.3935 261.9082 263.3018 274.1107 521.4723 -1.3952 262.1294 263.5246 274.2880 523.0700 -1.3958 262.3499 263.7457 274.4592 524.6729 -1.3964 262.5630 263.9594 274.6401 526.2861 -1.3989 262.7752 264.1742 274.8144 527.8838 -1.4004 262.9869 264.3873 274.9870 529.4968 -1.4029 263.2093 264.6122 275.1652 531.0996 -1.4053 263.4324 264.8377 275.3465 532.7230 -1.4073 263.6476 265.0549 275.5320 534.3311 -1.4087 263.8635 265.2722 275.7255 535.9391 -1.4104 264.0844 265.4948 275.9173 537.5471 -1.4138 264.3047 265.7185 276.1150 539.1501 -1.4167 264.5169 265.9336 276.3106 540.7633 -1.4193 264.7366 266.1559 276.5049 542.3509 -1.4224 264.9513 266.3738 276.7062 543.9640 -1.4246 265.1704 266.5950 276.9068 545.5876 -1.4277 265.3887 266.8164 277.1100 547.1958 -1.4301 265.6062 267.0363 277.3179 548.8040 -1.4325 265.8203 267.2528 277.5311 550.4121 -1.4357 266.0344 267.4702 277.7438 552.0151 -1.4380 266.2564 267.6943 277.9647 553.6128 -1.4414 266.4784 267.9198 278.1901 555.2209 -1.4456 266.6997 268.1453 278.4117 556.8393 -1.4483 266.9229 268.3712 278.6423 558.4420 -1.4516 267.1363 268.5879 278.8674 560.0499 -1.4548 267.3549 268.8097 279.0976 561.6530 -1.4579 267.5754 269.0333 279.3301 563.2559 -1.4607 267.7910 269.2518 279.5726 564.8690 -1.4640 268.0077 269.4717 279.8078 566.4720 -1.4681 268.2283 269.6965 280.0475 568.0958 -1.4713 268.4508 269.9221 280.2922 569.7036 -1.4744 268.6686 270.1430 280.5373 571.3066 -1.4781 268.8819 270.3599 280.7889 572.9200 -1.4805 269.0876 270.5681 281.0351 574.5228 -1.4839 269.3032 270.7871 281.2758 576.1360 -1.4871 269.5250 271.0121 281.5274 577.7390 -1.4902 269.7394 271.2295 281.7674 579.3626 -1.4938 269.9618 271.4556 282.0173 580.9709 -1.4978 270.1813 271.6791 282.2597 582.5739 -1.5011 270.3971 271.8982 282.4976 584.1871 -1.5054 270.6198 272.1251 282.7370 585.7901 -1.5096 270.8347 272.3443 282.9812 587.3878 -1.5141 271.0460 272.5601 283.2216 588.9908 -1.5184 271.2678 272.7862 283.4554 590.5834 -1.5218 271.4944 273.0162 283.6835 592.2018 -1.5245 271.7193 273.2438 283.9196 593.8099 -1.5286 271.9366 273.4652 284.1570 595.4129 -1.5323 272.1527 273.6850 284.3849 597.0260 -1.5364 272.3791 273.9155 284.6190 598.6288 -1.5399 272.5995 274.1395 284.8456 600.2366 -1.5439 272.8189 274.3628 285.0646 601.8449 -1.5471 273.0446 274.5917 285.2842 603.4685 -1.5508 273.2708 274.8216 285.5043 605.0765 -1.5541 273.4912 275.0452 285.7204 606.6795 -1.5570 273.7113 275.2683 285.9303 608.2926 -1.5603 273.9356 275.4959 286.1461 609.8954 -1.5630 274.1620 275.7249 286.3710 611.5034 -1.5658 274.3896 275.9554 286.5847 613.1114 -1.5693 274.6165 276.1858 286.7874 614.7351 -1.5745 274.8359 276.4104 286.9885 616.3328 -1.5778 275.0535 276.6313 287.1749 617.9305 -1.5812 275.2759 276.8571 287.3621 619.5281 -1.5850 275.4984 277.0834 287.5487 621.1414 -1.5881 275.7266 277.3146 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