DTA measure 3Gyors Date: 2025311:1130 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.41 s Mass = 923.900 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3734 -5.0479 436.7856 441.8335 419.7150 3.9805 -5.0521 436.8376 441.8897 419.7522 5.6031 -5.0574 436.8819 441.9393 419.8215 7.2103 -5.0640 436.9330 441.9971 419.9265 8.8176 -5.0697 436.9715 442.0412 420.0593 10.4194 -5.0755 437.0051 442.0805 420.2260 12.0316 -5.0834 437.0395 442.1229 420.4240 13.6338 -5.0929 437.0758 442.1687 420.6417 15.2408 -5.1033 437.1034 442.2067 420.8838 16.8635 -5.1154 437.1350 442.2504 421.1470 18.4759 -5.1259 437.1652 442.2911 421.4047 20.0831 -5.1369 437.1908 442.3277 421.6722 21.6901 -5.1483 437.2200 442.3683 421.9437 23.2975 -5.1594 437.2455 442.4049 422.2058 24.9041 -5.1717 437.2708 442.4424 422.4683 26.5064 -5.1843 437.2986 442.4829 422.7153 28.1290 -5.1976 437.3283 442.5258 422.9611 29.7156 -5.2104 437.3588 442.5691 423.1851 31.3126 -5.2222 437.3851 442.6073 423.3879 32.9248 -5.2349 437.4139 442.6489 423.5777 34.5268 -5.2481 437.4445 442.6926 423.7419 36.1336 -5.2609 437.4777 442.7386 423.8833 37.7409 -5.2739 437.5057 442.7797 424.0012 39.3375 -5.2856 437.5327 442.8183 424.0839 40.9448 -5.2973 437.5615 442.8589 424.1453 42.5673 -5.3087 437.5950 442.9037 424.1827 44.1691 -5.3199 437.6271 442.9470 424.1934 45.7819 -5.3301 437.6583 442.9884 424.1774 47.3841 -5.3391 437.6921 443.0312 424.1253 48.9966 -5.3484 437.7251 443.0736 424.0454 50.5934 -5.3581 437.7602 443.1183 423.9470 52.2056 -5.3665 437.7902 443.1568 423.8142 53.8128 -5.3735 437.8191 443.1926 423.6603 55.4355 -5.3812 437.8476 443.2288 423.4801 57.0428 -5.3870 437.8797 443.2667 423.2763 58.6241 -5.3923 437.9077 443.3000 423.0524 60.2313 -5.3982 437.9339 443.3321 422.8100 61.8334 -5.4029 437.9595 443.3624 422.5471 63.4354 -5.4077 437.9859 443.3935 422.2627 65.0374 -5.4105 438.0065 443.4170 421.9556 66.6445 -5.4144 438.0237 443.4382 421.6330 68.2464 -5.4170 438.0381 443.4551 421.3063 69.8539 -5.4191 438.0574 443.4765 420.9538 71.4610 -5.4214 438.0748 443.4962 420.5857 73.0685 -5.4219 438.0904 443.5123 420.2060 74.6756 -5.4221 438.1004 443.5225 419.8086 76.2624 -5.4233 438.0979 443.5212 419.4018 77.8901 -5.4235 438.0946 443.5182 418.9879 79.4766 -5.4221 438.0910 443.5132 418.5735 81.0838 -5.4215 438.0933 443.5148 418.1411 82.7066 -5.4197 438.0849 443.5045 417.7016 84.3191 -5.4179 438.0744 443.4922 417.2587 85.9261 -5.4153 438.0599 443.4752 416.8090 87.5335 -5.4138 438.0401 443.4539 416.3613 89.1406 -5.4120 438.0171 443.4291 415.9174 90.7480 -5.4084 437.9980 443.4064 415.4652 92.3293 -5.4051 437.9634 443.3685 415.0275 93.9369 -5.4024 437.9283 443.3307 414.5874 95.5598 -5.3992 437.8931 443.2923 414.1433 97.1564 -5.3963 437.8557 443.2519 413.7090 98.7638 -5.3940 437.8126 443.2065 413.2719 100.3658 -5.3903 437.7635 443.1538 412.8442 101.9680 -5.3868 437.7066 443.0934 412.4303 103.5803 -5.3830 437.6447 443.0276 412.0205 105.1823 -5.3805 437.5840 442.9645 411.6160 106.8049 -5.3777 437.5134 442.8911 411.2183 108.4120 -5.3762 437.4424 442.8185 410.8351 110.0140 -5.3740 437.3640 442.7379 410.4643 111.6264 -5.3714 437.2848 442.6562 410.1095 113.2386 -5.3692 437.2030 442.5722 409.7759 114.8458 -5.3670 437.1086 442.4756 409.4451 116.4373 -5.3646 437.0166 442.3812 409.1383 118.0498 -5.3630 436.9165 442.2795 408.8439 119.6726 -5.3618 436.8101 442.1719 408.5565 121.2749 -5.3596 436.7071 442.0667 408.2856 122.8873 -5.3573 436.6029 441.9603 408.0308 124.4841 -5.3563 436.4911 441.8474 407.7996 126.0861 -5.3554 436.3829 441.7383 407.5867 127.6880 -5.3544 436.2743 441.6287 407.3841 129.2954 -5.3543 436.1568 441.5111 407.1948 130.9075 -5.3529 436.0370 441.3899 407.0167 132.5201 -5.3529 435.9150 441.2679 406.8578 134.1221 -5.3536 435.7909 441.1444 406.7102 135.7343 -5.3535 435.6702 441.0237 406.5684 137.3364 -5.3541 435.5402 440.8943 406.4376 138.9431 -5.3562 435.4126 440.7688 406.3240 140.5403 -5.3575 435.2831 440.6406 406.2152 142.1424 -5.3592 435.1519 440.5111 406.1185 143.7598 -5.3615 435.0203 440.3818 406.0295 145.3620 -5.3637 434.8848 440.2485 405.9493 146.9745 -5.3664 434.7503 440.1166 405.8717 148.5766 -5.3681 434.6192 439.9874 405.8101 150.1891 -5.3709 434.4768 439.8477 405.7489 151.8014 -5.3741 434.3276 439.7017 405.6870 153.4034 -5.3772 434.1850 439.5622 405.6246 155.0105 -5.3801 434.0407 439.4208 405.5646 156.5918 -5.3834 433.9033 439.2867 405.5126 158.2095 -5.3851 433.7611 439.1463 405.4701 159.8166 -5.3878 433.6212 439.0089 405.4104 161.4186 -5.3906 433.4798 438.8705 405.3500 163.0310 -5.3930 433.3509 438.7439 405.2837 164.6276 -5.3952 433.2209 438.6161 405.2154 166.2245 -5.3970 433.0823 438.4793 405.1413 167.8263 -5.3994 432.9496 438.3490 405.0663 169.4386 -5.4015 432.8159 438.2174 404.9855 171.0565 -5.4039 432.6759 438.0798 404.8857 172.6639 -5.4056 432.5287 437.9343 404.7741 174.2710 -5.4084 432.3885 437.7970 404.6541 175.8781 -5.4108 432.2556 437.6664 404.5329 177.4853 -5.4117 432.1187 437.5304 404.4038 179.0976 -5.4125 431.9724 437.3849 404.2630 180.7048 -5.4135 431.8292 437.2428 404.1162 182.2965 -5.4143 431.6920 437.1063 403.9620 183.9193 -5.4149 431.5647 436.9796 403.7982 185.5316 -5.4151 431.4270 436.8422 403.6262 187.1335 -5.4145 431.2906 436.7051 403.4446 188.7303 -5.4153 431.1525 436.5678 403.2564 190.3325 -5.4154 431.0126 436.4279 403.0532 191.9190 -5.4152 430.8759 436.2911 402.8431 193.5261 -5.4139 430.7341 436.1480 402.6201 195.1283 -5.4127 430.5933 436.0060 402.4003 196.7510 -5.4112 430.4439 435.8552 402.1705 198.3584 -5.4091 430.3047 435.7138 401.9406 199.9655 -5.4073 430.1568 435.5641 401.7045 201.5779 -5.4043 430.0106 435.4148 401.4615 203.1696 -5.4021 429.8633 435.2655 401.2119 204.7716 -5.4007 429.7138 435.1145 400.9526 206.3839 -5.3974 429.5679 434.9653 400.6850 207.9961 -5.3938 429.4195 434.8133 400.4133 209.6240 -5.3901 429.2717 434.6618 400.1431 211.2314 -5.3861 429.1183 434.5045 399.8714 212.8281 -5.3833 428.9636 434.3468 399.5887 214.4353 -5.3808 428.8115 434.1923 399.3145 216.0478 -5.3778 428.6625 434.0403 399.0308 217.6601 -5.3751 428.5108 433.8859 398.7445 219.2623 -5.3708 428.3524 433.7232 398.4596 220.8851 -5.3651 428.1899 433.5550 398.1695 222.4818 -5.3612 428.0310 433.3923 397.8789 224.0684 -5.3572 427.8772 433.2345 397.5899 225.6808 -5.3533 427.7202 433.0735 397.2949 227.2878 -5.3488 427.5623 432.9111 396.9984 228.8898 -5.3436 427.4098 432.7534 396.7100 230.4921 -5.3395 427.2505 432.5900 396.4165 232.0838 -5.3352 427.0951 432.4303 396.1284 233.6911 -5.3306 426.9323 432.2629 395.8380 235.3190 -5.3258 426.7646 432.0903 395.5592 236.9056 -5.3216 426.5941 431.9157 395.2888 238.5283 -5.3162 426.4255 431.7417 395.0097 240.1305 -5.3113 426.2593 431.5706 394.7393 241.7433 -5.3073 426.0915 431.3988 394.4693 243.3504 -5.3017 425.9276 431.2294 394.2019 244.9575 -5.2964 425.7606 431.0570 393.9416 246.5699 -5.2924 425.5802 430.8726 393.6842 248.1616 -5.2884 425.4127 430.7010 393.4280 249.7688 -5.2841 425.2410 430.5251 393.1799 251.3914 -5.2786 425.0599 430.3385 392.9346 252.9883 -5.2742 424.8844 430.1586 392.6990 254.5904 -5.2702 424.7105 429.9807 392.4702 256.1874 -5.2656 424.5314 429.7969 392.2414 257.7896 -5.2620 424.3467 429.6087 392.0169 259.3814 -5.2584 424.1619 429.4204 391.8016 260.9833 -5.2547 423.9737 429.2284 391.5873 262.6010 -5.2509 423.7896 429.0405 391.3740 264.2236 -5.2477 423.6008 428.8484 391.1727 265.8201 -5.2449 423.4222 428.6671 390.9809 267.4328 -5.2410 423.2359 428.4768 390.7813 269.0245 -5.2362 423.0493 428.2856 390.5990 270.6319 -5.2319 422.8618 428.0937 390.4179 272.2388 -5.2290 422.6810 427.9100 390.2329 273.8459 -5.2260 422.4932 427.7193 390.0548 275.4530 -5.2223 422.3053 427.5276 389.8840 277.0756 -5.2181 422.1136 427.3317 389.7196 278.6779 -5.2143 421.9285 427.1429 389.5544 280.2904 -5.2109 421.7427 426.9537 389.3927 281.9024 -5.2074 421.5515 426.7588 389.2295 283.5046 -5.2038 421.3555 426.5593 389.0690 285.0964 -5.2005 421.1674 426.3679 388.9147 286.6985 -5.1966 420.9781 426.1747 388.7517 288.3059 -5.1925 420.7836 425.9762 388.5983 289.9080 -5.1883 420.5931 425.7815 388.4436 291.5050 -5.1854 420.4083 425.5937 388.2913 293.1174 -5.1822 420.2197 425.4019 388.1301 294.7195 -5.1789 420.0373 425.2162 387.9746 296.3320 -5.1760 419.8568 425.0328 387.8164 297.9339 -5.1727 419.6796 424.8522 387.6561 299.5410 -5.1690 419.4847 424.6536 387.4942 301.1534 -5.1666 419.2939 424.4605 387.3368 302.7656 -5.1631 419.0987 424.2618 387.1771 304.3726 -5.1601 418.9112 424.0713 387.0169 305.9901 -5.1569 418.7212 423.8782 386.8471 307.5973 -5.1526 418.5285 423.6810 386.6748 309.2044 -5.1491 418.3305 423.4796 386.5076 310.8114 -5.1460 418.1360 423.2820 386.3357 312.4238 -5.1431 417.9402 423.0833 386.1635 314.0155 -5.1384 417.7574 422.8958 385.9894 315.6226 -5.1351 417.5727 422.7078 385.8129 317.2351 -5.1306 417.3845 422.5151 385.6315 318.8320 -5.1272 417.1947 422.3219 385.4438 320.4444 -5.1224 417.0050 422.1274 385.2520 322.0463 -5.1194 416.8243 421.9437 385.0675 323.6433 -5.1169 416.6351 421.7520 384.8743 325.2556 -5.1139 416.4436 421.5575 384.6742 326.8574 -5.1087 416.2573 421.3660 384.4722 328.4804 -5.1035 416.0677 421.1712 384.2700 330.0929 -5.0994 415.8791 420.9785 384.0626 331.6948 -5.0956 415.6935 420.7891 383.8531 333.3073 -5.0917 415.5077 420.5994 383.6342 334.9093 -5.0881 415.3133 420.4015 383.4232 336.5164 -5.0828 415.1190 420.2018 383.2068 338.1238 -5.0773 414.9328 420.0101 382.9839 339.7464 -5.0727 414.7409 419.8136 382.7517 341.3535 -5.0681 414.5509 419.6190 382.5244 342.9658 -5.0619 414.3564 419.4183 382.2912 344.5678 -5.0570 414.1641 419.2211 382.0589 346.1804 -5.0521 413.9763 419.0284 381.8349 347.7824 -5.0472 413.7893 418.8365 381.6058 349.3896 -5.0415 413.6004 418.6419 381.3747 350.9711 -5.0367 413.4109 418.4476 381.1420 352.5939 -5.0322 413.2192 418.2514 380.9049 354.2010 -5.0280 413.0345 418.0625 380.6724 355.7978 -5.0231 412.8424 417.8655 380.4360 357.3946 -5.0181 412.6505 417.6687 380.2025 358.9969 -5.0135 412.4498 417.4633 379.9661 360.6039 -5.0085 412.2503 417.2589 379.7319 362.2114 -5.0034 412.0585 417.0619 379.4966 363.8029 -4.9972 411.8658 416.8630 379.2628 365.4153 -4.9925 411.6701 416.6626 379.0200 367.0379 -4.9871 411.4754 416.4625 378.7816 368.6399 -4.9817 411.2815 416.2632 378.5428 370.2519 -4.9756 411.0813 416.0569 378.3052 371.8436 -4.9701 410.8848 415.8549 378.0665 373.4510 -4.9646 410.6866 415.6512 377.8212 375.0581 -4.9597 410.4861 415.4458 377.5781 376.6653 -4.9542 410.2922 415.2465 377.3333 378.2725 -4.9487 410.0908 415.0395 377.0976 379.8951 -4.9431 409.8873 414.8304 376.8654 381.4974 -4.9375 409.6869 414.6244 376.6335 383.0943 -4.9317 409.4915 414.4232 376.4121 384.6963 -4.9253 409.3013 414.2266 376.1881 386.3086 -4.9191 409.1035 414.0227 375.9575 387.8950 -4.9141 408.9024 413.8165 375.7403 389.5074 -4.9083 408.7043 413.6126 375.5136 391.1148 -4.9029 408.5058 413.4087 375.2946 392.7375 -4.8971 408.2992 413.1962 375.0689 394.3240 -4.8917 408.1071 412.9988 374.8540 395.9364 -4.8853 407.9070 412.7923 374.6359 397.5384 -4.8796 407.7060 412.5855 374.4209 399.1508 -4.8739 407.5096 412.3835 374.2092 400.7525 -4.8682 407.3093 412.1775 374.0022 402.3600 -4.8624 407.1058 411.9682 373.8018 403.9724 -4.8577 406.9035 411.7612 373.5983 405.5951 -4.8526 406.6985 411.5511 373.3855 407.1970 -4.8482 406.4970 411.3452 373.1789 408.8095 -4.8438 406.2961 411.1400 372.9748 410.4166 -4.8390 406.0936 410.9326 372.7675 412.0239 -4.8332 405.8948 410.7280 372.5673 413.6364 -4.8286 405.6903 410.5189 372.3739 415.2486 -4.8246 405.4916 410.3163 372.1816 416.8559 -4.8203 405.2880 410.1083 371.9857 418.4629 -4.8148 405.0889 409.9037 371.7946 420.0546 -4.8085 404.8933 409.7019 371.6084 421.6564 -4.8042 404.6883 409.4925 371.4172 423.2689 -4.7989 404.4810 409.2799 371.2237 424.8709 -4.7943 404.2800 409.0743 371.0381 426.4781 -4.7905 404.0737 408.8641 370.8468 428.1009 -4.7856 403.8693 408.6549 370.6541 429.7083 -4.7810 403.6655 408.4465 370.4663 431.3154 -4.7769 403.4653 408.2422 370.2840 432.9175 -4.7722 403.2715 408.0437 370.0993 434.5296 -4.7670 403.0678 407.8348 369.9069 436.1320 -4.7613 402.8681 407.6294 369.7121 437.7394 -4.7567 402.6703 407.4269 369.5204 439.3621 -4.7508 402.4695 407.2203 369.3317 440.9695 -4.7461 402.2689 407.0150 369.1405 442.5773 -4.7410 402.0661 406.8071 368.9613 444.1794 -4.7364 401.8628 406.5992 368.7769 445.7869 -4.7314 401.6684 406.3998 368.5854 447.3734 -4.7255 401.4735 406.1990 368.3930 448.9758 -4.7211 401.2682 405.9894 368.2014 450.5778 -4.7157 401.0672 405.7829 368.0129 452.2006 -4.7107 400.8650 405.5757 367.8129 453.7975 -4.7062 400.6614 405.3676 367.6208 455.4100 -4.7007 400.4512 405.1519 367.4325 457.0121 -4.6958 400.2471 404.9429 367.2515 458.6244 -4.6914 400.0424 404.7338 367.0564 460.2264 -4.6862 399.8475 404.5337 366.8540 461.8181 -4.6809 399.6438 404.3247 366.6612 463.4255 -4.6761 399.4455 404.1216 366.4646 465.0431 -4.6710 399.2463 403.9172 366.2654 466.6558 -4.6646 399.0420 403.7065 366.0535 468.2576 -4.6591 398.8350 403.4941 365.8483 469.8701 -4.6539 398.6308 403.2847 365.6442 471.4723 -4.6481 398.4289 403.0770 365.4302 473.0844 -4.6426 398.2275 402.8701 365.2195 474.6916 -4.6372 398.0189 402.6561 365.0104 476.3141 -4.6319 397.8157 402.4476 364.8022 477.9160 -4.6271 397.6230 402.2502 364.5893 479.5233 -4.6219 397.4226 402.0444 364.3707 481.1251 -4.6172 397.2264 401.8437 364.1541 482.7274 -4.6122 397.0271 401.6393 363.9404 484.3293 -4.6066 396.8256 401.4322 363.7282 485.9364 -4.6010 396.6245 401.2255 363.5150 487.5538 -4.5947 396.4228 401.0175 363.3001 489.1611 -4.5889 396.2118 400.8007 363.0825 490.7631 -4.5842 396.0041 400.5884 362.8589 492.3755 -4.5799 395.7982 400.3780 362.6433 493.9776 -4.5749 395.5960 400.1709 362.4283 495.5848 -4.5703 395.3931 399.9634 362.2113 497.1920 -4.5658 395.2027 399.7684 361.9901 498.8200 -4.5612 394.9958 399.5570 361.7663 500.4116 -4.5547 394.7887 399.3435 361.5528 502.0343 -4.5499 394.5818 399.1317 361.3267 503.6361 -4.5448 394.3774 398.9221 361.1070 505.2486 -4.5399 394.1809 398.7208 360.8874 506.8509 -4.5341 393.9778 398.5119 360.6666 508.4629 -4.5286 393.7695 398.2981 360.4458 510.0855 -4.5226 393.5595 398.0821 360.2175 511.6723 -4.5167 393.3585 397.8752 359.9963 513.2691 -4.5106 393.1623 397.6729 359.7800 514.8761 -4.5046 392.9584 397.4630 359.5620 516.4783 -4.4978 392.7554 397.2532 359.3490 518.0804 -4.4924 392.5564 397.0488 359.1326 519.6926 -4.4862 392.3519 396.8381 358.9157 521.2894 -4.4809 392.1500 396.6308 358.7011 522.9121 -4.4748 391.9463 396.4211 358.4915 524.5140 -4.4691 391.7452 396.2144 358.2780 526.1420 -4.4630 391.5386 396.0017 358.0533 527.7440 -4.4565 391.3436 395.8001 357.8323 529.3565 -4.4498 391.1400 395.5898 357.6145 530.9588 -4.4432 390.9371 395.3803 357.3940 532.5865 -4.4381 390.7270 395.1651 357.1763 534.1938 -4.4329 390.5231 394.9560 356.9623 535.8010 -4.4277 390.3175 394.7452 356.7450 537.4031 -4.4215 390.1124 394.5339 356.5275 539.0156 -4.4168 389.9098 394.3266 356.3137 540.6228 -4.4121 389.7080 394.1201 356.0986 542.2299 -4.4063 389.5072 393.9135 355.8870 543.8114 -4.4002 389.3050 393.7053 355.6787 545.4236 -4.3943 389.0966 393.4909 355.4703 547.0360 -4.3883 388.8943 393.2826 355.2577 548.6383 -4.3823 388.6961 393.0784 355.0482 550.2504 -4.3767 388.4934 392.8701 354.8334 551.8474 -4.3708 388.2872 392.6579 354.6275 553.4599 -4.3647 388.0861 392.4508 354.4137 555.0618 -4.3586 387.8813 392.2399 354.2112 556.6844 -4.3527 387.6664 392.0191 354.0080 558.2916 -4.3473 387.4591 391.8064 353.8090 559.8989 -4.3421 387.2529 391.5950 353.6060 561.5113 -4.3367 387.0482 391.3849 353.4125 563.1135 -4.3325 386.8494 391.1819 353.2096 564.7204 -4.3279 386.6465 390.9744 352.9991 566.3275 -4.3229 386.4467 390.7696 352.7924 567.9453 -4.3164 386.2401 390.5565 352.5832 569.5575 -4.3109 386.0355 390.3464 352.3757 571.1699 -4.3063 385.8249 390.1312 352.1694 572.7720 -4.3027 385.6177 389.9203 351.9663 574.3845 -4.2974 385.4073 389.7048 351.7589 575.9656 -4.2922 385.2096 389.5018 351.5613 577.5676 -4.2869 385.0084 389.2953 351.3648 579.1748 -4.2818 384.8010 389.0828 351.1662 580.7924 -4.2763 384.5919 388.8681 350.9645 582.3993 -4.2720 384.3839 388.6559 350.7598 584.0014 -4.2669 384.1710 388.4379 350.5608 585.5984 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