DTA measure 1meres_1 Date: 202541:1553 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.41 s Mass = 1178.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1420 -1.2651 220.4931 221.7583 261.3094 1.9900 -1.2635 220.6817 221.9452 261.3326 2.7480 -1.2570 220.8443 222.1013 261.3266 3.5660 -1.2526 221.0037 222.2564 261.3178 4.3840 -1.2518 221.1737 222.4255 261.2890 5.1420 -1.2476 221.3444 222.5921 261.3042 5.9905 -1.2394 221.5254 222.7647 261.3119 6.7490 -1.2381 221.6714 222.9094 261.3395 7.5678 -1.2369 221.8290 223.0659 261.3480 8.3863 -1.2312 222.0282 223.2594 261.3881 9.1460 -1.2241 222.1859 223.4100 261.4217 9.9945 -1.2168 222.3455 223.5623 261.4405 10.7830 -1.2132 222.5326 223.7458 261.4944 11.5733 -1.2127 222.6666 223.8792 261.5358 12.3923 -1.2125 222.8363 224.0488 261.6102 13.1528 -1.2075 222.9914 224.1989 261.6667 14.0045 -1.2033 223.1561 224.3594 261.7544 14.7658 -1.2000 223.3099 224.5099 261.8147 15.5875 -1.1970 223.4586 224.6556 261.8990 16.4095 -1.1957 223.6329 224.8285 261.9889 17.1710 -1.1905 223.7869 224.9774 262.0923 18.0225 -1.1871 223.9608 225.1480 262.2156 18.7845 -1.1829 224.1363 225.3192 262.3051 19.6058 -1.1794 224.2843 225.4637 262.4269 20.4280 -1.1759 224.4549 225.6308 262.5714 21.1900 -1.1732 224.5986 225.7718 262.6885 22.0420 -1.1684 224.7669 225.9353 262.8238 22.8038 -1.1692 224.9078 226.0770 262.9629 23.6258 -1.1659 225.0905 226.2565 263.1135 24.4180 -1.1654 225.2523 226.4177 263.2773 25.2095 -1.1614 225.4055 226.5669 263.4028 26.0620 -1.1598 225.5568 226.7165 263.5719 26.8238 -1.1569 225.7256 226.8825 263.7375 27.6458 -1.1539 225.8924 227.0463 263.9046 28.4380 -1.1510 226.0622 227.2132 264.0751 29.2295 -1.1508 226.2160 227.3669 264.2638 30.0820 -1.1516 226.3720 227.5236 264.4379 30.8438 -1.1505 226.5117 227.6622 264.5914 31.6658 -1.1503 226.6841 227.8344 264.7842 32.4580 -1.1472 226.8316 227.9788 264.9693 33.2495 -1.1426 226.9877 228.1303 265.1491 34.1018 -1.1405 227.1632 228.3038 265.3593 34.8635 -1.1428 227.3237 228.4665 265.5297 35.6858 -1.1428 227.4775 228.6203 265.7202 36.4778 -1.1410 227.6308 228.7718 265.9118 37.2695 -1.1429 227.7811 228.9240 266.1205 38.1218 -1.1427 227.9689 229.1116 266.2995 38.8835 -1.1414 228.1064 229.2477 266.4939 39.7058 -1.1375 228.2615 229.3991 266.6509 40.5278 -1.1369 228.4204 229.5573 266.8640 41.2895 -1.1389 228.5762 229.7151 267.0300 42.1415 -1.1393 228.7463 229.8855 267.2363 42.9035 -1.1413 228.8882 230.0295 267.3994 43.7255 -1.1392 229.0548 230.1940 267.5708 44.5475 -1.1399 229.2267 230.3666 267.7438 45.3113 -1.1410 229.3758 230.5168 267.9146 46.1635 -1.1433 229.5351 230.6784 268.1010 46.9555 -1.1433 229.6795 230.8228 268.2816 47.7485 -1.1415 229.8252 230.9667 268.4574 48.5705 -1.1422 229.9820 231.1242 268.6131 49.3325 -1.1403 230.1453 231.2856 268.7620 50.1858 -1.1419 230.3053 231.4473 268.9279 50.9785 -1.1418 230.4740 231.6158 269.1148 51.7700 -1.1421 230.6459 231.7880 269.2573 52.5923 -1.1455 230.7765 231.9220 269.4007 53.3535 -1.1457 230.9417 232.0874 269.5392 54.2060 -1.1456 231.1033 232.2489 269.6881 54.9980 -1.1450 231.2535 232.3985 269.8271 55.7895 -1.1401 231.4104 232.5505 269.9751 56.6120 -1.1496 231.5806 232.7303 270.1246 57.4038 -1.1608 231.7079 232.8687 270.2554 58.2258 -1.1635 231.8631 233.0266 270.3803 59.0180 -1.1663 232.0168 233.1831 270.5326 59.8070 -1.1692 232.1668 233.3361 270.6418 60.6550 -1.1649 232.3496 233.5145 270.7823 61.4130 -1.1662 232.5001 233.6663 270.8976 62.2313 -1.1664 232.6469 233.8134 271.0073 63.0190 -1.1664 232.8046 233.9711 271.1248 63.8070 -1.1669 232.9516 234.1185 271.2481 64.6553 -1.1677 233.1145 234.2822 271.3529 65.4133 -1.1699 233.2648 234.4347 271.4639 66.2310 -1.1694 233.4326 234.6019 271.5641 67.0498 -1.1673 233.5777 234.7451 271.7058 67.8080 -1.1693 233.7289 234.8982 271.7920 68.6570 -1.1681 233.8923 235.0604 271.8972 69.4153 -1.1696 234.0420 235.2115 271.9846 70.2350 -1.1700 234.1966 235.3665 272.0943 71.0538 -1.1668 234.3710 235.5378 272.2002 71.8120 -1.1592 234.5000 235.6592 272.2887 72.6618 -1.1548 234.6615 235.8162 272.4062 73.4500 -1.1557 234.8214 235.9771 272.5261 74.2405 -1.1580 234.9801 236.1381 272.6228 75.0613 -1.1566 235.1377 236.2943 272.7088 75.8213 -1.1573 235.2635 236.4207 272.8223 76.6718 -1.1577 235.4398 236.5975 272.9208 77.4620 -1.1583 235.5967 236.7550 273.0289 78.2525 -1.1557 235.7542 236.9099 273.1386 79.0748 -1.1571 235.8890 237.0461 273.2552 79.8360 -1.1595 236.0532 237.2127 273.3489 80.6880 -1.1624 236.2069 237.3694 273.4592 81.4795 -1.1619 236.3598 237.5218 273.5739 82.2888 -1.1646 236.5100 237.6746 273.6983 83.0818 -1.1604 236.6567 237.8172 273.8234 83.8735 -1.1605 236.8038 237.9643 273.9372 84.6955 -1.1629 236.9649 238.1278 274.0512 85.4875 -1.1599 237.1069 238.2668 274.1594 86.3098 -1.1617 237.2446 238.4063 274.2826 87.1018 -1.1624 237.4076 238.5700 274.4075 87.8935 -1.1646 237.5745 238.7391 274.5205 88.7155 -1.1652 237.7198 238.8849 274.6485 89.4775 -1.1635 237.8620 239.0255 274.7513 90.3295 -1.1644 238.0274 239.1918 274.8872 91.1218 -1.1647 238.1590 239.3237 275.0236 91.9135 -1.1693 238.3200 239.4892 275.1567 92.7355 -1.1674 238.4570 239.6243 275.2749 93.4975 -1.1703 238.6181 239.7884 275.4059 94.3495 -1.1671 238.7794 239.9465 275.5391 95.1115 -1.1693 238.9284 240.0977 275.6627 95.9335 -1.1721 239.0820 240.2540 275.7846 96.7558 -1.1734 239.2374 240.4108 275.9115 97.5185 -1.1743 239.3710 240.5453 276.0488 98.3705 -1.1747 239.5372 240.7119 276.1847 99.1325 -1.1781 239.6723 240.8505 276.2972 99.9540 -1.1757 239.8256 241.0013 276.4335 100.7465 -1.1771 239.9761 241.1532 276.5613 101.5375 -1.1771 240.1112 241.2883 276.7222 102.3603 -1.1806 240.2844 241.4651 276.8428 103.1518 -1.1816 240.4178 241.5993 276.9881 103.9738 -1.1827 240.5772 241.7599 277.1493 104.7660 -1.1853 240.7203 241.9056 277.2795 105.5575 -1.1842 240.8769 242.0611 277.4035 106.3800 -1.1855 241.0215 242.2070 277.5527 107.1718 -1.1878 241.1841 242.3719 277.7154 107.9938 -1.1906 241.3546 242.5452 277.8492 108.7860 -1.1911 241.4935 242.6847 277.9893 109.5775 -1.1914 241.6341 242.8255 278.1320 110.4000 -1.1892 241.7638 242.9530 278.2829 111.1915 -1.1930 241.9145 243.1075 278.4329 112.0138 -1.1954 242.0725 243.2679 278.5795 112.7858 -1.1962 242.2277 243.4240 278.7291 113.6188 -1.2013 242.3872 243.5886 278.9026 114.4108 -1.2040 242.5304 243.7344 279.0354 115.2025 -1.2070 242.6739 243.8809 279.1870 116.0248 -1.2082 242.8417 244.0499 279.3283 116.8165 -1.2108 242.9802 244.1910 279.4605 117.6388 -1.2134 243.1239 244.3373 279.6214 118.4305 -1.2143 243.2740 244.4883 279.7521 119.2225 -1.2172 243.4067 244.6239 279.9085 120.0445 -1.2177 243.5631 244.7808 280.0526 120.8365 -1.2186 243.7065 244.9251 280.1808 121.6593 -1.2212 243.8499 245.0712 280.3350 122.4515 -1.2228 244.0130 245.2357 280.4809 123.2573 -1.2238 244.1767 245.4006 280.6327 124.0445 -1.2240 244.3125 245.5364 280.7681 124.8335 -1.2235 244.4481 245.6715 280.8943 125.6820 -1.2281 244.6298 245.8579 281.0457 126.4400 -1.2369 244.7721 246.0090 281.1772 127.2580 -1.2364 244.8994 246.1358 281.3169 128.0460 -1.2393 245.0630 246.3023 281.4427 128.8350 -1.2417 245.2000 246.4417 281.5928 129.6830 -1.2435 245.3659 246.6094 281.7482 130.4410 -1.2471 245.4944 246.7415 281.8846 131.2590 -1.2459 245.6332 246.8791 282.0253 132.0470 -1.2497 245.7701 247.0198 282.1517 132.8360 -1.2507 245.9261 247.1768 282.2818 133.6663 -1.2495 246.0694 247.3190 282.3963 134.4560 -1.2497 246.2269 247.4766 282.5566 135.2760 -1.2505 246.3858 247.6362 282.6901 136.0640 -1.2503 246.5165 247.7668 282.8023 136.8530 -1.2525 246.6688 247.9213 282.9293 137.7018 -1.2563 246.8050 248.0613 283.0779 138.4613 -1.2622 246.9561 248.2183 283.1983 139.2825 -1.2642 247.1218 248.3860 283.3435 140.0733 -1.2652 247.2792 248.5444 283.4601 140.8640 -1.2678 247.3933 248.6611 283.5944 141.7155 -1.2700 247.5670 248.8370 283.7216 142.4775 -1.2697 247.7075 248.9773 283.8467 143.2995 -1.2730 247.8548 249.1279 283.9906 144.0905 -1.2719 247.9991 249.2709 284.1068 144.8818 -1.2715 248.1449 249.4164 284.2490 145.7335 -1.2745 248.2825 249.5570 284.3949 146.4955 -1.2759 248.4292 249.7050 284.5321 147.3173 -1.2797 248.5987 249.8784 284.6491 148.1095 -1.2828 248.7575 250.0403 284.7682 148.9013 -1.2849 248.8785 250.1634 284.9043 149.7230 -1.2849 249.0206 250.3055 285.0247 150.5150 -1.2861 249.1802 250.4663 285.1385 151.3370 -1.2880 249.3252 250.6132 285.2675 152.1290 -1.2905 249.4688 250.7593 285.4216 152.9208 -1.2922 249.6168 250.9090 285.5390 153.7430 -1.2937 249.7702 251.0639 285.6722 154.5348 -1.2981 249.9080 251.2061 285.7812 155.3568 -1.2999 250.0609 251.3608 285.9234 156.1490 -1.2995 250.2108 251.5103 286.0451 156.9405 -1.3020 250.3544 251.6564 286.1510 157.7630 -1.3042 250.5068 251.8110 286.2831 158.5548 -1.3058 250.6495 251.9553 286.4331 159.3768 -1.3062 250.8081 252.1143 286.5556 160.1690 -1.3084 250.9339 252.2424 286.6671 160.9605 -1.3112 251.0936 252.4048 286.8025 161.8128 -1.3125 251.2437 252.5562 286.9331 162.5748 -1.3176 251.3781 252.6958 287.0456 163.3968 -1.3191 251.5174 252.8365 287.1624 164.1890 -1.3205 251.6615 252.9820 287.2884 164.9805 -1.3240 251.8029 253.1270 287.3902 165.8328 -1.3274 251.9717 253.2992 287.5516 166.5945 -1.3308 252.1083 253.4390 287.6436 167.4168 -1.3331 252.2525 253.5857 287.7621 168.2388 -1.3358 252.4022 253.7380 287.8989 169.0005 -1.3388 252.5624 253.9013 288.0257 169.8525 -1.3405 252.6907 254.0312 288.1698 170.6145 -1.3435 252.8213 254.1648 288.2791 171.4365 -1.3439 252.9843 254.3282 288.4148 172.2585 -1.3410 253.1426 254.4837 288.5284 173.0205 -1.3486 253.2682 254.6169 288.6642 173.8725 -1.3474 253.4158 254.7631 288.7837 174.6645 -1.3455 253.5592 254.9047 288.8996 175.4565 -1.3480 253.7084 255.0564 289.0079 176.2785 -1.3517 253.8545 255.2062 289.1328 177.0403 -1.3540 253.9978 255.3518 289.2584 177.8925 -1.3539 254.1435 255.4975 289.3990 178.6845 -1.3601 254.2873 255.6473 289.5164 179.4760 -1.3593 254.4330 255.7923 289.6435 180.2983 -1.3639 254.5837 255.9477 289.7979 181.0898 -1.3629 254.7561 256.1191 289.8980 181.9118 -1.3603 254.9120 256.2724 290.0258 182.7040 -1.3657 255.0071 256.3728 290.1457 183.4955 -1.3673 255.1461 256.5134 290.2801 184.3480 -1.3684 255.3205 256.6888 290.4143 185.1098 -1.3692 255.4640 256.8332 290.5480 185.9318 -1.3729 255.5966 256.9695 290.6724 186.7240 -1.3772 255.7547 257.1319 290.7993 187.5155 -1.3809 255.8840 257.2649 290.9417 188.3678 -1.3817 256.0485 257.4302 291.0860 189.1263 -1.3837 256.1816 257.5653 291.2206 189.9440 -1.3876 256.3381 257.7256 291.3765 190.7325 -1.3894 256.4735 257.8629 291.5041 191.5210 -1.3912 256.6172 258.0084 291.6281 192.3393 -1.3972 256.7663 258.1634 291.7574 193.1270 -1.3984 256.9201 258.3185 291.8957 193.9450 -1.4000 257.0527 258.4527 292.0468 194.7085 -1.4008 257.1844 258.5852 292.1704 195.5360 -1.4044 257.3278 258.7322 292.3004 196.3540 -1.4040 257.4786 258.8826 292.4397 197.1120 -1.4051 257.6264 259.0315 292.5815 197.9600 -1.4113 257.7877 259.1991 292.7404 198.7180 -1.4159 257.9240 259.3399 292.8660 199.5360 -1.4168 258.0695 259.4863 292.9864 200.3543 -1.4163 258.1917 259.6080 293.1413 201.1130 -1.4208 258.3437 259.7645 293.2708 201.9628 -1.4232 258.5028 259.9260 293.4181 202.7513 -1.4262 258.6418 260.0680 293.5537 203.5415 -1.4303 258.7809 260.2112 293.6791 204.3613 -1.4314 258.8986 260.3301 293.8307 205.1218 -1.4342 259.0555 260.4898 293.9730 205.9728 -1.4339 259.2208 260.6547 294.1241 206.7628 -1.4344 259.3660 260.8003 294.2717 207.5535 -1.4393 259.5084 260.9477 294.3863 208.3758 -1.4439 259.6478 261.0917 294.5423 209.1375 -1.4503 259.7857 261.2360 294.6829 209.9895 -1.4519 259.9404 261.3923 294.7990 210.7518 -1.4561 260.0538 261.5099 294.9276 211.5738 -1.4534 260.2128 261.6662 295.0747 212.3655 -1.4542 260.3584 261.8126 295.2034 213.1575 -1.4560 260.5047 261.9607 295.3505 213.9798 -1.4604 260.6283 262.0887 295.5055 214.7728 -1.4631 260.7711 262.2342 295.6397 215.5995 -1.4636 260.9312 262.3947 295.7787 216.3915 -1.4649 261.0792 262.5441 295.9146 217.1835 -1.4692 261.2359 262.7051 296.0534 218.0055 -1.4731 261.3555 262.8286 296.2080 218.7675 -1.4758 261.5107 262.9865 296.3307 219.6195 -1.4759 261.6627 263.1386 296.4912 220.3815 -1.4782 261.7987 263.2768 296.6072 221.2035 -1.4837 261.9446 263.4284 296.7517 221.9955 -1.4852 262.1019 263.5871 296.8899 222.7875 -1.4888 262.2382 263.7269 297.0084 223.6395 -1.4895 262.3875 263.8769 297.1597 224.4015 -1.4906 262.5128 264.0034 297.2787 225.2235 -1.4969 262.6660 264.1629 297.4244 226.0155 -1.4997 262.8045 264.3041 297.5644 226.8075 -1.4975 262.9434 264.4409 297.7046 227.6595 -1.5016 263.1192 264.6208 297.8195 228.4213 -1.5023 263.2422 264.7446 297.9508 229.2428 -1.5057 263.3923 264.8981 298.0856 230.0355 -1.5098 263.5215 265.0313 298.1797 230.8270 -1.5117 263.6731 265.1847 298.3050 231.6790 -1.5151 263.8483 265.3634 298.4399 232.4408 -1.5167 263.9748 265.4915 298.5454 233.2628 -1.5190 264.1074 265.6264 298.6867 234.0550 -1.5202 264.2442 265.7644 298.8247 234.8465 -1.5235 264.3877 265.9111 298.9468 235.7040 -1.5257 264.5446 266.0703 299.0570 236.4375 -1.5290 264.6661 266.1951 299.1463 237.2900 -1.5296 264.8243 266.3538 299.2803 238.0820 -1.5313 264.9666 266.4980 299.4049 238.8735 -1.5311 265.1301 266.6613 299.5289 239.6960 -1.5306 265.2770 266.8077 299.6379 240.4575 -1.5422 265.4176 266.9598 299.7738 241.3100 -1.5418 265.5667 267.1084 299.8891 242.1018 -1.5427 265.6919 267.2346 300.0040 242.8935 -1.5459 265.8521 267.3980 300.1097 243.7158 -1.5483 265.9886 267.5369 300.2442 244.5075 -1.5494 266.1258 267.6753 300.3676 245.3308 -1.5519 266.2729 267.8249 300.4999 246.1238 -1.5532 266.4176 267.9709 300.6552 246.9165 -1.5562 266.5421 268.0983 300.7569 247.7385 -1.5599 266.6809 268.2408 300.8793 248.5305 -1.5655 266.8474 268.4128 301.0033 249.3525 -1.5659 266.9760 268.5419 301.1304 250.1445 -1.5663 267.1375 268.7038 301.2453 250.9375 -1.5649 267.2808 268.8457 301.3733 251.7595 -1.5672 267.4120 268.9793 301.5036 252.5500 -1.5699 267.5573 269.1272 301.6233 253.3678 -1.5716 267.6901 269.2617 301.7438 254.1558 -1.5740 267.8288 269.4029 301.8707 254.9438 -1.5781 267.9848 269.5629 302.0234 255.7658 -1.5776 268.1384 269.7160 302.1665 256.5350 -1.5798 268.2719 269.8517 302.2719 257.3840 -1.5814 268.4310 270.0124 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