DTA measure 1gyors Date: 2024108:158 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.47 s Mass = 1305.100 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0918 -1.1329 225.6412 226.7741 259.1119 1.9138 -1.1121 225.8345 226.9466 259.0298 2.7350 -1.1259 225.9975 227.1234 259.1053 3.4965 -1.1255 226.0742 227.1997 259.1778 4.3495 -1.0917 226.2146 227.3063 259.1866 5.1115 -1.0837 226.3561 227.4398 259.2365 5.9338 -1.0738 226.5298 227.6036 259.0981 6.7278 -1.0756 226.6430 227.7186 259.0735 7.5195 -1.0762 226.7763 227.8525 259.1954 8.3718 -1.0804 226.8512 227.9316 259.1751 9.1343 -1.0641 226.9823 228.0463 259.2045 9.9578 -1.0879 227.1283 228.2162 259.2065 10.7525 -1.0874 227.2759 228.3633 259.2645 11.5485 -1.0651 227.3919 228.4570 259.2997 12.3715 -1.0493 227.5178 228.5671 259.3536 13.1345 -1.0347 227.6240 228.6587 259.3446 13.9865 -1.0625 227.8352 228.8978 259.5117 14.7785 -1.0702 227.9715 229.0418 259.5705 15.5705 -1.0615 228.1537 229.2152 259.6634 16.3930 -1.0518 228.2455 229.2973 259.7271 17.1555 -1.0441 228.3909 229.4349 259.8412 18.0075 -1.0585 228.4377 229.4962 259.9786 18.7995 -1.0438 228.5468 229.5906 259.9809 19.5915 -1.0346 228.6612 229.6958 260.0834 20.4130 -1.0180 228.8711 229.8892 260.2633 21.1983 -1.0199 228.9731 229.9930 260.4233 22.0188 -1.0417 229.0651 230.1068 260.5514 22.8370 -1.0237 229.1627 230.1863 260.6920 23.5950 -1.0101 229.2341 230.2442 260.7858 24.4440 -1.0005 229.4694 230.4699 260.9559 25.2020 -1.0015 229.6155 230.6170 261.1317 26.0200 -1.0015 229.6832 230.6847 261.1795 26.8383 -1.0097 229.8498 230.8594 261.4861 27.5970 -1.0094 229.9868 230.9962 261.5767 28.4455 -1.0075 230.0980 231.1055 261.7762 29.2340 -1.0099 230.2027 231.2126 261.9927 30.0230 -1.0129 230.4060 231.4188 262.1678 30.8420 -1.0042 230.4573 231.4614 262.3217 31.6328 -1.0120 230.5868 231.5988 262.4214 32.4535 -1.0257 230.7828 231.8085 262.6259 33.2460 -1.0298 230.8850 231.9147 262.7691 34.0385 -1.0330 230.9362 231.9692 262.8615 34.8605 -1.0139 231.1236 232.1375 263.2127 35.6225 -1.0165 231.2213 232.2378 263.3637 36.4758 -1.0205 231.3027 232.3231 263.5483 37.2675 -1.0090 231.3993 232.4083 263.6446 38.0595 -1.0126 231.5701 232.5826 263.8077 38.8823 -1.0032 231.6428 232.6460 264.0488 39.6445 -1.0141 231.8557 232.8697 264.1959 40.4965 -1.0145 232.0183 233.0328 264.4198 41.2385 -1.0224 232.1256 233.1480 264.6780 42.1085 -1.0194 232.3082 233.3276 264.8468 42.9005 -1.0303 232.3713 233.4016 264.9548 43.6925 -1.0222 232.5276 233.5498 265.2359 44.5145 -1.0176 232.7325 233.7502 265.4395 45.2765 -1.0119 232.7127 233.7246 265.5087 46.1285 -1.0212 232.9019 233.9230 265.7637 46.8910 -1.0325 233.0548 234.0873 265.8585 47.7145 -1.0400 233.1603 234.2004 265.9680 48.5363 -1.0506 233.3234 234.3740 266.1743 49.2980 -1.0533 233.3816 234.4349 266.2908 50.1500 -1.0483 233.6023 234.6507 266.4533 50.9120 -1.0519 233.6538 234.7056 266.6340 51.7348 -1.0604 233.7585 234.8190 266.8042 52.5533 -1.0513 233.9769 235.0282 267.0314 53.3130 -1.0450 234.0751 235.1201 267.1028 54.1635 -1.0437 234.2202 235.2639 267.2141 54.9223 -1.0519 234.3324 235.3843 267.3021 55.7403 -1.0553 234.5424 235.5977 267.5184 56.5288 -1.0576 234.6839 235.7415 267.6580 57.3168 -1.0528 234.7923 235.8451 267.8330 58.1650 -1.0684 234.9180 235.9864 267.9256 58.9230 -1.0638 234.9512 236.0149 268.0471 59.7418 -1.0642 235.1511 236.2153 268.2322 60.5603 -1.0745 235.2836 236.3580 268.3532 61.3190 -1.0754 235.3526 236.4280 268.4794 62.1855 -1.0820 235.4896 236.5715 268.6146 62.9453 -1.0797 235.5827 236.6623 268.7423 63.7663 -1.0608 235.7227 236.7835 268.8371 64.5565 -1.0687 235.8290 236.8978 268.8489 65.3485 -1.0541 236.0201 237.0742 268.9988 66.1720 -1.0768 236.1511 237.2279 269.0845 66.9645 -1.0855 236.1715 237.2569 269.1471 67.7865 -1.0705 236.3682 237.4387 269.2485 68.5785 -1.0587 236.5107 237.5694 269.4279 69.3705 -1.0643 236.6548 237.7191 269.5634 70.1925 -1.0576 236.8042 237.8617 269.6735 70.9845 -1.0706 236.8829 237.9536 269.8003 71.8065 -1.1118 237.1098 238.2215 269.8631 72.6020 -1.1081 237.1914 238.2995 269.9576 73.3953 -1.1047 237.2891 238.3938 270.1056 74.2173 -1.1128 237.4390 238.5517 270.1925 75.0088 -1.0876 237.4925 238.5801 270.2928 75.8308 -1.0743 237.7503 238.8246 270.4244 76.6253 -1.0833 237.8409 238.9243 270.4930 77.4185 -1.1127 237.9028 239.0154 270.5479 78.2410 -1.1203 238.0367 239.1570 270.7669 79.0328 -1.1000 238.2385 239.3384 270.8207 79.8548 -1.0903 238.4327 239.5230 271.0034 80.6480 -1.0920 238.4161 239.5081 271.0623 81.4418 -1.1146 238.5758 239.6904 271.2225 82.3390 -1.1118 238.7716 239.8834 271.3212 83.2670 -1.0882 238.8460 239.9342 271.4855 84.0588 -1.0819 239.0014 240.0833 271.5457 84.8808 -1.0874 239.2104 240.2978 271.7403 85.6658 -1.1022 239.3466 240.4488 271.8576 86.4560 -1.1134 239.4294 240.5428 271.9701 87.2740 -1.0975 239.4626 240.5600 272.1217 88.0320 -1.1119 239.6085 240.7204 272.2860 88.8830 -1.1074 239.7785 240.8859 272.3716 89.6715 -1.1043 240.0275 241.1318 272.5349 90.4590 -1.1032 240.2088 241.3120 272.6764 91.2775 -1.1071 240.1957 241.3028 272.7254 92.0653 -1.1185 240.2540 241.3725 272.8664 92.9065 -1.1271 240.4068 241.5338 273.0109 93.6653 -1.1071 240.5416 241.6488 273.1337 94.4860 -1.1071 240.6869 241.7940 273.2666 95.2758 -1.1449 240.7762 241.9211 273.3598 96.0660 -1.1323 240.9306 242.0629 273.6268 96.9160 -1.1162 241.0609 242.1771 273.7032 97.6768 -1.1132 241.1912 242.3044 273.8729 98.5008 -1.1328 241.3411 242.4740 274.0438 99.2923 -1.1318 241.4450 242.5769 274.1209 100.0835 -1.1250 241.5399 242.6649 274.1727 100.9360 -1.1409 241.6523 242.7932 274.3391 101.6983 -1.1502 241.9038 243.0540 274.5459 102.5218 -1.1595 242.0274 243.1869 274.6598 103.3140 -1.1574 242.1714 243.3287 274.7979 104.1055 -1.1540 242.1556 243.3096 274.8638 104.9580 -1.1253 242.2875 243.4128 275.0567 105.7200 -1.1443 242.5137 243.6580 275.2553 106.5428 -1.1458 242.6143 243.7601 275.2915 107.3350 -1.1501 242.8006 243.9508 275.4293 108.1265 -1.1409 242.8314 243.9723 275.6500 108.9790 -1.1389 243.0554 244.1943 275.6935 109.7410 -1.1375 243.1732 244.3107 275.8252 110.5638 -1.1386 243.3412 244.4799 276.0391 111.3558 -1.1429 243.3866 244.5295 276.1183 112.1475 -1.1476 243.4077 244.5553 276.1690 113.0000 -1.1435 243.5866 244.7301 276.3172 113.7615 -1.1496 243.7978 244.9474 276.4070 114.5838 -1.1524 243.8734 245.0259 276.5796 115.3755 -1.1472 244.0514 245.1987 276.7505 116.1675 -1.1595 244.1567 245.3162 276.9347 117.0193 -1.1642 244.2800 245.4442 277.0672 117.7763 -1.1618 244.4360 245.5978 277.2156 118.5950 -1.1675 244.5502 245.7177 277.2638 119.3823 -1.1747 244.7165 245.8912 277.3683 120.1720 -1.1830 244.8506 246.0336 277.5214 121.0200 -1.1845 244.9854 246.1699 277.7467 121.7780 -1.1734 245.0285 246.2019 277.9037 122.5960 -1.2005 245.1830 246.3835 278.0100 123.3965 -1.1962 245.3596 246.5558 278.1843 124.1910 -1.2227 245.5160 246.7387 278.4031 125.0095 -1.2195 245.6210 246.8405 278.4896 125.7983 -1.1835 245.7255 246.9090 278.6445 126.6175 -1.1809 245.8091 246.9900 278.8015 127.4068 -1.1797 246.0310 247.2106 278.8437 128.1960 -1.1791 246.1502 247.3292 278.9400 129.0450 -1.1822 246.2207 247.4029 279.2095 129.8035 -1.2126 246.3031 247.5157 279.1911 130.6248 -1.2296 246.4113 247.6410 279.2565 131.4180 -1.2277 246.5447 247.7724 279.3884 132.2105 -1.2317 246.6960 247.9277 279.6773 133.0630 -1.2232 246.8532 248.0764 279.7181 133.8248 -1.2430 247.0489 248.2919 279.8405 134.6478 -1.2301 247.1507 248.3808 280.0718 135.4400 -1.2332 247.1862 248.4195 280.1206 136.2315 -1.2148 247.3682 248.5830 280.2516 137.0838 -1.2098 247.5461 248.7559 280.4062 137.8455 -1.2156 247.6334 248.8490 280.5348 138.6675 -1.2212 247.7513 248.9725 280.6219 139.4598 -1.2016 247.9787 249.1803 280.7176 140.2515 -1.2046 248.0502 249.2549 280.9715 141.1035 -1.2203 248.1831 249.4034 281.1427 141.8655 -1.2135 248.3208 249.5343 281.2917 142.6875 -1.2229 248.4897 249.7126 281.3785 143.4858 -1.2227 248.6095 249.8322 281.4411 144.2945 -1.2219 248.6945 249.9163 281.5394 145.1165 -1.2276 248.7714 249.9990 281.7671 145.8785 -1.2334 248.9018 250.1352 281.9036 146.7328 -1.2430 249.1030 250.3461 281.9777 147.4945 -1.2372 249.2654 250.5026 282.1289 148.3165 -1.2357 249.3598 250.5955 282.2525 149.1060 -1.2321 249.4778 250.7099 282.3350 149.8953 -1.2447 249.5866 250.8313 282.4883 150.7438 -1.2493 249.6399 250.8892 282.5934 151.5020 -1.2526 249.7943 251.0470 282.7595 152.3210 -1.2515 249.9303 251.1818 282.8660 153.1090 -1.2395 250.0600 251.2995 282.9968 153.8970 -1.2449 250.2403 251.4852 283.1473 154.7450 -1.2620 250.4114 251.6735 283.2642 155.5030 -1.2562 250.5835 251.8396 283.3580 156.3210 -1.2495 250.6605 251.9100 283.5417 157.1393 -1.2447 250.7655 252.0101 283.6797 157.8980 -1.2668 250.8249 252.0918 283.7449 158.7475 -1.2531 251.0662 252.3193 283.9789 159.5360 -1.2597 251.2464 252.5061 284.0887 160.3250 -1.2651 251.2143 252.4795 284.1525 161.1445 -1.2843 251.2855 252.5698 284.1978 161.9355 -1.2724 251.5588 252.8313 284.3662 162.7573 -1.2748 251.6507 252.9255 284.5091 163.5495 -1.2752 251.7838 253.0589 284.6528 164.3425 -1.2729 251.9289 253.2019 284.7727 165.1645 -1.2883 252.1479 253.4361 284.9321 165.9265 -1.2884 252.1597 253.4481 285.0753 166.7785 -1.2918 252.3083 253.6001 285.2858 167.5705 -1.2921 252.4888 253.7808 285.3467 168.3625 -1.3010 252.5111 253.8121 285.5920 169.1850 -1.3001 252.6539 253.9540 285.6961 169.9475 -1.2940 252.8347 254.1287 285.8496 170.7995 -1.2990 252.9788 254.2778 285.9554 171.5643 -1.3066 253.1497 254.4563 286.0433 172.3865 -1.3085 253.1746 254.4831 286.2031 173.2085 -1.3086 253.3985 254.7071 286.4589 173.9705 -1.3046 253.4346 254.7392 286.4790 174.7963 -1.2935 253.5561 254.8495 286.6066 175.5915 -1.2928 253.8071 255.0998 286.6818 176.4435 -1.3069 253.9140 255.2209 286.8761 177.2055 -1.3120 254.0059 255.3179 287.0824 178.0285 -1.3228 254.2292 255.5520 287.1981 178.8205 -1.3148 254.3622 255.6770 287.2859 179.6123 -1.3132 254.4975 255.8106 287.3970 180.4640 -1.3223 254.5957 255.9180 287.5684 181.2250 -1.3100 254.7018 256.0118 287.5896 182.0463 -1.3167 254.6866 256.0033 287.7364 182.8348 -1.3106 254.8285 256.1391 287.8259 183.6238 -1.3306 255.0632 256.3938 287.9508 184.4418 -1.3235 255.2207 256.5442 288.1385 185.2298 -1.3251 255.2790 256.6042 288.2103 186.0480 -1.3191 255.4377 256.7568 288.3584 186.8360 -1.3201 255.6532 256.9733 288.5797 187.6240 -1.3364 255.8696 257.2059 288.7242 188.4725 -1.3416 255.9219 257.2634 288.8051 189.2310 -1.3425 256.0993 257.4418 288.8771 190.0518 -1.3474 256.1445 257.4919 289.0541 190.8400 -1.3482 256.2837 257.6318 289.1008 191.6290 -1.3511 256.4150 257.7661 289.3149 192.4785 -1.3514 256.5606 257.9120 289.4867 193.2383 -1.3454 256.7073 258.0527 289.5488 194.0595 -1.3506 256.7772 258.1278 289.7693 194.9543 -1.3631 256.9046 258.2678 289.8620 195.8785 -1.3591 257.0802 258.4393 290.0162 196.6405 -1.3567 257.2308 258.5876 290.1267 197.4935 -1.3562 257.3867 258.7429 290.3302 198.2855 -1.3605 257.4862 258.8467 290.4048 199.0775 -1.3689 257.6376 259.0066 290.4529 199.9005 -1.3625 257.7261 259.0886 290.6796 200.6635 -1.3788 257.8789 259.2576 290.7905 201.5155 -1.3631 257.9689 259.3320 291.0069 202.3075 -1.3685 258.0629 259.4314 291.0956 203.0995 -1.3806 258.1985 259.5791 291.2451 203.9225 -1.3860 258.3881 259.7741 291.4828 204.6850 -1.3879 258.5406 259.9285 291.4970 205.5128 -1.3835 258.5969 259.9804 291.7079 206.3075 -1.3857 258.7095 260.0951 291.7523 207.1600 -1.3730 258.9203 260.2933 292.0155 207.9218 -1.3800 259.0143 260.3943 292.1196 208.7458 -1.3904 259.2427 260.6331 292.2291 209.5380 -1.3848 259.3247 260.7095 292.3255 210.3295 -1.3969 259.4565 260.8534 292.4219 211.1820 -1.3966 259.5676 260.9642 292.6174 211.9438 -1.3987 259.7018 261.1005 292.7404 212.7685 -1.3999 259.8467 261.2466 292.8319 213.5610 -1.4011 259.9779 261.3790 292.9653 214.3510 -1.4083 260.1578 261.5661 293.1452 215.1953 -1.3895 260.2781 261.6676 293.1635 215.9553 -1.3983 260.3049 261.7032 293.3660 216.7750 -1.4131 260.4164 261.8295 293.5372 217.5635 -1.4114 260.6428 262.0542 293.4718 218.3510 -1.4127 260.7391 262.1518 293.7102 219.2000 -1.4113 260.9550 262.3663 293.8258 219.9583 -1.4185 261.0270 262.4456 293.9290 220.7763 -1.4232 261.2648 262.6880 294.0894 221.5945 -1.4275 261.3140 262.7415 294.1252 222.3525 -1.4205 261.5055 262.9260 294.3851 223.2013 -1.4239 261.5390 262.9629 294.4829 223.9903 -1.4309 261.6834 263.1143 294.5768 224.7805 -1.4457 261.8716 263.3173 294.7697 225.6095 -1.4397 262.0105 263.4502 295.0017 226.3800 -1.4376 262.0183 263.4559 295.1184 227.2043 -1.4511 262.1993 263.6504 295.1585 227.9958 -1.4426 262.3274 263.7699 295.2641 228.8178 -1.4312 262.4369 263.8681 295.3198 229.6105 -1.4455 262.6540 264.0995 295.5260 230.4035 -1.4490 262.8502 264.2992 295.6117 231.2260 -1.4571 262.8608 264.3179 295.7087 232.0178 -1.4575 263.0214 264.4788 295.8984 232.8398 -1.4680 263.1313 264.5993 296.0638 233.6330 -1.4624 263.3141 264.7765 296.1729 234.4255 -1.4706 263.3459 264.8165 296.2050 235.2480 -1.4594 263.5562 265.0156 296.4878 236.0095 -1.4661 263.7030 265.1691 296.6223 236.8650 -1.4677 263.8850 265.3527 296.7819 237.6580 -1.4616 263.9801 265.4418 296.8339 238.4495 -1.4775 264.0605 265.5379 296.9521 239.2720 -1.4614 264.3461 265.8075 297.1190 240.0335 -1.4900 264.4436 265.9336 297.2196 240.8860 -1.4935 264.4871 265.9806 297.2838 241.6780 -1.4895 264.5197 266.0091 297.3873 242.4695 -1.4903 264.7127 266.2030 297.5370 243.2920 -1.4990 264.9355 266.4345 297.7161 244.0545 -1.4948 265.0319 266.5267 297.8458 244.9068 -1.5024 265.1910 266.6934 297.9995 245.6988 -1.5025 265.3799 266.8825 298.1015 246.5155 -1.5054 265.5358 267.0412 298.2295 247.2740 -1.5056 265.4874 266.9931 298.3742 248.0920 -1.5181 265.6475 267.1656 298.5832 248.9100 -1.5068 265.7981 267.3049 298.6289 249.6680 -1.5013 266.0593 267.5607 298.7132 250.5168 -1.5132 265.9950 267.5082 298.8721 251.2753 -1.5155 266.2632 267.7787 298.9450 252.0930 -1.5055 266.3910 267.8965 299.2077 252.9125 -1.5148 266.5047 268.0195 299.2438 253.6710 -1.5270 266.6530 268.1800 299.4319 254.5200 -1.5194 266.8839 268.4034 299.5336 255.3093 -1.5225 266.9821 268.5046 299.6426 256.0990 -1.5359 267.0126 268.5485 299.8460 256.9233 -1.5337 267.1273 268.6610 299.9796 257.7123 -1.5244 267.2986 268.8230 300.0651 258.5328 -1.5411 267.4412 268.9823 300.1248 259.3255 -1.5408 267.5901 269.1309 300.2093 260.1175 -1.5486 267.6799 269.2285 300.3561 260.9400 -1.5512 267.7806 269.3317 300.5825 261.7015 -1.5423 267.9916 269.5339 300.7945 262.5550 -1.5317 268.0997 269.6314 300.8444 263.3470 -1.5390 268.1787 269.7177 300.9248 264.1385 -1.5471 268.3747 269.9218 301.1404 264.9615 -1.5568 268.4722 270.0290 301.1890 265.7235 -1.5507 268.5508 270.1015 301.3198 266.5760 -1.5535 268.7804 270.3339 301.5142 267.3680 -1.5600 268.8810 270.4410 301.5815 268.1595 -1.5543 269.0263 270.5806 301.6906 268.9825 -1.5647 269.1636 270.7283 301.8680 269.7455 -1.5626 269.3011 270.8637 302.0238 270.5975 -1.5759 269.4140 270.9899 302.1804 271.3918 -1.5698 269.6352 271.2051 302.3217 272.1855 -1.5578 269.6478 271.2057 302.4771 273.0075 -1.5509 269.8047 271.3556 302.5634 273.7695 -1.5624 270.0000 271.5624 302.7876 274.6215 -1.5715 270.0860 271.6575 302.9449 275.3840 -1.5761 270.1639 271.7400 302.9740 276.2075 -1.5721 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