DTA measure 2gyors Date: 2024108:1538 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.22 s Mass = 1305.100 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2886 -3.9275 415.5848 419.5123 418.0228 3.8885 -3.9292 415.6628 419.5920 418.0117 5.4884 -3.9228 415.6290 419.5519 418.0667 7.1175 -3.9232 415.7386 419.6618 417.9729 8.7185 -3.9193 415.9067 419.8260 417.8686 10.3325 -3.9194 415.9085 419.8279 417.9753 11.9320 -3.9243 415.8989 419.8233 417.9035 13.5315 -3.9274 415.9733 419.9006 417.7252 15.1608 -3.9196 416.0568 419.9764 417.6122 16.7615 -3.9166 416.0105 419.9271 417.6253 18.3614 -3.9306 416.0736 420.0042 417.3910 19.9794 -3.8983 416.2104 420.1086 417.1646 21.5779 -3.8887 416.2280 420.1167 417.0834 23.1784 -3.9043 416.2805 420.1847 416.8579 24.8259 -3.9016 416.2525 420.1541 416.6092 26.4250 -3.9094 416.3625 420.2719 416.4772 28.0263 -3.9003 416.4276 420.3279 416.1877 29.6420 -3.8831 416.3426 420.2258 416.0455 31.2423 -3.8773 416.4233 420.3007 415.7714 32.8734 -3.8765 416.5950 420.4715 415.6578 34.4726 -3.8602 416.4942 420.3544 415.3588 36.0716 -3.8643 416.5998 420.4641 415.1334 37.6889 -3.8516 416.5653 420.4168 414.8264 39.2909 -3.8537 416.6080 420.4618 414.5930 40.8906 -3.8298 416.6498 420.4796 414.4309 42.4950 -3.8337 416.6296 420.4633 414.0477 44.0873 -3.8186 416.7555 420.5741 413.8094 45.6945 -3.8205 416.7059 420.5265 413.7040 47.2870 -3.8195 416.6829 420.5024 413.4468 48.9149 -3.8056 416.6861 420.4917 413.2028 50.5245 -3.7982 416.7128 420.5111 412.9302 52.1170 -3.7781 416.8524 420.6305 412.7805 53.7230 -3.7588 416.8196 420.5784 412.4315 55.3153 -3.7557 416.8430 420.5987 412.3023 56.9388 -3.7693 416.7436 420.5129 412.0785 58.5404 -3.7553 416.6827 420.4379 411.9006 60.1424 -3.7481 416.7930 420.5411 411.7390 61.7529 -3.7351 416.7573 420.4923 411.5473 63.3489 -3.7306 416.8150 420.5456 411.3245 64.9620 -3.7159 416.7847 420.5007 411.2016 66.5756 -3.7075 416.7069 420.4145 410.9236 68.1745 -3.7049 416.6602 420.3652 410.7752 69.7874 -3.6990 416.6971 420.3961 410.5559 71.3891 -3.6865 416.6731 420.3596 410.3289 72.9903 -3.6495 416.7525 420.4020 410.2521 74.6200 -3.6067 416.5373 420.1440 410.0370 76.2190 -3.5735 416.6016 420.1751 409.8253 77.8188 -3.6082 416.4737 420.0819 409.7037 79.4328 -3.6319 416.5154 420.1474 409.4795 81.0339 -3.6203 416.5584 420.1787 409.2353 82.6554 -3.6265 416.5182 420.1447 409.0655 84.2549 -3.6179 416.4617 420.0796 408.8558 85.8688 -3.6041 416.3335 419.9376 408.6432 87.4675 -3.6231 416.4216 420.0447 408.5735 89.0698 -3.6395 416.3662 420.0057 408.3857 90.6905 -3.6892 416.2526 419.9418 408.1553 92.3048 -3.7136 416.2585 419.9720 408.0348 93.9055 -3.6970 416.1680 419.8651 407.8248 95.5198 -3.6917 416.1449 419.8367 407.6797 97.1215 -3.6772 416.1013 419.7786 407.3329 98.7355 -3.6810 416.1089 419.7899 407.1731 100.3563 -3.6689 416.1047 419.7736 407.0271 101.9699 -3.6640 416.0039 419.6679 406.8261 103.5691 -3.6552 415.9157 419.5709 406.6769 105.1651 -3.6444 415.8439 419.4883 406.4341 106.7716 -3.6469 415.9425 419.5893 406.3364 108.3793 -3.6366 415.7932 419.4299 406.1293 109.9781 -3.6347 415.7876 419.4223 405.8917 111.5774 -3.6247 415.6835 419.3082 405.7154 113.1691 -3.6032 415.5615 419.1647 405.4738 114.7751 -3.5928 415.4531 419.0459 405.2205 116.3814 -3.5832 415.4171 419.0004 405.1444 117.9873 -3.5750 415.3295 418.9045 404.9390 119.5966 -3.5812 415.3165 418.8978 404.6874 121.1936 -3.5786 415.1986 418.7772 404.5285 122.7876 -3.5638 415.2221 418.7859 404.2161 124.3956 -3.5546 415.1128 418.6674 404.0433 126.0191 -3.5338 415.1456 418.6794 403.9439 127.6124 -3.5286 415.0382 418.5668 403.7549 129.2239 -3.5278 414.9045 418.4323 403.6014 130.8240 -3.5224 414.7810 418.3034 403.3243 132.4303 -3.5199 414.6655 418.1854 403.1066 134.0296 -3.5189 414.5849 418.1038 402.8639 135.6608 -3.5170 414.5893 418.1063 402.6858 137.2629 -3.5083 414.5202 418.0286 402.4565 138.8625 -3.5010 414.3922 417.8932 402.2855 140.4746 -3.5015 414.2552 417.7568 402.1127 142.0715 -3.4706 414.0236 417.4943 401.9411 143.7005 -3.4748 414.0646 417.5394 401.7030 145.3295 -3.4644 413.9241 417.3885 401.4293 146.9189 -3.4649 413.9767 417.4416 401.2993 148.5375 -3.4709 413.9022 417.3731 401.1193 150.1365 -3.4617 413.7623 417.2239 400.8807 151.7503 -3.4570 413.6271 417.0841 400.7130 153.3669 -3.4520 413.3569 416.8089 400.5628 154.9809 -3.4526 413.4004 416.8530 400.3184 156.5819 -3.4384 413.3746 416.8130 399.9446 158.1838 -3.4344 413.2417 416.6761 399.7506 159.7838 -3.4168 413.2117 416.6285 399.5789 161.4174 -3.4145 412.9604 416.3749 399.4704 163.0179 -3.4153 412.9243 416.3396 399.1926 164.6316 -3.4048 412.7819 416.1867 398.9839 166.2336 -3.3921 412.5751 415.9671 398.8247 167.8345 -3.3938 412.6132 416.0070 398.6931 169.4436 -3.3948 412.4948 415.8896 398.5044 171.0264 -3.3987 412.3393 415.7379 398.3346 172.6540 -3.3887 412.2603 415.6490 398.1643 174.2453 -3.3665 412.0345 415.4011 397.9401 175.8370 -3.3293 412.0382 415.3675 397.7170 177.4446 -3.3532 412.0499 415.4031 397.5039 179.0510 -3.3594 411.8605 415.2199 397.3438 180.6570 -3.3575 411.5181 414.8756 397.2676 182.2666 -3.3540 411.5586 414.9126 397.0012 183.8593 -3.3501 411.5209 414.8710 396.7385 185.4665 -3.3368 411.3621 414.6989 396.5499 187.0736 -3.3195 411.2925 414.6120 396.3450 188.6809 -3.3122 411.1749 414.4870 396.0620 190.2888 -3.3059 410.9800 414.2858 395.8776 191.8831 -3.3158 410.7998 414.1156 395.8382 193.4948 -3.3200 410.7979 414.1179 395.5636 195.1126 -3.3145 410.6070 413.9215 395.4476 196.7115 -3.2957 410.4222 413.7179 395.1239 198.3110 -3.2870 410.3610 413.6481 394.9571 199.9255 -3.2929 410.1663 413.4592 394.8239 201.5254 -3.2724 410.0619 413.3343 394.4950 203.1400 -3.2653 409.9949 413.2601 394.4567 204.7541 -3.2452 409.7405 412.9858 394.2081 206.3538 -3.2522 409.6885 412.9407 393.8965 207.9678 -3.2600 409.5689 412.8288 393.8108 209.5711 -3.2470 409.4472 412.6942 393.5893 211.1725 -3.2485 409.3315 412.5799 393.3791 212.7871 -3.2502 409.1629 412.4131 393.1627 214.4018 -3.2440 409.1483 412.3922 392.9552 216.0038 -3.2308 408.9693 412.2001 392.7455 217.6075 -3.2286 408.7788 412.0075 392.7271 219.2075 -3.2120 408.7384 411.9503 392.3836 220.8365 -3.2231 408.4543 411.6774 392.3110 222.4378 -3.2019 408.2849 411.4868 392.0507 224.0535 -3.2052 408.2113 411.4166 391.7746 225.6540 -3.1862 408.0617 411.2480 391.5172 227.2545 -3.1979 407.8917 411.0896 391.3050 228.8834 -3.1867 407.8516 411.0383 391.0843 230.4853 -3.1864 407.7025 410.8888 390.9318 232.0890 -3.1772 407.5057 410.6829 390.8496 233.6893 -3.1747 407.4283 410.6030 390.5451 235.2953 -3.1718 407.3337 410.5054 390.3534 236.8871 -3.1547 407.0085 410.1632 390.1222 238.4783 -3.1433 406.9582 410.1015 389.9025 240.0999 -3.1451 406.7775 409.9226 389.7539 241.6915 -3.1548 406.5173 409.6722 389.4876 243.2921 -3.1311 406.5132 409.6443 389.3790 244.8893 -3.1417 406.4091 409.5507 389.0338 246.4953 -3.1237 406.2749 409.3986 388.9666 248.1173 -3.1295 406.0645 409.1941 388.8338 249.7099 -3.1190 405.9444 409.0633 388.4773 251.3045 -3.1121 405.7857 408.8977 388.3041 252.9228 -3.1027 405.6503 408.7530 388.0939 254.5111 -3.0986 405.4022 408.5008 388.0178 256.1386 -3.0847 405.2875 408.3721 387.7156 257.7490 -3.0838 405.1745 408.2583 387.5686 259.3468 -3.0886 404.9537 408.0424 387.2937 260.9606 -3.0816 404.8183 407.8999 387.1031 262.5601 -3.0792 404.5575 407.6366 386.9751 264.1629 -3.0713 404.4621 407.5334 386.7533 265.7810 -3.0634 404.2909 407.3543 386.5544 267.3863 -3.0665 404.1340 407.2005 386.3749 269.0065 -3.0583 404.0403 407.0986 386.0465 270.6055 -3.0588 403.8331 406.8920 385.9939 272.2058 -3.0532 403.7309 406.7841 385.7268 273.8210 -3.0460 403.6168 406.6628 385.4549 275.4365 -3.0368 403.4155 406.4523 385.3291 277.0386 -3.0355 403.2004 406.2359 385.1353 278.6591 -3.0277 402.9845 406.0123 384.9062 280.2518 -3.0176 402.9337 405.9513 384.5973 281.8680 -3.0171 402.6980 405.7152 384.5698 283.4669 -3.0061 402.5233 405.5294 384.1933 285.1006 -3.0185 402.4232 405.4417 384.0801 286.6999 -2.9986 402.2022 405.2008 383.8810 288.3138 -2.9996 402.0956 405.0952 383.7345 289.9141 -2.9894 401.9269 404.9163 383.5123 291.5138 -2.9804 401.7226 404.7030 383.2218 293.1466 -2.9784 401.5947 404.5731 383.0556 294.7411 -2.9831 401.5604 404.5434 382.8302 296.3571 -2.9778 401.4156 404.3934 382.6802 297.9491 -2.9710 401.0400 404.0110 382.5220 299.5393 -2.9688 400.9787 403.9476 382.2716 301.1478 -2.9654 400.6739 403.6394 382.1312 302.7609 -2.9583 400.5869 403.5452 381.9818 304.3576 -2.9377 400.5043 403.4420 381.6883 305.9548 -2.9311 400.3853 403.3164 381.4130 307.5483 -2.9344 400.2712 403.2057 381.1914 309.1600 -2.9194 399.9645 402.8839 381.0365 310.7670 -2.9227 399.7746 402.6973 380.8928 312.3631 -2.9220 399.5846 402.5065 380.6437 313.9811 -2.9109 399.3397 402.2506 380.4632 315.5721 -2.9113 399.2873 402.1986 380.2472 317.1721 -2.9102 399.1409 402.0511 379.9896 318.7884 -2.9142 398.9759 401.8901 379.7760 320.3993 -2.9078 398.7049 401.6127 379.6553 322.0134 -2.8983 398.6163 401.5146 379.4368 323.6125 -2.8815 398.3926 401.2741 379.2390 325.2165 -2.8771 398.1959 401.0730 378.9600 326.8249 -2.8750 398.0459 400.9209 378.7633 328.4238 -2.8579 397.9183 400.7762 378.5544 330.0535 -2.8675 397.8410 400.7085 378.3338 331.6595 -2.8560 397.6017 400.4578 378.1852 333.2685 -2.8488 397.4504 400.2991 378.0683 334.8704 -2.8622 397.2810 400.1431 377.7931 336.4708 -2.8481 397.0610 399.9091 377.4789 338.0711 -2.8346 396.7795 399.6141 377.3968 339.6919 -2.8260 396.7564 399.5824 377.0804 341.3059 -2.8284 396.6112 399.4396 376.8750 342.9198 -2.8355 396.4185 399.2540 376.7037 344.5220 -2.8201 396.1657 398.9857 376.4961 346.1286 -2.8212 396.0455 398.8667 376.3602 347.7345 -2.8042 395.8870 398.6912 376.1041 349.3494 -2.8009 395.5769 398.3779 375.9877 350.9635 -2.7837 395.4115 398.1952 375.7383 352.5629 -2.7897 395.2608 398.0504 375.6220 354.1625 -2.7784 395.1539 397.9323 375.3444 355.7765 -2.7861 394.8915 397.6775 375.1596 357.3908 -2.7754 394.7786 397.5540 374.9881 359.0084 -2.7792 394.5890 397.3682 374.7686 360.6134 -2.7706 394.2801 397.0507 374.6305 362.2135 -2.7637 394.1902 396.9539 374.4009 363.8110 -2.7530 393.9829 396.7359 374.1916 365.4043 -2.7500 393.8622 396.6123 374.0467 367.0104 -2.7322 393.7806 396.5129 373.7485 368.6046 -2.7452 393.5604 396.3056 373.5659 370.2156 -2.7385 393.3580 396.0965 373.4042 371.8085 -2.7198 393.1729 395.8927 373.1856 373.4144 -2.7131 393.0192 395.7322 372.9718 375.0355 -2.7280 392.8166 395.5446 372.8171 376.6194 -2.7282 392.6351 395.3633 372.6617 378.2346 -2.7111 392.4624 395.1735 372.4861 379.8298 -2.6979 392.3482 395.0461 372.2026 381.4386 -2.6997 392.1039 394.8036 372.1060 383.0624 -2.7006 391.9274 394.6280 371.8262 384.6563 -2.6823 391.6554 394.3376 371.6079 386.2663 -2.6961 391.5627 394.2588 371.3223 387.8663 -2.6725 391.2979 393.9704 370.9602 389.4671 -2.6752 391.0295 393.7047 370.7534 391.0970 -2.6652 390.9559 393.6211 370.5157 392.6959 -2.6590 390.7968 393.4558 370.2412 394.2994 -2.6630 390.5748 393.2377 370.0348 395.9028 -2.6644 390.3694 393.0338 369.8870 397.5120 -2.6610 390.1572 392.8182 369.8304 399.1115 -2.6599 389.9758 392.6357 369.6115 400.7405 -2.6548 389.8317 392.4865 369.3759 402.3431 -2.6534 389.6773 392.3307 369.2554 403.9455 -2.6332 389.3630 391.9962 368.9697 405.5595 -2.6339 389.1494 391.7833 368.7340 407.1594 -2.6189 389.0573 391.6762 368.4995 408.7735 -2.6187 388.9731 391.5918 368.3368 410.3876 -2.6273 388.8271 391.4544 368.1291 411.9871 -2.6196 388.4825 391.1022 367.9419 413.5864 -2.6206 388.3196 390.9402 367.8149 415.2008 -2.6095 388.1776 390.7871 367.6129 416.8091 -2.6106 387.8743 390.4849 367.4607 418.4068 -2.6227 387.8766 390.4993 367.2155 420.0360 -2.6048 387.5413 390.1461 367.0095 421.6348 -2.5832 387.4356 390.0189 366.7992 423.2486 -2.5864 387.1821 389.7685 366.6518 424.8476 -2.5866 386.9475 389.5341 366.3846 426.4413 -2.5865 386.8331 389.4196 366.2081 428.0624 -2.5905 386.6749 389.2654 366.0057 429.6560 -2.5706 386.4348 389.0054 365.8280 431.2505 -2.5625 386.1726 388.7351 365.5545 432.8420 -2.5634 386.0675 388.6309 365.3841 434.4330 -2.5592 385.8509 388.4100 365.0269 436.0540 -2.5471 385.6985 388.2456 364.9150 437.6474 -2.5446 385.5261 388.0707 364.7316 439.2590 -2.5321 385.3780 387.9100 364.4940 440.8500 -2.5328 385.1008 387.6336 364.3218 442.4625 -2.5440 385.0012 387.5451 364.0062 444.0720 -2.5456 384.7523 387.2980 363.8636 445.6691 -2.5394 384.5910 387.1305 363.6432 447.2864 -2.5237 384.3412 386.8648 363.5612 448.8878 -2.5371 384.2441 386.7812 363.2659 450.4870 -2.5213 384.0643 386.5856 363.0907 452.0896 -2.5195 383.8736 386.3931 362.8347 453.7053 -2.5101 383.6992 386.2093 362.5652 455.3046 -2.5015 383.4441 385.9455 362.4102 456.9080 -2.5039 383.3675 385.8714 362.2782 458.5225 -2.5013 383.1531 385.6544 362.0876 460.1220 -2.4929 382.8313 385.3242 361.8176 461.7213 -2.4832 382.7465 385.2297 361.6760 463.3501 -2.4628 382.4058 384.8686 361.4099 464.9495 -2.4763 382.3147 384.7910 361.2220 466.5498 -2.4788 382.1302 384.6089 360.9266 468.1563 -2.4711 381.9809 384.4520 360.9189 469.7635 -2.4752 381.7786 384.2538 360.5955 471.3628 -2.4671 381.6626 384.1297 360.4262 472.9930 -2.4403 381.4090 383.8493 360.1624 474.5916 -2.4516 381.2072 383.6588 360.0344 476.1906 -2.4400 381.0063 383.4463 359.7859 477.8045 -2.4443 380.8048 383.2491 359.6742 479.4069 -2.4293 380.4895 382.9187 359.4975 481.0223 -2.4237 380.4240 382.8477 359.3301 482.6365 -2.4267 380.1914 382.6181 359.1038 484.2359 -2.4116 379.9637 382.3753 358.8580 485.8505 -2.4288 379.8089 382.2377 358.5969 487.4495 -2.4062 379.6624 382.0685 358.3982 489.0664 -2.4141 379.5303 381.9444 358.2120 490.6524 -2.3982 379.1931 381.5913 358.0435 492.2749 -2.4094 379.0501 381.4595 357.7693 493.8668 -2.3933 378.8704 381.2637 357.5335 495.4579 -2.4044 378.7240 381.1284 357.3805 497.0638 -2.4057 378.4659 380.8717 357.1950 498.6629 -2.3922 378.2233 380.6156 356.9868 500.2729 -2.3869 378.2514 380.6383 356.7144 501.8788 -2.3793 377.8892 380.2685 356.4836 503.4708 -2.3731 377.6845 380.0576 356.3498 505.0630 -2.3696 377.5781 379.9478 356.1084 506.6761 -2.3605 377.3661 379.7266 355.9793 508.2863 -2.3637 377.0689 379.4326 355.7255 509.8873 -2.3605 377.0141 379.3746 355.5231 511.4869 -2.3578 376.7887 379.1465 355.3741 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