DTA measure 1elso Date: 20251021:1529 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.12 s Mass = 959.500 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2398 0.5322 231.1810 230.6488 276.5430 1.9953 0.5352 231.4429 230.9077 276.6043 2.8330 0.5392 231.7153 231.1761 276.6246 3.6195 0.5379 231.9464 231.4085 276.6332 4.4158 0.5419 232.2396 231.6977 276.5969 5.2125 0.5445 232.4786 231.9341 276.5467 5.9990 0.5437 232.7294 232.1857 276.4323 6.8158 0.5457 232.9858 232.4401 276.2866 7.5920 0.5509 233.2372 232.6864 276.1532 8.4298 0.5512 233.5139 232.9627 276.0161 9.1850 0.5525 233.7888 233.2363 275.8580 10.0433 0.5545 234.0704 233.5158 275.6817 10.8090 0.5562 234.3236 233.7674 275.5278 11.6260 0.5590 234.5929 234.0339 275.3565 12.4225 0.5615 234.8404 234.2789 275.2064 13.2195 0.5614 235.0838 234.5224 275.0472 14.0465 0.5601 235.3534 234.7933 274.8567 14.8020 0.5611 235.6162 235.0551 274.7226 15.6605 0.5582 235.9058 235.3475 274.5844 16.3953 0.5589 236.1358 235.5769 274.5042 17.2535 0.5627 236.3844 235.8217 274.4254 18.0093 0.5676 236.6249 236.0572 274.4319 18.8670 0.5680 236.8773 236.3093 274.4605 19.6330 0.5671 237.1132 236.5461 274.4705 20.4605 0.5700 237.3725 236.8026 274.5877 21.2465 0.5750 237.6358 237.0608 274.7804 22.0430 0.5775 237.9083 237.3308 274.9843 22.8400 0.5794 238.1575 237.5781 275.2496 23.6363 0.5841 238.4211 237.8369 275.5751 24.4635 0.5849 238.6942 238.1092 275.9266 25.2193 0.5833 238.9402 238.3569 276.2794 26.0875 0.5840 239.2379 238.6539 276.7217 26.8430 0.5831 239.4722 238.8890 277.1458 27.6705 0.5849 239.7194 239.1346 277.6419 28.4568 0.5858 239.9237 239.3379 278.1030 29.2843 0.5887 240.1645 239.5758 278.6145 30.0808 0.5870 240.4085 239.8215 279.0931 30.8773 0.5815 240.6313 240.0498 279.5622 31.7048 0.5801 240.8512 240.2711 279.9950 32.4605 0.5843 241.0793 240.4950 280.4029 33.3285 0.5869 241.3552 240.7683 280.8445 34.0535 0.5888 241.6053 241.0165 281.1868 34.9115 0.5893 241.8805 241.2912 281.5434 35.6773 0.5851 242.1213 241.5363 281.8297 36.5148 0.5806 242.3756 241.7950 282.0768 37.3015 0.5789 242.6104 242.0314 282.2570 38.1080 0.5783 242.8309 242.2527 282.4266 38.9150 0.5767 243.0750 242.4983 282.5558 39.7015 0.5764 243.3193 242.7429 282.6415 40.5388 0.5740 243.5549 242.9809 282.7015 41.2945 0.5691 243.7787 243.2096 282.7346 42.1525 0.5665 244.0551 243.4886 282.7422 42.9183 0.5646 244.2929 243.7283 282.7019 43.7455 0.5650 244.5508 243.9858 282.6315 44.5423 0.5615 244.7706 244.2090 282.5170 45.3388 0.5563 245.0172 244.4609 282.4100 46.1660 0.5586 245.2371 244.6786 282.3083 46.9423 0.5573 245.4636 244.9063 282.2009 47.7900 0.5518 245.7227 245.1709 282.0528 48.5353 0.5491 245.9346 245.3855 281.8764 49.4038 0.5525 246.1677 245.6152 281.7027 50.1593 0.5536 246.3594 245.8057 281.5320 50.9968 0.5545 246.6427 246.0882 281.3638 51.7833 0.5537 246.8753 246.3216 281.2289 52.5798 0.5523 247.0890 246.5367 281.0830 53.4070 0.5522 247.3032 246.7511 280.9734 54.1730 0.5544 247.5600 247.0056 280.8803 55.0310 0.5526 247.8364 247.2838 280.7804 55.7660 0.5526 248.0680 247.5154 280.7793 56.6243 0.5542 248.2853 247.7311 280.8431 57.3900 0.5561 248.5052 247.9491 280.9079 58.2175 0.5572 248.7291 248.1719 281.0326 59.0143 0.5545 248.9529 248.3984 281.1826 59.8105 0.5531 249.1969 248.6437 281.3948 60.6380 0.5525 249.4430 248.8905 281.6241 61.4038 0.5530 249.6531 249.1001 281.8886 62.2515 0.5500 249.8697 249.3197 282.2217 63.0275 0.5468 250.0702 249.5234 282.5648 63.8448 0.5451 250.3060 249.7609 282.9793 64.6515 0.5443 250.5085 249.9642 283.4106 65.4378 0.5427 250.7201 250.1774 283.8479 66.2755 0.5387 250.9753 250.4366 284.3247 67.0310 0.5355 251.1909 250.6554 284.7473 67.8890 0.5362 251.4557 250.9195 285.2597 68.6653 0.5348 251.6530 251.1182 285.7090 69.4925 0.5327 251.8995 251.3668 286.1320 70.2380 0.5335 252.1186 251.5851 286.5188 71.0860 0.5323 252.3552 251.8229 286.9345 71.8515 0.5281 252.5581 252.0300 287.3163 72.6790 0.5229 252.8065 252.2836 287.6512 73.4655 0.5216 253.0418 252.5202 287.9383 74.2618 0.5204 253.2637 252.7433 288.2111 75.0893 0.5173 253.4657 252.9484 288.4436 75.8450 0.5132 253.6709 253.1576 288.6186 76.7028 0.5075 253.9325 253.4251 288.8098 77.4688 0.5042 254.1179 253.6137 288.9249 78.2960 0.5018 254.3464 253.8446 289.0384 79.0925 0.4947 254.5926 254.0979 289.0773 79.8788 0.4916 254.8421 254.3505 289.1067 80.6858 0.4884 255.0525 254.5641 289.0916 81.4720 0.4868 255.2566 254.7698 289.0226 82.2993 0.4839 255.4768 254.9929 288.9744 83.0653 0.4804 255.6616 255.1812 288.8761 83.9233 0.4778 255.8826 255.4048 288.7168 84.6788 0.4780 256.1085 255.6305 288.5609 85.5063 0.4758 256.3342 255.8585 288.3725 86.3028 0.4729 256.5508 256.0779 288.2171 87.0993 0.4719 256.7545 256.2826 288.0644 87.9165 0.4732 256.9755 256.5024 287.8949 88.6925 0.4729 257.1757 256.7029 287.7429 89.5300 0.4674 257.4095 256.9422 287.5843 90.3063 0.4642 257.6394 257.1752 287.4520 91.1233 0.4621 257.8947 257.4325 287.3416 91.8890 0.4637 258.1008 257.6371 287.2558 92.7473 0.4600 258.3322 257.8721 287.2000 93.5233 0.4578 258.5221 258.0643 287.1833 94.3403 0.4566 258.7041 258.2475 287.1968 95.1370 0.4545 258.8988 258.4444 287.2653 95.9335 0.4533 259.1139 258.6606 287.3731 96.7608 0.4530 259.3490 258.8961 287.4856 97.5268 0.4511 259.5437 259.0926 287.6253 98.3745 0.4505 259.7678 259.3173 287.8639 99.1505 0.4461 259.9853 259.5391 288.1280 99.9883 0.4435 260.2070 259.7634 288.4138 100.7335 0.4468 260.3631 259.9163 288.7520 101.5813 0.4473 260.5751 260.1278 289.1488 102.3473 0.4452 260.7700 260.3249 289.5568 103.1745 0.4408 260.9947 260.5540 290.0113 103.9710 0.4381 261.1607 260.7226 290.4628 104.7678 0.4359 261.3706 260.9347 290.9539 105.5848 0.4301 261.5900 261.1599 291.4060 106.3610 0.4292 261.7795 261.3503 291.8449 107.2088 0.4248 261.9747 261.5499 292.3022 107.9745 0.4204 262.1583 261.7379 292.7253 108.8018 0.4155 262.3881 261.9726 293.1682 109.5985 0.4132 262.5904 262.1771 293.5585 110.4155 0.4112 262.8039 262.3928 293.9108 111.2223 0.4083 263.0186 262.6103 294.2219 112.0090 0.4075 263.1990 262.7915 294.4792 112.8360 0.4026 263.4274 263.0248 294.7333 113.6020 0.4002 263.6320 263.2318 294.9216 114.4603 0.3970 263.8943 263.4972 295.0976 115.2258 0.3942 264.0834 263.6892 295.1992 116.0430 0.3884 264.2890 263.9006 295.2689 116.8500 0.3819 264.5133 264.1314 295.3375 117.6360 0.3754 264.7306 264.3552 295.3579 118.4635 0.3724 264.9080 264.5356 295.3388 119.2295 0.3688 265.0990 264.7302 295.2897 120.0975 0.3603 265.3108 264.9505 295.1890 120.8533 0.3548 265.5086 265.1539 295.1212 121.6808 0.3509 265.7413 265.3903 295.0141 122.4770 0.3510 265.9365 265.5856 294.8726 123.2738 0.3486 266.1452 265.7967 294.7024 124.1013 0.3416 266.3771 266.0354 294.5735 124.8565 0.3380 266.6002 266.2622 294.4430 125.7250 0.3385 266.7991 266.4606 294.2725 126.4910 0.3316 267.0010 266.6695 294.1314 127.3180 0.3270 267.2043 266.8773 294.0003 128.1048 0.3242 267.4090 267.0848 293.8862 128.9115 0.3269 267.6100 267.2831 293.7968 129.7283 0.3260 267.8392 267.5133 293.6781 130.5150 0.3243 268.0270 267.7026 293.6311 131.3423 0.3176 268.2208 267.9032 293.6071 132.1080 0.3191 268.3820 268.0628 293.6071 132.9660 0.3160 268.6202 268.3042 293.6575 133.7320 0.3154 268.8203 268.5049 293.7282 134.5488 0.3168 269.0291 268.7123 293.8796 135.3455 0.3147 269.2385 268.9237 294.0546 136.1320 0.3115 269.4538 269.1423 294.2342 136.9283 0.3064 269.6204 269.3140 294.4642 137.7250 0.3078 269.8363 269.5286 294.7402 138.5525 0.3032 270.0745 269.7713 295.0709 139.3078 0.2986 270.2666 269.9680 295.4159 140.1660 0.2952 270.4501 270.1549 295.8394 140.9423 0.2938 270.6253 270.3315 296.2282 141.7590 0.2897 270.8011 270.5115 296.6784 142.5250 0.2892 270.9428 270.6535 297.0915 143.3525 0.2870 271.1535 270.8664 297.5218 144.1488 0.2851 271.3872 271.1022 297.9494 144.9455 0.2800 271.5825 271.3024 298.3674 145.7628 0.2773 271.7768 271.4995 298.8177 146.5283 0.2751 271.9611 271.6860 299.2096 147.3865 0.2704 272.2044 271.9340 299.6352 148.1423 0.2638 272.3937 272.1299 299.9511 148.9795 0.2573 272.5692 272.3119 300.2890 149.7660 0.2543 272.7059 272.4516 300.5629 150.5628 0.2488 272.8738 272.6250 300.8161 151.3693 0.2454 273.0525 272.8071 301.0056 152.1660 0.2434 273.2088 272.9654 301.1784 152.9935 0.2417 273.3981 273.1565 301.2915 153.7590 0.2403 273.5882 273.3480 301.3580 154.6070 0.2330 273.8123 273.5793 301.3823 155.3833 0.2285 274.0169 273.7884 301.4150 156.2000 0.2255 274.2485 274.0230 301.4164 156.9968 0.2215 274.4487 274.2272 301.3982 157.7935 0.2164 274.6349 274.4184 301.3339 158.6205 0.2079 274.8471 274.6392 301.2669 159.3865 0.2041 274.9947 274.7907 301.1762 160.2343 0.1960 275.2144 275.0184 301.0167 160.9898 0.1903 275.3802 275.1899 300.8708 161.8580 0.1830 275.6015 275.4185 300.7439 162.6240 0.1834 275.7865 275.6031 300.6467 163.4513 0.1841 275.9801 275.7960 300.5021 164.2478 0.1796 276.1575 275.9779 300.3718 165.0343 0.1767 276.3495 276.1727 300.2597 165.8718 0.1734 276.5361 276.3626 300.1710 166.6273 0.1760 276.7029 276.5269 300.0700 167.4855 0.1795 276.8978 276.7184 299.9698 168.2513 0.1818 277.0954 276.9136 299.9088 169.0785 0.1795 277.2959 277.1164 299.8948 169.8753 0.1779 277.4975 277.3196 299.9085 170.6718 0.1774 277.6691 277.4918 299.9630 171.4993 0.1754 277.8780 277.7027 300.0847 172.2653 0.1704 278.0729 277.9025 300.2032 173.1230 0.1676 278.2912 278.1236 300.3993 173.8788 0.1641 278.4606 278.2964 300.5708 174.7165 0.1631 278.6480 278.4849 300.7913 175.5025 0.1602 278.7990 278.6388 301.0533 176.2995 0.1609 278.9800 278.8191 301.3653 177.1268 0.1573 279.1556 278.9983 301.7195 177.8925 0.1535 279.3240 279.1705 302.0927 178.7505 0.1514 279.5057 279.3543 302.5069 179.5063 0.1508 279.6765 279.5257 302.8965 180.3438 0.1488 279.8986 279.7498 303.3294 181.1095 0.1504 280.0812 279.9308 303.7366 181.9370 0.1463 280.2708 280.1245 304.1884 182.7333 0.1444 280.4606 280.3162 304.6189 183.5303 0.1447 280.6450 280.5003 305.0317 184.3575 0.1373 280.8473 280.7101 305.4376 185.1233 0.1348 281.0080 280.8732 305.7701 185.9815 0.1332 281.2108 281.0775 306.1392 186.7473 0.1289 281.3606 281.2317 306.4410 187.5745 0.1217 281.5288 281.4071 306.7100 188.3713 0.1147 281.7167 281.6020 306.9350 189.1678 0.1075 281.8881 281.7806 307.1475 189.9950 0.1064 282.0744 281.9679 307.3308 190.7610 0.1024 282.2302 282.1278 307.4619 191.5883 0.0952 282.4124 282.3172 307.5595 192.3848 0.0896 282.5824 282.4928 307.6204 193.2018 0.0881 282.7758 282.6877 307.6449 193.9678 0.0840 282.9699 282.8859 307.6503 194.8258 0.0767 283.1864 283.1097 307.6669 195.5918 0.0752 283.3451 283.2698 307.6334 196.4190 0.0730 283.5257 283.4526 307.5769 197.2053 0.0636 283.7070 283.6434 307.4722 198.0123 0.0590 283.8800 283.8211 307.3169 198.8293 0.0567 284.0896 284.0329 307.1908 199.5845 0.0545 284.2805 284.2259 307.0989 200.4123 0.0544 284.4931 284.4387 306.9678 201.1780 0.0513 284.6656 284.6143 306.8610 202.0358 0.0489 284.8726 284.8237 306.7112 202.7918 0.0483 285.0566 285.0083 306.5870 203.6088 0.0424 285.2567 285.2143 306.4963 204.3745 0.0419 285.4294 285.3875 306.4002 205.2328 0.0366 285.6471 285.6106 306.3113 205.9883 0.0348 285.8316 285.7968 306.2273 206.8155 0.0269 285.9944 285.9675 306.2207 207.6123 0.0259 286.1689 286.1430 306.2425 208.3985 0.0283 286.3435 286.3152 306.2716 209.2053 0.0270 286.5346 286.5076 306.3494 209.9918 0.0253 286.7036 286.6783 306.4370 210.8088 0.0247 286.9065 286.8818 306.5958 211.5848 0.0230 287.0983 287.0753 306.8000 212.4430 0.0227 287.2987 287.2760 307.0768 213.1883 0.0178 287.4902 287.4725 307.3241 214.0360 0.0137 287.6517 287.6380 307.6300 214.8020 0.0116 287.7845 287.7730 307.9753 215.6395 0.0104 287.9571 287.9467 308.3912 216.4258 0.0092 288.1558 288.1466 308.7761 217.2125 0.0089 288.2897 288.2808 309.1836 218.0498 0.0041 288.4682 288.4641 309.6178 218.8055 0.0024 288.6455 288.6431 310.0110 219.6330 -0.0009 288.8321 288.8329 310.4583 220.3985 -0.0054 288.9867 288.9921 310.8740 221.2570 -0.0129 289.1651 289.1780 311.3130 222.0228 -0.0150 289.3422 289.3572 311.6922 222.8705 -0.0186 289.5193 289.5380 312.0586 223.6368 -0.0189 289.6896 289.7086 312.3746 224.4535 -0.0247 289.8729 289.8976 312.6828 225.2605 -0.0303 290.0147 290.0451 312.8883 226.0470 -0.0360 290.1782 290.2143 313.0946 226.8433 -0.0404 290.3600 290.4004 313.2924 227.6400 -0.0425 290.5307 290.5732 313.4547 228.4675 -0.0454 290.7309 290.7764 313.5842 229.2330 -0.0481 290.9142 290.9623 313.6727 230.0813 -0.0509 291.1186 291.1695 313.7606 230.8573 -0.0544 291.2961 291.3505 313.7957 231.6743 -0.0572 291.4882 291.5454 313.8011 232.4813 -0.0605 291.6705 291.7310 313.7859 233.2880 -0.0622 291.8032 291.8655 313.7141 234.0845 -0.0641 291.9687 292.0327 313.6260 234.8813 -0.0714 292.1575 292.2289 313.5198 235.7085 -0.0756 292.3188 292.3944 313.4210 236.4745 -0.0766 292.4582 292.5348 313.3599 237.3223 -0.0799 292.6089 292.6889 313.2186 238.0983 -0.0875 292.7922 292.8797 313.0922 238.9155 -0.0915 292.9826 293.0741 312.9667 239.7123 -0.0926 293.1264 293.2190 312.8396 240.5085 -0.0935 293.2621 293.3556 312.7332 241.3360 -0.0916 293.4394 293.5311 312.6349 242.1020 -0.0876 293.6448 293.7324 312.5453 242.9495 -0.0917 293.8722 293.9640 312.4737 243.6950 -0.0956 294.0617 294.1573 312.4302 244.5430 -0.0999 294.2448 294.3447 312.3964 245.3188 -0.1036 294.3853 294.4889 312.4296 246.1360 -0.1033 294.5482 294.6515 312.4934 246.9430 -0.1032 294.7242 294.8274 312.6022 247.7290 -0.1076 294.8929 295.0005 312.7493 248.5565 -0.1127 295.0768 295.1895 312.9741 249.3225 -0.1137 295.2424 295.3561 313.2037 250.1803 -0.1171 295.4395 295.5566 313.5050 250.9463 -0.1176 295.6026 295.7202 313.7886 251.7635 -0.1192 295.7731 295.8923 314.1236 252.5703 -0.1213 295.9517 296.0731 314.4793 253.3670 -0.1221 296.1916 296.3138 314.8691 254.1533 -0.1272 296.3482 296.4754 315.2672 254.9805 -0.1323 296.4950 296.6273 315.6831 255.7773 -0.1360 296.6798 296.8157 316.0789 256.5635 -0.1391 296.8678 297.0069 316.4834 257.4013 -0.1463 297.0499 297.1962 316.9509 258.1568 -0.1510 297.2412 297.3922 317.3365 259.0148 -0.1520 297.4517 297.6037 317.7140 259.7808 -0.1552 297.5790 297.7343 318.0537 260.6083 -0.1557 297.6833 297.8390 318.3982 261.4045 -0.1591 297.8352 297.9943 318.7167 262.1910 -0.1623 297.9900 298.1523 318.9603 263.0185 -0.1682 298.1564 298.3245 319.1777 263.7943 -0.1743 298.3274 298.5016 319.3531 264.6218 -0.1774 298.4928 298.6702 319.4928 265.3775 -0.1816 298.6107 298.7923 319.6306 266.2045 -0.1819 298.8234 299.0053 319.7218 266.9705 -0.1820 299.0001 299.1821 319.7603 267.8185 -0.1841 299.1763 299.3604 319.7939 268.5943 -0.1868 299.3314 299.5182 319.8201 269.4115 -0.1898 299.4846 299.6744 319.7944 270.1980 -0.1900 299.6019 299.7919 319.7433 270.9943 -0.1930 299.7727 299.9657 319.7279 271.8218 -0.1972 299.9783 300.1755 319.6339 272.5775 -0.2036 300.1718 300.3754 319.5252 273.4353 -0.2050 300.3396 300.5446 319.3773 274.1910 -0.2057 300.5141 300.7198 319.2712 275.0185 -0.2086 300.7132 300.9219 319.1722 275.7843 -0.2094 300.8882 301.0976 319.0713 276.6323 -0.2106 301.0640 301.2746 318.9668 277.4083 -0.2126 301.2215 301.4341 318.8971 278.2255 -0.2138 301.3972 301.6110 318.8076 279.0223 -0.2140 301.5778 301.7918 318.7215 279.8185 -0.2137 301.7593 301.9730 318.6757 280.6460 -0.2168 301.8943 302.1111 318.6641 281.4120 -0.2197 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