DTA measure 3elso Date: 20251021:1551 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1224.36 s Mass = 959.500 mg data_number = 1524 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1785 -4.9887 449.5399 454.5287 434.4422 1.9958 -4.9621 449.6185 454.5806 434.6023 2.7720 -4.9339 449.7035 454.6374 434.7203 3.5990 -4.9062 449.8003 454.7065 434.8502 4.3648 -4.8776 449.9014 454.7789 434.9214 5.2233 -4.8487 449.9942 454.8428 435.0115 5.9888 -4.8237 450.0555 454.8792 435.0465 6.8058 -4.7948 450.1466 454.9414 435.0407 7.6128 -4.7690 450.2355 455.0045 434.9591 8.3990 -4.7429 450.3250 455.0679 434.9064 9.2160 -4.7178 450.4131 455.1308 434.8311 9.9923 -4.6929 450.5254 455.2184 434.7248 10.8400 -4.6674 450.6194 455.2868 434.5941 11.6058 -4.6435 450.7180 455.3615 434.4137 12.4435 -4.6185 450.7906 455.4091 434.2281 13.1990 -4.5971 450.8660 455.4631 434.0547 14.0465 -4.5703 450.9871 455.5574 433.8231 14.8228 -4.5428 451.0562 455.5990 433.5998 15.6398 -4.5185 451.1153 455.6338 433.3344 16.4465 -4.4964 451.1745 455.6709 433.0845 17.2328 -4.4721 451.2693 455.7414 432.8298 18.0703 -4.4499 451.3751 455.8250 432.5237 18.8260 -4.4275 451.4897 455.9172 432.2531 19.6838 -4.4010 451.6026 456.0036 431.9597 20.4495 -4.3759 451.6845 456.0604 431.7001 21.2768 -4.3535 451.7637 456.1172 431.4016 22.0735 -4.3283 451.8207 456.1490 431.1107 22.8903 -4.3009 451.8947 456.1956 430.8145 23.6665 -4.2781 452.0012 456.2793 430.5403 24.4940 -4.2561 452.0471 456.3032 430.2811 25.2800 -4.2358 452.0983 456.3341 430.0405 26.0868 -4.2146 452.1822 456.3968 429.8103 26.9040 -4.1953 452.2687 456.4640 429.5976 27.6698 -4.1747 452.3304 456.5051 429.4177 28.5278 -4.1488 452.3462 456.4951 429.1876 29.2938 -4.1238 452.4304 456.5542 429.0245 30.1210 -4.1042 452.5241 456.6283 428.8425 30.9073 -4.0830 452.5881 456.6711 428.7370 31.7143 -4.0627 452.6126 456.6753 428.6492 32.5620 -4.0392 452.6927 456.7319 428.5380 33.3278 -4.0181 452.7508 456.7688 428.4721 34.1550 -3.9977 452.7961 456.7938 428.4208 34.9210 -3.9829 452.8780 456.8609 428.3808 35.7685 -3.9648 452.9544 456.9192 428.3859 36.5448 -3.9480 453.0015 456.9495 428.3945 37.3620 -3.9299 453.0549 456.9848 428.4273 38.1583 -3.9092 453.0910 457.0003 428.4865 38.9550 -3.8947 453.1211 457.0158 428.5456 39.7925 -3.8773 453.1472 457.0245 428.5968 40.5480 -3.8605 453.2288 457.0892 428.6455 41.4060 -3.8448 453.2785 457.1234 428.7292 42.1720 -3.8313 453.3178 457.1492 428.7838 42.9993 -3.8185 453.3763 457.1948 428.8192 43.7853 -3.8035 453.4037 457.2072 428.8725 44.6128 -3.7903 453.4191 457.2094 428.8980 45.4093 -3.7821 453.4583 457.2404 428.9057 46.1955 -3.7709 453.5037 457.2746 428.8947 47.0330 -3.7578 453.5703 457.3281 428.8902 47.7888 -3.7456 453.6649 457.4106 428.8445 48.6468 -3.7310 453.7032 457.4342 428.8132 49.4125 -3.7196 453.7398 457.4594 428.7790 50.2398 -3.7078 453.7641 457.4720 428.6880 51.0263 -3.6945 453.7901 457.4846 428.6003 51.8225 -3.6811 453.8048 457.4858 428.5243 52.6500 -3.6700 453.8123 457.4823 428.4199 53.4055 -3.6640 453.8539 457.5179 428.2817 54.2328 -3.6541 453.8625 457.5165 428.1357 54.9985 -3.6437 453.8790 457.5227 428.0063 55.8463 -3.6321 453.9267 457.5588 427.8198 56.6123 -3.6177 453.9792 457.5969 427.6190 57.4395 -3.6088 454.0488 457.6577 427.4047 58.2363 -3.5967 454.1031 457.6998 427.1941 59.0225 -3.5841 454.1315 457.7156 427.0178 59.8495 -3.5724 454.1711 457.7435 426.7942 60.6155 -3.5598 454.1744 457.7343 426.5921 61.4635 -3.5492 454.2260 457.7753 426.3492 62.2088 -3.5398 454.2417 457.7815 426.1325 63.0568 -3.5298 454.2612 457.7910 425.9364 63.8225 -3.5208 454.2900 457.8107 425.7634 64.6495 -3.5076 454.3178 457.8254 425.5872 65.4463 -3.4962 454.3357 457.8319 425.3751 66.2328 -3.4834 454.3492 457.8326 425.1582 67.0598 -3.4755 454.3978 457.8733 424.9236 67.8258 -3.4690 454.4144 457.8833 424.7323 68.6840 -3.4626 454.4257 457.8884 424.5220 69.4393 -3.4523 454.4464 457.8987 424.3771 70.2770 -3.4416 454.4459 457.8875 424.1894 71.0633 -3.4329 454.4699 457.9027 424.0440 71.8598 -3.4244 454.4785 457.9029 423.9024 72.6870 -3.4169 454.4907 457.9076 423.7688 73.4530 -3.4076 454.4668 457.8744 423.6562 74.3110 -3.4017 454.4493 457.8510 423.5920 75.0665 -3.3924 454.4402 457.8326 423.5432 75.9040 -3.3854 454.4661 457.8515 423.4890 76.6905 -3.3752 454.5191 457.8943 423.4374 77.4868 -3.3621 454.5604 457.9225 423.4219 78.3143 -3.3524 454.5618 457.9142 423.3891 79.0800 -3.3464 454.5630 457.9093 423.3611 79.9380 -3.3354 454.5570 457.8924 423.3283 80.6935 -3.3329 454.5896 457.9225 423.3177 81.5310 -3.3304 454.5836 457.9140 423.3109 82.3175 -3.3275 454.5984 457.9258 423.2937 83.1138 -3.3221 454.5984 457.9205 423.2754 83.9410 -3.3159 454.5992 457.9151 423.2565 84.7070 -3.3098 454.5938 457.9036 423.2114 85.5650 -3.3038 454.6238 457.9276 423.1642 86.3205 -3.2964 454.6262 457.9226 423.1208 87.1583 -3.2941 454.6248 457.9190 423.0950 87.9445 -3.2861 454.6130 457.8991 423.0122 88.7410 -3.2798 454.6116 457.8915 422.9743 89.5685 -3.2758 454.5869 457.8627 422.9204 90.3343 -3.2712 454.5699 457.8411 422.8481 91.1923 -3.2715 454.5686 457.8401 422.7767 91.9480 -3.2649 454.5778 457.8427 422.6990 92.7855 -3.2564 454.5659 457.8223 422.5825 93.5718 -3.2534 454.5784 457.8318 422.4765 94.3890 -3.2507 454.5092 457.7599 422.3961 95.1855 -3.2416 454.5146 457.7562 422.2883 95.9820 -3.2341 454.5280 457.7622 422.1763 96.8093 -3.2306 454.5234 457.7540 422.0425 97.5855 -3.2288 454.5194 457.7482 421.9298 98.4330 -3.2238 454.5207 457.7444 421.8035 99.1990 -3.2194 454.5280 457.7474 421.6618 100.0263 -3.2153 454.4884 457.7037 421.5078 100.8228 -3.2137 454.4540 457.6678 421.3447 101.6193 -3.2089 454.4746 457.6835 421.1884 102.4363 -3.2026 454.4792 457.6818 421.0089 103.2125 -3.1996 454.4679 457.6675 420.8544 104.0600 -3.1959 454.4382 457.6341 420.6679 104.8155 -3.1922 454.4198 457.6121 420.5211 105.6533 -3.1872 454.4086 457.5957 420.3661 106.4190 -3.1870 454.3936 457.5807 420.2279 107.2665 -3.1805 454.3454 457.5258 420.0435 108.0428 -3.1732 454.3203 457.4935 419.8930 108.8700 -3.1682 454.3277 457.4959 419.7177 109.6665 -3.1666 454.3098 457.4764 419.5692 110.4528 -3.1647 454.2872 457.4519 419.4236 111.2905 -3.1598 454.2773 457.4371 419.2698 112.0563 -3.1583 454.2648 457.4230 419.1285 112.9143 -3.1586 454.2884 457.4470 418.9957 113.6700 -3.1559 454.2612 457.4171 418.8928 114.5075 -3.1532 454.2482 457.4014 418.7961 115.2528 -3.1487 454.2334 457.3821 418.6993 116.1108 -3.1413 454.1684 457.3097 418.5842 116.8768 -3.1376 454.1391 457.2767 418.5040 117.6935 -3.1324 454.0968 457.2292 418.4332 118.4903 -3.1290 454.0771 457.2061 418.3469 119.2870 -3.1303 454.0318 457.1621 418.2663 120.0730 -3.1265 454.0079 457.1344 418.2097 120.8695 -3.1248 453.9921 457.1169 418.1262 121.6970 -3.1240 453.9369 457.0609 418.0309 122.4525 -3.1230 453.9267 457.0497 417.9627 123.3208 -3.1207 453.9044 457.0251 417.8937 124.0765 -3.1171 453.9225 457.0396 417.8103 124.9140 -3.1149 453.8751 456.9901 417.7222 125.6593 -3.1127 453.8594 456.9721 417.6712 126.5173 -3.1086 453.8421 456.9507 417.5839 127.2833 -3.1073 453.7907 456.8980 417.5255 128.1105 -3.1071 453.7439 456.8510 417.4201 128.9070 -3.1052 453.6583 456.7635 417.3750 129.6935 -3.1014 453.6362 456.7376 417.2836 130.4898 -3.1014 453.6154 456.7169 417.2387 131.2865 -3.0997 453.5996 456.6993 417.1930 132.1038 -3.0959 453.5538 456.6496 417.1226 132.8795 -3.0878 453.5270 456.6148 417.0642 133.7275 -3.0880 453.4801 456.5681 417.0001 134.4935 -3.0833 453.4500 456.5333 416.9156 135.3308 -3.0779 453.4318 456.5097 416.7992 136.0865 -3.0770 453.4029 456.4799 416.6786 136.9343 -3.0730 453.3391 456.4121 416.5779 137.7103 -3.0723 453.3182 456.3905 416.4584 138.5273 -3.0706 453.2923 456.3628 416.3589 139.3238 -3.0697 453.2665 456.3362 416.2517 140.1205 -3.0679 453.2173 456.2853 416.1279 140.9475 -3.0645 453.1563 456.2208 416.0139 141.7135 -3.0633 453.1239 456.1872 415.9152 142.5613 -3.0614 453.0719 456.1333 415.8139 143.3373 -3.0632 453.0271 456.0903 415.7121 144.1540 -3.0613 452.9787 456.0400 415.5955 144.9200 -3.0531 452.9599 456.0130 415.4858 145.7680 -3.0535 452.8826 455.9362 415.3118 146.5338 -3.0536 452.8430 455.8966 415.2032 147.3610 -3.0559 452.7890 455.8449 415.1076 148.1578 -3.0556 452.7201 455.7757 414.9760 148.9540 -3.0566 452.6786 455.7352 414.8488 149.7813 -3.0568 452.6568 455.7137 414.7051 150.5473 -3.0542 452.6151 455.6692 414.6248 151.4053 -3.0510 452.5931 455.6441 414.4717 152.1403 -3.0480 452.6042 455.6522 414.3371 152.9883 -3.0471 452.5590 455.6061 414.2279 153.7643 -3.0381 452.5049 455.5430 414.1108 154.5915 -3.0362 452.4616 455.4978 413.9900 155.3883 -3.0354 452.4007 455.4361 413.8427 156.2155 -3.0367 452.3732 455.4099 413.6961 157.0018 -3.0355 452.3451 455.3807 413.5562 157.7985 -3.0357 452.3106 455.3463 413.4384 158.5950 -3.0339 452.2856 455.3195 413.3113 159.4018 -3.0308 452.2226 455.2534 413.2083 160.2190 -3.0255 452.1455 455.1710 413.0766 160.9848 -3.0228 452.1132 455.1359 412.9630 161.8425 -3.0216 452.0230 455.0446 412.8536 162.6188 -3.0176 451.9265 454.9441 412.7237 163.4360 -3.0173 451.8523 454.8696 412.6243 164.2323 -3.0141 451.8141 454.8283 412.5361 165.0290 -3.0127 451.7945 454.8072 412.4353 165.8563 -3.0138 451.7462 454.7600 412.3203 166.6425 -3.0104 451.7175 454.7279 412.1755 167.4595 -3.0058 451.6553 454.6611 412.0835 168.2253 -3.0015 451.5972 454.5986 411.9896 169.0835 -2.9993 451.5325 454.5318 411.9069 169.8490 -3.0015 451.4858 454.4873 411.8460 170.6765 -3.0024 451.4324 454.4348 411.7583 171.4630 -2.9999 451.3952 454.3951 411.7004 172.2695 -2.9994 451.3641 454.3635 411.6281 173.0865 -2.9971 451.2980 454.2951 411.5595 173.8525 -2.9937 451.2194 454.2131 411.4703 174.6798 -2.9944 451.1223 454.1167 411.3685 175.4558 -2.9966 451.0483 454.0449 411.2760 176.3035 -2.9932 450.9728 453.9661 411.2047 177.0695 -2.9921 450.9189 453.9110 411.1485 177.8965 -2.9937 450.8755 453.8692 411.0677 178.6930 -2.9918 450.8347 453.8265 410.9826 179.4795 -2.9885 450.7790 453.7675 410.8738 180.3068 -2.9881 450.7479 453.7359 410.7716 181.0620 -2.9837 450.6999 453.6836 410.7089 181.8895 -2.9839 450.6201 453.6040 410.6228 182.6555 -2.9820 450.5618 453.5438 410.5246 183.5030 -2.9780 450.5085 453.4865 410.4055 184.2688 -2.9785 450.4471 453.4256 410.3121 185.0963 -2.9746 450.3828 453.3574 410.1980 185.8825 -2.9698 450.3330 453.3028 410.0935 186.6790 -2.9686 450.2461 453.2147 410.0067 187.4755 -2.9692 450.1790 453.1482 409.8980 188.2723 -2.9692 450.1301 453.0993 409.7906 189.0993 -2.9699 450.0652 453.0351 409.6691 189.8548 -2.9686 449.9994 452.9680 409.5557 190.7130 -2.9726 449.9809 452.9536 409.4250 191.4788 -2.9720 449.9476 452.9197 409.3271 192.2958 -2.9730 449.8321 452.8051 409.1800 193.0718 -2.9671 449.7240 452.6911 409.0782 193.8888 -2.9666 449.6503 452.6169 408.9655 194.6853 -2.9636 449.6086 452.5722 408.8277 195.4815 -2.9601 449.5652 452.5253 408.7170 196.3090 -2.9556 449.5130 452.4686 408.5991 197.0748 -2.9552 449.4458 452.4010 408.4867 197.9225 -2.9568 449.3423 452.2991 408.3615 198.6678 -2.9549 449.2950 452.2498 408.2851 199.5158 -2.9511 449.2289 452.1800 408.1249 200.2815 -2.9529 449.1604 452.1133 407.9923 201.1085 -2.9511 449.1080 452.0591 407.8900 201.9053 -2.9522 449.0685 452.0207 407.7801 202.7020 -2.9504 449.0168 451.9672 407.6809 203.5290 -2.9458 448.9352 451.8810 407.5736 204.2950 -2.9480 448.8663 451.8144 407.4381 205.1223 -2.9474 448.8169 451.7643 407.2810 205.8880 -2.9448 448.7595 451.7043 407.1918 206.7358 -2.9400 448.6824 451.6224 407.0655 207.5120 -2.9354 448.6295 451.5650 406.9299 208.3290 -2.9318 448.5593 451.4911 406.8331 209.1358 -2.9308 448.5038 451.4345 406.7415 209.9223 -2.9319 448.4369 451.3687 406.6587 210.7598 -2.9297 448.3533 451.2830 406.5757 211.5153 -2.9265 448.2844 451.2109 406.4740 212.3425 -2.9256 448.2185 451.1441 406.3614 213.1085 -2.9242 448.1297 451.0539 406.2399 213.9663 -2.9207 448.0625 450.9833 406.1293 214.7323 -2.9222 448.0170 450.9391 406.0409 215.5495 -2.9214 447.9415 450.8629 405.9202 216.3560 -2.9220 447.8860 450.8080 405.8341 217.1423 -2.9170 447.8223 450.7393 405.7497 217.9800 -2.9127 447.7466 450.6593 405.6422 218.7355 -2.9110 447.6635 450.5745 405.5288 219.6038 -2.9099 447.5708 450.4807 405.4549 220.3698 -2.9094 447.4801 450.3895 405.3762 221.1970 -2.9083 447.4262 450.3345 405.2856 221.9830 -2.9102 447.3576 450.2679 405.2319 222.7900 -2.9097 447.2747 450.1844 405.1435 223.5765 -2.9055 447.1827 450.0882 405.0477 224.3830 -2.9053 447.0941 449.9994 404.9784 225.2000 -2.9075 446.9992 449.9067 404.8799 225.9763 -2.9078 446.9358 449.8437 404.7683 226.8240 -2.9059 446.8541 449.7600 404.6517 227.6000 -2.9049 446.8051 449.7100 404.5680 228.4173 -2.9006 446.7582 449.6588 404.4517 229.1933 -2.8999 446.6653 449.5652 404.3499 230.0203 -2.9004 446.5974 449.4978 404.2283 230.8168 -2.9003 446.5220 449.4223 404.1256 231.6033 -2.8992 446.4633 449.3626 404.0195 232.4408 -2.8968 446.3542 449.2509 403.9123 233.2065 -2.8963 446.2654 449.1616 403.8018 234.0648 -2.8918 446.1903 449.0821 403.6910 234.8203 -2.8900 446.1049 448.9949 403.5910 235.6578 -2.8900 446.0267 448.9167 403.4774 236.4440 -2.8869 445.9462 448.8331 403.3538 237.2408 -2.8865 445.8816 448.7681 403.2422 238.0680 -2.8799 445.8190 448.6989 403.1446 238.8338 -2.8769 445.7351 448.6120 403.0329 239.6920 -2.8720 445.6144 448.4865 402.9071 240.4475 -2.8673 445.5605 448.4278 402.8122 241.2853 -2.8662 445.4505 448.3167 402.7027 242.0715 -2.8665 445.4000 448.2665 402.5895 242.8680 -2.8660 445.3497 448.2157 402.4809 243.6648 -2.8656 445.2708 448.1364 402.3335 244.4510 -2.8657 445.1943 448.0600 402.2593 245.2680 -2.8643 445.1217 447.9860 402.1645 246.0440 -2.8637 445.0405 447.9042 402.0565 246.8920 -2.8631 444.9877 447.8508 401.9252 247.6473 -2.8609 444.9292 447.7901 401.8302 248.4850 -2.8601 444.8650 447.7251 401.7431 249.2715 -2.8591 444.7543 447.6133 401.6357 250.0678 -2.8609 444.6569 447.5177 401.5242 250.8955 -2.8574 444.6009 447.4582 401.4053 251.6510 -2.8534 444.5429 447.3963 401.2743 252.5088 -2.8532 444.4243 447.2775 401.1531 253.2440 -2.8518 444.3168 447.1687 401.0328 254.0920 -2.8484 444.2318 447.0802 400.9046 254.8678 -2.8468 444.1631 447.0099 400.7815 255.6848 -2.8436 444.0878 446.9313 400.6505 256.4918 -2.8393 444.0375 446.8768 400.5420 257.2780 -2.8367 443.9820 446.8188 400.4551 258.1053 -2.8352 443.8933 446.7286 400.3389 258.8713 -2.8344 443.8112 446.6456 400.2284 259.7190 -2.8318 443.7129 446.5448 400.1089 260.4848 -2.8339 443.6343 446.4682 399.9956 261.3123 -2.8322 443.5271 446.3593 399.8771 262.1088 -2.8296 443.4473 446.2768 399.7648 262.9053 -2.8293 443.3412 446.1705 399.6906 263.7225 -2.8278 443.2360 446.0638 399.6046 264.4985 -2.8291 443.1494 445.9785 399.4890 265.3463 -2.8263 443.0891 445.9154 399.3963 266.0813 -2.8226 443.0214 445.8440 399.3037 266.9395 -2.8189 442.9788 445.7977 399.2035 267.7053 -2.8181 442.8897 445.7078 399.0975 268.5328 -2.8180 442.7790 445.5970 398.9955 269.3293 -2.8145 442.6845 445.4990 398.9042 270.1255 -2.8105 442.5946 445.4051 398.8280 270.9530 -2.8091 442.5423 445.3514 398.7014 271.7188 -2.8099 442.4584 445.2682 398.6115 272.5665 -2.8099 442.3800 445.1899 398.5302 273.3425 -2.8090 442.2919 445.1009 398.4682 274.1598 -2.8071 442.2143 445.0214 398.3732 274.9563 -2.8079 442.1263 444.9342 398.3006 275.7525 -2.8073 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748.9393 3.1282 387.3526 384.2245 335.9748 749.7360 3.2038 387.3299 384.1260 335.8516 750.5528 3.2805 387.2758 383.9953 335.7620 751.3290 3.3552 387.2576 383.9025 335.6498 752.1770 3.4391 387.2507 383.8116 335.5378 752.9425 3.5157 387.2467 383.7309 335.4596 753.7700 3.5947 387.2365 383.6418 335.3667 754.5668 3.6674 387.2192 383.5517 335.2673 755.3630 3.7402 387.2048 383.4646 335.1674 756.1700 3.8125 387.2014 383.3889 335.0685 756.9563 3.8818 387.1505 383.2687 334.9569 757.7835 3.9601 387.1355 383.1754 334.8278 758.5390 4.0302 387.1371 383.1069 334.7453 759.3973 4.1126 387.1145 383.0018 334.6535 760.1528 4.1845 387.0983 382.9137 334.5435 760.9798 4.2631 387.1090 382.8460 334.4418 761.7460 4.3372 387.0837 382.7464 334.3513 762.5733 4.4178 387.0728 382.6550 334.2364 763.3593 4.4881 387.0437 382.5556 334.1288 764.1560 4.5622 387.0323 382.4701 334.0447 764.9835 4.6421 387.0074 382.3653 333.9458 765.7388 4.7114 386.9883 382.2769 333.8419 766.5970 4.7902 386.9861 382.1959 333.6870 767.3525 4.8651 386.9684 382.1033 333.5894 768.1798 4.9383 386.9243 381.9859 333.4646 768.9763 5.0100 386.8784 381.8683 333.3878 769.7628 5.0835 386.8697 381.7862 333.3098 770.5900 5.1598 386.8310 381.6712 333.1899 771.3555 5.2323 386.8091 381.5768 333.0756 772.2138 5.3176 386.7741 381.4565 332.9005 773.0410 5.3951 386.7710 381.3759 332.7835 773.7965 5.4672 386.7579 381.2907 332.6354 774.6545 5.5456 386.7462 381.2006 332.5314 775.4203 5.6123 386.7297 381.1175 332.4368 776.2373 5.6864 386.7204 381.0340 332.3332 777.0440 5.7597 386.7204 380.9608 332.2244 777.8303 5.8324 386.7356 380.9032 332.1301 778.6578 5.9121 386.7224 380.8103 332.0156 779.4235 5.9852 386.7136 380.7284 331.9359 780.2815 6.0684 386.6909 380.6225 331.8114 781.0475 6.1345 386.6614 380.5269 331.7028 781.8645 6.2095 386.6271 380.4176 331.6026 782.6710 6.2805 386.5912 380.3108 331.5032 783.4575 6.3500 386.5801 380.2301 331.4210 784.2850 6.4264 386.5540 380.1276 331.3486 785.0505 6.4961 386.5385 380.0424 331.2383 785.9088 6.5764 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