DTA measure 1lassufutes Date: 2024101:1156 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1273.99 s Mass = 954.300 mg data_number = 1584 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2765 -0.8717 253.2498 254.1215 266.3676 2.0985 -0.8692 253.3952 254.2644 266.3430 2.8605 -0.8711 253.4948 254.3659 266.3251 3.7125 -0.8618 253.5942 254.4560 266.3035 4.5045 -0.8494 253.6644 254.5137 266.3772 5.2965 -0.8280 253.7137 254.5416 266.2825 6.1193 -0.8606 253.8782 254.7387 266.4399 6.8825 -0.8383 254.0064 254.8447 266.4313 7.7345 -0.8219 254.0989 254.9208 266.4908 8.4960 -0.8126 254.2169 255.0295 266.5190 9.3185 -0.8190 254.3455 255.1645 266.5043 10.1403 -0.8040 254.3967 255.2007 266.4592 10.9020 -0.8009 254.5462 255.3472 266.5214 11.7540 -0.8106 254.7040 255.5146 266.6608 12.5158 -0.8145 254.7374 255.5519 266.7103 13.3378 -0.8071 254.9430 255.7501 266.6912 14.1598 -0.7960 255.1566 255.9525 266.9504 14.9215 -0.8015 255.2552 256.0566 267.2198 15.7738 -0.7968 255.3046 256.1014 267.1808 16.5355 -0.7930 255.5206 256.3136 267.3309 17.3585 -0.7989 255.6898 256.4887 267.3832 18.1810 -0.7940 255.8775 256.6715 267.3705 18.9435 -0.7914 255.9973 256.7887 267.4895 19.7958 -0.7729 256.0338 256.8068 267.6225 20.5575 -0.7770 256.1180 256.8951 267.6720 21.3798 -0.7619 256.2379 256.9999 267.7674 22.1635 -0.7606 256.3963 257.1570 267.9728 22.9925 -0.7643 256.5382 257.3026 268.1870 23.7845 -0.7542 256.7040 257.4582 268.2328 24.5765 -0.7477 256.8535 257.6013 268.4318 25.3988 -0.7496 256.8588 257.6084 268.5116 26.1615 -0.7436 256.9676 257.7112 268.6329 27.0135 -0.7447 257.1800 257.9248 268.8861 27.8055 -0.7552 257.2140 257.9692 269.2203 28.5975 -0.7520 257.3080 258.0600 269.2863 29.4195 -0.7282 257.4614 258.1896 269.4188 30.1815 -0.7168 257.6018 258.3186 269.5189 31.0338 -0.7134 257.8619 258.5753 269.6396 31.8260 -0.7277 257.8617 258.5894 269.7161 32.6175 -0.7369 257.9312 258.6681 269.7798 33.4398 -0.7252 258.0487 258.7739 269.8762 34.2015 -0.7273 258.2871 259.0143 270.0822 35.0538 -0.7171 258.4147 259.1318 270.1052 35.8458 -0.7206 258.3870 259.1076 270.2254 36.6375 -0.7128 258.4762 259.1890 270.3288 37.4595 -0.7172 258.5719 259.2891 270.3813 38.2185 -0.7256 258.6250 259.3507 270.5469 39.0688 -0.7026 258.7232 259.4258 270.6962 39.8273 -0.6993 258.8752 259.5746 270.8368 40.6470 -0.6993 258.9382 259.6375 270.8545 41.4658 -0.6860 259.0001 259.6861 270.9568 42.2350 -0.6891 258.9343 259.6234 271.0356 43.0445 -0.7015 259.0051 259.7066 271.1132 43.8330 -0.6947 259.2613 259.9560 271.1623 44.6810 -0.6860 259.4637 260.1497 271.3205 45.4393 -0.6835 259.5484 260.2318 271.4433 46.2590 -0.6719 259.6477 260.3197 271.5967 47.0470 -0.6809 259.6188 260.2997 271.6324 47.8370 -0.6711 259.6662 260.3373 271.7526 48.6880 -0.6760 259.8560 260.5320 271.8561 49.4495 -0.6641 260.0676 260.7317 271.9507 50.2708 -0.6761 260.1326 260.8087 272.0135 51.0628 -0.6822 260.2463 260.9285 272.1262 51.8543 -0.6756 260.3425 261.0182 272.2447 52.6745 -0.6815 260.4867 261.1682 272.2658 53.4663 -0.6598 260.5685 261.2283 272.3018 54.2875 -0.6507 260.5418 261.1925 272.4023 55.0795 -0.6596 260.8205 261.4802 272.4905 55.8715 -0.6576 260.8762 261.5338 272.6588 56.6938 -0.6654 260.8748 261.5402 272.8158 57.4555 -0.6438 260.9172 261.5610 272.8308 58.3073 -0.6528 261.0555 261.7083 272.9117 59.0985 -0.6301 261.0968 261.7269 273.1131 59.8905 -0.6275 261.1553 261.7828 273.2498 60.7125 -0.6357 261.3535 261.9891 273.3251 61.4745 -0.6194 261.3999 262.0193 273.3807 62.3265 -0.6352 261.4302 262.0654 273.5313 63.0998 -0.6479 261.5015 262.1494 273.6744 63.9245 -0.6475 261.7062 262.3537 273.8075 64.7165 -0.6319 261.7770 262.4090 273.8340 65.5085 -0.6361 261.7911 262.4272 273.9409 66.3303 -0.6297 261.8403 262.4701 274.0256 67.1225 -0.6428 261.8813 262.5241 274.1840 67.9443 -0.6441 262.0114 262.6555 274.2808 68.7360 -0.6437 262.0383 262.6820 274.4021 69.5278 -0.6501 262.0439 262.6940 274.5123 70.3798 -0.6453 262.0008 262.6460 274.7100 71.1418 -0.6510 262.1859 262.8368 274.7828 71.9638 -0.6494 262.3095 262.9589 274.8137 72.7560 -0.6484 262.4240 263.0724 274.9669 73.5475 -0.6459 262.3659 263.0117 275.0644 74.3998 -0.6416 262.5606 263.2022 275.0725 75.1615 -0.6354 262.6919 263.3273 275.1387 75.9838 -0.6391 262.7896 263.4288 275.3205 76.8058 -0.6532 262.9074 263.5606 275.4579 77.5675 -0.6426 262.9468 263.5894 275.6219 78.4198 -0.6481 263.1240 263.7721 275.7291 79.1815 -0.6591 263.1707 263.8298 275.8073 80.0035 -0.6504 263.2636 263.9140 275.9412 80.8255 -0.6463 263.4648 264.1111 276.0760 81.5875 -0.6471 263.5090 264.1561 276.2038 82.4395 -0.6447 263.7115 264.3562 276.2444 83.2315 -0.6392 263.7674 264.4067 276.2651 84.0235 -0.6384 263.8579 264.4964 276.4834 84.8455 -0.6444 264.0042 264.6486 276.5811 85.6375 -0.6357 264.0798 264.7154 276.6432 86.4595 -0.6296 264.1497 264.7793 276.7663 87.2515 -0.6414 264.3019 264.9433 276.9329 88.0435 -0.6291 264.5368 265.1659 277.0416 88.8655 -0.6223 264.6868 265.3091 277.1104 89.6575 -0.6099 264.9092 265.5191 277.1939 90.4788 -0.6279 265.0220 265.6499 277.3451 91.2710 -0.6238 265.1639 265.7877 277.3441 92.0635 -0.6249 265.3882 266.0131 277.4506 92.8860 -0.6243 265.5117 266.1360 277.6187 93.6545 -0.6347 265.6011 266.2357 277.7364 94.5095 -0.6349 265.6398 266.2747 277.8243 95.3018 -0.6422 265.7859 266.4281 277.9760 96.0945 -0.6373 265.9033 266.5406 278.0104 96.9168 -0.6271 266.0672 266.6943 278.1004 97.6785 -0.6306 266.2131 266.8438 278.1742 98.5308 -0.6331 266.1907 266.8238 278.3475 99.3228 -0.6295 266.3014 266.9309 278.4016 100.1155 -0.6318 266.3537 266.9856 278.5318 100.9380 -0.6344 266.4941 267.1285 278.7128 101.7290 -0.6307 266.4728 267.1035 278.7859 102.5483 -0.6348 266.6098 267.2446 278.8962 103.3370 -0.6441 266.8059 267.4499 278.9567 104.1260 -0.6398 266.9516 267.5913 279.1021 104.9448 -0.6433 267.0166 267.6600 279.1738 105.7038 -0.6336 267.1443 267.7778 279.2268 106.5535 -0.6359 267.2784 267.9143 279.3348 107.3130 -0.6368 267.3479 267.9848 279.5060 108.1318 -0.6430 267.5122 268.1552 279.6677 108.9513 -0.6478 267.6209 268.2687 279.7453 109.7110 -0.6441 267.7427 268.3868 279.8185 110.5598 -0.6548 267.8070 268.4618 279.9697 111.3490 -0.6535 267.9091 268.5626 280.0363 112.1385 -0.6543 268.0473 268.7017 280.2079 112.9573 -0.6513 268.1773 268.8286 280.2728 113.7173 -0.6522 268.2844 268.9366 280.3605 114.5793 -0.6485 268.4199 269.0684 280.4910 115.3408 -0.6708 268.5159 269.1867 280.5987 116.1628 -0.6770 268.6535 269.3304 280.7486 116.9545 -0.6657 268.7413 269.4070 280.8009 117.7465 -0.6685 268.9154 269.5839 280.7871 118.5685 -0.6553 269.0210 269.6763 280.9479 119.3295 -0.6662 269.0001 269.6663 281.0192 120.1818 -0.6698 269.0998 269.7696 281.1282 120.9435 -0.6762 269.2807 269.9569 281.2381 121.7655 -0.6749 269.4880 270.1630 281.3546 122.5875 -0.6807 269.6248 270.3055 281.4926 123.3495 -0.6867 269.7941 270.4808 281.6955 124.2013 -0.6892 269.8548 270.5440 281.7850 124.9630 -0.6810 270.0011 270.6821 281.9611 125.7853 -0.6807 270.0181 270.6988 281.9862 126.5773 -0.6908 270.1959 270.8868 282.0610 127.3688 -0.6834 270.3345 271.0180 282.2197 128.1913 -0.6816 270.3895 271.0712 282.2987 128.9825 -0.6903 270.4855 271.1758 282.3560 129.8048 -0.6910 270.6380 271.3290 282.6264 130.5968 -0.6858 270.7481 271.4339 282.8255 131.3885 -0.6734 270.9484 271.6218 282.9679 132.2108 -0.6790 270.9949 271.6739 283.1419 133.0025 -0.6873 271.1425 271.8298 283.1842 133.8248 -0.6833 271.1776 271.8609 283.2101 134.5943 -0.6823 271.3580 272.0403 283.2757 135.4248 -0.6729 271.4022 272.0751 283.3981 136.2168 -0.6751 271.4929 272.1680 283.4982 137.0085 -0.6837 271.5717 272.2554 283.5226 137.8308 -0.6827 271.6504 272.3331 283.6618 138.6225 -0.6792 271.8585 272.5376 283.9090 139.4445 -0.6825 271.9485 272.6310 283.9243 140.2365 -0.6850 272.0497 272.7347 284.0636 141.0285 -0.7074 272.1020 272.8094 284.0135 141.8515 -0.6976 272.2034 272.9010 284.1457 142.6435 -0.6657 272.3838 273.0495 284.2072 143.4655 -0.6509 272.5171 273.1680 284.2888 144.2575 -0.6530 272.6037 273.2567 284.3161 145.0505 -0.6443 272.7339 273.3782 284.4812 145.8725 -0.6573 272.7034 273.3607 284.6003 146.6345 -0.6755 272.8323 273.5078 284.7419 147.4865 -0.6951 273.0148 273.7099 284.7911 148.2785 -0.6968 273.1726 273.8694 284.9908 149.0708 -0.7018 273.2497 273.9515 285.1500 149.8933 -0.7130 273.4797 274.1927 285.3523 150.6545 -0.7090 273.5493 274.2583 285.4048 151.5070 -0.7015 273.5675 274.2690 285.4317 152.2988 -0.7131 273.7104 274.4235 285.4396 153.0905 -0.7035 273.7369 274.4405 285.4028 153.9140 -0.7122 273.8958 274.6081 285.4295 154.6765 -0.7090 274.0851 274.7941 285.5092 155.5060 -0.7029 274.1352 274.8381 285.6762 156.2985 -0.7000 274.2386 274.9386 285.8774 157.1208 -0.6911 274.3627 275.0538 286.0315 157.9125 -0.6979 274.4285 275.1263 286.0742 158.7348 -0.7036 274.5818 275.2854 286.2718 159.5268 -0.7113 274.6116 275.3229 286.3786 160.3195 -0.7085 274.8386 275.5471 286.4591 161.1415 -0.7026 275.0184 275.7211 286.5453 161.9335 -0.7106 275.0094 275.7200 286.6443 162.7563 -0.7160 275.1420 275.8580 286.6504 163.5485 -0.7229 275.2376 275.9605 286.7355 164.3415 -0.7154 275.3140 276.0294 286.8897 165.1638 -0.7284 275.4367 276.1651 286.9732 165.9565 -0.7273 275.6285 276.3558 287.0315 166.7768 -0.7081 275.6775 276.3856 287.1241 167.5650 -0.7150 275.7687 276.4838 287.2118 168.3540 -0.7212 275.8679 276.5891 287.3755 169.2023 -0.7228 275.9632 276.6860 287.4787 169.9608 -0.7251 276.0566 276.7817 287.5174 170.7795 -0.7203 276.2165 276.9369 287.6953 171.5680 -0.7400 276.4285 277.1686 287.8181 172.3570 -0.7392 276.4625 277.2017 287.8256 173.2055 -0.7192 276.5071 277.2263 288.0859 173.9638 -0.7242 276.6502 277.3744 288.2136 174.7833 -0.7381 276.7104 277.4485 288.2592 175.6018 -0.7270 276.9327 277.6597 288.4822 176.3623 -0.7332 277.0364 277.7696 288.5003 177.2118 -0.7427 277.1495 277.8922 288.5809 177.9718 -0.7411 277.2366 277.9777 288.6407 178.7925 -0.7626 277.4395 278.2021 288.7448 179.6120 -0.7419 277.4876 278.2296 288.8068 180.3735 -0.7449 277.5622 278.3071 289.0256 181.2250 -0.7655 277.6255 278.3910 289.1898 181.9860 -0.7545 277.7259 278.4804 289.2508 182.8078 -0.7584 277.8446 278.6030 289.3077 183.6283 -0.7637 277.9376 278.7013 289.4735 184.3898 -0.7522 277.9955 278.7476 289.6001 185.2420 -0.7522 278.1479 278.9000 289.7531 186.0030 -0.7644 278.2671 279.0315 289.8836 186.8248 -0.7704 278.5053 279.2757 289.8642 187.6468 -0.7560 278.5436 279.2996 289.9071 188.4085 -0.7611 278.5099 279.2710 290.0860 189.2608 -0.7532 278.6820 279.4351 290.0453 190.0228 -0.7630 278.8196 279.5826 290.1566 190.8448 -0.7561 278.8747 279.6308 290.2741 191.6665 -0.7653 279.0636 279.8289 290.3606 192.4285 -0.7698 279.2198 279.9896 290.6038 193.2808 -0.7587 279.3414 280.1000 290.6851 194.0425 -0.7609 279.3695 280.1304 290.8256 194.8648 -0.7606 279.5154 280.2759 290.9697 195.6865 -0.7786 279.6444 280.4230 290.9979 196.4485 -0.7718 279.7203 280.4921 290.9475 197.3005 -0.7716 279.7848 280.5564 291.1170 198.0925 -0.7703 279.9292 280.6995 291.4560 198.8845 -0.7740 280.0970 280.8710 291.4075 199.7065 -0.7825 280.2364 281.0189 291.4219 200.4685 -0.7801 280.3071 281.0871 291.4354 201.3205 -0.7894 280.4468 281.2362 291.5692 202.1128 -0.7763 280.5123 281.2886 291.8516 202.9055 -0.7778 280.5665 281.3442 291.8915 203.7273 -0.7888 280.7120 281.5009 292.0724 204.4895 -0.7913 280.8444 281.6357 292.0132 205.3415 -0.7743 281.0101 281.7844 292.2205 206.1333 -0.7855 280.9885 281.7740 292.5264 206.9248 -0.7996 281.1346 281.9343 292.5120 207.7473 -0.7888 281.2969 282.0857 292.5377 208.5088 -0.7797 281.3944 282.1741 292.9501 209.3610 -0.7919 281.5401 282.3321 293.0306 210.1240 -0.7819 281.5847 282.3666 293.1172 210.9488 -0.7953 281.7394 282.5347 293.0215 211.7708 -0.7840 281.9352 282.7192 293.0469 212.5325 -0.7953 282.0332 282.8285 293.2097 213.3848 -0.8052 282.1061 282.9113 293.5490 214.1465 -0.8173 282.2438 283.0610 293.4745 214.9688 -0.8055 282.3909 283.1964 293.5118 215.7908 -0.7952 282.5843 283.3795 293.6700 216.5525 -0.8115 282.6506 283.4621 293.7450 217.4045 -0.8019 282.8653 283.6672 293.7778 218.1665 -0.8069 283.1071 283.9140 294.0706 218.9885 -0.8051 283.2510 284.0561 294.1680 219.8105 -0.8024 283.3629 284.1653 294.1275 220.5725 -0.8231 283.5624 284.3855 294.2910 221.4245 -0.8220 283.5857 284.4077 294.3794 222.1865 -0.8207 283.6753 284.4960 294.5522 223.0085 -0.8219 283.8398 284.6617 294.5635 223.8305 -0.8284 283.8491 284.6775 294.7558 224.5925 -0.8209 284.0028 284.8237 294.8898 225.4445 -0.8290 284.2016 285.0306 294.9208 226.2063 -0.8283 284.0375 284.8658 295.4590 227.0285 -0.8492 284.4211 285.2703 295.5004 227.8503 -0.8674 284.5928 285.4602 295.7587 228.6115 -0.8715 284.6673 285.5388 295.7354 229.4640 -0.8636 284.7547 285.6182 295.6851 230.2255 -0.8739 284.8573 285.7311 295.9386 231.0450 -0.8663 285.0807 285.9470 295.6438 231.8330 -0.8492 285.3314 286.1806 295.5316 232.6200 -0.8673 285.4055 286.2728 295.7231 233.4680 -0.8731 285.5333 286.4064 295.9238 234.2260 -0.8712 285.5881 286.4593 296.1574 235.0440 -0.8734 285.7212 286.5946 296.0573 235.8323 -0.8772 285.7873 286.6646 295.9691 236.6225 -0.8642 285.7228 286.5869 296.1588 237.4513 -0.8650 285.8252 286.6902 296.1661 238.2103 -0.8813 285.8918 286.7731 296.1842 239.0583 -0.8824 286.0105 286.8929 296.2697 239.8460 -0.8802 286.0808 286.9610 296.4337 240.6340 -0.8867 286.0966 286.9833 296.6099 241.4523 -0.8785 286.1554 287.0339 296.7553 242.2110 -0.8716 286.2711 287.1427 296.8504 243.0610 -0.8581 286.3863 287.2445 296.9449 243.8495 -0.8853 286.4400 287.3253 297.0282 244.6390 -0.8706 286.4688 287.3394 297.1973 245.4575 -0.8676 286.6855 287.5531 297.2790 246.2473 -0.8895 286.7941 287.6836 297.3171 247.0768 -0.8974 286.8518 287.7492 297.5230 247.8453 -0.9103 286.9503 287.8607 297.6054 248.6663 -0.8837 287.1028 287.9865 297.7627 249.4575 -0.8773 287.3382 288.2155 297.9454 250.2493 -0.8961 287.4398 288.3360 298.1064 251.0705 -0.8789 287.4885 288.3674 298.2235 251.8625 -0.8775 287.6088 288.4863 298.4070 252.6845 -0.8930 287.8906 288.7836 298.6036 253.4765 -0.8872 287.9488 288.8360 298.6251 254.2685 -0.8928 287.9795 288.8723 298.6941 255.0910 -0.8944 287.9535 288.8479 298.8648 255.8835 -0.9185 288.0160 288.9345 299.0890 256.7055 -0.9080 288.1954 289.1034 299.3658 257.4725 -0.9404 288.2488 289.1892 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