DTA measure 1pb_elso Date: 202548:153 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.18 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2160 -0.1766 205.5875 205.7641 260.8079 2.0343 -0.1716 205.8365 206.0082 260.8111 2.7930 -0.1650 206.0581 206.2230 260.8293 3.6410 -0.1574 206.2834 206.4408 260.8503 4.3990 -0.1507 206.4876 206.6383 260.8572 5.2178 -0.1450 206.7606 206.9056 260.8680 6.0378 -0.1382 207.0068 207.1450 260.8937 6.7970 -0.1361 207.2350 207.3711 260.9432 7.6458 -0.1295 207.4829 207.6125 260.9738 8.4343 -0.1241 207.7118 207.8358 261.0162 9.2248 -0.1212 207.9356 208.0568 261.0567 10.0433 -0.1167 208.1781 208.2948 261.1180 10.8023 -0.1088 208.3826 208.4914 261.1382 11.6525 -0.1045 208.6839 208.7884 261.2199 12.4425 -0.0985 208.8975 208.9960 261.3095 13.2333 -0.0948 209.1130 209.2077 261.3681 14.0545 -0.0911 209.3430 209.4341 261.4557 14.8155 -0.0908 209.5677 209.6585 261.5448 15.6673 -0.0871 209.8139 209.9010 261.6421 16.4578 -0.0825 209.9958 210.0783 261.7381 17.2495 -0.0834 210.2361 210.3194 261.8507 18.0705 -0.0831 210.4778 210.5609 261.9706 18.8325 -0.0800 210.6976 210.7776 262.0807 19.6845 -0.0748 210.9355 211.0103 262.2241 20.4765 -0.0713 211.1883 211.2597 262.3561 21.2685 -0.0691 211.4106 211.4797 262.4889 22.0913 -0.0660 211.6374 211.7034 262.6315 22.8535 -0.0664 211.8343 211.9007 262.7654 23.7055 -0.0637 212.0610 212.1247 262.9295 24.4975 -0.0598 212.2979 212.3577 263.0905 25.2895 -0.0581 212.5186 212.5767 263.2566 26.1115 -0.0546 212.7351 212.7896 263.4390 26.8735 -0.0475 212.9542 213.0017 263.5817 27.7253 -0.0473 213.2028 213.2502 263.7653 28.4888 -0.0575 213.4097 213.4672 263.9242 29.3155 -0.0599 213.6427 213.7026 264.1096 30.1380 -0.0571 213.8520 213.9092 264.2930 30.8995 -0.0485 214.0901 214.1386 264.4884 31.7520 -0.0405 214.3239 214.3644 264.6813 32.5138 -0.0426 214.5123 214.5549 264.8785 33.3358 -0.0417 214.7428 214.7845 265.0635 34.1580 -0.0422 214.9671 215.0093 265.2372 34.9195 -0.0437 215.1796 215.2233 265.4181 35.7720 -0.0412 215.4209 215.4621 265.6224 36.5338 -0.0461 215.6234 215.6695 265.8076 37.3558 -0.0425 215.8444 215.8868 265.9963 38.1780 -0.0412 216.0684 216.1096 266.1918 38.9395 -0.0397 216.2557 216.2954 266.3726 39.7920 -0.0382 216.4818 216.5200 266.5645 40.5535 -0.0434 216.7030 216.7464 266.7360 41.3758 -0.0403 216.9281 216.9684 266.9197 42.1978 -0.0393 217.1554 217.1947 267.1012 42.9595 -0.0392 217.3565 217.3956 267.2840 43.8118 -0.0326 217.5835 217.6161 267.4869 44.6038 -0.0339 217.7911 217.8250 267.6348 45.3955 -0.0374 218.0241 218.0616 267.7930 46.2180 -0.0371 218.2247 218.2618 267.9662 46.9805 -0.0368 218.4241 218.4609 268.1258 47.8325 -0.0366 218.6656 218.7021 268.2809 48.6245 -0.0333 218.8828 218.9162 268.4331 49.4165 -0.0328 219.0878 219.1206 268.5807 50.2385 -0.0341 219.2924 219.3265 268.7515 51.0005 -0.0381 219.4853 219.5233 268.8879 51.8525 -0.0340 219.7210 219.7550 269.0677 52.6445 -0.0393 219.9254 219.9647 269.1894 53.4375 -0.0382 220.1497 220.1880 269.3241 54.2595 -0.0382 220.3691 220.4073 269.4828 55.0215 -0.0361 220.5755 220.6116 269.6046 55.8733 -0.0365 220.7937 220.8302 269.7523 56.6655 -0.0388 221.0106 221.0494 269.8988 57.4570 -0.0384 221.2083 221.2467 270.0229 58.2785 -0.0453 221.4139 221.4592 270.1490 59.0395 -0.0490 221.6270 221.6759 270.2959 59.8935 -0.0473 221.8398 221.8871 270.4058 60.6525 -0.0434 222.0381 222.0815 270.4952 61.4713 -0.0398 222.2610 222.3008 270.6148 62.2898 -0.0400 222.4693 222.5092 270.7544 63.0470 -0.0409 222.6541 222.6950 270.8563 63.8955 -0.0434 222.8926 222.9360 270.9938 64.6533 -0.0407 223.0577 223.0985 271.0952 65.4743 -0.0425 223.2741 223.3167 271.2207 66.2928 -0.0417 223.5003 223.5421 271.3428 67.0503 -0.0427 223.7086 223.7513 271.4518 67.8995 -0.0433 223.9384 223.9817 271.5833 68.6875 -0.0444 224.1388 224.1832 271.6738 69.4773 -0.0415 224.3149 224.3564 271.7793 70.2960 -0.0390 224.5415 224.5805 271.8737 71.0555 -0.0418 224.7179 224.7598 271.9770 71.9040 -0.0415 224.9431 224.9846 272.1095 72.6925 -0.0432 225.1542 225.1973 272.2207 73.4810 -0.0472 225.3573 225.4045 272.3348 74.3013 -0.0496 225.5685 225.6182 272.4608 75.0620 -0.0505 225.7464 225.7970 272.5718 75.9133 -0.0491 225.9743 226.0234 272.6817 76.7045 -0.0447 226.1600 226.2047 272.8055 77.4950 -0.0477 226.3594 226.4072 272.8915 78.3170 -0.0531 226.5755 226.6285 273.0260 79.0780 -0.0546 226.7812 226.8359 273.1478 79.9300 -0.0520 226.9799 227.0319 273.2802 80.7220 -0.0534 227.1679 227.2213 273.3818 81.5135 -0.0522 227.3779 227.4302 273.5163 82.3360 -0.0558 227.5794 227.6352 273.6425 83.0975 -0.0576 227.7901 227.8477 273.7445 83.9500 -0.0579 227.9832 228.0411 273.8947 84.7118 -0.0576 228.1732 228.2308 273.9968 85.5338 -0.0582 228.3699 228.4282 274.1250 86.3560 -0.0564 228.5857 228.6422 274.2897 87.1175 -0.0590 228.7688 228.8278 274.4117 87.9698 -0.0574 228.9994 229.0568 274.5231 88.7318 -0.0581 229.1758 229.2339 274.6501 89.5538 -0.0570 229.3847 229.4417 274.7614 90.3760 -0.0593 229.5965 229.6558 274.9131 91.1375 -0.0621 229.7688 229.8309 275.0404 91.9898 -0.0616 229.9942 230.0557 275.1722 92.7515 -0.0621 230.1803 230.2424 275.2892 93.5738 -0.0610 230.3816 230.4426 275.4043 94.3958 -0.0598 230.5749 230.6347 275.5337 95.1575 -0.0607 230.7563 230.8170 275.6726 96.0095 -0.0614 230.9462 231.0076 275.8028 96.7715 -0.0646 231.1439 231.2085 275.9190 97.5938 -0.0686 231.3451 231.4136 276.0658 98.3855 -0.0727 231.5294 231.6021 276.2039 99.1775 -0.0726 231.7229 231.7955 276.3237 100.0345 -0.0613 231.9323 231.9936 276.4908 100.7715 -0.0625 232.1030 232.1655 276.6217 101.6235 -0.0585 232.3397 232.3982 276.7715 102.4155 -0.0606 232.5235 232.5841 276.8929 103.2075 -0.0640 232.7039 232.7679 277.0318 104.0295 -0.0637 232.8974 232.9611 277.1892 104.7915 -0.0640 233.0843 233.1483 277.3326 105.6455 -0.0663 233.2830 233.3493 277.4803 106.4375 -0.0688 233.4600 233.5288 277.6020 107.2295 -0.0720 233.6577 233.7297 277.7350 108.0515 -0.0727 233.8572 233.9298 277.8843 108.8133 -0.0810 234.0465 234.1275 278.0280 109.6650 -0.0898 234.2281 234.3179 278.1896 110.4293 -0.0898 234.4348 234.5246 278.3460 111.2538 -0.0923 234.6334 234.7257 278.4868 112.0460 -0.0948 234.7935 234.8883 278.6320 112.8375 -0.0966 234.9607 235.0573 278.7630 113.6900 -0.1003 235.1998 235.3001 278.9204 114.4518 -0.0989 235.3947 235.4937 279.0448 115.2738 -0.0973 235.5675 235.6648 279.1825 116.0960 -0.0973 235.7692 235.8666 279.3194 116.8575 -0.0988 235.9468 236.0456 279.4498 117.7100 -0.0996 236.1661 236.2657 279.6281 118.4718 -0.1051 236.3287 236.4338 279.7317 119.2938 -0.1050 236.5060 236.6110 279.8667 120.1160 -0.1045 236.7200 236.8245 279.9992 120.8785 -0.1043 236.9102 237.0145 280.0894 121.7313 -0.1074 237.0916 237.1990 280.2214 122.4935 -0.1099 237.2688 237.3787 280.3656 123.3150 -0.1120 237.4577 237.5697 280.5196 124.1030 -0.1121 237.6175 237.7296 280.6589 124.8910 -0.1143 237.8070 237.9213 280.7879 125.7390 -0.1089 238.0216 238.1306 280.9049 126.4970 -0.1114 238.2227 238.3341 281.0221 127.3150 -0.1150 238.3959 238.5109 281.1625 128.1035 -0.1160 238.5727 238.6887 281.3128 128.8920 -0.1138 238.7654 238.8793 281.4252 129.7400 -0.1149 238.9536 239.0686 281.5217 130.4983 -0.1175 239.1161 239.2336 281.6367 131.3180 -0.1174 239.3288 239.4462 281.7580 132.1363 -0.1213 239.5088 239.6301 281.8803 132.8960 -0.1215 239.6676 239.7891 282.0069 133.7445 -0.1164 239.8508 239.9672 282.1297 134.5030 -0.1194 240.0425 240.1619 282.2484 135.3220 -0.1222 240.2319 240.3541 282.3703 136.1403 -0.1228 240.4195 240.5422 282.4873 136.9000 -0.1450 240.5896 240.7346 282.6276 137.7495 -0.1275 240.8101 240.9376 282.7561 138.5380 -0.1204 240.9866 241.1071 282.8865 139.3285 -0.1184 241.1523 241.2707 282.9682 140.1498 -0.1234 241.3551 241.4785 283.1145 140.9110 -0.1228 241.5308 241.6535 283.2381 141.7625 -0.1275 241.7113 241.8388 283.3725 142.5538 -0.1318 241.8842 242.0159 283.4751 143.3455 -0.1334 242.0557 242.1891 283.6184 144.1675 -0.1319 242.2472 242.3791 283.7453 144.9295 -0.1333 242.4081 242.5414 283.8806 145.7815 -0.1355 242.6068 242.7423 284.0291 146.5735 -0.1381 242.7745 242.9126 284.1378 147.3655 -0.1422 242.9481 243.0903 284.2659 148.1875 -0.1399 243.1631 243.3030 284.3947 148.9495 -0.1416 243.3418 243.4834 284.5218 149.8015 -0.1433 243.5153 243.6586 284.6636 150.5635 -0.1432 243.6927 243.8359 284.7866 151.3933 -0.1465 243.8672 244.0137 284.9183 152.1875 -0.1518 244.0471 244.1990 285.0649 152.9795 -0.1520 244.2400 244.3920 285.2247 153.8315 -0.1532 244.4236 244.5768 285.3473 154.5938 -0.1550 244.6014 244.7564 285.4723 155.4165 -0.1554 244.7733 244.9287 285.6186 156.2085 -0.1553 244.9230 245.0783 285.7591 157.0005 -0.1580 245.1113 245.2692 285.8953 157.8525 -0.1621 245.3069 245.4690 286.0409 158.6140 -0.1621 245.4768 245.6389 286.1677 159.4358 -0.1627 245.6502 245.8129 286.2975 160.2283 -0.1614 245.8588 246.0202 286.4463 161.0200 -0.1620 246.0159 246.1779 286.5835 161.8720 -0.1647 246.1955 246.3602 286.7337 162.6338 -0.1658 246.3738 246.5396 286.8709 163.4558 -0.1696 246.5398 246.7093 287.0105 164.2780 -0.1723 246.7246 246.8969 287.1470 165.0395 -0.1770 246.8972 247.0742 287.2766 165.8920 -0.1733 247.0723 247.2456 287.4306 166.6538 -0.1772 247.2525 247.4297 287.5652 167.4758 -0.1782 247.4189 247.5971 287.7247 168.2983 -0.1781 247.5963 247.7744 287.8497 169.0605 -0.1809 247.7852 247.9661 287.9775 169.9130 -0.1755 247.9485 248.1240 288.1286 170.7048 -0.1792 248.1238 248.3030 288.2638 171.4965 -0.1825 248.2991 248.4816 288.4361 172.3188 -0.1827 248.4702 248.6529 288.5651 173.0805 -0.1840 248.6373 248.8213 288.6934 173.9328 -0.1877 248.8229 249.0107 288.8386 174.7248 -0.1857 249.0009 249.1865 288.9734 175.5175 -0.1933 249.1825 249.3758 289.1092 176.3395 -0.1948 249.3585 249.5533 289.2925 177.1315 -0.1936 249.5337 249.7273 289.4291 177.9543 -0.1964 249.7240 249.9204 289.5813 178.7465 -0.1971 249.8746 250.0717 289.7291 179.5385 -0.1968 250.0382 250.2351 289.8632 180.3910 -0.1998 250.2384 250.4382 289.9956 181.1535 -0.2041 250.3985 250.6026 290.1527 181.9763 -0.2032 250.5724 250.7756 290.2712 182.7685 -0.2046 250.7461 250.9506 290.3944 183.5605 -0.2021 250.9050 251.1070 290.5269 184.4125 -0.2048 251.0716 251.2763 290.6586 185.1745 -0.2078 251.2418 251.4496 290.7974 185.9965 -0.2076 251.4269 251.6345 290.9290 186.8183 -0.2108 251.6021 251.8129 291.0596 187.5760 -0.2130 251.7896 252.0026 291.1902 188.4255 -0.2112 251.9552 252.1664 291.3361 189.1833 -0.2131 252.1089 252.3221 291.4524 190.0013 -0.2189 252.2919 252.5108 291.5682 190.7893 -0.2181 252.4816 252.6997 291.6986 191.5773 -0.2209 252.6506 252.8715 291.8156 192.4258 -0.2211 252.8306 253.0517 291.9414 193.1833 -0.2221 252.9956 253.2177 292.0755 194.0028 -0.2255 253.1569 253.3824 292.1993 194.7908 -0.2258 253.3201 253.5460 292.3232 195.5793 -0.2287 253.4905 253.7192 292.4164 196.4283 -0.2348 253.6995 253.9342 292.5727 197.1863 -0.2354 253.8435 254.0788 292.6807 198.0070 -0.2386 253.9973 254.2359 292.7813 198.7958 -0.2351 254.1676 254.4026 292.9051 199.5848 -0.2360 254.3249 254.5609 293.0273 200.4340 -0.2347 254.5088 254.7435 293.1482 201.1923 -0.2373 254.6637 254.9011 293.2621 202.0120 -0.2406 254.8475 255.0881 293.3921 202.8025 -0.2423 255.0124 255.2548 293.5208 203.5930 -0.2421 255.1842 255.4263 293.6436 204.4433 -0.2434 255.3443 255.5877 293.7977 205.2053 -0.2447 255.4961 255.7408 293.9081 206.0253 -0.2445 255.6692 255.9137 294.0219 206.8170 -0.2487 255.8515 256.1002 294.1343 207.6085 -0.2533 256.0206 256.2739 294.2734 208.4310 -0.2523 256.2032 256.4554 294.4055 209.1925 -0.2579 256.3459 256.6039 294.5360 210.0450 -0.2560 256.5175 256.7735 294.6456 210.8370 -0.2567 256.6834 256.9402 294.7786 211.6285 -0.2589 256.8552 257.1141 294.9234 212.4510 -0.2607 257.0443 257.3050 295.0423 213.2128 -0.2599 257.2187 257.4787 295.1557 214.0650 -0.2658 257.3942 257.6600 295.3073 214.8268 -0.2654 257.5379 257.8033 295.4324 215.6488 -0.2645 257.6959 257.9604 295.5707 216.4410 -0.2666 257.8629 258.1295 295.7069 217.2325 -0.2709 258.0132 258.2840 295.8366 218.0848 -0.2710 258.1974 258.4684 295.9705 218.8468 -0.2764 258.3488 258.6252 296.1277 219.6688 -0.2793 258.5275 258.8068 296.2717 220.4610 -0.2773 258.6996 258.9770 296.3926 221.2525 -0.2783 258.8728 259.1510 296.5049 222.1055 -0.2791 259.0325 259.3116 296.6717 222.8400 -0.2803 259.1872 259.4675 296.7785 223.7008 -0.2818 259.3581 259.6399 296.8989 224.4925 -0.2885 259.5201 259.8086 297.0432 225.2845 -0.2912 259.6749 259.9660 297.1728 226.1065 -0.2940 259.8591 260.1531 297.3128 226.8685 -0.2939 260.0307 260.3246 297.4351 227.7205 -0.2933 260.1933 260.4866 297.5797 228.5125 -0.2964 260.3579 260.6543 297.7129 229.3045 -0.2978 260.5146 260.8124 297.8754 230.1265 -0.2974 260.6768 260.9743 298.0218 230.8885 -0.3011 260.8237 261.1248 298.1332 231.7405 -0.3027 261.0124 261.3151 298.2742 232.5025 -0.3065 261.1838 261.4903 298.3981 233.3245 -0.3034 261.3374 261.6408 298.5142 234.1465 -0.3076 261.5006 261.8082 298.6459 234.9085 -0.3115 261.6677 261.9791 298.7746 235.7605 -0.3125 261.8460 262.1585 298.9397 236.5223 -0.3143 261.9949 262.3092 299.0715 237.3440 -0.3190 262.1541 262.4731 299.2184 238.1665 -0.3211 262.3386 262.6597 299.3381 238.9283 -0.3203 262.4988 262.8191 299.4583 239.7805 -0.3211 262.6523 262.9734 299.5987 240.5428 -0.3282 262.8171 263.1453 299.7170 241.3648 -0.3289 262.9788 263.3078 299.8605 242.1873 -0.3324 263.1596 263.4920 300.0007 242.9495 -0.3353 263.3024 263.6377 300.1384 243.8025 -0.3372 263.4613 263.7986 300.2546 244.5648 -0.3390 263.6274 263.9664 300.3967 245.3868 -0.3390 263.7848 264.1238 300.5302 246.2093 -0.3416 263.9398 264.2815 300.6490 246.9715 -0.3452 264.1054 264.4505 300.7873 247.8245 -0.3413 264.2780 264.6193 300.9143 248.5865 -0.3425 264.4202 264.7627 301.0601 249.4088 -0.3458 264.5761 264.9220 301.1877 250.2310 -0.3492 264.7592 265.1083 301.3270 250.9935 -0.3465 264.9153 265.2618 301.4269 251.8403 -0.3504 265.0913 265.4417 301.5701 252.5978 -0.3507 265.2554 265.6061 301.6840 253.4160 -0.3539 265.3902 265.7441 301.8035 254.2040 -0.3568 265.5456 265.9024 301.9475 254.9920 -0.3576 265.7257 266.0833 302.0903 255.8400 -0.3604 265.9028 266.2633 302.2262 256.5970 -0.3645 266.0185 266.3830 302.3648 257.4160 -0.3649 266.1909 266.5557 302.4784 258.2040 -0.3686 266.3533 266.7219 302.6207 258.9920 -0.3693 266.5291 266.8984 302.7421 259.8405 -0.3713 266.7023 267.0737 302.8525 260.5993 -0.3710 266.8465 267.2175 302.9754 261.4178 -0.3750 266.9905 267.3655 303.1205 262.2360 -0.3739 267.1641 267.5380 303.2650 262.9950 -0.3781 267.3287 267.7068 303.3982 263.8435 -0.3835 267.5032 267.8868 303.5113 264.6320 -0.3816 267.6696 268.0512 303.6321 265.4210 -0.3850 267.8130 268.1980 303.7588 266.2393 -0.3825 267.9710 268.3535 303.9045 267.0280 -0.3829 268.1216 268.5045 304.0103 267.8475 -0.3891 268.2627 268.6518 304.1284 268.6388 -0.3898 268.4166 268.8064 304.2663 269.4305 -0.3941 268.6039 268.9980 304.4062 270.2525 -0.3986 268.7690 269.1676 304.5508 271.0435 -0.4016 268.9059 269.3075 304.6572 271.8655 -0.3982 269.0636 269.4617 304.7798 272.6578 -0.4001 269.2436 269.6437 304.8997 273.4495 -0.4019 269.4025 269.8044 305.0186 274.2715 -0.4023 269.5483 269.9506 305.1567 275.0635 -0.4058 269.6999 270.1057 305.2963 275.8855 -0.4104 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