DTA measure 1pb4 Date: 2025326:1027 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1722.77 s Mass = 925.500 mg data_number = 1071 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4660 -1.0826 217.4620 218.5446 208.5892 4.0535 -1.0837 217.4578 218.5415 208.6454 5.6666 -1.0843 217.4513 218.5355 208.6956 7.2696 -1.0854 217.4484 218.5338 208.7406 8.8779 -1.0876 217.4496 218.5371 208.7925 10.4705 -1.0882 217.4446 218.5328 208.8402 12.0889 -1.0882 217.4421 218.5302 208.8830 13.7020 -1.0900 217.4443 218.5343 208.9327 15.3049 -1.0918 217.4522 218.5440 208.9805 16.9183 -1.0933 217.4440 218.5373 209.0338 18.5213 -1.0945 217.4386 218.5331 209.0899 20.1449 -1.0958 217.4325 218.5283 209.1490 21.7684 -1.0965 217.4291 218.5255 209.2135 23.3714 -1.0978 217.4305 218.5283 209.2886 24.9845 -1.0982 217.4347 218.5329 209.3668 26.5875 -1.0985 217.4347 218.5332 209.4564 28.2008 -1.0984 217.4338 218.5323 209.5420 29.8036 -1.0989 217.4370 218.5359 209.6310 31.4116 -1.0992 217.4399 218.5391 209.7337 33.0041 -1.1005 217.4470 218.5475 209.8424 34.6226 -1.1009 217.4518 218.5527 209.9689 36.2361 -1.1012 217.4583 218.5595 210.1129 37.8389 -1.1033 217.4631 218.5664 210.2549 39.4519 -1.1048 217.4720 218.5768 210.4043 41.0549 -1.1063 217.4758 218.5821 210.5642 42.6633 -1.1080 217.4801 218.5881 210.7324 44.2711 -1.1099 217.4876 218.5975 210.9165 45.8998 -1.1117 217.4877 218.5994 211.1185 47.5026 -1.1138 217.4942 218.6080 211.3207 49.0899 -1.1163 217.5050 218.6213 211.5296 50.6876 -1.1185 217.5110 218.6296 211.7466 52.3006 -1.1201 217.5261 218.6462 211.9727 53.8984 -1.1225 217.5328 218.6554 212.2045 55.5010 -1.1255 217.5423 218.6678 212.4543 57.1040 -1.1284 217.5592 218.6877 212.7140 58.7225 -1.1303 217.5762 218.7065 212.9847 60.3251 -1.1337 217.5968 218.7305 213.2676 61.9283 -1.1361 217.6094 218.7456 213.5540 63.5416 -1.1380 217.6180 218.7561 213.8472 65.1393 -1.1404 217.6302 218.7706 214.1451 66.7526 -1.1430 217.6520 218.7949 214.4547 68.3505 -1.1458 217.6787 218.8245 214.7753 69.9741 -1.1495 217.6971 218.8466 215.0953 71.5824 -1.1533 217.7274 218.8807 215.4150 73.1749 -1.1569 217.7600 218.9170 215.7266 74.7775 -1.1613 217.7863 218.9476 216.0369 76.3906 -1.1645 217.8141 218.9786 216.3533 77.9886 -1.1670 217.8358 219.0029 216.6669 79.5965 -1.1703 217.8730 219.0433 216.9883 81.2045 -1.1740 217.9130 219.0870 217.3030 82.8283 -1.1772 217.9507 219.1279 217.6197 84.4209 -1.1813 217.9905 219.1717 217.9268 86.0286 -1.1843 218.0306 219.2149 218.2343 87.6419 -1.1867 218.0741 219.2608 218.5390 89.2449 -1.1898 218.1128 219.3026 218.8316 90.8528 -1.1935 218.1556 219.3491 219.1237 92.4608 -1.1974 218.2120 219.4094 219.4086 94.0686 -1.2013 218.2663 219.4676 219.6904 95.6665 -1.2044 218.3161 219.5205 219.9663 97.2900 -1.2073 218.3733 219.5806 220.2411 98.8926 -1.2099 218.4278 219.6377 220.4936 100.5059 -1.2120 218.4786 219.6905 220.7410 102.0983 -1.2142 218.5264 219.7406 220.9803 103.7063 -1.2166 218.5808 219.7974 221.2202 105.3141 -1.2183 218.6440 219.8623 221.4464 106.9224 -1.2207 218.7096 219.9304 221.6723 108.5304 -1.2230 218.7684 219.9914 221.8869 110.1541 -1.2243 218.8304 220.0547 222.0896 111.7411 -1.2264 218.8914 220.1178 222.2806 113.3390 -1.2288 218.9602 220.1891 222.4713 114.9469 -1.2306 219.0366 220.2673 222.6623 116.5499 -1.2317 219.1035 220.3352 222.8443 118.1529 -1.2321 219.1824 220.4146 223.0200 119.7506 -1.2312 219.2636 220.4948 223.1934 121.3535 -1.2322 219.3366 220.5689 223.3573 122.9770 -1.2315 219.4159 220.6474 223.5182 124.5643 -1.2316 219.4979 220.7295 223.6717 126.1670 -1.2327 219.5764 220.8091 223.8131 127.7751 -1.2325 219.6551 220.8876 223.9536 129.3780 -1.2321 219.7407 220.9728 224.0867 130.9808 -1.2320 219.8272 221.0592 224.2206 132.5889 -1.2313 219.9129 221.1442 224.3642 134.1969 -1.2302 219.9984 221.2286 224.4937 135.8151 -1.2292 220.0857 221.3149 224.6243 137.4230 -1.2281 220.1761 221.4042 224.7510 139.0311 -1.2272 220.2671 221.4944 224.8764 140.6391 -1.2257 220.3535 221.5792 225.0036 142.2421 -1.2242 220.4450 221.6692 225.1309 143.8553 -1.2232 220.5377 221.7609 225.2589 145.4580 -1.2213 220.6416 221.8628 225.3848 147.0816 -1.2184 220.7466 221.9650 225.5189 148.6898 -1.2156 220.8451 222.0607 225.6585 150.2981 -1.2130 220.9429 222.1559 225.8036 151.9061 -1.2105 221.0394 222.2499 225.9383 153.5091 -1.2085 221.1365 222.3449 226.0809 155.1224 -1.2074 221.2393 222.4466 226.2275 156.7249 -1.2042 221.3437 222.5479 226.3751 158.3485 -1.2017 221.4531 222.6548 226.5424 159.9616 -1.1997 221.5519 222.7516 226.7020 161.5645 -1.1972 221.6504 222.8475 226.8642 163.1779 -1.1944 221.7568 222.9512 227.0388 164.7810 -1.1922 221.8638 223.0560 227.2076 166.3893 -1.1893 221.9729 223.1622 227.3889 167.9975 -1.1860 222.0825 223.2685 227.5739 169.5901 -1.1835 222.1920 223.3755 227.7603 171.2138 -1.1815 222.2959 223.4774 227.9598 172.8218 -1.1791 222.4017 223.5809 228.1612 174.4298 -1.1767 222.5077 223.6844 228.3644 176.0275 -1.1737 222.6283 223.8019 228.5733 177.6096 -1.1715 222.7464 223.9179 228.7783 179.2126 -1.1702 222.8572 224.0273 228.9980 180.8155 -1.1680 222.9685 224.1365 229.2223 182.4185 -1.1660 223.0871 224.2531 229.4503 184.0214 -1.1638 223.2038 224.3676 229.6769 185.6243 -1.1626 223.3116 224.4742 229.9105 187.2324 -1.1608 223.4327 224.5935 230.1456 188.8351 -1.1583 223.5579 224.7162 230.3868 190.4380 -1.1563 223.6795 224.8357 230.6298 192.0459 -1.1544 223.7998 224.9542 230.8746 193.6486 -1.1525 223.9230 225.0755 231.1267 195.2463 -1.1518 224.0441 225.1959 231.3750 196.8493 -1.1513 224.1663 225.3176 231.6348 198.4729 -1.1502 224.2908 225.4410 231.9060 200.0810 -1.1510 224.4105 225.5615 232.1745 201.6838 -1.1518 224.5381 225.6899 232.4422 203.2815 -1.1532 224.6734 225.8266 232.7076 204.8841 -1.1531 224.8022 225.9553 232.9707 206.4973 -1.1524 224.9362 226.0885 233.2408 208.1003 -1.1515 225.0612 226.2127 233.5123 209.7081 -1.1512 225.1939 226.3451 233.7808 211.3320 -1.1504 225.3284 226.4787 234.0468 212.9350 -1.1500 225.4682 226.6182 234.3139 214.5326 -1.1481 225.6105 226.7586 234.5766 216.1406 -1.1467 225.7448 226.8915 234.8375 217.7486 -1.1458 225.8792 227.0250 235.0960 219.3516 -1.1454 226.0132 227.1586 235.3502 220.9598 -1.1446 226.1529 227.2975 235.6130 222.5680 -1.1432 226.2946 227.4378 235.8692 224.1863 -1.1434 226.4367 227.5801 236.1229 225.7994 -1.1430 226.5811 227.7241 236.3713 227.4024 -1.1418 226.7268 227.8686 236.6180 229.0156 -1.1422 226.8820 228.0241 236.8584 230.6189 -1.1422 227.0304 228.1726 237.0931 232.2268 -1.1417 227.1790 228.3206 237.3216 233.8351 -1.1418 227.3272 228.4690 237.5449 235.4536 -1.1403 227.4791 228.6195 237.7741 237.0666 -1.1386 227.6261 228.7648 237.9959 238.6695 -1.1389 227.7775 228.9164 238.2091 240.2779 -1.1396 227.9357 229.0753 238.4221 241.8809 -1.1393 228.0989 229.2382 238.6328 243.4786 -1.1389 228.2595 229.3984 238.8367 245.0815 -1.1388 228.4110 229.5498 239.0373 246.6946 -1.1381 228.5700 229.7081 239.2361 248.2871 -1.1378 228.7322 229.8700 239.4322 249.8901 -1.1383 228.8904 230.0287 239.6252 251.4930 -1.1385 229.0423 230.1807 239.8024 253.1064 -1.1375 229.2034 230.3409 239.9871 254.7040 -1.1360 229.3682 230.5042 240.1655 256.3174 -1.1357 229.5349 230.6706 240.3444 257.9151 -1.1349 229.7032 230.8381 240.5164 259.5233 -1.1334 229.8699 231.0034 240.6935 261.1314 -1.1328 230.0388 231.1716 240.8614 262.7293 -1.1319 230.2081 231.3400 241.0307 264.3423 -1.1309 230.3717 231.5027 241.1903 265.9453 -1.1292 230.5387 231.6680 241.3583 267.5533 -1.1280 230.7018 231.8298 241.5311 269.1613 -1.1266 230.8652 231.9918 241.6966 270.7691 -1.1248 231.0278 232.1526 241.8651 272.3774 -1.1234 231.2017 232.3251 242.0361 273.9853 -1.1222 231.3728 232.4949 242.2073 275.5934 -1.1203 231.5428 232.6631 242.3802 277.2013 -1.1188 231.7226 232.8414 242.5506 278.8041 -1.1175 231.8938 233.0113 242.7199 280.4175 -1.1159 232.0553 233.1713 242.8879 282.0049 -1.1153 232.2230 233.3384 243.0552 283.6181 -1.1130 232.4001 233.5131 243.2301 285.2213 -1.1115 232.5710 233.6825 243.4020 286.8449 -1.1090 232.7456 233.8546 243.5796 288.4530 -1.1076 232.9194 234.0270 243.7568 290.0405 -1.1066 233.0931 234.1997 243.9372 291.6536 -1.1052 233.2625 234.3677 244.1256 293.2566 -1.1037 233.4367 234.5404 244.3092 294.8699 -1.1026 233.6081 234.7106 244.4972 296.4728 -1.1002 233.7848 234.8850 244.6871 298.0809 -1.0997 233.9599 235.0596 244.8813 299.7045 -1.0986 234.1376 235.2362 245.0841 301.3178 -1.0970 234.3144 235.4114 245.2889 302.9206 -1.0947 234.4925 235.5873 245.4919 304.5236 -1.0944 234.6765 235.7709 245.7011 306.1163 -1.0928 234.8497 235.9425 245.9106 307.7191 -1.0918 235.0275 236.1193 246.1268 309.3168 -1.0918 235.2037 236.2955 246.3389 310.9195 -1.0911 235.3791 236.4702 246.5568 312.5275 -1.0904 235.5556 236.6460 246.7683 314.1303 -1.0899 235.7355 236.8253 246.9818 315.7281 -1.0899 235.9172 237.0071 247.1977 317.3415 -1.0899 236.1011 237.1910 247.4149 318.9443 -1.0895 236.2783 237.3678 247.6347 320.5473 -1.0890 236.4569 237.5459 247.8573 322.1553 -1.0893 236.6331 237.7224 248.0927 323.7631 -1.0893 236.8231 237.9124 248.3288 325.3505 -1.0900 237.0034 238.0935 248.5536 326.9740 -1.0905 237.1870 238.2776 248.7907 328.5820 -1.0898 237.3710 238.4608 249.0202 330.1903 -1.0903 237.5549 238.6453 249.2574 331.7933 -1.0907 237.7387 238.8294 249.4973 333.3961 -1.0905 237.9257 239.0161 249.7359 335.0041 -1.0908 238.1150 239.2058 249.9767 336.6121 -1.0909 238.3014 239.3923 250.2172 338.2354 -1.0908 238.4927 239.5835 250.4540 339.8438 -1.0918 238.6802 239.7719 250.6918 341.4466 -1.0928 238.8737 239.9665 250.9365 343.0598 -1.0932 239.0707 240.1640 251.1829 344.6628 -1.0944 239.2596 240.3539 251.4277 346.2708 -1.0954 239.4463 240.5417 251.6688 347.8788 -1.0956 239.6393 240.7349 251.9074 349.5024 -1.0976 239.8345 240.9321 252.1523 351.1106 -1.0993 240.0249 241.1242 252.3933 352.7136 -1.1007 240.2174 241.3181 252.6336 354.3266 -1.1020 240.4079 241.5099 252.8837 355.9295 -1.1041 240.5972 241.7013 253.1164 357.5529 -1.1049 240.7955 241.9004 253.3458 359.1506 -1.1052 240.9868 242.0920 253.5778 360.7590 -1.1055 241.1794 242.2849 253.8091 362.3774 -1.1061 241.3818 242.4879 254.0418 363.9905 -1.1075 241.5928 242.7004 254.2734 365.6089 -1.1085 241.7858 242.8942 254.5001 367.2221 -1.1100 241.9790 243.0891 254.7194 368.8043 -1.1121 242.1735 243.2857 254.9334 370.4178 -1.1135 242.3760 243.4895 255.1531 372.0000 -1.1139 242.5701 243.6840 255.3650 373.6029 -1.1155 242.7706 243.8860 255.5758 375.2058 -1.1167 242.9711 244.0878 255.7773 376.8085 -1.1183 243.1715 244.2898 255.9817 378.4111 -1.1189 243.3683 244.4872 256.1800 380.0090 -1.1206 243.5700 244.6907 256.3786 381.6226 -1.1221 243.7722 244.8943 256.5769 383.2256 -1.1227 243.9705 245.0932 256.7717 384.8285 -1.1242 244.1808 245.3050 256.9684 386.4211 -1.1258 244.3825 245.5083 257.1562 388.0241 -1.1265 244.5836 245.7101 257.3492 389.6320 -1.1273 244.7862 245.9135 257.5379 391.2555 -1.1283 244.9882 246.1164 257.7338 392.8480 -1.1286 245.1904 246.3190 257.9247 394.4455 -1.1292 245.3950 246.5242 258.1076 396.0589 -1.1297 245.6012 246.7309 258.2933 397.6618 -1.1306 245.8055 246.9362 258.4725 399.2698 -1.1325 246.0079 247.1404 258.6512 400.8779 -1.1348 246.2055 247.3403 258.8323 402.4860 -1.1370 246.4123 247.5493 259.0116 404.1094 -1.1385 246.6115 247.7500 259.1930 405.7123 -1.1412 246.8146 247.9557 259.3685 407.3258 -1.1441 247.0211 248.1652 259.5487 408.9285 -1.1459 247.2269 248.3728 259.7278 410.5470 -1.1470 247.4321 248.5791 259.9114 412.1396 -1.1484 247.6407 248.7892 260.0961 413.7471 -1.1500 247.8531 249.0031 260.2793 415.3553 -1.1508 248.0557 249.2066 260.4626 416.9789 -1.1520 248.2680 249.4200 260.6607 418.5870 -1.1543 248.4736 249.6279 260.8588 420.1899 -1.1553 248.6845 249.8398 261.0550 421.8033 -1.1560 248.8890 250.0451 261.2481 423.4061 -1.1560 249.0900 250.2460 261.4356 425.0141 -1.1578 249.2929 250.4508 261.6348 426.6224 -1.1602 249.4967 250.6568 261.8346 428.2510 -1.1635 249.7061 250.8696 262.0343 429.8590 -1.1659 249.9069 251.0728 262.2450 431.4673 -1.1677 250.1152 251.2828 262.4589 433.0701 -1.1694 250.3337 251.5031 262.6649 434.6679 -1.1714 250.5454 251.7167 262.8719 436.2605 -1.1733 250.7487 251.9221 263.0784 437.8585 -1.1753 250.9628 252.1381 263.2926 439.4664 -1.1780 251.1752 252.3532 263.5165 441.0796 -1.1806 251.3808 252.5614 263.7482 442.6825 -1.1827 251.5903 252.7731 263.9836 444.2906 -1.1847 251.7978 252.9825 264.2174 445.8934 -1.1871 252.0073 253.1944 264.4473 447.4960 -1.1897 252.2117 253.4014 264.6748 449.1041 -1.1918 252.4155 253.6073 264.9054 450.7069 -1.1934 252.6277 253.8211 265.1294 452.3355 -1.1964 252.8372 254.0336 265.3657 453.9334 -1.1987 253.0470 254.2457 265.6018 455.5465 -1.2005 253.2479 254.4484 265.8408 457.1491 -1.2033 253.4552 254.6585 266.0757 458.7574 -1.2055 253.6673 254.8728 266.3035 460.3653 -1.2084 253.8819 255.0903 266.5469 461.9735 -1.2117 254.0911 255.3028 266.7899 463.5970 -1.2145 254.3063 255.5208 267.0223 465.1996 -1.2170 254.5139 255.7310 267.2525 466.8131 -1.2204 254.7344 255.9549 267.4880 468.4160 -1.2235 254.9482 256.1718 267.7208 470.0241 -1.2269 255.1559 256.3828 267.9587 471.6325 -1.2289 255.3635 256.5924 268.2017 473.2404 -1.2315 255.5766 256.8081 268.4395 474.8640 -1.2343 255.7851 257.0193 268.6745 476.4666 -1.2358 255.9880 257.2238 268.9050 478.0801 -1.2391 256.2017 257.4408 269.1374 479.6831 -1.2418 256.4170 257.6588 269.3634 481.2911 -1.2446 256.6271 257.8717 269.5934 482.9044 -1.2485 256.8404 258.0889 269.8183 484.5125 -1.2525 257.0565 258.3089 270.0409 486.1360 -1.2567 257.2810 258.5377 270.2664 487.7443 -1.2610 257.4961 258.7570 270.4869 489.3473 -1.2642 257.7070 258.9712 270.7063 490.9604 -1.2675 257.9227 259.1902 270.9322 492.5633 -1.2703 258.1382 259.4085 271.1494 494.1711 -1.2731 258.3550 259.6281 271.3674 495.7845 -1.2769 258.5793 259.8562 271.5839 497.4029 -1.2804 258.7996 260.0800 271.7896 499.0004 -1.2843 259.0097 260.2940 271.9919 500.5981 -1.2868 259.2239 260.5107 272.1877 502.2061 -1.2890 259.4437 260.7327 272.3874 503.8144 -1.2909 259.6639 260.9548 272.5809 505.4124 -1.2934 259.8861 261.1794 272.7777 506.9994 -1.2970 260.1023 261.3993 272.9635 508.6024 -1.2997 260.3226 261.6223 273.1490 510.2256 -1.3026 260.5461 261.8487 273.3371 511.8236 -1.3054 260.7616 262.0670 273.5366 513.4369 -1.3082 260.9820 262.2901 273.7277 515.0396 -1.3107 261.1940 262.5047 273.9092 516.6476 -1.3142 261.4076 262.7219 274.1022 518.2504 -1.3162 261.6228 262.9390 274.2888 519.8636 -1.3184 261.8388 263.1572 274.4654 521.4820 -1.3207 262.0570 263.3777 274.6443 523.0903 -1.3226 262.2719 263.5944 274.8229 524.6983 -1.3246 262.5017 263.8263 275.0005 526.3011 -1.3259 262.7176 264.0435 275.1871 527.9145 -1.3287 262.9340 264.2627 275.3711 529.5171 -1.3321 263.1505 264.4826 275.5501 531.1149 -1.3341 263.3656 264.6997 275.7309 532.7179 -1.3373 263.5829 264.9202 275.9091 534.3416 -1.3403 263.8107 265.1510 276.0914 535.9496 -1.3427 264.0219 265.3646 276.2733 537.5526 -1.3464 264.2372 265.5835 276.4562 539.1660 -1.3495 264.4562 265.8057 276.6402 540.7689 -1.3522 264.6755 266.0277 276.8333 542.3820 -1.3541 264.8960 266.2501 277.0309 543.9850 -1.3570 265.1092 266.4663 277.2269 545.6088 -1.3593 265.3266 266.6859 277.4247 547.2169 -1.3616 265.5535 266.9152 277.6300 548.8196 -1.3659 265.7692 267.1350 277.8317 550.4331 -1.3697 265.9996 267.3693 278.0359 552.0359 -1.3733 266.2185 267.5917 278.2419 553.6490 -1.3769 266.4344 267.8113 278.4557 555.2521 -1.3808 266.6508 268.0316 278.6690 556.8758 -1.3847 266.8691 268.2538 278.8823 558.4836 -1.3887 267.0866 268.4754 279.1005 560.0865 -1.3924 267.3055 268.6980 279.3140 561.6949 -1.3954 267.5249 268.9203 279.5310 563.2874 -1.3991 267.7334 269.1325 279.7538 564.8851 -1.4037 267.9475 269.3512 279.9853 566.4830 -1.4071 268.1662 269.5733 280.2122 568.0856 -1.4110 268.3820 269.7930 280.4437 569.7093 -1.4132 268.5978 270.0109 280.6785 571.3124 -1.4154 268.8203 270.2357 280.9147 572.9203 -1.4184 269.0481 270.4665 281.1424 574.5076 -1.4228 269.2687 270.6915 281.3685 576.1104 -1.4273 269.4891 270.9164 281.6036 577.7234 -1.4321 269.7020 271.1341 281.8356 579.3263 -1.4345 269.9207 271.3552 282.0681 580.9341 -1.4369 270.1332 271.5701 282.3042 582.5578 -1.4406 270.3528 271.7934 282.5447 584.1601 -1.4451 270.5697 272.0148 282.7859 585.7526 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