DTA measure 3pb3 Date: 2025326:935 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.66 s Mass = 925.500 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5430 -5.2520 436.3195 441.5714 419.7724 4.1503 -5.2589 436.3669 441.6258 419.7758 5.7626 -5.2659 436.4029 441.6688 419.8302 7.3645 -5.2732 436.4409 441.7141 419.9168 8.9769 -5.2817 436.4764 441.7581 420.0363 10.5841 -5.2910 436.5087 441.7997 420.1840 12.2015 -5.2991 436.5512 441.8503 420.3616 13.8140 -5.3094 436.5803 441.8897 420.5614 15.4263 -5.3197 436.6026 441.9222 420.7877 17.0283 -5.3305 436.6235 441.9540 421.0198 18.6254 -5.3423 436.6474 441.9898 421.2656 20.2118 -5.3547 436.6711 442.0258 421.5113 21.8190 -5.3687 436.7002 442.0689 421.7784 23.4208 -5.3825 436.7325 442.1149 422.0390 25.0178 -5.3947 436.7577 442.1525 422.2953 26.6301 -5.4075 436.7802 442.1877 422.5481 28.2269 -5.4209 436.8021 442.2230 422.7869 29.8394 -5.4342 436.8281 442.2623 423.0118 31.4416 -5.4477 436.8597 442.3074 423.2194 33.0439 -5.4615 436.8812 442.3427 423.4099 34.6510 -5.4736 436.9076 442.3812 423.5787 36.2480 -5.4855 436.9412 442.4267 423.7262 37.8499 -5.4982 436.9728 442.4710 423.8503 39.4726 -5.5110 436.9980 442.5090 423.9510 41.0796 -5.5234 437.0271 442.5505 424.0252 42.6715 -5.5348 437.0533 442.5881 424.0798 44.2786 -5.5453 437.0810 442.6263 424.0990 45.8910 -5.5558 437.1024 442.6583 424.0964 47.4929 -5.5659 437.1312 442.6971 424.0698 49.1054 -5.5756 437.1626 442.7382 424.0128 50.7076 -5.5849 437.1932 442.7781 423.9262 52.3148 -5.5926 437.2239 442.8165 423.8233 53.9221 -5.6006 437.2492 442.8498 423.6875 55.5293 -5.6078 437.2713 442.8790 423.5303 57.1366 -5.6157 437.2970 442.9127 423.3440 58.7488 -5.6232 437.3220 442.9453 423.1345 60.3506 -5.6290 437.3532 442.9822 422.8996 61.9630 -5.6332 437.3770 443.0102 422.6494 63.5649 -5.6372 437.4058 443.0430 422.3784 65.1771 -5.6415 437.4409 443.0824 422.0878 66.7843 -5.6442 437.4692 443.1134 421.7875 68.3915 -5.6469 437.4926 443.1395 421.4669 69.9986 -5.6501 437.5092 443.1593 421.1263 71.6109 -5.6521 437.5200 443.1721 420.7663 73.2129 -5.6540 437.5329 443.1869 420.3981 74.8044 -5.6559 437.5390 443.1949 420.0228 76.4169 -5.6561 437.5398 443.1959 419.6296 78.0241 -5.6560 437.5388 443.1948 419.2252 79.6414 -5.6552 437.5353 443.1905 418.8112 81.2486 -5.6540 437.5271 443.1811 418.3906 82.8559 -5.6528 437.5126 443.1654 417.9690 84.4529 -5.6525 437.4960 443.1485 417.5261 86.0496 -5.6520 437.4791 443.1310 417.0845 87.6518 -5.6511 437.4604 443.1116 416.6393 89.2540 -5.6483 437.4356 443.0839 416.1923 90.8611 -5.6462 437.4100 443.0563 415.7462 92.4580 -5.6447 437.3721 443.0169 415.2985 94.0651 -5.6430 437.3334 442.9764 414.8507 95.6724 -5.6411 437.2909 442.9320 414.4001 97.2691 -5.6393 437.2472 442.8865 413.9539 98.8815 -5.6374 437.1991 442.8365 413.5146 100.4834 -5.6347 437.1446 442.7793 413.0845 102.0906 -5.6318 437.0891 442.7210 412.6624 103.7134 -5.6285 437.0247 442.6532 412.2414 105.3204 -5.6255 436.9545 442.5800 411.8367 106.9278 -5.6226 436.8819 442.5046 411.4393 108.5299 -5.6203 436.8101 442.4304 411.0584 110.1423 -5.6195 436.7348 442.3543 410.6825 111.7288 -5.6183 436.6549 442.2732 410.3235 113.3514 -5.6173 436.5705 442.1878 409.9665 114.9740 -5.6160 436.4732 442.0892 409.6218 116.5815 -5.6148 436.3712 441.9860 409.2920 118.1890 -5.6142 436.2711 441.8854 408.9783 119.7910 -5.6128 436.1691 441.7819 408.6839 121.4034 -5.6120 436.0644 441.6764 408.4026 123.0056 -5.6112 435.9590 441.5703 408.1327 124.6128 -5.6110 435.8513 441.4624 407.8886 126.2048 -5.6109 435.7436 441.3545 407.6619 127.8429 -5.6108 435.6269 441.2377 407.4375 129.4345 -5.6104 435.5186 441.1290 407.2364 131.0466 -5.6104 435.3993 441.0098 407.0554 132.6591 -5.6114 435.2788 440.8902 406.8861 134.2610 -5.6119 435.1518 440.7638 406.7256 135.8784 -5.6127 435.0223 440.6350 406.5793 137.4856 -5.6141 434.8960 440.5101 406.4482 139.1084 -5.6159 434.7676 440.3835 406.3239 140.7103 -5.6169 434.6363 440.2532 406.2148 142.3073 -5.6197 434.5002 440.1199 406.1205 143.9145 -5.6227 434.3656 439.9884 406.0347 145.5218 -5.6255 434.2256 439.8511 405.9519 147.1081 -5.6286 434.0902 439.7188 405.8773 148.7153 -5.6308 433.9498 439.5806 405.8125 150.3119 -5.6331 433.8153 439.4484 405.7529 151.9139 -5.6356 433.6806 439.3162 405.6963 153.5213 -5.6389 433.5433 439.1822 405.6434 155.1076 -5.6428 433.4085 439.0513 405.5952 156.7303 -5.6462 433.2693 438.9155 405.5372 158.3321 -5.6489 433.1293 438.7782 405.4850 159.9395 -5.6524 432.9923 438.6448 405.4281 161.5264 -5.6559 432.8491 438.5050 405.3701 163.1388 -5.6590 432.7028 438.3618 405.3037 164.7408 -5.6626 432.5554 438.2180 405.2392 166.3481 -5.6651 432.4253 438.0904 405.1651 167.9605 -5.6684 432.2850 437.9534 405.0866 169.5524 -5.6716 432.1468 437.8183 405.0070 171.1595 -5.6748 432.0019 437.6766 404.9213 172.7823 -5.6774 431.8658 437.5432 404.8173 174.3845 -5.6791 431.7314 437.4105 404.7094 175.9966 -5.6813 431.5898 437.2712 404.5959 177.5989 -5.6837 431.4463 437.1300 404.4719 179.2058 -5.6846 431.3034 436.9880 404.3367 180.8130 -5.6860 431.1636 436.8496 404.2071 182.4203 -5.6883 431.0265 436.7148 404.0627 184.0273 -5.6888 430.8870 436.5759 403.9073 185.6396 -5.6898 430.7492 436.4390 403.7503 187.2523 -5.6896 430.6076 436.2972 403.5802 188.8750 -5.6900 430.4567 436.1467 403.3919 190.4770 -5.6903 430.3167 436.0070 403.2036 192.0894 -5.6892 430.1796 435.8687 402.9976 193.6913 -5.6881 430.0389 435.7270 402.7915 195.2983 -5.6867 429.9032 435.5899 402.5696 196.9055 -5.6857 429.7696 435.4553 402.3431 198.5126 -5.6844 429.6316 435.3160 402.1154 200.1354 -5.6821 429.4889 435.1709 401.8781 201.7376 -5.6805 429.3473 435.0278 401.6307 203.3498 -5.6800 429.2003 434.8803 401.3800 204.9571 -5.6781 429.0529 434.7309 401.1226 206.5644 -5.6751 428.9084 434.5835 400.8585 208.1714 -5.6715 428.7665 434.4380 400.5855 209.7734 -5.6681 428.6271 434.2952 400.3135 211.3959 -5.6652 428.4817 434.1468 400.0328 212.9979 -5.6620 428.3318 433.9939 399.7572 214.5791 -5.6589 428.1828 433.8417 399.4799 216.1809 -5.6542 428.0261 433.6803 399.1983 217.7933 -5.6489 427.8706 433.5195 398.9130 219.3901 -5.6450 427.7222 433.3671 398.6252 220.9923 -5.6404 427.5707 433.2111 398.3367 222.5994 -5.6360 427.4192 433.0552 398.0378 224.2168 -5.6326 427.2657 432.8983 397.7483 225.8241 -5.6282 427.1088 432.7370 397.4522 227.4109 -5.6229 426.9533 432.5762 397.1596 229.0384 -5.6186 426.7931 432.4117 396.8632 230.6249 -5.6139 426.6339 432.2477 396.5774 232.2323 -5.6086 426.4732 432.0818 396.2910 233.8395 -5.6027 426.3084 431.9111 396.0027 235.4466 -5.5980 426.1464 431.7444 395.7142 237.0693 -5.5935 425.9831 431.5765 395.4243 238.6714 -5.5886 425.8171 431.4057 395.1458 240.2839 -5.5838 425.6490 431.2328 394.8708 241.8758 -5.5789 425.4892 431.0681 394.6064 243.4831 -5.5743 425.3150 430.8893 394.3407 245.0904 -5.5699 425.1449 430.7148 394.0773 246.6975 -5.5647 424.9763 430.5410 393.8199 248.3099 -5.5596 424.8025 430.3621 393.5647 249.9015 -5.5555 424.6286 430.1841 393.3204 251.5086 -5.5508 424.4556 430.0064 393.0676 253.1160 -5.5470 424.2734 429.8204 392.8294 254.7436 -5.5436 424.0924 429.6360 392.5865 256.3303 -5.5394 423.9092 429.4486 392.3603 257.9428 -5.5348 423.7276 429.2624 392.1319 259.5500 -5.5314 423.5401 429.0714 391.9069 261.1673 -5.5275 423.3553 428.8829 391.6859 262.7693 -5.5236 423.1782 428.7017 391.4736 264.3818 -5.5192 422.9961 428.5154 391.2684 265.9785 -5.5153 422.8227 428.3380 391.0669 267.5808 -5.5112 422.6381 428.1493 390.8704 269.2035 -5.5085 422.4569 427.9654 390.6812 270.7953 -5.5037 422.2718 427.7756 390.4904 272.4179 -5.4995 422.0819 427.5813 390.3056 274.0253 -5.4952 421.8892 427.3844 390.1218 275.6224 -5.4901 421.7032 427.1933 389.9466 277.2191 -5.4859 421.5199 427.0057 389.7727 278.8213 -5.4818 421.3351 426.8169 389.6028 280.4338 -5.4777 421.1475 426.6252 389.4309 282.0254 -5.4735 420.9577 426.4312 389.2705 283.6275 -5.4713 420.7631 426.2344 389.1107 285.2398 -5.4684 420.5701 426.0386 388.9530 286.8520 -5.4652 420.3814 425.8466 388.7971 288.4593 -5.4613 420.1883 425.6497 388.6447 290.0510 -5.4593 419.9989 425.4583 388.4906 291.6580 -5.4559 419.8112 425.2671 388.3324 293.2704 -5.4519 419.6207 425.0727 388.1790 294.8723 -5.4482 419.4308 424.8790 388.0209 296.4793 -5.4445 419.2375 424.6821 387.8708 298.0861 -5.4411 419.0433 424.4843 387.7158 299.6985 -5.4373 418.8548 424.2921 387.5559 301.2903 -5.4331 418.6668 424.0999 387.4057 302.9284 -5.4293 418.4695 423.8988 387.2419 304.5355 -5.4266 418.2792 423.7058 387.0860 306.1273 -5.4233 418.0923 423.5155 386.9235 307.7499 -5.4207 417.9005 423.3212 386.7534 309.3366 -5.4175 417.7180 423.1354 386.5893 310.9539 -5.4137 417.5264 422.9401 386.4236 312.5716 -5.4099 417.3330 422.7429 386.2584 314.1789 -5.4064 417.1410 422.5474 386.0885 315.7858 -5.4032 416.9635 422.3667 385.9059 317.4086 -5.3989 416.7731 422.1720 385.7273 319.0108 -5.3944 416.5814 421.9759 385.5503 320.5975 -5.3902 416.3942 421.7844 385.3592 322.2305 -5.3872 416.2063 421.5935 385.1688 323.8429 -5.3836 416.0165 421.4001 384.9793 325.4501 -5.3794 415.8276 421.2070 384.7924 327.0573 -5.3752 415.6371 421.0123 384.5894 328.6698 -5.3709 415.4504 420.8213 384.3829 330.2819 -5.3672 415.2627 420.6299 384.1758 331.8736 -5.3625 415.0788 420.4413 383.9698 333.4859 -5.3580 414.8900 420.2480 383.7549 335.0930 -5.3536 414.7066 420.0603 383.5444 336.7105 -5.3496 414.5236 419.8732 383.3332 338.3128 -5.3456 414.3358 419.6813 383.1172 339.9096 -5.3404 414.1568 419.4972 382.8997 341.5119 -5.3349 413.9657 419.3006 382.6824 343.1193 -5.3295 413.7770 419.1065 382.4527 344.7056 -5.3243 413.5884 418.9127 382.2195 346.3024 -5.3194 413.4002 418.7195 381.9906 347.9095 -5.3149 413.2084 418.5233 381.7562 349.5270 -5.3088 413.0134 418.3221 381.5192 351.1188 -5.3029 412.8253 418.1282 381.2813 352.7260 -5.2971 412.6355 417.9326 381.0384 354.3333 -5.2921 412.4483 417.7404 380.7957 355.9353 -5.2864 412.2593 417.5456 380.5528 357.5476 -5.2798 412.0659 417.3457 380.3080 359.1293 -5.2747 411.8854 417.1601 380.0656 360.7365 -5.2694 411.7036 416.9729 379.8271 362.3438 -5.2628 411.5143 416.7771 379.5832 363.9666 -5.2564 411.3197 416.5761 379.3405 365.5688 -5.2514 411.1256 416.3770 379.1012 367.1658 -5.2460 410.9295 416.1755 378.8621 368.7731 -5.2400 410.7427 415.9827 378.6224 370.3749 -5.2343 410.5607 415.7950 378.3820 371.9874 -5.2285 410.3730 415.6015 378.1376 373.5945 -5.2211 410.1854 415.4065 377.8950 375.1863 -5.2143 409.9891 415.2034 377.6652 376.7986 -5.2086 409.7911 414.9997 377.4305 378.4160 -5.2029 409.5956 414.7986 377.1875 380.0234 -5.1974 409.3955 414.5929 376.9526 381.6308 -5.1922 409.1978 414.3900 376.7190 383.2379 -5.1863 409.0044 414.1907 376.4858 384.8453 -5.1813 408.8099 413.9912 376.2515 386.4573 -5.1755 408.6089 413.7843 376.0245 388.0490 -5.1696 408.4134 413.5830 375.8015 389.6563 -5.1643 408.2197 413.3839 375.5785 391.2791 -5.1591 408.0172 413.1762 375.3506 392.8810 -5.1534 407.8224 412.9758 375.1289 394.4934 -5.1484 407.6248 412.7732 374.9100 396.1056 -5.1434 407.4234 412.5668 374.6908 397.7075 -5.1392 407.2251 412.3643 374.4729 399.3199 -5.1338 407.0171 412.1509 374.2628 400.9273 -5.1287 406.8080 411.9367 374.0519 402.5445 -5.1230 406.5993 411.7224 373.8397 404.1414 -5.1190 406.3911 411.5101 373.6390 405.7384 -5.1138 406.1932 411.3070 373.4410 407.3508 -5.1071 405.9891 411.0961 373.2393 408.9528 -5.1010 405.7919 410.8929 373.0403 410.5499 -5.0965 405.5981 410.6947 372.8440 412.1571 -5.0922 405.3907 410.4829 372.6519 413.7643 -5.0870 405.1801 410.2670 372.4578 415.3868 -5.0806 404.9756 410.0562 372.2637 416.9785 -5.0759 404.7815 409.8574 372.0762 418.5804 -5.0706 404.5925 409.6631 371.8841 420.1926 -5.0659 404.3840 409.4499 371.6937 421.7943 -5.0600 404.1828 409.2429 371.5053 423.4068 -5.0540 403.9862 409.0402 371.3167 425.0088 -5.0495 403.7833 408.8328 371.1393 426.6160 -5.0442 403.5776 408.6218 370.9623 428.2386 -5.0395 403.3716 408.4111 370.7764 429.8408 -5.0353 403.1714 408.2067 370.5872 431.4531 -5.0314 402.9651 407.9965 370.3985 433.0653 -5.0267 402.7653 407.7920 370.2053 434.6675 -5.0214 402.5709 407.5923 370.0239 436.2694 -5.0159 402.3622 407.3781 369.8443 437.8766 -5.0102 402.1541 407.1643 369.6568 439.4998 -5.0050 401.9444 406.9494 369.4634 441.1069 -4.9989 401.7421 406.7410 369.2763 442.7140 -4.9934 401.5411 406.5345 369.0905 444.3261 -4.9886 401.3432 406.3318 368.9067 445.9285 -4.9837 401.1506 406.1343 368.7251 447.5409 -4.9789 400.9453 405.9242 368.5344 449.1584 -4.9733 400.7399 405.7132 368.3419 450.7659 -4.9687 400.5402 405.5089 368.1482 452.3888 -4.9638 400.3414 405.3053 367.9532 453.9961 -4.9590 400.1433 405.1023 367.7567 455.6033 -4.9547 399.9426 404.8974 367.5634 457.2105 -4.9492 399.7470 404.6962 367.3634 458.8178 -4.9438 399.5415 404.4853 367.1709 460.4300 -4.9380 399.3381 404.2761 366.9795 462.0373 -4.9342 399.1390 404.0732 366.7795 463.6445 -4.9295 398.9389 403.8684 366.5798 465.2518 -4.9244 398.7371 403.6615 366.3780 466.8488 -4.9200 398.5396 403.4596 366.1798 468.4508 -4.9152 398.3398 403.2550 365.9743 470.0530 -4.9104 398.1343 403.0448 365.7747 471.6551 -4.9052 397.9432 402.8484 365.5703 473.2570 -4.9006 397.7412 402.6418 365.3700 474.8643 -4.8958 397.5376 402.4333 365.1579 476.4715 -4.8904 397.3436 402.2340 364.9524 478.0684 -4.8846 397.1402 402.0248 364.7475 479.6808 -4.8783 396.9450 401.8232 364.5397 481.2828 -4.8732 396.7446 401.6178 364.3242 482.8745 -4.8684 396.5478 401.4162 364.1110 484.4819 -4.8627 396.3499 401.2126 363.8956 486.0891 -4.8566 396.1517 401.0082 363.6794 487.7120 -4.8509 395.9513 400.8021 363.4648 489.3140 -4.8449 395.7487 400.5937 363.2503 490.9264 -4.8396 395.5400 400.3797 363.0366 492.5284 -4.8335 395.3299 400.1633 362.8130 494.1200 -4.8278 395.1330 399.9608 362.5948 495.7325 -4.8213 394.9373 399.7586 362.3753 497.3343 -4.8150 394.7417 399.5567 362.1570 498.9468 -4.8094 394.5432 399.3527 361.9345 500.5694 -4.8031 394.3379 399.1410 361.7121 502.1716 -4.7958 394.1280 398.9238 361.4901 503.7838 -4.7894 393.9166 398.7060 361.2616 505.3859 -4.7833 393.7137 398.4970 361.0388 506.9933 -4.7765 393.5065 398.2830 360.8174 508.6055 -4.7703 393.2999 398.0702 360.5921 510.2126 -4.7645 393.0946 397.8591 360.3708 511.8354 -4.7574 392.8910 397.6484 360.1457 513.4271 -4.7519 392.6885 397.4404 359.9222 515.0396 -4.7462 392.4785 397.2247 359.6932 516.6415 -4.7393 392.2719 397.0113 359.4676 518.2540 -4.7333 392.0687 396.8020 359.2422 519.8561 -4.7276 391.8704 396.5980 359.0238 521.4684 -4.7221 391.6697 396.3919 358.7953 523.0756 -4.7161 391.4676 396.1837 358.5674 524.6984 -4.7104 391.2626 395.9730 358.3375 526.3105 -4.7057 391.0544 395.7600 358.1118 527.9178 -4.7002 390.8505 395.5507 357.8899 529.5251 -4.6951 390.6466 395.3416 357.6784 531.1270 -4.6888 390.4478 395.1366 357.4639 532.7239 -4.6830 390.2430 394.9260 357.2524 534.3156 -4.6769 390.0456 394.7225 357.0412 535.9228 -4.6701 389.8473 394.5174 356.8200 537.5354 -4.6635 389.6428 394.3063 356.5992 539.1426 -4.6585 389.4418 394.1002 356.3847 540.7444 -4.6529 389.2352 393.8881 356.1734 542.3465 -4.6474 389.0283 393.6757 355.9619 543.9588 -4.6413 388.8214 393.4627 355.7623 545.5556 -4.6340 388.6242 393.2582 355.5563 547.1529 -4.6296 388.4204 393.0500 355.3532 548.7545 -4.6247 388.2152 392.8399 355.1465 550.3773 -4.6194 388.0126 392.6321 354.9328 551.9845 -4.6139 387.8004 392.4142 354.7283 553.5915 -4.6085 387.5974 392.2059 354.5251 555.1986 -4.6033 387.3906 391.9939 354.3141 556.8006 -4.5977 387.1837 391.7814 354.1099 558.4130 -4.5926 386.9844 391.5770 353.9050 560.0149 -4.5882 386.7855 391.3736 353.7044 561.6376 -4.5823 386.5797 391.1620 353.5018 563.2449 -4.5773 386.3766 390.9539 353.3058 564.8520 -4.5728 386.1708 390.7437 353.1063 566.4644 -4.5679 385.9631 390.5310 352.9056 568.0665 -4.5628 385.7558 390.3186 352.7128 569.6738 -4.5576 385.5506 390.1082 352.5187 571.2859 -4.5521 385.3449 389.8970 352.3199 572.9085 -4.5473 385.1345 389.6818 352.1166 574.5105 -4.5425 384.9254 389.4679 351.9112 576.1233 -4.5372 384.7205 389.2577 351.7163 577.7251 -4.5326 384.5134 389.0460 351.5240 579.3376 -4.5271 384.3050 388.8320 351.3264 580.9500 -4.5220 384.0972 388.6191 351.1304 582.5520 -4.5168 383.8978 388.4146 350.9296 584.1746 -4.5119 383.6941 388.2060 350.7335 585.7823 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