DTA measure 2masodikmerespu4 Date: 2026422:1021 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.56 s Mass = 1156.700 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2420 -2.0705 211.9386 214.0091 247.8035 2.0290 -2.0599 212.0103 214.0703 247.8578 2.8365 -2.0628 212.1414 214.2042 247.7389 3.6235 -2.0499 212.2653 214.3151 247.7151 4.4215 -2.0389 212.5630 214.6019 247.6339 5.2498 -2.0279 212.5954 214.6234 247.5820 6.0163 -2.0367 212.5922 214.6290 247.5947 6.8750 -2.0289 212.7304 214.7593 247.4895 7.6318 -2.0069 212.7447 214.7515 247.4715 8.4705 -2.0220 213.0405 215.0625 247.4555 9.2575 -2.0321 213.1753 215.2074 247.4769 10.0548 -2.0195 213.2926 215.3122 247.3363 10.8828 -2.0081 213.4452 215.4534 247.2696 11.6498 -1.9988 213.5502 215.5489 247.3225 12.5090 -2.0118 213.8195 215.8312 247.3968 13.2653 -2.0140 213.8694 215.8834 247.2636 14.1035 -2.0143 214.1151 216.1294 247.0616 14.8910 -2.0097 214.1727 216.1825 246.9810 15.6888 -2.0080 214.2341 216.2421 247.0184 16.4860 -2.0045 214.3882 216.3926 247.0515 17.2833 -1.9958 214.6417 216.6375 247.0634 18.1115 -1.9993 214.9083 216.9077 247.0718 18.8685 -2.0030 214.9796 216.9827 247.0154 19.7375 -1.9990 215.0789 217.0779 246.9970 20.5040 -1.9918 215.2084 217.2003 246.9674 21.3320 -1.9893 215.3339 217.3232 246.9480 22.1198 -1.9771 215.5863 217.5634 246.8887 22.9275 -1.9829 215.7657 217.7487 246.9864 23.7453 -1.9621 215.9585 217.9206 246.9835 24.5118 -1.9375 216.0731 218.0105 246.9912 25.3713 -1.9232 216.1819 218.1050 246.9481 26.1380 -1.9199 216.2528 218.1727 246.9602 26.9660 -1.9211 216.3620 218.2831 247.0249 27.7530 -1.9233 216.5033 218.4266 247.0412 28.5605 -1.9144 216.5615 218.4759 246.9688 29.3793 -1.9114 216.5980 218.5094 246.9972 30.1458 -1.9153 216.7365 218.6518 247.0612 31.0045 -1.8971 216.9587 218.8558 247.1812 31.7410 -1.9129 217.1661 219.0790 247.2496 32.6000 -1.9084 217.2981 219.2065 247.2873 33.3665 -1.9088 217.4378 219.3467 247.4680 34.1945 -1.9074 217.5507 219.4581 247.4739 34.9820 -1.8924 217.7659 219.6582 247.4990 35.7695 -1.8859 217.8222 219.7081 247.5784 36.5975 -1.8964 217.8709 219.7672 247.6165 37.3640 -1.9064 217.9211 219.8276 247.5691 38.2125 -1.9057 218.0691 219.9748 247.5535 38.9793 -1.9036 218.1773 220.0809 247.5850 39.8080 -1.8913 218.2655 220.1569 247.6526 40.5643 -1.8743 218.4302 220.3044 247.7219 41.3923 -1.8625 218.6253 220.4878 247.7833 42.1793 -1.8485 218.8247 220.6732 247.8743 42.9768 -1.8687 218.9399 220.8086 248.1274 43.8055 -1.8813 219.0299 220.9112 248.2672 44.5720 -1.8732 219.1305 221.0037 248.2124 45.4205 -1.8628 219.2223 221.0851 248.4065 46.1870 -1.8564 219.2966 221.1529 248.4300 47.0160 -1.8605 219.3988 221.2592 248.6012 47.8030 -1.8503 219.5641 221.4144 248.8168 48.6003 -1.8451 219.5689 221.4140 248.9497 49.4283 -1.8340 219.7163 221.5503 249.2315 50.1848 -1.8227 219.8335 221.6562 249.3601 51.0545 -1.8157 219.9991 221.8148 249.4389 51.8108 -1.8153 220.1885 222.0038 249.5361 52.6285 -1.7955 220.4291 222.2246 249.6208 53.4360 -1.7813 220.5018 222.2831 249.7305 54.2238 -1.7744 220.7627 222.5371 249.9546 55.0520 -1.7800 220.8578 222.6378 250.1311 55.8185 -1.7791 220.9978 222.7769 250.3107 56.6670 -1.7809 221.1474 222.9283 250.3520 57.4338 -1.7676 221.0835 222.8511 250.5716 58.2625 -1.7638 221.2663 223.0301 250.9031 59.0598 -1.7699 221.4741 223.2440 251.1105 59.8570 -1.7831 221.6139 223.3970 251.2582 60.6748 -1.7697 221.7849 223.5546 251.3407 61.4525 -1.7707 221.7697 223.5404 251.3957 62.3010 -1.7617 221.9552 223.7169 251.5853 63.0675 -1.7664 221.9419 223.7083 251.7360 63.8955 -1.7669 221.9258 223.6926 251.9256 64.6930 -1.7598 222.0395 223.7992 252.0577 65.4910 -1.7576 222.2473 224.0049 252.1211 66.3088 -1.7676 222.3739 224.1415 252.2641 67.0855 -1.7596 222.5033 224.2630 252.4878 67.9343 -1.7638 222.6186 224.3824 252.6126 68.7015 -1.7777 222.6951 224.4727 252.8128 69.5295 -1.7908 222.8098 224.6006 252.9754 70.3268 -1.7867 222.9658 224.7525 252.9808 71.1240 -1.7773 223.0385 224.8158 253.0516 71.9423 -1.7691 223.0990 224.8680 253.2302 72.7195 -1.7656 223.2634 225.0290 253.3874 73.5680 -1.7758 223.4030 225.1788 253.6304 74.3345 -1.7850 223.5933 225.3783 253.8872 75.1625 -1.7797 223.6718 225.4515 253.9590 75.9598 -1.7871 223.7514 225.5385 254.0843 76.7580 -1.8003 223.8369 225.6372 254.2315 77.5758 -1.8029 223.8590 225.6619 254.4661 78.3525 -1.7986 223.9178 225.7163 254.4224 79.2010 -1.7865 224.0177 225.8042 254.4851 79.9683 -1.7764 224.1376 225.9140 254.5782 80.7965 -1.7585 224.4373 226.1958 254.6379 81.5938 -1.7544 224.5764 226.3308 254.5988 82.3910 -1.7363 224.7324 226.4687 254.7031 83.2093 -1.7351 224.8568 226.5919 254.8897 83.9865 -1.7365 224.9812 226.7177 255.0982 84.8350 -1.7391 225.0421 226.7811 255.1575 85.5810 -1.7407 225.1482 226.8889 255.3374 86.4295 -1.7591 225.4443 227.2034 255.4603 87.2073 -1.7460 225.5753 227.3213 255.6247 88.0250 -1.7246 225.8052 227.5298 255.8131 88.8223 -1.7281 225.9702 227.6983 255.9319 89.6195 -1.7369 226.1503 227.8872 256.0156 90.4475 -1.7381 226.3242 228.0623 256.1586 91.2150 -1.7270 226.3427 228.0697 256.2690 92.0635 -1.7308 226.3843 228.1152 256.3172 92.8403 -1.7413 226.2929 228.0342 256.3941 93.6580 -1.7396 226.4442 228.1838 256.5647 94.4250 -1.7338 226.6126 228.3464 256.7194 95.2535 -1.7303 226.7730 228.5033 256.8783 96.0508 -1.7301 226.9607 228.6907 257.0393 96.8480 -1.7289 227.0912 228.8200 257.2519 97.6660 -1.7450 227.2120 228.9569 257.3818 98.4435 -1.7563 227.3756 229.1319 257.5127 99.2920 -1.7472 227.4948 229.2421 257.7039 100.0483 -1.7565 227.5500 229.3066 257.8361 100.8763 -1.7599 227.6324 229.3924 257.7559 101.6430 -1.7420 227.6745 229.4165 257.8150 102.4615 -1.7437 227.8866 229.6303 257.8630 103.2588 -1.7481 228.0104 229.7585 258.0600 104.0560 -1.7336 228.1632 229.8968 258.2361 104.8738 -1.7353 228.3408 230.0761 258.2754 105.6405 -1.7387 228.5271 230.2658 258.3672 106.4898 -1.7332 228.6140 230.3472 258.4764 107.2563 -1.7351 228.6787 230.4138 258.5802 108.0843 -1.7397 228.6918 230.4315 258.6719 108.8405 -1.7504 228.6548 230.4051 258.7966 109.6685 -1.7315 228.8266 230.5581 258.8893 110.4668 -1.7438 228.8832 230.6270 258.8995 111.2640 -1.7593 229.0582 230.8175 259.0393 112.0818 -1.7558 229.1443 230.9001 259.1433 112.8483 -1.7541 229.3813 231.1354 259.2414 113.7073 -1.7508 229.4648 231.2156 259.3073 114.4643 -1.7356 229.4697 231.2053 259.3731 115.3025 -1.7331 229.5801 231.3131 259.4350 116.0588 -1.7343 229.7543 231.4886 259.5582 116.8868 -1.7341 229.9220 231.6561 259.6596 117.6845 -1.7324 229.8546 231.5870 259.7665 118.4720 -1.7550 229.9234 231.6783 259.7174 119.3000 -1.7566 229.9900 231.7466 259.8613 120.0665 -1.7606 230.1145 231.8751 259.8972 120.9255 -1.7413 230.2179 231.9592 260.0183 121.6928 -1.7330 230.3208 232.0538 260.2126 122.5105 -1.7422 230.4176 232.1598 260.3604 123.3180 -1.7587 230.6210 232.3798 260.4648 124.1050 -1.7488 230.7837 232.5325 260.6951 124.9235 -1.7515 230.9342 232.6857 260.7456 125.7005 -1.7506 231.1338 232.8844 260.7254 126.5593 -1.7405 231.3611 233.1016 260.6908 127.2950 -1.7367 231.3554 233.0921 260.7702 128.1435 -1.7488 231.4049 233.1537 260.9427 128.9213 -1.7448 231.4168 233.1617 260.9682 129.7390 -1.7453 231.6160 233.3613 261.0230 130.5363 -1.7461 231.7454 233.4914 261.0618 131.3335 -1.7323 231.8751 233.6074 261.1420 132.1615 -1.7334 231.9717 233.7051 261.2270 132.9285 -1.7257 232.1135 233.8392 261.2505 133.7775 -1.7238 232.2719 233.9957 261.3933 134.5543 -1.7341 232.3381 234.0722 261.6281 135.3720 -1.7278 232.4879 234.2157 261.7633 136.1693 -1.7327 232.6087 234.3415 261.7749 136.9670 -1.7427 232.7745 234.5172 261.9164 137.7955 -1.7488 232.9074 234.6563 261.9556 138.5620 -1.7551 233.1311 234.8861 261.9549 139.4105 -1.7593 233.2411 235.0004 262.1791 140.1875 -1.7542 233.2857 235.0399 262.2909 141.0060 -1.7353 233.3799 235.1152 262.3547 141.8033 -1.7281 233.3869 235.1150 262.5512 142.6005 -1.7412 233.5515 235.2927 262.6323 143.4288 -1.7425 233.7665 235.5090 262.7872 144.1960 -1.7421 234.0088 235.7509 262.9649 145.0445 -1.7439 234.1926 235.9365 262.9659 145.8213 -1.7619 234.2548 236.0167 263.1504 146.6390 -1.7518 234.3000 236.0518 263.2634 147.4165 -1.7310 234.2837 236.0147 263.3092 148.2345 -1.7190 234.3299 236.0489 263.2963 149.0420 -1.7192 234.4908 236.2099 263.4349 149.8290 -1.7290 234.5984 236.3274 263.5613 150.6578 -1.7362 234.7806 236.5168 263.7231 151.4245 -1.7225 234.8524 236.5749 263.8010 152.2833 -1.7173 235.0946 236.8119 263.7773 153.0498 -1.7125 235.2109 236.9234 263.8042 153.8680 -1.6998 235.4217 237.1214 263.9329 154.6760 -1.7122 235.5357 237.2479 264.0751 155.4630 -1.7174 235.6123 237.3296 264.2147 156.2910 -1.7319 235.6667 237.3986 264.3993 157.0575 -1.7418 235.7757 237.5175 264.5353 157.9173 -1.7433 235.9312 237.6746 264.5735 158.6838 -1.7286 236.0199 237.7484 264.6373 159.5015 -1.7247 236.1981 237.9228 264.7365 160.3090 -1.7157 236.2973 238.0130 264.7893 161.0963 -1.7207 236.3077 238.0284 264.8144 161.9250 -1.7228 236.3787 238.1016 264.9569 162.6915 -1.6909 236.5608 238.2517 265.1677 163.5400 -1.6820 236.6181 238.3001 265.2730 164.2963 -1.6886 236.7351 238.4237 265.4077 165.1245 -1.6995 236.9551 238.6546 265.5841 165.9225 -1.6932 237.1780 238.8713 265.5652 166.7095 -1.6912 237.3025 238.9937 265.6329 167.5375 -1.6943 237.3652 239.0595 265.7376 168.3040 -1.6909 237.4686 239.1595 265.8391 169.1535 -1.6747 237.6469 239.3216 265.9481 169.9200 -1.6705 237.6755 239.3460 265.9861 170.7480 -1.6845 237.7825 239.4671 266.1685 171.5350 -1.6842 237.8128 239.4969 266.2672 172.3330 -1.6800 237.8797 239.5597 266.2431 173.1613 -1.7004 237.9921 239.6926 266.3849 173.9175 -1.7118 238.1128 239.8246 266.5068 174.7455 -1.6984 238.2163 239.9147 266.5733 175.5123 -1.6930 238.3360 240.0290 266.7305 176.3615 -1.7083 238.4169 240.1252 266.7379 177.1383 -1.7210 238.3892 240.1102 266.8219 177.9560 -1.7299 238.4674 240.1973 266.9677 178.7430 -1.7423 238.5824 240.3247 267.1753 179.5515 -1.7629 238.6736 240.4365 267.3709 180.3693 -1.7673 238.9041 240.6714 267.5555 181.1255 -1.7549 239.0185 240.7734 267.7040 181.9945 -1.7337 239.1240 240.8576 267.7903 182.7518 -1.7201 239.4411 241.1612 267.8574 183.5798 -1.6956 239.6043 241.3000 267.8358 184.3770 -1.6923 239.6267 241.3190 268.0563 185.1743 -1.6860 239.7231 241.4091 268.0788 186.0025 -1.6699 239.8526 241.5225 268.0427 186.7595 -1.6764 239.8138 241.4903 268.1594 187.6183 -1.6871 239.9226 241.6096 268.3373 188.3540 -1.7011 240.0359 241.7370 268.4792 189.2025 -1.6962 240.1124 241.8086 268.5627 189.9803 -1.6995 240.2242 241.9237 268.6750 190.7980 -1.6871 240.2964 241.9835 268.8529 191.5953 -1.6757 240.4669 242.1427 269.0150 192.3925 -1.6653 240.5456 242.2109 269.1909 193.2208 -1.6661 240.7918 242.4579 269.3624 193.9880 -1.6646 240.9750 242.6396 269.4178 194.8365 -1.6670 241.1273 242.7943 269.4237 195.6133 -1.6805 241.2240 242.9045 269.5240 196.4313 -1.6894 241.3671 243.0565 269.6489 197.1985 -1.6739 241.4766 243.1506 269.6919 198.0265 -1.6712 241.7703 243.4416 269.8748 198.8238 -1.6547 241.8555 243.5102 269.8740 199.6210 -1.6598 242.0757 243.7355 269.9173 200.4395 -1.6868 242.1482 243.8350 270.0870 201.2165 -1.7116 242.1620 243.8736 270.3114 202.0650 -1.7133 242.2896 244.0029 270.5359 202.8315 -1.7066 242.3762 244.0828 270.6923 203.6595 -1.7065 242.5418 244.2483 270.7876 204.4573 -1.7136 242.6191 244.3327 270.9722 205.2550 -1.6981 242.6739 244.3720 270.9829 206.0523 -1.7002 242.7806 244.4808 271.0619 206.8495 -1.7067 242.9615 244.6683 271.2037 207.6775 -1.6997 243.0597 244.7594 271.2270 208.4450 -1.6961 243.0025 244.6986 271.3005 209.2935 -1.6840 243.0555 244.7395 271.4176 210.0703 -1.6638 243.0589 244.7226 271.4521 210.8880 -1.6542 243.2388 244.8930 271.5053 211.6858 -1.6481 243.3923 245.0403 271.5894 212.4835 -1.6437 243.4604 245.1041 271.7568 213.3115 -1.6571 243.5291 245.1862 271.9317 214.0780 -1.6642 243.7000 245.3642 272.0142 214.9270 -1.6699 243.7272 245.3970 272.0924 215.7043 -1.6784 243.6517 245.3300 272.2628 216.5220 -1.6870 243.7930 245.4800 272.3343 217.3193 -1.6926 243.8960 245.5886 272.4938 218.1168 -1.6936 243.9346 245.6282 272.5134 218.9455 -1.6891 243.9698 245.6588 272.5639 219.7120 -1.6902 244.1386 245.8289 272.6377 220.5298 -1.6837 244.3298 246.0135 272.7880 221.3065 -1.6903 244.5978 246.2880 272.8192 222.1558 -1.6976 244.9187 246.6163 272.8856 222.9225 -1.7082 245.0038 246.7120 273.0953 223.7505 -1.7143 245.0740 246.7884 273.0227 224.5478 -1.7101 245.1311 246.8412 273.0830 225.3450 -1.7035 245.2753 246.9788 273.1864 226.1638 -1.6866 245.2505 246.9370 273.2049 226.9405 -1.6993 245.4252 247.1245 273.3186 227.7890 -1.7048 245.6740 247.3788 273.4991 228.5453 -1.6898 245.7846 247.4743 273.6832 229.3735 -1.6821 245.7308 247.4129 273.7952 230.1613 -1.7066 245.9278 247.6344 273.7162 230.9585 -1.7055 246.1139 247.8195 273.7051 231.7558 -1.7018 246.3472 248.0490 273.8194 232.5530 -1.6817 246.4749 248.1566 273.9372 233.3718 -1.6718 246.5819 248.2536 274.0952 234.1383 -1.6780 246.6922 248.3701 274.1687 234.9970 -1.6847 246.7581 248.4427 274.3647 235.7533 -1.6888 246.9744 248.6631 274.4864 236.5918 -1.6808 247.1415 248.8222 274.5522 237.3795 -1.6585 247.1759 248.8344 274.5735 238.1665 -1.6511 247.2309 248.8821 274.7483 239.0048 -1.6416 247.1991 248.8408 274.9385 239.7610 -1.6287 247.2953 248.9240 274.9552 240.5898 -1.6342 247.4685 249.1027 274.9978 241.3565 -1.6361 247.5336 249.1697 275.0839 242.2050 -1.6429 247.7047 249.3476 275.1853 242.9715 -1.6408 247.8339 249.4747 275.3663 243.8000 -1.6495 247.9293 249.5788 275.5018 244.5978 -1.6483 248.1161 249.7644 275.5768 245.3950 -1.6371 248.3968 250.0339 275.8485 246.2128 -1.6453 248.4776 250.1228 276.1243 246.9895 -1.6530 248.5305 250.1836 276.2551 247.8388 -1.6555 248.8187 250.4742 276.4399 248.6055 -1.6551 248.9079 250.5630 276.4441 249.4335 -1.6749 248.9730 250.6479 276.5509 250.2308 -1.6722 249.0804 250.7526 276.6290 251.0283 -1.6635 249.1914 250.8549 276.6822 251.8468 -1.6517 249.2557 250.9074 276.7238 252.6133 -1.6568 249.2132 250.8700 276.8923 253.4720 -1.6545 249.1630 250.8174 277.0373 254.2283 -1.6472 249.2336 250.8808 277.0978 255.0675 -1.6597 249.4741 251.1338 277.2098 255.8545 -1.6533 249.6713 251.3246 277.4312 256.6518 -1.6419 249.7746 251.4165 277.6332 257.4798 -1.6349 249.8602 251.4951 277.8340 258.2473 -1.6523 250.0260 251.6783 277.9684 259.1060 -1.6533 250.2035 251.8568 278.0759 259.8623 -1.6651 250.3876 252.0527 278.1353 260.7005 -1.6748 250.5120 252.1868 278.0855 261.4880 -1.6797 250.5585 252.2382 278.2232 262.2858 -1.6996 250.5860 252.2856 278.4825 263.1138 -1.6941 250.6398 252.3338 278.5162 263.8803 -1.6997 250.6850 252.3847 278.6211 264.7393 -1.6833 250.7909 252.4742 278.7328 265.4963 -1.6767 250.8803 252.5570 278.7716 266.3345 -1.7056 251.0656 252.7712 278.9542 267.1215 -1.7122 251.2466 252.9588 278.9592 267.9188 -1.7180 251.3485 253.0665 278.9532 268.7475 -1.7162 251.3885 253.1047 279.1801 269.5143 -1.7132 251.5116 253.2248 279.2247 270.3730 -1.7259 251.6361 253.3620 279.2781 271.1293 -1.7080 251.7363 253.4442 279.4395 271.9675 -1.6946 251.7809 253.4755 279.6096 272.7243 -1.6792 251.9063 253.5855 279.7458 273.5630 -1.6589 252.0879 253.7469 279.8920 274.3500 -1.6610 252.2068 253.8679 280.0168 275.1575 -1.6527 252.3896 254.0423 280.1598 275.9753 -1.6628 252.7069 254.3697 280.1823 276.7423 -1.6579 252.8620 254.5198 280.2160 277.6015 -1.6756 253.0022 254.6778 280.3732 278.3680 -1.6863 252.9802 254.6665 280.4163 279.1960 -1.6875 253.1155 254.8030 280.4932 279.9833 -1.6693 253.1581 254.8274 280.5927 280.7915 -1.6796 253.1778 254.8574 280.8340 281.6093 -1.6781 253.3057 254.9838 280.9513 282.3758 -1.6787 253.4831 255.1618 281.0101 283.2345 -1.6762 253.5040 255.1802 281.1525 284.0020 -1.6821 253.6619 255.3440 281.1461 284.8300 -1.6802 253.6600 255.3403 281.1565 285.6170 -1.6805 253.8106 255.4911 281.1585 286.4245 -1.6848 254.0080 255.6927 281.2642 287.2428 -1.6874 254.0408 255.7282 281.3557 288.0098 -1.6833 254.0885 255.7719 281.4293 288.8685 -1.6865 254.3013 255.9879 281.3891 289.6350 -1.6853 254.3868 256.0721 281.4138 290.4633 -1.6662 254.3933 256.0595 281.5383 291.2510 -1.6728 254.5604 256.2332 281.6198 292.0483 -1.6945 254.6106 256.3051 281.6631 292.8353 -1.7068 254.7523 256.4591 281.8544 293.6325 -1.7197 254.7601 256.4798 281.9467 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