DTA measure 1Gyors Date: 202534:1049 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 916.01 s Mass = 957.70 mg data_number = 1135 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2873 -0.7743 202.0596 202.8340 260.5382 2.0750 -0.7693 202.3169 203.0861 260.5432 2.8630 -0.7607 202.5596 203.3203 260.5210 3.6813 -0.7568 202.8279 203.5848 260.5575 4.4700 -0.7529 203.0783 203.8312 260.5702 5.2895 -0.7541 203.3239 204.0780 260.5869 6.0798 -0.7529 203.5762 204.3291 260.6133 6.8700 -0.7512 203.8234 204.5746 260.6485 7.6920 -0.7459 204.0694 204.8153 260.6797 8.4835 -0.7372 204.3534 205.0905 260.7397 9.3055 -0.7272 204.6042 205.3314 260.7865 10.0978 -0.7218 204.8340 205.5559 260.8400 10.8895 -0.7183 205.0794 205.7977 260.8935 11.7118 -0.7147 205.3170 206.0317 260.9579 12.4735 -0.7055 205.5511 206.2566 261.0204 13.3260 -0.7020 205.8205 206.5226 261.1344 14.1178 -0.6959 206.0716 206.7675 261.2407 14.9095 -0.6944 206.3066 207.0010 261.3251 15.7318 -0.6895 206.5601 207.2497 261.4146 16.4935 -0.6891 206.7835 207.4726 261.5220 17.3455 -0.6836 207.0412 207.7248 261.6531 18.1378 -0.6793 207.2864 207.9657 261.7717 18.9295 -0.6753 207.5195 208.1948 261.9069 19.7518 -0.6744 207.7636 208.4380 262.0696 20.5135 -0.6727 207.9889 208.6615 262.1928 21.3655 -0.6683 208.2494 208.9176 262.3172 22.1575 -0.6658 208.4929 209.1587 262.4654 22.9495 -0.6610 208.7411 209.4021 262.6133 23.7715 -0.6571 208.9787 209.6358 262.7933 24.5420 -0.6399 209.1940 209.8340 262.9495 25.3935 -0.6347 209.4317 210.0664 263.1121 26.1555 -0.6329 209.6667 210.2996 263.2923 26.9775 -0.6342 209.9350 210.5692 263.4661 27.7695 -0.6311 210.1539 210.7850 263.6349 28.5625 -0.6296 210.3847 211.0143 263.8110 29.3845 -0.6271 210.6119 211.2389 264.0046 30.1738 -0.6281 210.8586 211.4867 264.1869 30.9920 -0.6255 211.1041 211.7297 264.3765 31.7798 -0.6240 211.3587 211.9827 264.5514 32.5675 -0.6218 211.5828 212.2046 264.7252 33.3855 -0.6168 211.8237 212.4405 264.9107 34.1453 -0.6205 212.0423 212.6628 265.0901 35.0020 -0.5904 212.2803 212.8707 265.2778 35.7910 -0.5779 212.4867 213.0647 265.4979 36.5800 -0.5809 212.7146 213.2955 265.6786 37.3990 -0.5869 212.9639 213.5508 265.8825 38.1883 -0.5895 213.1944 213.7839 266.0623 39.0095 -0.5939 213.4221 214.0160 266.2338 39.8305 -0.5880 213.6539 214.2419 266.4179 40.5925 -0.5832 213.8728 214.4559 266.5860 41.4445 -0.5807 214.1232 214.7040 266.7867 42.2065 -0.5868 214.3444 214.9311 266.9565 43.0285 -0.5930 214.5845 215.1775 267.1493 43.8205 -0.5981 214.8111 215.4092 267.2980 44.6125 -0.5968 215.0306 215.6274 267.4782 45.4645 -0.5975 215.2698 215.8673 267.6591 46.2265 -0.6036 215.4980 216.1015 267.8030 47.0485 -0.6006 215.7138 216.3143 267.9996 47.8405 -0.5973 215.9531 216.5505 268.1549 48.6325 -0.5997 216.1724 216.7721 268.3030 49.4545 -0.5970 216.3934 216.9904 268.4688 50.2465 -0.5997 216.6106 217.2103 268.6263 51.0685 -0.5996 216.8552 217.4548 268.7880 51.8605 -0.5995 217.0848 217.6844 268.9211 52.6525 -0.5979 217.2917 217.8897 269.0451 53.4745 -0.5952 217.5477 218.1429 269.2019 54.2665 -0.5929 217.7699 218.3628 269.3577 55.0885 -0.5915 218.0074 218.5990 269.5149 55.8805 -0.5926 218.2185 218.8111 269.6348 56.6723 -0.5983 218.4525 219.0508 269.7508 57.5245 -0.5949 218.6698 219.2647 269.8891 58.2860 -0.5973 218.8861 219.4834 270.0204 59.1088 -0.6011 219.1094 219.7105 270.1747 59.9010 -0.5996 219.3367 219.9362 270.3109 60.6925 -0.5993 219.5496 220.1489 270.4032 61.5443 -0.5980 219.7745 220.3724 270.5086 62.3003 -0.5995 219.9692 220.5687 270.6376 63.1203 -0.5978 220.1913 220.7890 270.7391 63.9083 -0.5970 220.4257 221.0227 270.8466 64.6960 -0.5947 220.6471 221.2418 270.9808 65.5148 -0.5896 220.8723 221.4619 271.0963 66.3030 -0.5931 221.0938 221.6869 271.1948 67.1218 -0.5948 221.3018 221.8966 271.3152 67.9113 -0.5997 221.5231 222.1228 271.4182 68.7010 -0.5980 221.7268 222.3248 271.4989 69.5498 -0.6002 221.9509 222.5512 271.6377 70.3110 -0.6017 222.1501 222.7518 271.7327 71.1310 -0.5913 222.3878 222.9791 271.8372 71.9525 -0.5895 222.6235 223.2130 271.9433 72.7118 -0.5860 222.8233 223.4092 272.0452 73.5635 -0.5890 223.0415 223.6305 272.1595 74.3255 -0.5914 223.2523 223.8436 272.2691 75.1475 -0.5925 223.4782 224.0707 272.3718 75.9695 -0.5919 223.6711 224.2630 272.4784 76.7315 -0.5909 223.8876 224.4786 272.5838 77.5835 -0.5880 224.1127 224.7007 272.7266 78.4055 -0.5894 224.3403 224.9297 272.8432 79.1675 -0.5899 224.5268 225.1168 272.9516 80.0193 -0.5888 224.7725 225.3613 273.0865 80.8115 -0.5853 224.9689 225.5541 273.2060 81.6028 -0.5850 225.1719 225.7569 273.2993 82.4253 -0.5863 225.3957 225.9819 273.4207 83.2170 -0.5831 225.6038 226.1869 273.5363 84.0390 -0.5858 225.8160 226.4019 273.6493 84.8913 -0.5827 226.0541 226.6368 273.7913 85.7730 -0.5845 226.2670 226.8515 273.9334 86.6250 -0.5826 226.4809 227.0635 274.0606 87.4468 -0.5839 226.7012 227.2851 274.1835 88.2993 -0.5817 226.9329 227.5146 274.3398 89.0608 -0.5822 227.1082 227.6904 274.4696 89.8828 -0.5831 227.3280 227.9111 274.6066 90.7050 -0.5844 227.5332 228.1176 274.7324 91.5870 -0.5872 227.7717 228.3588 274.8965 92.4090 -0.5897 227.9815 228.5712 275.0306 93.2310 -0.5921 228.1919 228.7840 275.1368 94.0225 -0.5899 228.4142 229.0042 275.2604 94.8425 -0.5889 228.6101 229.1990 275.4175 95.5990 -0.5902 228.8077 229.3979 275.5537 96.4460 -0.5890 229.0356 229.6245 275.7019 97.2050 -0.5851 229.2151 229.8002 275.8204 98.0230 -0.5873 229.4033 229.9907 275.9915 98.8410 -0.5860 229.6139 230.1998 276.1379 99.5990 -0.5871 229.8008 230.3878 276.2837 100.4473 -0.5887 230.0412 230.6298 276.4093 101.2355 -0.5926 230.2581 230.8508 276.5418 102.0245 -0.5957 230.4492 231.0450 276.6690 102.8450 -0.5964 230.6590 231.2553 276.8388 103.6065 -0.5962 230.8339 231.4301 276.9610 104.4590 -0.5965 231.0326 231.6291 277.1060 105.2510 -0.5946 231.2540 231.8485 277.2683 106.0425 -0.5961 231.4513 232.0474 277.4048 106.8658 -0.5990 231.6546 232.2536 277.5575 107.6275 -0.6017 231.8485 232.4502 277.7221 108.4800 -0.6040 232.0348 232.6387 277.8384 109.2420 -0.6055 232.2275 232.8330 277.9620 110.0638 -0.6028 232.4498 233.0526 278.1104 110.8860 -0.5955 232.6337 233.2292 278.2929 111.6475 -0.5916 232.8326 233.4242 278.4129 112.5000 -0.5821 233.0223 233.6043 278.5744 113.2920 -0.5819 233.2491 233.8310 278.7168 114.1740 -0.5849 233.4899 234.0748 278.8840 114.9355 -0.5888 233.6737 234.2625 279.0238 115.7880 -0.5874 233.8787 234.4661 279.1624 116.5943 -0.5851 234.0787 234.6638 279.2869 117.4760 -0.5898 234.3029 234.8927 279.4484 118.2675 -0.6048 234.4894 235.0942 279.5942 119.0898 -0.6186 234.6834 235.3019 279.7578 119.8818 -0.6200 234.8702 235.4902 279.9022 120.6735 -0.6179 235.0624 235.6803 280.0460 121.4958 -0.6206 235.2704 235.8911 280.1966 122.2875 -0.6201 235.4645 236.0846 280.3484 123.1098 -0.6248 235.6694 236.2941 280.4736 123.9018 -0.6307 235.8641 236.4948 280.6014 124.6935 -0.6308 236.0537 236.6845 280.7634 125.5463 -0.6329 236.2415 236.8744 280.8969 126.3085 -0.6369 236.4284 237.0653 281.0389 127.1290 -0.6329 236.6316 237.2645 281.1686 127.9175 -0.6338 236.8319 237.4657 281.2916 128.7060 -0.6337 237.0232 237.6569 281.4486 129.5248 -0.6337 237.2186 237.8523 281.5844 130.3130 -0.6356 237.4171 238.0527 281.7076 131.1318 -0.6364 237.6183 238.2547 281.8357 131.9205 -0.6383 237.8051 238.4434 281.9727 132.7100 -0.6381 237.9859 238.6239 282.0955 133.5283 -0.6352 238.1546 238.7897 282.2140 134.3170 -0.6382 238.3632 239.0014 282.3589 135.1365 -0.6404 238.5694 239.2098 282.4860 135.9263 -0.6401 238.7541 239.3942 282.5900 136.7175 -0.6435 238.9528 239.5964 282.7166 137.5400 -0.6434 239.1613 239.8047 282.8368 138.3015 -0.6445 239.3238 239.9684 282.9791 139.1540 -0.6478 239.5247 240.1725 283.1046 139.9460 -0.6494 239.7170 240.3664 283.2274 140.7375 -0.6472 239.9199 240.5671 283.3359 141.5598 -0.6523 240.0863 240.7386 283.4711 142.3215 -0.6490 240.2691 240.9181 283.5923 143.1738 -0.6485 240.4659 241.1144 283.6991 143.9358 -0.6524 240.6407 241.2932 283.8326 144.7578 -0.6538 240.8426 241.4964 283.9675 145.5795 -0.6560 241.0555 241.7115 284.0775 146.3415 -0.6563 241.2373 241.8936 284.1921 147.1938 -0.6533 241.4256 242.0788 284.3229 147.9555 -0.6554 241.5875 242.2429 284.4421 148.7778 -0.6576 241.7979 242.4555 284.5490 149.5998 -0.6587 241.9683 242.6270 284.6707 150.3615 -0.6589 242.1555 242.8145 284.7984 151.2135 -0.6625 242.3531 243.0157 284.9299 151.9755 -0.6664 242.5365 243.2029 285.0375 152.7975 -0.6690 242.7532 243.4222 285.1740 153.6195 -0.6717 242.9289 243.6007 285.2945 154.3815 -0.6701 243.0962 243.7663 285.3935 155.2335 -0.6693 243.2892 243.9584 285.5339 155.9955 -0.6686 243.4535 244.1222 285.6372 156.8175 -0.6701 243.6431 244.3131 285.7755 157.5995 -0.6713 243.8182 244.4895 285.9070 158.4215 -0.6765 244.0088 244.6853 286.0451 159.2378 -0.6788 244.2104 244.8892 286.1653 159.9975 -0.6764 244.4090 245.0854 286.2825 160.8460 -0.6755 244.5830 245.2585 286.4313 161.6025 -0.6765 244.7565 245.4329 286.5715 162.4218 -0.6790 244.9531 245.6321 286.7041 163.2400 -0.6787 245.1212 245.7998 286.8377 163.9980 -0.6836 245.3026 245.9861 286.9790 164.8480 -0.6847 245.4898 246.1745 287.1055 165.6370 -0.6843 245.6705 246.3548 287.2289 166.4268 -0.6841 245.8742 246.5583 287.3645 167.2465 -0.6857 246.0615 246.7472 287.5093 168.0363 -0.6893 246.2082 246.8975 287.6566 168.8565 -0.6904 246.4156 247.1061 287.7930 169.6488 -0.6907 246.5849 247.2756 287.9102 170.4405 -0.6941 246.7626 247.4566 288.0508 171.2625 -0.6959 246.9468 247.6427 288.1973 172.0545 -0.6931 247.1315 247.8246 288.3197 172.8765 -0.6955 247.3263 248.0219 288.4790 173.6688 -0.6980 247.5115 248.2095 288.6372 174.4605 -0.7007 247.6780 248.3787 288.7543 175.2825 -0.7007 247.8634 248.5641 288.8885 176.0745 -0.6986 248.0428 248.7414 289.0296 176.8965 -0.6979 248.2065 248.9045 289.1839 177.6888 -0.7038 248.3918 249.0956 289.3261 178.4815 -0.7019 248.5704 249.2723 289.4463 179.3035 -0.7028 248.7492 249.4520 289.5919 180.0955 -0.7061 248.9308 249.6369 289.7110 180.9175 -0.7122 249.1338 249.8461 289.8758 181.7095 -0.7028 249.3157 250.0185 290.0266 182.5015 -0.6988 249.4761 250.1750 290.1440 183.3235 -0.7064 249.6574 250.3638 290.2873 184.1155 -0.7153 249.8416 250.5569 290.4351 184.9373 -0.7180 250.0311 250.7492 290.5781 185.7295 -0.7178 250.2038 250.9215 290.7116 186.5210 -0.7196 250.3821 251.1018 290.8478 187.3435 -0.7202 250.5429 251.2631 291.0044 188.1048 -0.7201 250.7010 251.4211 291.1241 188.9570 -0.7235 250.8758 251.5993 291.2534 189.7490 -0.7246 251.0621 251.7867 291.4138 190.5405 -0.7274 251.2675 251.9949 291.5530 191.3595 -0.7324 251.4406 252.1730 291.6966 192.1175 -0.7313 251.6048 252.3361 291.8075 192.9660 -0.7350 251.7810 252.5160 291.9686 193.7538 -0.7332 251.9569 252.6902 292.0958 194.5420 -0.7335 252.1253 252.8588 292.2141 195.3603 -0.7355 252.3000 253.0355 292.3713 196.1190 -0.7466 252.4762 253.2229 292.4943 196.9678 -0.7524 252.6717 253.4242 292.6526 197.7570 -0.7442 252.8462 253.5904 292.8015 198.5470 -0.7410 253.0433 253.7842 292.9360 199.3685 -0.7413 253.2002 253.9415 293.0873 200.1295 -0.7397 253.3755 254.1152 293.1975 200.9815 -0.7516 253.5405 254.2922 293.3255 201.7735 -0.7535 253.7090 254.4626 293.4648 202.5655 -0.7577 253.8718 254.6296 293.6280 203.3875 -0.7586 254.0413 254.7999 293.7749 204.1495 -0.7674 254.2140 254.9813 293.8778 205.0015 -0.7669 254.4012 255.1682 294.0207 205.7635 -0.7644 254.5717 255.3361 294.1609 206.5855 -0.7614 254.7667 255.5281 294.2829 207.4075 -0.7675 254.9350 255.7025 294.4498 208.1695 -0.7810 255.0905 255.8715 294.5873 209.0215 -0.7893 255.2975 256.0868 294.7239 209.7835 -0.7758 255.4539 256.2296 294.8607 210.6055 -0.7702 255.6343 256.4045 294.9858 211.4273 -0.7725 255.8063 256.5788 295.1243 212.1890 -0.7738 255.9638 256.7376 295.2584 213.0413 -0.7776 256.1473 256.9249 295.4053 213.8333 -0.7798 256.2937 257.0736 295.5153 214.6245 -0.7804 256.4724 257.2528 295.6661 215.4470 -0.7846 256.6600 257.4446 295.8006 216.2085 -0.7877 256.8186 257.6063 295.9241 217.0610 -0.7879 257.0021 257.7900 296.0476 217.8530 -0.7905 257.1676 257.9580 296.1638 218.6445 -0.7891 257.3577 258.1468 296.2856 219.4670 -0.7895 257.5343 258.3239 296.4039 220.2295 -0.7979 257.6966 258.4945 296.5118 221.0820 -0.8021 257.8738 258.6758 296.6399 221.8740 -0.8028 258.0283 258.8311 296.7581 222.6655 -0.8020 258.1796 258.9816 296.8817 223.4875 -0.8023 258.3542 259.1564 297.0016 224.2748 -0.8069 258.5499 259.3568 297.1126 225.0915 -0.8079 258.7166 259.5245 297.2305 225.8793 -0.8099 258.8790 259.6888 297.3573 226.6670 -0.8117 259.0534 259.8651 297.4723 227.4850 -0.8132 259.2113 260.0245 297.6081 228.2430 -0.8136 259.3757 260.1893 297.7232 229.0923 -0.8153 259.5699 260.3853 297.8497 229.8805 -0.8213 259.7306 260.5519 297.9811 230.6690 -0.8223 259.8974 260.7197 298.0850 231.4883 -0.8207 260.0504 260.8711 298.2001 232.2773 -0.8232 260.2291 261.0523 298.3397 233.0960 -0.8213 260.3880 261.2093 298.4469 233.8863 -0.8286 260.5717 261.4003 298.5716 234.6775 -0.8308 260.7217 261.5526 298.7027 235.5000 -0.8291 260.9117 261.7407 298.8343 236.2615 -0.8336 261.0763 261.9098 298.9767 237.1140 -0.8359 261.2466 262.0825 299.1017 237.9060 -0.8390 261.4068 262.2458 299.2012 238.6975 -0.8405 261.5671 262.4076 299.3536 239.5243 -0.8385 261.7300 262.5684 299.4747 240.2855 -0.8434 261.9140 262.7575 299.6158 241.1380 -0.8459 262.0913 262.9371 299.7481 241.8998 -0.8504 262.2394 263.0898 299.8565 242.7218 -0.8491 262.4185 263.2676 300.0022 243.5140 -0.8511 262.5832 263.4343 300.1087 244.3055 -0.8546 262.7334 263.5880 300.2594 245.1580 -0.8522 262.9112 263.7634 300.3827 245.9200 -0.8546 263.0736 263.9282 300.4951 246.7418 -0.8580 263.2436 264.1017 300.6364 247.5340 -0.8629 263.4202 264.2832 300.7628 248.3265 -0.8632 263.5710 264.4342 300.8967 249.1488 -0.8623 263.7482 264.6105 301.0118 249.9405 -0.8642 263.9035 264.7677 301.1526 250.7635 -0.8644 264.0584 264.9227 301.2973 251.5558 -0.8662 264.2264 265.0926 301.4270 252.3475 -0.8701 264.3797 265.2498 301.5332 253.1698 -0.8709 264.5530 265.4239 301.6773 253.9615 -0.8712 264.7313 265.6025 301.8080 254.7845 -0.8726 264.9218 265.7944 301.9290 255.5765 -0.8732 265.0698 265.9430 302.0613 256.3665 -0.8730 265.2362 266.1093 302.2100 257.2180 -0.8747 265.4163 266.2910 302.3306 257.9803 -0.8733 265.5302 266.4035 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