DTA measure 1Lassu Date: 202534:1143 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1411.87 s Mass = 957.7 mg data_number = 1748 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2795 0.8138 240.7196 239.9058 228.3169 2.0415 0.8112 240.6635 239.8522 228.2625 2.8933 0.8143 240.6035 239.7893 228.2188 3.6853 0.8158 240.5567 239.7410 228.1697 4.4773 0.8134 240.5037 239.6903 228.1196 5.2993 0.8133 240.4661 239.6528 228.0768 6.0605 0.8165 240.4215 239.6050 228.0396 6.9130 0.8201 240.3507 239.5305 227.9855 7.7050 0.8209 240.2914 239.4705 227.9576 8.4975 0.8227 240.2326 239.4099 227.9144 9.3200 0.8229 240.1697 239.3468 227.8978 10.1118 0.8249 240.1225 239.2976 227.8661 10.9345 0.8258 240.0634 239.2376 227.8314 11.7270 0.8265 240.0244 239.1980 227.8110 12.5195 0.8247 239.9808 239.1561 227.8110 13.3433 0.8233 239.9257 239.1024 227.8003 14.1108 0.8238 239.8782 239.0544 227.8096 14.9630 0.8148 239.8119 238.9971 227.8100 15.7548 0.8214 239.7828 238.9614 227.7876 16.5475 0.8219 239.7441 238.9222 227.8138 17.3698 0.8285 239.6872 238.8587 227.8162 18.1615 0.8279 239.6212 238.7933 227.8169 18.9838 0.8301 239.5623 238.7322 227.8538 19.7755 0.8298 239.4952 238.6654 227.8802 20.5675 0.8261 239.4618 238.6357 227.9115 21.3895 0.8168 239.4127 238.5959 227.9261 22.1815 0.8226 239.3662 238.5436 227.9668 23.0035 0.8275 239.3132 238.4858 228.0022 23.7945 0.8217 239.2572 238.4354 228.0439 24.5830 0.8193 239.2098 238.3904 228.0836 25.3993 0.8160 239.1651 238.3491 228.1679 26.1580 0.8169 239.1184 238.3014 228.2282 27.0060 0.8234 239.0742 238.2509 228.3290 27.7940 0.8185 239.0259 238.2074 228.3843 28.5820 0.8143 238.9835 238.1692 228.4455 29.4000 0.8173 238.9549 238.1377 228.5363 30.1580 0.8191 238.9000 238.0809 228.6410 31.0065 0.8257 238.8418 238.0161 228.7190 31.7950 0.8255 238.8045 237.9789 228.8013 32.5840 0.8254 238.7708 237.9454 228.9072 33.4020 0.8257 238.7191 237.8934 229.0067 34.1600 0.8256 238.6647 237.8391 229.1083 35.0093 0.8262 238.6282 237.8021 229.2198 35.7980 0.8226 238.5859 237.7633 229.3137 36.5870 0.8195 238.5531 237.7336 229.4106 37.4055 0.8197 238.5199 237.7002 229.5378 38.1653 0.8174 238.4705 237.6532 229.6349 39.0148 0.8160 238.4109 237.5949 229.7582 39.8055 0.8132 238.3593 237.5460 229.8988 40.5975 0.8110 238.3221 237.5110 230.0054 41.4188 0.8103 238.2757 237.4654 230.1344 42.1800 0.8069 238.2368 237.4299 230.2626 43.0315 0.8026 238.2036 237.4010 230.3972 43.7935 0.7998 238.1624 237.3626 230.5298 44.6155 0.7979 238.1261 237.3283 230.6443 45.4075 0.7965 238.0773 237.2809 230.7729 46.1995 0.7954 238.0377 237.2423 230.9089 47.0515 0.7929 238.0017 237.2088 231.0406 47.8135 0.7889 237.9620 237.1731 231.1750 48.6355 0.7848 237.9473 237.1625 231.2956 49.4275 0.7825 237.8913 237.1087 231.4512 50.2195 0.7830 237.8259 237.0428 231.5728 51.0415 0.7808 237.8200 237.0392 231.7138 51.8333 0.7774 237.7684 236.9911 231.8638 52.6548 0.7751 237.7301 236.9550 231.9924 53.4473 0.7714 237.6929 236.9215 232.1187 54.2385 0.7683 237.6643 236.8959 232.2375 55.0613 0.7675 237.6420 236.8745 232.3677 55.8528 0.7662 237.5926 236.8264 232.4896 56.6748 0.7637 237.5696 236.8059 232.6242 57.4670 0.7603 237.5307 236.7703 232.7505 58.2585 0.7559 237.4975 236.7416 232.8884 59.0810 0.7524 237.4708 236.7184 232.9990 59.8728 0.7499 237.4333 236.6833 233.1394 60.6985 0.7470 237.3998 236.6527 233.2465 61.4718 0.7462 237.3719 236.6258 233.3505 62.2938 0.7429 237.3325 236.5896 233.4761 63.1160 0.7389 237.3185 236.5796 233.6035 63.8775 0.7331 237.2632 236.5301 233.7095 64.7300 0.7343 237.2391 236.5047 233.8311 65.4918 0.7314 237.2307 236.4993 233.9424 66.3168 0.7297 237.2190 236.4893 234.0624 67.1388 0.7281 237.1828 236.4547 234.1757 67.9005 0.7237 237.1479 236.4242 234.2670 68.7528 0.7223 237.1081 236.3858 234.3737 69.5145 0.7182 237.0831 236.3649 234.4821 70.3365 0.7153 237.0503 236.3350 234.5900 71.1585 0.7125 237.0262 236.3138 234.6994 71.9205 0.7065 237.0067 236.3002 234.8022 72.7725 0.7032 236.9951 236.2920 234.9084 73.5645 0.7010 236.9600 236.2590 235.0013 74.3575 0.6984 236.9448 236.2465 235.1085 75.1795 0.6940 236.9214 236.2274 235.2116 75.9415 0.6897 236.8913 236.2016 235.3132 76.7935 0.6863 236.8697 236.1834 235.4150 77.5555 0.6867 236.8696 236.1829 235.4917 78.3775 0.7058 236.8411 236.1353 235.5675 79.1995 0.7073 236.8099 236.1026 235.6833 79.9615 0.6935 236.7911 236.0977 235.7913 80.8140 0.6920 236.7801 236.0881 235.9075 81.6365 0.6849 236.7407 236.0558 235.9719 82.4298 0.6941 236.7455 236.0514 236.0728 83.2553 0.6904 236.7278 236.0375 236.1613 84.0470 0.6844 236.7044 236.0201 236.2446 84.8713 0.6861 236.6865 236.0004 236.3217 85.6935 0.6817 236.6706 235.9889 236.4189 86.4890 0.6724 236.6539 235.9815 236.4925 87.2845 0.6612 236.6280 235.9668 236.5863 88.5855 0.6595 236.6057 235.9462 236.7243 89.3453 0.6571 236.6082 235.9512 236.8223 90.1945 0.6495 236.5844 235.9349 236.9036 90.9843 0.6428 236.5583 235.9155 236.9917 91.7750 0.6416 236.5443 235.9027 237.0566 92.5940 0.6403 236.5350 235.8947 237.1488 93.4130 0.6334 236.5276 235.8942 237.2330 94.2010 0.6261 236.5151 235.8890 237.3176 95.0503 0.6118 236.5021 235.8903 237.4080 95.8083 0.6088 236.4873 235.8785 237.4938 96.6260 0.6153 236.4640 235.8487 237.5779 97.4155 0.6164 236.4577 235.8413 237.6664 98.2070 0.6178 236.4414 235.8236 237.7496 99.0560 0.6125 236.4300 235.8175 237.8308 99.8143 0.6071 236.4089 235.8018 237.8955 100.6335 0.6039 236.4029 235.7990 238.0063 101.4250 0.6052 236.3962 235.7910 238.0901 102.2160 0.6048 236.3894 235.7846 238.1594 103.0660 0.6002 236.4121 235.8119 238.2617 103.8263 0.5953 236.4039 235.8086 238.3448 104.6470 0.5938 236.3808 235.7870 238.4542 105.4358 0.5904 236.3781 235.7878 238.5488 106.2265 0.5869 236.3671 235.7802 238.6150 107.0790 0.5839 236.3574 235.7735 238.7072 107.8408 0.5782 236.3695 235.7913 238.7904 108.6628 0.5741 236.3528 235.7787 238.8877 109.4550 0.5680 236.3351 235.7671 238.9658 110.2465 0.5644 236.3357 235.7713 239.0767 111.0700 0.5636 236.3315 235.7678 239.1628 111.8618 0.5596 236.3416 235.7820 239.2542 112.6838 0.5569 236.3306 235.7737 239.3591 113.4760 0.5556 236.3128 235.7573 239.4499 114.2675 0.5513 236.3029 235.7515 239.5528 115.0898 0.5473 236.3125 235.7652 239.6592 115.8815 0.5451 236.3138 235.7687 239.7410 116.7035 0.5450 236.3059 235.7609 239.8382 117.4955 0.5430 236.2952 235.7522 239.9229 118.2875 0.5428 236.2854 235.7426 240.0125 119.1095 0.5387 236.3038 235.7651 240.1108 119.9015 0.5393 236.3201 235.7808 240.2219 120.7235 0.5335 236.3132 235.7797 240.3375 121.5155 0.5334 236.3172 235.7838 240.4382 122.3075 0.5296 236.3045 235.7749 240.5275 123.1295 0.5281 236.3074 235.7794 240.6088 123.8915 0.5251 236.3068 235.7817 240.6962 124.7435 0.5243 236.2966 235.7723 240.7927 125.5355 0.5238 236.3104 235.7866 240.9056 126.3275 0.5217 236.2977 235.7760 240.9872 127.1495 0.5192 236.3160 235.7968 241.0958 127.9115 0.5176 236.3253 235.8076 241.1978 128.7635 0.5126 236.3376 235.8250 241.2958 129.5555 0.5111 236.3299 235.8189 241.4008 130.3473 0.5117 236.3311 235.8194 241.4880 131.1695 0.5110 236.3464 235.8354 241.5900 131.9313 0.5081 236.3562 235.8480 241.6946 132.7833 0.5103 236.3678 235.8575 241.8104 133.5750 0.5101 236.3611 235.8510 241.9118 134.3665 0.5063 236.3599 235.8537 242.0167 135.1890 0.4996 236.3618 235.8622 242.1048 135.9505 0.4960 236.3815 235.8855 242.2127 136.8030 0.4921 236.3885 235.8964 242.3283 137.5950 0.4888 236.4049 235.9161 242.4320 138.3865 0.4876 236.4123 235.9247 242.5248 139.2090 0.4827 236.4255 235.9428 242.6293 139.9705 0.4791 236.4118 235.9327 242.7329 140.8230 0.4789 236.4108 235.9318 242.8552 141.6148 0.4781 236.4504 235.9723 242.9699 142.4075 0.4759 236.4418 235.9659 243.0764 143.2298 0.4736 236.4622 235.9886 243.1707 144.0218 0.4709 236.4739 236.0029 243.2746 144.8438 0.4713 236.4918 236.0205 243.3808 145.6358 0.4693 236.5226 236.0533 243.4797 146.4285 0.4647 236.5348 236.0701 243.5792 147.2508 0.4613 236.5373 236.0760 243.6965 148.0425 0.4556 236.5320 236.0764 243.8003 148.8663 0.4522 236.5629 236.1106 243.8895 149.6585 0.4524 236.5760 236.1236 244.0051 150.4515 0.4515 236.5907 236.1392 244.0959 151.2738 0.4502 236.5988 236.1486 244.2074 152.0338 0.4469 236.6005 236.1536 244.3141 152.8805 0.4453 236.6236 236.1783 244.4269 153.6700 0.4423 236.6631 236.2208 244.5304 154.4580 0.4385 236.6845 236.2459 244.6449 155.2763 0.4379 236.6861 236.2482 244.7237 156.0340 0.4348 236.7141 236.2793 244.8221 156.8830 0.4316 236.7287 236.2971 244.9451 157.6710 0.4268 236.7354 236.3086 245.0441 158.4590 0.4261 236.7529 236.3268 245.1451 159.2770 0.4248 236.7589 236.3341 245.2521 160.0650 0.4219 236.7834 236.3614 245.3434 160.8838 0.4170 236.8053 236.3884 245.4427 161.6723 0.4165 236.8499 236.4334 245.5464 162.4620 0.4144 236.8613 236.4468 245.6524 163.2805 0.4115 236.8670 236.4555 245.7437 164.0690 0.4105 236.8797 236.4692 245.8326 164.8878 0.4035 236.9037 236.5002 245.9521 165.7063 0.4049 236.9319 236.5270 246.0509 166.4650 0.4022 236.9680 236.5658 246.1371 167.3138 0.3984 236.9710 236.5726 246.2472 168.0748 0.3958 236.9955 236.5997 246.3451 168.8965 0.3927 237.0187 236.6261 246.4446 169.7170 0.3941 237.0306 236.6364 246.5248 170.4783 0.3922 237.0751 236.6829 246.6177 171.3288 0.3886 237.0890 236.7004 246.7247 172.0905 0.3839 237.1296 236.7456 246.8263 172.9125 0.3839 237.1466 236.7626 246.9312 173.7045 0.3822 237.1562 236.7740 247.0340 174.4965 0.3823 237.1866 236.8043 247.1174 175.3485 0.3801 237.2142 236.8341 247.2152 176.1105 0.3767 237.2489 236.8722 247.2957 176.9323 0.3755 237.2736 236.8982 247.3779 177.7245 0.3768 237.3061 236.9293 247.4855 178.5158 0.3746 237.3228 236.9482 247.5769 179.3685 0.3730 237.3601 236.9871 247.6590 180.1305 0.3709 237.3924 237.0215 247.7639 180.9520 0.3669 237.3892 237.0223 247.8720 181.7445 0.3638 237.4220 237.0582 247.9756 182.5355 0.3606 237.4504 237.0897 248.0679 183.3583 0.3597 237.4663 237.1065 248.1705 184.1553 0.3580 237.5172 237.1593 248.2707 184.9768 0.3595 237.5570 237.1975 248.3680 185.7690 0.3569 237.5673 237.2104 248.4715 186.5605 0.3550 237.5939 237.2390 248.5559 187.3830 0.3500 237.6371 237.2871 248.6737 188.1445 0.3480 237.6819 237.3339 248.7565 188.9970 0.3454 237.7201 237.3747 248.8649 189.7890 0.3432 237.7251 237.3819 248.9654 190.5805 0.3404 237.7574 237.4171 249.0612 191.4028 0.3406 237.8120 237.4714 249.1546 192.1645 0.3409 237.8409 237.4999 249.2551 193.0168 0.3354 237.8668 237.5314 249.3576 193.7800 0.3354 237.8809 237.5456 249.4830 194.6055 0.3337 237.9034 237.5698 249.5912 195.3978 0.3320 237.9601 237.6281 249.6821 196.1895 0.3337 237.9848 237.6510 249.7638 197.0418 0.3282 238.0074 237.6792 249.8659 197.8035 0.3285 238.0611 237.7326 249.9768 198.6255 0.3245 238.1065 237.7819 250.0791 199.4175 0.3251 238.1310 237.8059 250.1677 200.2095 0.3197 238.1861 237.8664 250.2482 201.0615 0.3200 238.2156 237.8955 250.3597 201.8235 0.3162 238.2314 237.9152 250.4784 202.6455 0.3164 238.2727 237.9562 250.5913 203.4375 0.3148 238.3026 237.9878 250.6807 204.2295 0.3099 238.3481 238.0382 250.7808 205.0820 0.3087 238.3790 238.0702 250.8874 205.8445 0.3062 238.4174 238.1111 250.9908 206.6665 0.3036 238.4702 238.1666 251.0908 207.4885 0.3032 238.4871 238.1839 251.1949 208.2505 0.3017 238.5444 238.2427 251.2851 209.1025 0.2991 238.5837 238.2845 251.3806 209.8643 0.2969 238.6178 238.3209 251.4797 210.6865 0.2955 238.6680 238.3725 251.5859 211.5080 0.2919 238.7058 238.4139 251.6855 212.2695 0.2907 238.7309 238.4403 251.7715 213.1220 0.2885 238.7756 238.4871 251.8997 213.9143 0.2890 238.8130 238.5240 251.9793 214.7055 0.2837 238.8383 238.5546 252.0700 215.5278 0.2845 238.8742 238.5896 252.1512 216.2860 0.2841 238.9298 238.6457 252.2482 217.1330 0.2787 238.9724 238.6937 252.3663 217.9223 0.2793 239.0177 238.7384 252.4639 218.7103 0.2761 239.0662 238.7901 252.5536 219.5280 0.2741 239.1225 238.8484 252.6554 220.2860 0.2698 239.1440 238.8741 252.7595 221.1343 0.2740 239.2042 238.9302 252.8641 221.9225 0.2709 239.2303 238.9594 252.9801 222.7110 0.2683 239.2718 239.0034 253.0923 223.5298 0.2667 239.3254 239.0587 253.1951 224.2880 0.2614 239.3738 239.1123 253.3004 225.1485 0.2625 239.4106 239.1481 253.4183 225.9083 0.2599 239.4718 239.2119 253.5198 226.7260 0.2589 239.5000 239.2411 253.6179 227.5448 0.2572 239.5357 239.2786 253.7361 228.3040 0.2523 239.5828 239.3306 253.8334 229.1538 0.2521 239.6375 239.3854 253.9690 229.9123 0.2519 239.6710 239.4191 254.0524 230.7328 0.2493 239.7165 239.4672 254.1394 231.5550 0.2461 239.7753 239.5292 254.2698 232.3163 0.2417 239.8133 239.5716 254.3578 233.1700 0.2412 239.8408 239.5996 254.4888 233.9310 0.2394 239.9100 239.6706 254.5862 234.7528 0.2392 239.9687 239.7295 254.7122 235.5463 0.2387 240.0157 239.7770 254.8100 236.3375 0.2382 240.0454 239.8072 254.9104 237.1600 0.2341 240.0994 239.8653 255.0394 237.9215 0.2294 240.1363 239.9069 255.1474 238.7758 0.2259 240.1986 239.9727 255.2731 239.5388 0.2248 240.2420 240.0173 255.3686 240.3608 0.2268 240.2857 240.0589 255.4950 241.1828 0.2232 240.3315 240.1083 255.5926 241.9445 0.2225 240.3952 240.1727 255.6867 242.7970 0.2193 240.4477 240.2285 255.8142 243.5593 0.2174 240.4933 240.2759 255.9049 244.3825 0.2156 240.5475 240.3319 256.0150 245.1778 0.2136 240.5823 240.3687 256.1207 245.9725 0.2115 240.6519 240.4404 256.2295 246.7945 0.2089 240.7271 240.5183 256.3406 247.5865 0.2055 240.7805 240.5749 256.4517 248.4085 0.2039 240.8229 240.6190 256.5703 249.2005 0.2037 240.8643 240.6607 256.6747 249.9925 0.1994 240.9183 240.7189 256.7604 250.8145 0.2005 240.9645 240.7640 256.8734 251.6065 0.2005 241.0363 240.8359 256.9828 252.4285 0.1987 241.0804 240.8816 257.0961 253.2205 0.1978 241.1381 240.9403 257.1934 254.0125 0.1949 241.2045 241.0096 257.2916 254.8345 0.1915 241.2385 241.0470 257.4207 255.6035 0.1875 241.2709 241.0833 257.5390 256.4575 0.1869 241.3530 241.1661 257.6406 257.2195 0.1858 241.4145 241.2287 257.7883 258.0415 0.1849 241.4791 241.2942 257.8571 258.8635 0.1853 241.5246 241.3392 257.9602 259.6253 0.1826 241.5730 241.3904 258.0740 260.4773 0.1832 241.6411 241.4579 258.1700 261.2693 0.1806 241.7026 241.5220 258.2752 262.0610 0.1802 241.7476 241.5674 258.3557 262.8833 0.1787 241.7986 241.6199 258.4709 263.6448 0.1736 241.8393 241.6656 258.5651 264.4970 0.1746 241.9057 241.7311 258.6950 265.2890 0.1774 241.9685 241.7911 258.8033 266.0915 0.1723 242.0449 241.8725 258.8903 266.9140 0.1654 242.0954 241.9299 259.0039 267.6755 0.1637 242.1537 241.9900 259.1196 268.5280 0.1631 242.2243 242.0612 259.2198 269.2898 0.1602 242.2705 242.1103 259.3079 270.1118 0.1619 242.3167 242.1548 259.4023 270.9340 0.1575 242.3818 242.2243 259.5118 271.6955 0.1521 242.4323 242.2802 259.5912 272.5478 0.1542 242.5029 242.3487 259.7045 273.3095 0.1531 242.5624 242.4093 259.8099 274.1318 0.1510 242.6119 242.4609 259.8964 274.9540 0.1482 242.6727 242.5245 259.9951 275.7165 0.1447 242.7330 242.5883 260.0985 276.5693 0.1452 242.8138 242.6686 260.2202 277.3315 0.1426 242.8712 242.7285 260.3143 278.1535 0.1412 242.9214 242.7802 260.4029 278.9758 0.1402 242.9795 242.8394 260.5166 279.7393 0.1365 243.0441 242.9076 260.6111 280.5913 0.1366 243.1055 242.9689 260.7160 281.3498 0.1344 243.1664 243.0320 260.7942 282.1678 0.1329 243.2308 243.0978 260.8965 282.9548 0.1323 243.2967 243.1643 261.0203 283.7440 0.1288 243.3613 243.2325 261.1069 284.5920 0.1288 243.4200 243.2912 261.1981 285.3503 0.1269 243.4834 243.3565 261.2879 286.1690 0.1238 243.5539 243.4301 261.3970 286.9570 0.1264 243.6164 243.4900 261.4948 287.7450 0.1247 243.6888 243.5641 261.5908 288.5935 0.1171 243.7508 243.6338 261.6935 289.3523 0.1151 243.8082 243.6931 261.7786 290.1718 0.1111 243.8579 243.7468 261.8656 290.9610 0.1128 243.9403 243.8275 261.9767 291.7510 0.1100 244.0077 243.8977 262.0731 292.5995 0.1068 244.0657 243.9589 262.1683 293.3580 0.1061 244.1258 244.0197 262.2568 294.1778 0.1065 244.1893 244.0828 262.3570 294.9663 0.1025 244.2624 244.1599 262.4493 295.7560 0.1018 244.3442 244.2425 262.5462 296.6048 0.1027 244.3965 244.2937 262.6275 297.3665 0.1013 244.4636 244.3623 262.7310 298.1880 0.0955 244.5172 244.4217 262.8299 298.9780 0.0925 244.5693 244.4767 262.9101 299.7690 0.0900 244.6418 244.5518 263.0067 300.6205 0.0900 244.7254 244.6353 263.1121 301.3825 0.0888 244.7787 244.6899 263.1930 302.2045 0.0858 244.8584 244.7726 263.2965 302.9965 0.0869 244.9257 244.8388 263.4012 303.7885 0.0829 244.9747 244.8918 263.4972 304.6105 0.0804 245.0582 244.9778 263.6016 305.4025 0.0779 245.1291 245.0512 263.6917 306.2243 0.0782 245.1885 245.1103 263.8056 307.0165 0.0799 245.2748 245.1949 263.8990 307.8080 0.0803 245.3575 245.2772 264.0036 308.6303 0.0770 245.4169 245.3399 264.1076 309.4218 0.0748 245.5002 245.4254 264.2031 310.2440 0.0733 245.5594 245.4861 264.3136 311.0360 0.0708 245.6189 245.5481 264.4274 311.8275 0.0683 245.6788 245.6105 264.5384 312.6503 0.0675 245.7628 245.6953 264.6492 313.4418 0.0663 245.8214 245.7551 264.7342 314.2638 0.0621 245.8843 245.8222 264.8590 315.0560 0.0631 245.9538 245.8906 264.9588 315.8475 0.0605 246.0248 245.9643 265.0686 316.6700 0.0585 246.1004 246.0419 265.1735 317.4618 0.0574 246.1684 246.1110 265.2769 318.2838 0.0566 246.2419 246.1854 265.4031 319.0758 0.0573 246.3187 246.2614 265.5019 319.8675 0.0568 246.3975 246.3407 265.5927 320.6900 0.0529 246.4729 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