DTA measure 1lassufelle Date: 2026317:1627 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.74 s Mass = 1165.700 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4953 0.0496 234.4334 234.3838 214.7909 4.0846 0.0516 234.4284 234.3768 214.9223 5.6894 0.0487 234.4024 234.3537 215.0567 7.2935 0.0500 234.4083 234.3583 215.1560 8.8825 0.0479 234.3944 234.3465 215.2804 10.5078 0.0453 234.3584 234.3131 215.4282 12.1074 0.0445 234.3368 234.2923 215.6099 13.7173 0.0412 234.3246 234.2834 215.8183 15.3214 0.0375 234.3137 234.2762 216.0384 16.9258 0.0336 234.2619 234.2283 216.2762 18.5356 0.0254 234.1791 234.1537 216.5300 20.1404 0.0186 234.1531 234.1345 216.8081 21.7503 0.0131 234.1059 234.0928 217.0634 23.3548 0.0074 234.0964 234.0890 217.3619 24.9690 -0.0006 234.0914 234.0920 217.6389 26.5738 -0.0093 234.0705 234.0797 217.9064 28.1836 -0.0145 234.0559 234.0704 218.1484 29.7884 -0.0198 234.0367 234.0565 218.4439 31.4028 -0.0295 234.0180 234.0475 218.6907 33.0071 -0.0359 234.0107 234.0466 218.9038 34.6273 -0.0432 233.9966 234.0398 219.1222 36.2320 -0.0488 233.9648 234.0135 219.3476 37.8308 -0.0549 233.9476 234.0025 219.5577 39.4303 -0.0665 233.9407 234.0072 219.7866 41.0401 -0.0738 233.9465 234.0203 219.9777 42.6446 -0.0831 233.9397 234.0228 220.1871 44.2486 -0.0928 233.9224 234.0152 220.3333 45.8431 -0.1000 233.9258 234.0258 220.4864 47.4479 -0.1056 233.8643 233.9700 220.6060 49.0578 -0.1123 233.8451 233.9574 220.7554 50.6773 -0.1236 233.8852 234.0087 220.8583 52.2816 -0.1353 233.9004 234.0356 220.9790 53.8915 -0.1404 233.8784 234.0188 221.1624 55.4963 -0.1499 233.8638 234.0137 221.3641 57.1058 -0.1583 233.8191 233.9774 221.5540 58.7099 -0.1614 233.8199 233.9814 221.7294 60.3198 -0.1651 233.7952 233.9603 221.8734 61.9399 -0.1738 233.7877 233.9615 222.1098 63.5488 -0.1830 233.7940 233.9770 222.3538 65.1638 -0.1919 233.7997 233.9916 222.6178 66.7685 -0.1968 233.7576 233.9544 222.8435 68.3681 -0.2035 233.7486 233.9521 223.0796 69.9565 -0.2108 233.7609 233.9717 223.3525 71.5561 -0.2169 233.7789 233.9959 223.6270 73.1609 -0.2273 233.8205 234.0478 223.9086 74.7810 -0.2366 233.8351 234.0717 224.1764 76.3906 -0.2423 233.7921 234.0344 224.4242 77.9946 -0.2501 233.7582 234.0084 224.6938 79.5994 -0.2594 233.7832 234.0427 224.9285 81.1939 -0.2665 233.8469 234.1134 225.1287 82.7986 -0.2727 233.8444 234.1171 225.3410 84.4080 -0.2730 233.8663 234.1393 225.5293 86.0123 -0.2771 233.8764 234.1536 225.7090 87.6375 -0.2814 233.8950 234.1763 225.8744 89.2423 -0.2842 233.9413 234.2255 226.0148 90.8465 -0.2908 233.9436 234.2344 226.1721 92.4559 -0.3017 233.9516 234.2532 226.3390 94.0606 -0.3075 233.9869 234.2944 226.5127 95.6705 -0.3127 234.0177 234.3304 226.6558 97.2748 -0.3166 234.0644 234.3809 226.8082 98.8944 -0.3201 234.0792 234.3993 226.9780 100.4838 -0.3250 234.0914 234.4164 227.1680 102.0833 -0.3286 234.1157 234.4443 227.3703 103.6923 -0.3325 234.1195 234.4520 227.5471 105.2970 -0.3388 234.1571 234.4959 227.7682 106.8864 -0.3484 234.1942 234.5426 228.0148 108.4909 -0.3607 234.2401 234.6009 228.2583 110.0949 -0.3618 234.2897 234.6515 228.4956 111.7048 -0.3626 234.3107 234.6733 228.7383 113.3249 -0.3639 234.3543 234.7182 228.9526 114.9290 -0.3642 234.3987 234.7630 229.2337 116.5385 -0.3696 234.4421 234.8117 229.4753 118.1433 -0.3757 234.5007 234.8763 229.7454 119.7529 -0.3790 234.5511 234.9301 229.9893 121.3569 -0.3783 234.5597 234.9380 230.2087 122.9719 -0.3805 234.6025 234.9831 230.4188 124.5765 -0.3882 234.6538 235.0420 230.6125 126.1855 -0.3903 234.6974 235.0877 230.8284 127.7903 -0.3928 234.7970 235.1898 231.0242 129.4001 -0.3949 234.8838 235.2788 231.2355 131.0045 -0.3975 234.9404 235.3379 231.4760 132.6035 -0.3985 234.9672 235.3657 231.6714 134.2083 -0.4052 235.0150 235.4202 231.8954 135.8130 -0.4086 235.1129 235.5215 232.0801 137.3965 -0.4144 235.1727 235.5871 232.2421 139.0164 -0.4139 235.2352 235.6491 232.4093 140.6211 -0.4176 235.2801 235.6977 232.6006 142.2259 -0.4211 235.3563 235.7774 232.8104 143.8348 -0.4195 235.4340 235.8535 233.0276 145.4395 -0.4213 235.4894 235.9106 233.2270 147.0494 -0.4195 235.5076 235.9272 233.4355 148.6539 -0.4242 235.5823 236.0066 233.6088 150.2733 -0.4233 235.6683 236.0916 233.7637 151.8831 -0.4234 235.7520 236.1754 233.9422 153.4879 -0.4234 235.8458 236.2692 234.1780 155.0978 -0.4215 235.9201 236.3416 234.3848 156.7024 -0.4217 236.0009 236.4226 234.6020 158.3114 -0.4202 236.0849 236.5051 234.8087 159.9161 -0.4209 236.1541 236.5751 235.0422 161.5363 -0.4221 236.2538 236.6758 235.2557 163.1456 -0.4235 236.3432 236.7667 235.5202 164.7499 -0.4276 236.4113 236.8388 235.7443 166.3495 -0.4318 236.4967 236.9285 235.9932 167.9389 -0.4348 236.5629 236.9976 236.2240 169.5385 -0.4345 236.6619 237.0964 236.4232 171.1478 -0.4390 236.7508 237.1898 236.6275 172.7521 -0.4380 236.8322 237.2702 236.8075 174.3723 -0.4374 236.9195 237.3569 237.0047 175.9821 -0.4403 237.0388 237.4791 237.2226 177.5869 -0.4428 237.1655 237.6084 237.4446 179.1960 -0.4395 237.2343 237.6737 237.6501 180.7851 -0.4421 237.3259 237.7680 237.8818 182.3950 -0.4418 237.4244 237.8663 238.1008 184.0048 -0.4385 237.5493 237.9878 238.3170 185.6138 -0.4372 237.6609 238.0981 238.5222 187.2339 -0.4367 237.7787 238.2154 238.7340 188.8386 -0.4318 237.8703 238.3021 238.9264 190.4484 -0.4310 237.9560 238.3870 239.1158 192.0369 -0.4308 238.0760 238.5068 239.3142 193.6468 -0.4309 238.1639 238.5948 239.5264 195.2515 -0.4304 238.2715 238.7019 239.7481 196.8561 -0.4329 238.3833 238.8163 239.9616 198.4549 -0.4337 238.4962 238.9299 240.1476 200.0699 -0.4360 238.5799 239.0159 240.3614 201.6746 -0.4359 238.7006 239.1364 240.5889 203.2691 -0.4338 238.8233 239.2571 240.7617 204.8730 -0.4350 238.9523 239.3874 240.9315 206.4776 -0.4327 239.1198 239.5525 241.1166 208.0824 -0.4293 239.2310 239.6603 241.3207 209.6864 -0.4285 239.3643 239.7928 241.5003 211.2960 -0.4298 239.4611 239.8909 241.7332 212.9161 -0.4312 239.6051 240.0362 241.9643 214.5158 -0.4302 239.7175 240.1477 242.2076 216.1199 -0.4254 239.8013 240.2267 242.4692 217.7191 -0.4190 239.9424 240.3613 242.7022 219.3341 -0.4198 240.0803 240.5001 242.9379 220.9389 -0.4198 240.2141 240.6339 243.1827 222.5479 -0.4164 240.3173 240.7337 243.4027 224.1525 -0.4143 240.4660 240.8803 243.6709 225.7624 -0.4112 240.6230 241.0342 243.8904 227.3723 -0.4151 240.7408 241.1559 244.1041 228.9664 -0.4143 240.8745 241.2889 244.3062 230.5654 -0.4164 241.0085 241.4249 244.5181 232.1906 -0.4192 241.1485 241.5677 244.6769 233.7954 -0.4162 241.2852 241.7015 244.8677 235.3943 -0.4157 241.4319 241.8476 245.0465 237.0039 -0.4136 241.5731 241.9866 245.2013 238.6086 -0.4113 241.6809 242.0922 245.3487 240.2031 -0.4139 241.7831 242.1971 245.5226 241.8075 -0.4103 241.9272 242.3375 245.7229 243.4168 -0.4063 242.0899 242.4962 245.9346 245.0369 -0.4088 242.2304 242.6393 246.1246 246.6416 -0.4086 242.3270 242.7356 246.3189 248.2514 -0.4071 242.4556 242.8628 246.5418 249.8553 -0.4024 242.6782 243.0806 246.7825 251.4651 -0.3997 242.8374 243.2371 246.9848 253.0699 -0.3942 242.9650 243.3592 247.2272 254.6798 -0.3959 243.1180 243.5139 247.4853 256.2999 -0.3971 243.2618 243.6589 247.7390 257.9088 -0.3975 243.4373 243.8348 247.9906 259.5186 -0.3959 243.6339 244.0297 248.2372 261.1183 -0.4012 243.7435 244.1447 248.4671 262.7281 -0.4016 243.8998 244.3015 248.7308 264.3269 -0.3979 244.0339 244.4318 248.9867 265.9110 -0.3980 244.1636 244.5615 249.1914 267.5209 -0.4009 244.2960 244.6969 249.4081 269.1401 -0.4016 244.5034 244.9051 249.6218 270.7448 -0.3999 244.6592 245.0591 249.8297 272.3495 -0.3959 244.8414 245.2373 250.0334 273.9539 -0.3951 244.9770 245.3721 250.2368 275.5631 -0.3941 245.1049 245.4990 250.4157 277.1679 -0.3951 245.2855 245.6807 250.5726 278.7624 -0.3920 245.4530 245.8450 250.7304 280.3661 -0.3871 245.6305 246.0176 250.9674 281.9863 -0.3858 245.7953 246.1811 251.1266 283.5961 -0.3816 245.9797 246.3613 251.2866 285.2009 -0.3805 246.1331 246.5136 251.4558 286.8103 -0.3794 246.2816 246.6609 251.6643 288.4145 -0.3769 246.4613 246.8382 251.9052 290.0244 -0.3793 246.6492 247.0285 252.1380 291.6291 -0.3796 246.8463 247.2259 252.3356 293.2435 -0.3731 247.0213 247.3945 252.5463 294.8376 -0.3763 247.2206 247.5969 252.7513 296.4373 -0.3755 247.3656 247.7410 252.9865 298.0369 -0.3782 247.4942 247.8724 253.2015 299.6310 -0.3754 247.6614 248.0368 253.4348 301.2403 -0.3754 247.8216 248.1969 253.6543 302.8501 -0.3728 248.0292 248.4020 253.8942 304.4549 -0.3752 248.1979 248.5731 254.1458 306.0494 -0.3767 248.3579 248.7347 254.3656 307.6541 -0.3726 248.5352 248.9078 254.5856 309.2735 -0.3718 248.6700 249.0418 254.8336 310.8831 -0.3710 248.8327 249.2037 255.0634 312.4879 -0.3765 249.0082 249.3847 255.2607 314.0975 -0.3764 249.2104 249.5868 255.4358 315.7015 -0.3736 249.4438 249.8174 255.6604 317.3114 -0.3755 249.6069 249.9824 255.9035 318.9161 -0.3735 249.7717 250.1452 256.1093 320.5158 -0.3748 249.9452 250.3200 256.2740 322.1350 -0.3740 250.1091 250.4831 256.4962 323.7396 -0.3760 250.2898 250.6658 256.7113 325.3444 -0.3731 250.5106 250.8837 256.9345 326.9439 -0.3792 250.6835 251.0627 257.1385 328.5426 -0.3841 250.8658 251.2499 257.3059 330.1525 -0.3864 251.0361 251.4225 257.4797 331.7521 -0.3835 251.2247 251.6082 257.6262 333.3719 -0.3794 251.4088 251.7882 257.8355 334.9709 -0.3755 251.5576 251.9332 258.0295 336.5705 -0.3769 251.7389 252.1158 258.2133 338.1804 -0.3794 251.9382 252.3175 258.3841 339.7851 -0.3803 252.1235 252.5038 258.5921 341.3948 -0.3834 252.3124 252.6957 258.8394 342.9988 -0.3841 252.5171 252.9013 259.0530 344.6035 -0.3825 252.7146 253.0971 259.3076 346.2288 -0.3837 252.8805 253.2642 259.5291 347.8334 -0.3824 253.0696 253.4520 259.7843 349.4425 -0.3850 253.2615 253.6466 260.0161 351.0471 -0.3845 253.4611 253.8456 260.2612 352.6621 -0.3845 253.6981 254.0826 260.4897 354.2664 -0.3830 253.8853 254.2684 260.7297 355.8706 -0.3855 254.0405 254.4260 260.9990 357.4908 -0.3796 254.2011 254.5807 261.2248 359.0903 -0.3822 254.3789 254.7610 261.4625 360.6941 -0.3869 254.5869 254.9739 261.7110 362.3040 -0.3921 254.7991 255.1912 261.9406 363.8875 -0.3938 254.9866 255.3803 262.0920 365.4971 -0.3956 255.1810 255.5766 262.2747 367.1019 -0.3987 255.3576 255.7563 262.4709 368.7118 -0.3954 255.5565 255.9519 262.6446 370.3314 -0.3943 255.7761 256.1704 262.8355 371.9356 -0.3971 255.9799 256.3770 263.0448 373.5455 -0.3990 256.1829 256.5819 263.2230 375.1503 -0.4005 256.4019 256.8023 263.4243 376.7593 -0.4060 256.6170 257.0230 263.6196 378.3639 -0.4052 256.7822 257.1874 263.8010 379.9738 -0.4006 256.9602 257.3608 263.9608 381.5939 -0.3973 257.1136 257.5108 264.1395 383.1981 -0.3984 257.3036 257.7020 264.3503 384.8075 -0.4030 257.5206 257.9236 264.5373 386.4123 -0.4017 257.7541 258.1558 264.7559 388.0221 -0.4050 257.9670 258.3720 264.9724 389.6265 -0.4076 258.1646 258.5722 265.1957 391.2306 -0.4111 258.3374 258.7485 265.4147 392.8149 -0.4116 258.5384 258.9500 265.6495 394.4350 -0.4141 258.7327 259.1468 265.8701 396.0340 -0.4134 258.9533 259.3667 266.1321 397.6435 -0.4129 259.1748 259.5877 266.3519 399.2329 -0.4131 259.4190 259.8320 266.5845 400.8428 -0.4164 259.6152 260.0316 266.8518 402.4475 -0.4162 259.8245 260.2407 267.0677 404.0564 -0.4216 260.0280 260.4495 267.3073 405.6611 -0.4236 260.2382 260.6618 267.5301 407.2813 -0.4220 260.4139 260.8359 267.7429 408.8911 -0.4201 260.6288 261.0489 267.9728 410.4959 -0.4224 260.8450 261.2674 268.2017 412.1050 -0.4214 261.0309 261.4523 268.4108 413.7095 -0.4210 261.2399 261.6609 268.6224 415.3194 -0.4232 261.4128 261.8360 268.8228 416.9241 -0.4245 261.6046 262.0291 269.0197 418.5441 -0.4294 261.8342 262.2636 269.2105 420.1531 -0.4331 262.0649 262.4980 269.3601 421.7579 -0.4371 262.2528 262.6898 269.5592 423.3421 -0.4371 262.4601 262.8971 269.7566 424.9463 -0.4366 262.6718 263.1084 269.9403 426.5455 -0.4403 262.8693 263.3097 270.1361 428.1554 -0.4439 263.0758 263.5197 270.3107 429.7591 -0.4459 263.3131 263.7591 270.5097 431.3793 -0.4460 263.5382 263.9841 270.7108 432.9840 -0.4416 263.7403 264.1819 270.9305 434.5888 -0.4440 263.9818 264.4258 271.1432 436.1986 -0.4472 264.2172 264.6644 271.4071 437.8030 -0.4520 264.4451 264.8970 271.7039 439.4071 -0.4537 264.6439 265.0976 271.9500 441.0170 -0.4601 264.8911 265.3513 272.2253 442.6371 -0.4610 265.0890 265.5500 272.4851 444.2470 -0.4624 265.2764 265.7389 272.6984 445.8508 -0.4661 265.4660 265.9321 272.9506 447.4606 -0.4664 265.6791 266.1455 273.1803 449.0654 -0.4676 265.9120 266.3795 273.3792 450.6753 -0.4718 266.1512 266.6230 273.5928 452.2850 -0.4653 266.3588 266.8241 273.7352 453.8991 -0.4713 266.5733 267.0446 273.9065 455.5039 -0.4724 266.7565 267.2289 274.0556 457.1035 -0.4731 266.9635 267.4366 274.2033 458.7083 -0.4740 267.1483 267.6223 274.3911 460.3171 -0.4737 267.3378 267.8115 274.5833 461.9219 -0.4733 267.5451 268.0185 274.7700 463.5164 -0.4774 267.7674 268.2448 274.9432 465.1209 -0.4818 267.9884 268.4702 275.1272 466.7403 -0.4871 268.2338 268.7210 275.2936 468.3501 -0.4909 268.4690 268.9599 275.5411 469.9549 -0.4948 268.7079 269.2027 275.7662 471.5645 -0.4939 268.9316 269.4255 276.0254 473.1685 -0.4978 269.1195 269.6173 276.3173 474.7784 -0.4957 269.3451 269.8408 276.5862 476.3831 -0.4960 269.5525 270.0485 276.8184 478.0033 -0.4970 269.7685 270.2655 277.0494 479.6131 -0.5030 269.9959 270.4988 277.2835 481.2169 -0.5068 270.2054 270.7122 277.5505 482.8268 -0.5122 270.4357 270.9479 277.8035 484.4418 -0.5172 270.6547 271.1719 278.0742 486.0464 -0.5172 270.8413 271.3585 278.3156 487.6451 -0.5212 271.0682 271.5894 278.5044 489.2601 -0.5252 271.3076 271.8328 278.6765 490.8700 -0.5335 271.5414 272.0749 278.8780 492.4696 -0.5376 271.7457 272.2833 279.0838 494.0734 -0.5465 271.9775 272.5240 279.2501 495.6833 -0.5465 272.2258 272.7723 279.3939 497.2880 -0.5522 272.4302 272.9823 279.5586 498.8979 -0.5533 272.6555 273.2088 279.7142 500.5178 -0.5547 272.8763 273.4310 279.8552 502.1269 -0.5630 273.0787 273.6417 280.0444 503.7316 -0.5674 273.3303 273.8976 280.2215 505.3364 -0.5717 273.5473 274.1190 280.4064 506.9460 -0.5686 273.7417 274.3103 280.6191 508.5500 -0.5662 273.9741 274.5404 280.8190 510.1599 -0.5635 274.2099 274.7733 281.0594 511.7851 -0.5620 274.4183 274.9803 281.3107 513.3944 -0.5682 274.6558 275.2240 281.5390 514.9988 -0.5751 274.8930 275.4680 281.8078 516.6086 -0.5763 275.1101 275.6864 282.0572 518.2083 -0.5828 275.3051 275.8879 282.3205 519.8079 -0.5945 275.5219 276.1164 282.5659 521.4119 -0.5960 275.7502 276.3462 282.8271 523.0318 -0.5948 275.9843 276.5791 283.0835 524.6314 -0.5935 276.2141 276.8076 283.3156 526.2259 -0.5927 276.4146 277.0073 283.5221 527.8298 -0.5990 276.6187 277.2177 283.7212 529.4344 -0.6042 276.8443 277.4485 283.9589 531.0443 -0.6095 277.0971 277.7066 284.1632 532.6490 -0.6198 277.3285 277.9484 284.3484 534.2583 -0.6226 277.5770 278.1996 284.5523 535.8780 -0.6234 277.8096 278.4330 284.7620 537.4879 -0.6234 278.0052 278.6286 284.9168 539.0926 -0.6282 278.2402 278.8684 285.0751 540.6968 -0.6345 278.4921 279.1266 285.2739 542.3063 -0.6371 278.6835 279.3206 285.4533 543.9110 -0.6397 278.8789 279.5186 285.6365 545.5209 -0.6439 279.1733 279.8172 285.8388 547.1410 -0.6467 279.4327 280.0794 286.0251 548.7509 -0.6489 279.6672 280.3161 286.2327 550.3598 -0.6501 279.8899 280.5401 286.4456 551.9543 -0.6556 280.0968 280.7523 286.6333 553.5488 -0.6589 280.3257 280.9846 286.8562 555.1535 -0.6624 280.5729 281.2353 287.0938 556.7470 -0.6669 280.7832 281.4501 287.3193 558.3569 -0.6733 281.0159 281.6892 287.5414 559.9770 -0.6798 281.2220 281.9018 287.8003 561.5864 -0.6860 281.4507 282.1368 288.0581 563.1906 -0.6935 281.6926 282.3862 288.3076 564.7954 -0.7013 281.9284 282.6297 288.5675 566.4053 -0.7018 282.1566 282.8585 288.8011 568.0091 -0.7059 282.3788 283.0847 289.0281 569.6189 -0.7094 282.6106 283.3200 289.2662 571.2390 -0.7156 282.8219 283.5374 289.4877 572.8489 -0.7111 283.0285 283.7396 289.6886 574.4536 -0.7175 283.2728 283.9903 289.8728 576.0574 -0.7254 283.4987 284.2241 290.0671 577.6724 -0.7282 283.7751 284.5033 290.2430 579.2771 -0.7316 284.0504 284.7820 290.4160 580.8716 -0.7331 284.2895 285.0226 290.5881 582.4760 -0.7350 284.5158 285.2508 290.7902 584.0904 -0.7375 284.7345 285.4719 290.9533 585.6951 -0.7427 284.9713 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