DTA measure 1felle2 Date: 2025917:1010 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1724.26 s Mass = 100.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4215 -0.8402 228.4840 229.3242 215.4025 4.0309 -0.8381 228.4980 229.3361 215.4143 5.6300 -0.8368 228.5385 229.3753 215.3508 7.2450 -0.8331 228.5055 229.3386 215.3064 8.8334 -0.8333 228.4656 229.2988 215.1881 10.4381 -0.8348 228.4550 229.2898 215.0613 12.0429 -0.8356 228.4580 229.2935 214.9981 13.6365 -0.8344 228.4813 229.3157 215.0098 15.2360 -0.8331 228.4937 229.3268 215.0479 16.8408 -0.8307 228.4948 229.3255 215.0907 18.4445 -0.8288 228.5144 229.3432 215.1627 20.0493 -0.8281 228.4793 229.3074 215.3505 21.6585 -0.8298 228.4948 229.3246 215.5928 23.2629 -0.8268 228.4584 229.2852 215.8466 24.8675 -0.8324 228.4097 229.2422 216.1492 26.4765 -0.8318 228.3954 229.2273 216.5307 28.0813 -0.8344 228.3912 229.2256 216.9410 29.6910 -0.8439 228.3985 229.2424 217.3465 31.2949 -0.8554 228.4379 229.2933 217.8214 32.9048 -0.8564 228.4067 229.2631 218.3123 34.4940 -0.8627 228.3991 229.2618 218.7194 36.1133 -0.8635 228.3900 229.2535 219.0967 37.7231 -0.8661 228.4052 229.2713 219.4237 39.3330 -0.8686 228.4268 229.2955 219.7486 40.9419 -0.8725 228.4118 229.2843 219.9863 42.5466 -0.8793 228.3862 229.2655 220.1846 44.1564 -0.8864 228.4158 229.3023 220.3609 45.7603 -0.8900 228.4592 229.3492 220.4864 47.3855 -0.8956 228.5015 229.3971 220.5958 48.9900 -0.9014 228.5277 229.4291 220.6736 50.5940 -0.9003 228.5323 229.4326 220.7541 52.2039 -0.9077 228.4966 229.4043 220.7918 53.8078 -0.9117 228.4577 229.3694 220.8183 55.4175 -0.9140 228.4585 229.3726 220.8971 57.0221 -0.9170 228.4694 229.3864 220.9428 58.6465 -0.9165 228.5276 229.4441 220.9520 60.2564 -0.9283 228.5588 229.4871 221.0328 61.8658 -0.9311 228.5436 229.4747 221.1579 63.4700 -0.9344 228.5535 229.4878 221.2925 65.0746 -0.9357 228.5336 229.4693 221.5186 66.6836 -0.9420 228.5459 229.4879 221.7391 68.2935 -0.9473 228.5801 229.5273 221.9882 69.9186 -0.9556 228.6059 229.5615 222.2536 71.5020 -0.9623 228.6601 229.6224 222.5698 73.1016 -0.9656 228.7212 229.6869 222.9221 74.7061 -0.9740 228.7114 229.6854 223.2750 76.3050 -0.9833 228.7112 229.6945 223.6445 77.9046 -0.9900 228.7407 229.7307 224.0376 79.5090 -0.9941 228.7769 229.7710 224.3934 81.1183 -0.9950 228.8093 229.8042 224.7338 82.7330 -0.9954 228.8177 229.8131 225.0740 84.3268 -1.0011 228.8642 229.8652 225.3806 85.9315 -1.0092 228.9210 229.9302 225.6229 87.5408 -1.0105 228.9779 229.9884 225.8205 89.1451 -1.0132 229.0204 230.0336 225.9640 90.7550 -1.0173 229.0600 230.0773 226.0696 92.3589 -1.0248 229.0468 230.0716 226.2169 93.9481 -1.0279 229.1000 230.1279 226.3101 95.5575 -1.0318 229.1521 230.1840 226.4082 97.1771 -1.0350 229.1731 230.2081 226.4665 98.7869 -1.0408 229.2579 230.2987 226.5296 100.3908 -1.0462 229.3346 230.3809 226.6046 102.0006 -1.0423 229.3792 230.4215 226.7131 103.5900 -1.0498 229.4987 230.5485 226.8141 105.1938 -1.0482 229.5343 230.5824 226.9422 106.8036 -1.0497 229.5723 230.6220 227.0880 108.4084 -1.0488 229.6260 230.6749 227.2731 110.0333 -1.0488 229.6368 230.6856 227.4485 111.6374 -1.0535 229.6855 230.7391 227.6949 113.2473 -1.0564 229.7384 230.7948 227.9743 114.8520 -1.0572 229.8385 230.8956 228.3024 116.4564 -1.0652 229.9076 230.9728 228.6232 118.0656 -1.0726 229.9627 231.0353 228.9480 119.6704 -1.0754 230.0523 231.1277 229.1806 121.2954 -1.0791 230.1453 231.2244 229.5341 122.8840 -1.0849 230.1427 231.2276 229.8424 124.4990 -1.0899 230.1559 231.2458 230.1851 126.1028 -1.0925 230.2328 231.3253 230.4917 127.7126 -1.1009 230.3184 231.4193 230.8036 129.3221 -1.1005 230.4228 231.5233 231.0587 130.9314 -1.1014 230.4693 231.5707 231.2788 132.5361 -1.1025 230.5273 231.6298 231.4942 134.1554 -1.1082 230.5662 231.6744 231.6449 135.7600 -1.1077 230.6159 231.7236 231.7582 137.3390 -1.1136 230.7162 231.8298 231.8741 138.9429 -1.1157 230.8121 231.9279 231.9559 140.5528 -1.1175 230.9362 232.0537 232.0817 142.1573 -1.1213 231.0398 232.1611 232.2052 143.7459 -1.1229 231.0942 232.2172 232.3363 145.3506 -1.1208 231.1557 232.2765 232.3910 146.9550 -1.1174 231.2485 232.3659 232.5104 148.5745 -1.1185 231.3741 232.4926 232.6393 150.1791 -1.1203 231.4466 232.5669 232.8290 151.7881 -1.1230 231.5290 232.6520 233.0324 153.3929 -1.1316 231.6284 232.7599 233.2308 155.0028 -1.1376 231.7118 232.8494 233.5247 156.6065 -1.1418 231.7756 232.9174 233.7835 158.2164 -1.1418 231.8743 233.0161 234.0637 159.8206 -1.1350 231.9994 233.1344 234.3751 161.4403 -1.1417 232.0986 233.2403 234.7041 163.0501 -1.1435 232.1961 233.3396 234.9834 164.6540 -1.1413 232.2915 233.4327 235.2828 166.2535 -1.1399 232.3878 233.5278 235.6106 167.8580 -1.1432 232.4482 233.5913 235.8776 169.4671 -1.1468 232.5167 233.6634 236.1550 171.0719 -1.1534 232.6883 233.8417 236.4328 172.6964 -1.1545 232.8226 233.9771 236.6343 174.3163 -1.1535 232.9298 234.0833 236.8207 175.9210 -1.1544 233.0422 234.1966 237.0193 177.5300 -1.1596 233.1383 234.2979 237.1983 179.1346 -1.1622 233.2505 234.4126 237.3476 180.7440 -1.1633 233.3679 234.5313 237.4594 182.3483 -1.1597 233.4767 234.6364 237.5475 183.9735 -1.1545 233.5684 234.7228 237.6619 185.5781 -1.1501 233.6614 234.8115 237.7966 187.1820 -1.1466 233.7578 234.9044 237.9047 188.7970 -1.1513 233.8284 234.9796 237.9929 190.4013 -1.1522 233.9428 235.0950 238.1620 192.0106 -1.1527 234.0601 235.2129 238.3154 193.6154 -1.1553 234.1913 235.3465 238.4620 195.2400 -1.1529 234.3025 235.4554 238.7568 196.8444 -1.1510 234.4449 235.5958 239.0243 198.4338 -1.1489 234.5469 235.6958 239.3196 200.0376 -1.1515 234.6683 235.8198 239.6103 201.6371 -1.1512 234.7518 235.9029 239.9166 203.2368 -1.1489 234.8580 236.0069 240.2472 204.8406 -1.1515 234.9787 236.1302 240.5647 206.4299 -1.1515 235.1248 236.2763 240.8326 208.0395 -1.1490 235.2734 236.4224 241.0988 209.6538 -1.1517 235.4296 236.5813 241.3964 211.2585 -1.1580 235.5678 236.7257 241.6515 212.8631 -1.1592 235.7084 236.8676 241.8685 214.4516 -1.1624 235.8546 237.0169 242.0668 216.0564 -1.1648 235.9748 237.1396 242.2692 217.6653 -1.1679 236.0746 237.2426 242.4823 219.2649 -1.1709 236.2242 237.3951 242.6465 220.8745 -1.1690 236.3456 237.5146 242.8146 222.4939 -1.1650 236.4864 237.6514 242.9414 224.0986 -1.1625 236.6809 237.8434 243.0673 225.7079 -1.1648 236.8295 237.9943 243.1439 227.3123 -1.1653 236.9578 238.1231 243.2051 228.9068 -1.1636 237.0630 238.2266 243.3389 230.5105 -1.1593 237.1754 238.3347 243.4812 232.1204 -1.1572 237.2656 238.4229 243.6362 233.7296 -1.1614 237.3910 238.5524 243.8738 235.3545 -1.1619 237.5572 238.7190 244.0795 236.9593 -1.1589 237.7016 238.8606 244.2836 238.5686 -1.1531 237.8618 239.0149 244.5196 240.1780 -1.1486 238.0184 239.1670 244.7788 241.7828 -1.1473 238.1716 239.3189 245.0359 243.3926 -1.1508 238.3420 239.4927 245.3133 244.9810 -1.1520 238.4996 239.6516 245.6736 246.6063 -1.1503 238.6486 239.7989 246.0351 248.2103 -1.1486 238.8248 239.9734 246.3756 249.8199 -1.1447 238.9791 240.1238 246.6598 251.4298 -1.1487 239.1462 240.2948 246.9409 253.0388 -1.1431 239.2720 240.4150 247.2132 254.6434 -1.1394 239.4205 240.5599 247.4492 256.2579 -1.1404 239.5523 240.6927 247.6519 257.8621 -1.1483 239.6993 240.8476 247.8274 259.4874 -1.1477 239.8679 241.0156 247.9874 261.0968 -1.1498 240.0338 241.1836 248.1254 262.6959 -1.1549 240.1805 241.3354 248.2885 264.3006 -1.1539 240.3097 241.4636 248.4008 265.8840 -1.1483 240.4742 241.6225 248.5268 267.4835 -1.1427 240.6457 241.7884 248.6662 269.0934 -1.1425 240.7736 241.9161 248.8085 270.6923 -1.1485 240.9248 242.0733 248.9390 272.3121 -1.1480 241.1427 242.2907 249.0793 273.9169 -1.1457 241.3283 242.4740 249.2135 275.5209 -1.1443 241.4996 242.6439 249.3810 277.1203 -1.1445 241.6076 242.7522 249.5198 278.7298 -1.1444 241.7017 242.8461 249.7446 280.3236 -1.1463 241.8800 243.0262 250.0220 281.9335 -1.1467 242.0415 243.1882 250.2990 283.5373 -1.1482 242.2259 243.3741 250.5465 285.1625 -1.1544 242.3923 243.5468 250.8615 286.7518 -1.1513 242.5888 243.7401 251.1661 288.3556 -1.1516 242.7948 243.9464 251.4930 289.9655 -1.1517 242.9758 244.1275 251.7985 291.5703 -1.1525 243.1712 244.3237 252.0755 293.1796 -1.1565 243.3427 244.4992 252.3689 294.7839 -1.1553 243.4677 244.6229 252.6360 296.3938 -1.1492 243.6600 244.8092 252.9126 298.0134 -1.1521 243.8612 245.0133 253.1378 299.6228 -1.1566 244.0531 245.2097 253.3039 301.2326 -1.1606 244.2053 245.3659 253.4518 302.8370 -1.1588 244.3524 245.5113 253.6153 304.4309 -1.1536 244.5486 245.7022 253.7929 306.0356 -1.1572 244.6891 245.8463 253.8630 307.6446 -1.1568 244.8414 245.9982 254.0270 309.2493 -1.1592 245.0440 246.2033 254.2101 310.8745 -1.1631 245.2767 246.4398 254.3533 312.4788 -1.1646 245.4560 246.6206 254.4794 314.0830 -1.1661 245.5718 246.7379 254.6599 315.6929 -1.1684 245.7591 246.9274 254.8164 317.2968 -1.1664 245.9059 247.0724 254.9761 318.9065 -1.1661 246.0991 247.2652 255.1376 320.5164 -1.1696 246.2649 247.4345 255.3449 322.1099 -1.1712 246.4045 247.5757 255.5540 323.7300 -1.1675 246.5837 247.7512 255.8195 325.3446 -1.1674 246.7782 247.9456 256.1125 326.9385 -1.1716 246.9967 248.1683 256.3828 328.5433 -1.1734 247.1748 248.3482 256.6983 330.1473 -1.1714 247.3478 248.5192 257.0013 331.7466 -1.1736 247.5405 248.7141 257.3143 333.3510 -1.1767 247.7547 248.9314 257.5480 334.9398 -1.1673 247.9620 249.1293 257.7932 336.5599 -1.1667 248.1348 249.3015 258.0872 338.1644 -1.1692 248.3139 249.4832 258.3684 339.7735 -1.1704 248.4428 249.6132 258.5719 341.3629 -1.1732 248.6391 249.8123 258.7766 342.9675 -1.1729 248.8007 249.9736 258.9582 344.5714 -1.1795 249.0140 250.1936 259.1131 346.1761 -1.1841 249.2304 250.4145 259.2591 347.7854 -1.1840 249.4434 250.6274 259.4242 349.4051 -1.1817 249.6180 250.7997 259.5398 351.0150 -1.1828 249.7755 250.9583 259.6925 352.6188 -1.1847 249.9385 251.1232 259.8338 354.2286 -1.1856 250.0891 251.2746 259.9947 355.8329 -1.1863 250.3000 251.4863 260.1295 357.4371 -1.1879 250.5183 251.7062 260.2651 359.0470 -1.1914 250.7656 251.9571 260.4330 360.6666 -1.1950 250.9812 252.1762 260.6234 362.2760 -1.1993 251.1939 252.3932 260.8489 363.8808 -1.2020 251.3823 252.5842 261.0576 365.4906 -1.2034 251.5430 252.7464 261.3034 367.0954 -1.2066 251.7222 252.9288 261.5897 368.6991 -1.2079 251.9107 253.1186 261.8985 370.3090 -1.2044 252.0922 253.2966 262.2084 371.9291 -1.2093 252.3187 253.5280 262.4839 373.5383 -1.2102 252.5068 253.7170 262.8000 375.1428 -1.2102 252.7242 253.9344 263.1280 376.7526 -1.2093 252.9370 254.1462 263.4219 378.3568 -1.2133 253.1272 254.3405 263.6994 379.9663 -1.2195 253.2573 254.4769 263.9657 381.5761 -1.2252 253.4226 254.6478 264.2068 383.1954 -1.2237 253.6290 254.8528 264.3995 384.8051 -1.2302 253.8559 255.0862 264.5169 386.4099 -1.2343 254.1024 255.3367 264.6830 388.0239 -1.2333 254.2936 255.5269 264.8174 389.6286 -1.2371 254.4924 255.7295 264.9598 391.2334 -1.2352 254.6637 255.8988 265.1170 392.8168 -1.2388 254.7863 256.0252 265.2024 394.4214 -1.2504 255.0037 256.2541 265.2950 396.0364 -1.2516 255.2113 256.4629 265.4172 397.6403 -1.2497 255.4844 256.7341 265.5812 399.2398 -1.2468 255.6994 256.9462 265.7520 400.8445 -1.2487 255.8658 257.1145 265.9350 402.4338 -1.2520 256.0747 257.3267 266.0985 404.0376 -1.2571 256.3098 257.5669 266.3254 405.6424 -1.2605 256.5019 257.7624 266.5535 407.2471 -1.2582 256.7107 257.9689 266.8199 408.8670 -1.2582 256.9075 258.1657 267.1217 410.4761 -1.2608 257.0783 258.3391 267.4310 412.0809 -1.2605 257.3169 258.5774 267.7288 413.6901 -1.2604 257.5605 258.8208 268.0943 415.2945 -1.2598 257.7497 259.0094 268.4207 416.9041 -1.2618 257.9251 259.1869 268.7610 418.5081 -1.2628 258.1185 259.3813 269.0725 420.1283 -1.2683 258.3672 259.6354 269.3133 421.7376 -1.2691 258.5575 259.8267 269.5285 423.3316 -1.2701 258.7424 260.0125 269.7388 424.9415 -1.2725 258.9582 260.2307 269.9051 426.5453 -1.2758 259.1374 260.4132 270.1125 428.1551 -1.2742 259.3766 260.6508 270.2204 429.7593 -1.2779 259.6049 260.8828 270.3070 431.3688 -1.2830 259.7948 261.0778 270.4398 432.9939 -1.2796 259.9726 261.2523 270.5311 434.6029 -1.2859 260.1733 261.4592 270.6690 436.2076 -1.2844 260.3737 261.6581 270.8169 437.8118 -1.2814 260.5728 261.8542 270.9210 439.4213 -1.2881 260.8168 262.1049 271.0230 441.0256 -1.2905 261.0407 262.3312 271.1816 442.6349 -1.2885 261.2271 262.5156 271.4203 444.2550 -1.2873 261.4682 262.7555 271.6558 445.8640 -1.2977 261.6943 262.9920 271.9163 447.4686 -1.2982 261.9040 263.2022 272.1788 449.0830 -1.2985 262.1542 263.4527 272.4453 450.6874 -1.3008 262.3418 263.6426 272.7274 452.2971 -1.3041 262.5265 263.8306 273.0935 453.9010 -1.3071 262.7578 264.0649 273.4098 455.5211 -1.3065 262.9708 264.2773 273.6972 457.1200 -1.3036 263.1417 264.4453 273.9941 458.7245 -1.3035 263.2989 264.6024 274.2858 460.3289 -1.3072 263.4988 264.8060 274.5360 461.9330 -1.3126 263.7450 265.0576 274.7996 463.5224 -1.3152 263.9939 265.3092 275.0099 465.1215 -1.3199 264.1718 265.4917 275.2193 466.7309 -1.3289 264.4025 265.7314 275.4184 468.3509 -1.3332 264.6051 265.9383 275.5882 469.9599 -1.3307 264.8242 266.1549 275.7361 471.5595 -1.3281 265.0140 266.3421 275.8474 473.1638 -1.3367 265.2072 266.5438 275.9602 474.7731 -1.3423 265.4319 266.7742 276.0776 476.3779 -1.3468 265.6569 267.0037 276.1828 477.9868 -1.3519 265.8317 267.1837 276.3134 479.6069 -1.3508 266.0337 267.3845 276.4367 481.2115 -1.3532 266.2623 267.6155 276.5183 482.8205 -1.3594 266.4952 267.8546 276.6822 484.4253 -1.3576 266.7047 268.0623 276.8859 486.0351 -1.3593 266.9271 268.2864 277.0972 487.6390 -1.3613 267.1621 268.5234 277.3270 489.2488 -1.3604 267.3783 268.7387 277.5867 490.8688 -1.3627 267.5940 268.9566 277.8873 492.4778 -1.3637 267.8219 269.1856 278.2603 494.0876 -1.3694 268.0475 269.4169 278.6429 495.6918 -1.3730 268.2673 269.6403 279.0411 497.3013 -1.3740 268.4803 269.8543 279.3438 498.9060 -1.3818 268.7423 270.1241 279.6602 500.5149 -1.3821 268.9543 270.3364 279.9573 502.1350 -1.3812 269.1592 270.5404 280.2297 503.7446 -1.3879 269.3505 270.7383 280.4812 505.3486 -1.3901 269.5539 270.9440 280.6857 506.9585 -1.3915 269.8045 271.1960 280.8580 508.5678 -1.3967 270.0507 271.4474 280.9964 510.1721 -1.4005 270.2445 271.6450 281.0762 511.7820 -1.4064 270.4724 271.8788 281.1481 513.4011 -1.4101 270.7138 272.1238 281.2400 515.0110 -1.4065 270.9086 272.3151 281.3128 516.6155 -1.4066 271.1466 272.5532 281.4163 518.2246 -1.4069 271.3662 272.7731 281.4996 519.8243 -1.4017 271.5735 272.9753 281.5735 521.4238 -1.3954 271.7871 273.1825 281.7522 523.0276 -1.3991 272.0008 273.3999 281.9412 524.6478 -1.4006 272.2062 273.6068 282.1519 526.2368 -1.4039 272.4060 273.8099 282.3647 527.8409 -1.4057 272.5935 273.9992 282.6724 529.4405 -1.4094 272.8143 274.2236 283.0112 531.0504 -1.4182 273.0426 274.4608 283.3231 532.6593 -1.4211 273.2956 274.7167 283.6846 534.2691 -1.4188 273.5191 274.9379 283.9968 535.8734 -1.4218 273.7588 275.1806 284.3428 537.4828 -1.4227 273.9729 275.3956 284.6922 539.1029 -1.4210 274.1998 275.6208 284.9849 540.6964 -1.4294 274.3899 275.8193 285.2681 542.3114 -1.4328 274.6064 276.0392 285.4868 543.9210 -1.4375 274.8175 276.2551 285.7212 545.5250 -1.4416 275.0184 276.4600 285.8805 547.1144 -1.4371 275.2470 276.6841 286.0346 548.7235 -1.4362 275.4719 276.9082 286.2065 550.3280 -1.4376 275.7052 277.1427 286.3394 551.9529 -1.4445 275.9555 277.4000 286.4644 553.5724 -1.4497 276.1845 277.6342 286.5650 555.1823 -1.4518 276.4379 277.8898 286.6237 556.7866 -1.4524 276.6514 278.1038 286.6812 558.3908 -1.4488 276.8768 278.3257 286.7781 560.0004 -1.4501 277.0715 278.5216 286.9133 561.6044 -1.4497 277.2788 278.7285 287.0896 563.2296 -1.4503 277.4632 278.9135 287.2746 564.8334 -1.4508 277.6792 279.1300 287.5408 566.4484 -1.4567 277.9311 279.3877 287.8047 568.0528 -1.4608 278.1511 279.6119 288.0721 569.6620 -1.4697 278.3823 279.8521 288.3268 571.2514 -1.4668 278.6186 280.0854 288.5991 572.8766 -1.4725 278.8233 280.2958 288.9708 574.5010 -1.4731 279.0539 280.5270 289.3462 576.1056 -1.4761 279.2777 280.7538 289.6771 577.7001 -1.4767 279.4730 280.9497 290.0300 579.3194 -1.4834 279.6959 281.1793 290.3478 580.9291 -1.4912 279.9485 281.4397 290.5756 582.5339 -1.4994 280.1975 281.6968 290.8353 584.1433 -1.5035 280.4054 281.9088 291.0811 585.7424 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437.5226 442.1793 437.4873 1700.1328 -4.6573 437.7547 442.4119 437.8826 1701.7370 -4.6642 437.9643 442.6284 438.3191 1703.3418 -4.6698 438.1903 442.8602 438.7698 1704.9510 -4.6739 438.3927 443.0666 439.1456 1706.5554 -4.6809 438.6684 443.3493 439.4870 1708.1806 -4.6908 438.9063 443.5971 439.8451 1709.7850 -4.7041 439.1360 443.8401 440.1239 1711.3943 -4.7113 439.3455 444.0568 440.3397 1712.9990 -4.7236 439.5843 444.3079 440.5065 1714.6036 -4.7332 439.8076 444.5408 440.6602 1716.2126 -4.7346 440.0694 444.8040 440.7021 1717.8174 -4.7386 440.2935 445.0321 440.7070 1719.4421 -4.7391 440.5512 445.2903 440.7293 1721.0464 -4.7424 440.7855 445.5279 440.7240 1722.6563 -4.7422 440.9613 445.7035 440.7210 1724.2601 -4.7459 441.1671 445.9130 440.7549