DTA measure 21s Date: 2024102:102 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.67 s Mass = 956.900 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4605 -4.4593 441.8145 446.2738 424.7475 4.0548 -4.4711 441.8486 446.3197 424.7409 5.6801 -4.4626 441.8488 446.3114 424.6942 7.2798 -4.4654 441.8778 446.3432 424.6341 8.8786 -4.4762 441.8931 446.3694 424.5669 10.4926 -4.4996 441.9237 446.4233 424.4700 12.0925 -4.5125 441.9232 446.4357 424.3597 13.6914 -4.5185 441.9402 446.4586 424.2211 15.3201 -4.5212 441.9549 446.4762 424.0679 16.9190 -4.5100 441.9722 446.4822 423.8931 18.5209 -4.5076 441.9872 446.4948 423.6933 20.1220 -4.5428 441.9961 446.5389 423.4685 21.7376 -4.5442 441.9894 446.5336 423.2570 23.3518 -4.5440 442.0024 446.5465 423.0346 24.9550 -4.5489 441.9970 446.5459 422.8178 26.5635 -4.5515 442.0062 446.5577 422.5959 28.1775 -4.5568 442.0189 446.5756 422.3494 29.7773 -4.5588 442.0070 446.5659 422.1359 31.3915 -4.5632 442.0080 446.5712 421.9164 33.0058 -4.5622 441.9951 446.5573 421.6715 34.6055 -4.5677 441.9859 446.5536 421.4591 36.2188 -4.5696 441.9759 446.5455 421.2463 37.8189 -4.5714 441.9590 446.5304 421.0303 39.4338 -4.5724 441.9495 446.5219 420.8306 41.0479 -4.5798 441.9369 446.5168 420.6054 42.6486 -4.5842 441.9055 446.4897 420.4147 44.2626 -4.5870 441.8928 446.4798 420.2087 45.8714 -4.5878 441.8692 446.4570 420.0132 47.4536 -4.5920 441.8430 446.4349 419.8149 49.0730 -4.5941 441.8134 446.4075 419.6297 50.6640 -4.5997 441.7809 446.3806 419.4456 52.2725 -4.6002 441.7406 446.3408 419.2547 53.8660 -4.6004 441.7076 446.3080 419.0446 55.4570 -4.6053 441.6891 446.2945 418.8862 57.0781 -4.6067 441.6441 446.2508 418.7100 58.6871 -4.6076 441.5969 446.2045 418.5091 60.2824 -4.6131 441.5601 446.1732 418.3472 61.8740 -4.6137 441.4965 446.1102 418.1498 63.4806 -4.6128 441.4606 446.0733 417.9533 65.1023 -4.6192 441.4081 446.0273 417.7539 66.6954 -4.6231 441.3539 445.9769 417.5704 68.3033 -4.6291 441.3262 445.9553 417.3513 69.8969 -4.6318 441.2655 445.8973 417.1455 71.5203 -4.6343 441.2064 445.8407 416.9516 73.1318 -4.6370 441.1455 445.7825 416.7460 74.7303 -4.6397 441.0961 445.7359 416.5492 76.3419 -4.6396 441.0200 445.6596 416.3655 77.9370 -4.6448 440.9387 445.5834 416.1583 79.5506 -4.6446 440.8908 445.5354 415.9549 81.1668 -4.6484 440.8294 445.4778 415.7518 82.7806 -4.6477 440.7578 445.4055 415.5646 84.3800 -4.6492 440.6867 445.3360 415.3720 85.9795 -4.6524 440.6196 445.2720 415.1556 87.5935 -4.6545 440.5379 445.1925 414.9383 89.2075 -4.6582 440.4682 445.1264 414.7320 90.8215 -4.6652 440.3907 445.0559 414.5164 92.4205 -4.6697 440.3154 444.9851 414.2869 94.0199 -4.6705 440.2306 444.9011 414.0894 95.6338 -4.6720 440.1632 444.8352 413.8812 97.2628 -4.6634 440.0637 444.7271 413.6577 98.8619 -4.6643 439.9688 444.6331 413.4514 100.4616 -4.6665 439.8960 444.5624 413.2476 102.0773 -4.6680 439.7984 444.4664 413.0513 103.6783 -4.6705 439.7096 444.3802 412.8463 105.2955 -4.6696 439.6290 444.2986 412.6362 106.8985 -4.6657 439.5321 444.1978 412.4409 108.5045 -4.6701 439.4375 444.1077 412.2434 110.1166 -4.6720 439.3349 444.0068 412.0417 111.7083 -4.6730 439.2271 443.9001 411.8408 113.3026 -4.6739 439.1346 443.8084 411.6483 114.9106 -4.6735 439.0274 443.7009 411.4609 116.5033 -4.6765 438.9194 443.5959 411.2625 118.1124 -4.6765 438.8335 443.5100 411.0809 119.7049 -4.6777 438.7338 443.4115 410.8991 121.3120 -4.6782 438.6200 443.2982 410.7121 122.9205 -4.6807 438.5040 443.1847 410.5123 124.5280 -4.6820 438.3961 443.0781 410.3069 126.1213 -4.6822 438.2806 442.9628 410.0960 127.7446 -4.6822 438.1539 442.8361 409.8994 129.3334 -4.6839 438.0543 442.7382 409.6816 130.9436 -4.6813 437.9444 442.6256 409.4672 132.5554 -4.6830 437.8305 442.5135 409.2421 134.1534 -4.6844 437.7306 442.4150 409.0397 135.7544 -4.6799 437.6023 442.2822 408.8408 137.3546 -4.6827 437.4910 442.1737 408.6273 138.9693 -4.6811 437.3491 442.0302 408.4190 140.5839 -4.6789 437.2296 441.9084 408.1976 142.2001 -4.6797 437.1072 441.7870 407.9848 143.7995 -4.6809 436.9900 441.6708 407.7804 145.3985 -4.6746 436.8493 441.5239 407.5701 146.9975 -4.6692 436.7226 441.3917 407.3741 148.8020 -4.6750 436.5854 441.2604 407.1395 150.4208 -4.6744 436.4616 441.1359 406.9353 152.0353 -4.6757 436.3272 441.0029 406.7251 153.6489 -4.6760 436.1848 440.8608 406.5307 155.2628 -4.6722 436.0641 440.7364 406.3406 156.8629 -4.6649 435.9352 440.6000 406.1508 158.4699 -4.6744 435.7882 440.4626 405.9407 160.0816 -4.6733 435.6528 440.3261 405.7411 161.6821 -4.6728 435.5223 440.1952 405.5564 163.3116 -4.6729 435.3902 440.0632 405.3570 164.9125 -4.6716 435.2449 439.9166 405.1567 166.5265 -4.6716 435.0976 439.7691 404.9470 168.1260 -4.6721 434.9556 439.6277 404.7330 169.7263 -4.6721 434.8241 439.4962 404.5321 171.3555 -4.6700 434.6808 439.3508 404.3104 172.9544 -4.6644 434.5404 439.2048 404.0878 174.5644 -4.6623 434.3851 439.0474 403.8580 176.1568 -4.6598 434.2288 438.8886 403.6720 177.7511 -4.6599 434.0860 438.7459 403.4539 179.3499 -4.6621 433.9394 438.6014 403.2358 180.9598 -4.6625 433.8138 438.4763 403.0245 182.5659 -4.6597 433.6614 438.3211 402.8046 184.1586 -4.6600 433.5185 438.1785 402.5846 185.7656 -4.6565 433.3576 438.0142 402.3849 187.3578 -4.6569 433.2286 437.8854 402.1776 188.9806 -4.6522 433.0561 437.7083 401.9745 190.5890 -4.6499 432.9054 437.5553 401.7584 192.1818 -4.6464 432.7422 437.3886 401.5396 193.7754 -4.6451 432.5971 437.2422 401.3357 195.3856 -4.6448 432.4283 437.0731 401.1415 197.0110 -4.6412 432.2756 436.9168 400.9399 198.6076 -4.6391 432.1317 436.7707 400.7612 200.2056 -4.6399 431.9683 436.6081 400.5520 201.8051 -4.6352 431.8205 436.4557 400.3696 203.4195 -4.6331 431.6696 436.3027 400.1638 205.0346 -4.6317 431.4932 436.1249 399.9619 206.6485 -4.6275 431.3350 435.9625 399.7764 208.2480 -4.6261 431.1692 435.7954 399.5914 209.8475 -4.6228 431.0089 435.6317 399.3982 211.4609 -4.6210 430.8414 435.4625 399.2118 213.0769 -4.6188 430.6889 435.3077 399.0172 214.6773 -4.6164 430.5246 435.1410 398.8091 216.2926 -4.6149 430.3690 434.9839 398.6075 217.8926 -4.6105 430.2006 434.8111 398.3758 219.4926 -4.6023 430.0441 434.6464 398.1780 221.1216 -4.6033 429.8540 434.4574 397.9674 222.7215 -4.6056 429.7105 434.3161 397.7469 224.3355 -4.5464 429.5465 434.0929 397.5364 225.9345 -4.4845 429.3828 433.8673 397.3425 227.5343 -4.5261 429.2198 433.7459 397.1179 229.1635 -4.5688 429.0602 433.6291 396.8956 230.7775 -4.5743 428.8842 433.4586 396.6784 232.3774 -4.5805 428.7057 433.2862 396.4669 233.9778 -4.5765 428.5364 433.1129 396.2645 235.5923 -4.5715 428.3576 432.9291 396.0620 237.2098 -4.5691 428.1870 432.7561 395.8572 238.8046 -4.5675 428.0327 432.6002 395.6475 240.4118 -4.5689 427.8532 432.4221 395.4288 242.0041 -4.5677 427.6822 432.2499 395.2558 243.5950 -4.5579 427.5127 432.0706 395.0615 245.2160 -4.5564 427.3450 431.9013 394.8501 246.8081 -4.5617 427.1634 431.7252 394.6640 248.4150 -4.5595 426.9934 431.5529 394.4622 250.0070 -4.5564 426.8308 431.3872 394.2638 251.6169 -4.5525 426.6588 431.2114 394.0774 253.2260 -4.5492 426.4770 431.0262 393.8721 254.8345 -4.5476 426.2969 430.8445 393.6712 256.4284 -4.5388 426.1154 430.6543 393.4821 258.0365 -4.5372 425.9344 430.4717 393.2735 259.6450 -4.5401 425.7717 430.3117 393.0595 261.2644 -4.5337 425.5862 430.1199 392.8287 262.8661 -4.5302 425.4123 429.9425 392.6193 264.4665 -4.5272 425.2135 429.7408 392.4179 266.0805 -4.5224 425.0475 429.5699 392.1913 267.6794 -4.5205 424.8746 429.3950 391.9778 269.2933 -4.5178 424.6938 429.2117 391.7569 270.9069 -4.5107 424.5155 429.0262 391.5463 272.5058 -4.5087 424.3353 428.8440 391.3305 274.1196 -4.5046 424.1507 428.6552 391.1227 275.7199 -4.5009 423.9685 428.4694 390.9082 277.3346 -4.4977 423.7884 428.2861 390.7116 278.9488 -4.4936 423.6007 428.0943 390.4950 280.5486 -4.4888 423.4271 427.9159 390.2814 282.1625 -4.4849 423.2563 427.7411 390.0573 283.7621 -4.4801 423.0728 427.5529 389.8543 285.3785 -4.4741 422.8812 427.3553 389.6422 286.9925 -4.4712 422.6884 427.1596 389.4434 288.6065 -4.4680 422.5078 426.9757 389.2524 290.2054 -4.4609 422.3361 426.7970 389.0369 291.8114 -4.4596 422.1432 426.6028 388.8258 293.4278 -4.4556 421.9618 426.4174 388.6360 295.0421 -4.4539 421.7656 426.2195 388.4113 296.6416 -4.4500 421.5929 426.0429 388.2142 298.2556 -4.4457 421.3965 425.8423 388.0120 299.8546 -4.4402 421.2066 425.6468 387.8160 301.4696 -4.4390 421.0252 425.4642 387.6227 303.0815 -4.4352 420.8344 425.2696 387.3960 304.6724 -4.4317 420.6476 425.0793 387.2001 306.2790 -4.4237 420.4549 424.8787 387.0090 307.8700 -4.4222 420.2828 424.7050 386.8126 309.4760 -4.4156 420.0876 424.5032 386.6104 311.0829 -4.4124 419.8934 424.3058 386.4142 312.6866 -4.4089 419.7007 424.1097 386.2007 314.2933 -4.4043 419.5337 423.9380 386.0047 315.8850 -4.4019 419.3354 423.7373 385.8153 317.4916 -4.3977 419.1584 423.5561 385.5997 319.1144 -4.3915 418.9556 423.3471 385.3849 320.7074 -4.3881 418.7721 423.1602 385.1700 322.3168 -4.3844 418.5799 422.9644 384.9734 323.9119 -4.3799 418.4060 422.7860 384.7360 325.5394 -4.3741 418.2084 422.5825 384.5138 327.1406 -4.3740 418.0080 422.3820 384.3122 328.7408 -4.3689 417.8116 422.1804 384.0949 330.3544 -4.3641 417.6462 422.0103 383.8809 331.9526 -4.3591 417.4480 421.8071 383.6584 333.5668 -4.3562 417.2500 421.6062 383.4533 335.1808 -4.3508 417.0535 421.4043 383.2339 336.7800 -4.3453 416.8708 421.2162 383.0329 338.3946 -4.3375 416.6626 421.0001 382.7970 339.9935 -4.3341 416.4768 420.8109 382.5908 341.6228 -4.3301 416.2831 420.6132 382.3732 343.2286 -4.3278 416.1041 420.4319 382.1635 344.8295 -4.3220 415.8984 420.2203 381.9677 346.4435 -4.3193 415.7139 420.0332 381.7355 348.0431 -4.3129 415.5238 419.8367 381.5447 349.6570 -4.3106 415.3110 419.6216 381.3443 351.2709 -4.3049 415.1158 419.4207 381.1379 352.8739 -4.3001 414.9252 419.2253 380.9238 354.4876 -4.2951 414.7422 419.0373 380.7243 356.0866 -4.2923 414.5449 418.8372 380.5187 357.7006 -4.2860 414.3525 418.6385 380.3162 359.3148 -4.2820 414.1662 418.4482 380.1215 360.9145 -4.2753 413.9492 418.2245 379.9307 362.5316 -4.2696 413.7569 418.0265 379.7217 364.1230 -4.2662 413.5625 417.8287 379.5141 365.7375 -4.2606 413.3689 417.6295 379.3156 367.3346 -4.2519 413.1755 417.4274 379.1196 368.9410 -4.2482 412.9786 417.2268 378.9216 370.5470 -4.2438 412.7990 417.0428 378.7321 372.1380 -4.2390 412.5954 416.8344 378.5441 373.7305 -4.2352 412.3935 416.6287 378.3412 375.3230 -4.2302 412.2112 416.4415 378.1441 376.9440 -4.2250 412.0007 416.2257 377.9237 378.5368 -4.2212 411.8091 416.0304 377.7250 380.1433 -4.2191 411.6034 415.8225 377.5166 381.7359 -4.2127 411.4065 415.6192 377.2958 383.3291 -4.2071 411.2107 415.4178 377.0892 384.9510 -4.2037 411.0363 415.2400 376.8805 386.5590 -4.1973 410.8146 415.0119 376.6466 388.1548 -4.1912 410.6275 414.8187 376.4433 389.7513 -4.1890 410.4309 414.6199 376.2167 391.3481 -4.1856 410.2361 414.4218 375.9989 392.9766 -4.1778 410.0402 414.2180 375.7787 394.7684 -4.1728 409.8129 413.9857 375.5491 396.3676 -4.1690 409.6189 413.7878 375.3351 397.9691 -4.1636 409.4133 413.5769 375.1109 399.5996 -4.1576 409.2036 413.3613 374.8941 401.1990 -4.1541 409.0067 413.1607 374.6822 402.7985 -4.1469 408.8196 412.9665 374.4715 404.4094 -4.1394 408.6209 412.7603 374.2555 406.0125 -4.1365 408.4466 412.5831 374.0330 407.6281 -4.1319 408.2316 412.3635 373.8225 409.2420 -4.1253 408.0275 412.1529 373.6297 410.8418 -4.1214 407.8268 411.9482 373.4224 412.4556 -4.1177 407.6170 411.7347 373.2064 414.0561 -4.1113 407.4269 411.5382 373.0046 415.6708 -4.1066 407.2296 411.3361 372.7826 417.2848 -4.1026 407.0137 411.1163 372.5660 418.8839 -4.0975 406.8218 410.9194 372.3756 420.4986 -4.0917 406.6210 410.7127 372.1756 422.0975 -4.0853 406.4192 410.5045 371.9655 423.7266 -4.0814 406.2220 410.3034 371.7682 425.5183 -4.0739 405.9939 410.0678 371.5532 427.1324 -4.0697 405.7892 409.8590 371.3492 428.7479 -4.0636 405.5859 409.6495 371.1431 430.3619 -4.0587 405.3975 409.4562 370.9650 431.9559 -4.0550 405.1871 409.2420 370.7582 433.5478 -4.0470 405.0024 409.0494 370.5564 435.1458 -4.0433 404.7893 408.8326 370.3693 436.7445 -4.0392 404.5935 408.6327 370.1733 438.3528 -4.0322 404.4016 408.4338 369.9687 439.9605 -4.0283 404.1963 408.2246 369.7962 441.5534 -4.0237 403.9976 408.0213 369.5902 443.1605 -4.0154 403.7822 407.7976 369.3774 444.7526 -4.0096 403.5826 407.5921 369.1719 446.3754 -4.0096 403.3945 407.4041 368.9375 447.9831 -4.0019 403.1959 407.1977 368.7484 449.5754 -3.9961 402.9924 406.9884 368.5363 451.1850 -3.9911 402.7922 406.7834 368.3062 452.7821 -3.9866 402.5882 406.5748 368.0999 454.4105 -3.9797 402.3840 406.3637 367.8631 456.0046 -3.9741 402.1774 406.1515 367.6497 457.6185 -3.9671 401.9791 405.9462 367.4225 459.2179 -3.9622 401.7827 405.7449 367.2069 460.8175 -3.9592 401.5684 405.5276 367.0160 462.4173 -3.9562 401.3795 405.3358 366.7854 464.0465 -3.9511 401.1721 405.1232 366.5670 465.6464 -3.9442 400.9639 404.9081 366.3536 467.2599 -3.9414 400.7777 404.7191 366.1404 468.8600 -3.9330 400.5783 404.5113 365.9318 470.4596 -3.9287 400.3825 404.3112 365.7277 472.0755 -3.9234 400.1660 404.0894 365.5051 473.6908 -3.9197 399.9616 403.8813 365.2960 475.2973 -3.9157 399.7582 403.6739 365.1081 476.9025 -3.9092 399.5449 403.4541 364.8902 478.5166 -3.9048 399.3467 403.2515 364.6997 480.1170 -3.8982 399.1450 403.0433 364.4858 481.7315 -3.8937 398.9521 402.8458 364.2798 483.3456 -3.8872 398.7469 402.6341 364.0701 484.9455 -3.8818 398.5368 402.4185 363.8799 486.5469 -3.8783 398.3393 402.2176 363.6763 488.1610 -3.8714 398.1479 402.0193 363.4740 489.7598 -3.8687 397.9411 401.8098 363.2864 491.3898 -3.8617 397.7259 401.5876 363.0837 492.9886 -3.8581 397.5257 401.3838 362.8828 494.5883 -3.8537 397.3157 401.1694 362.6836 496.1970 -3.8470 397.1167 400.9636 362.4807 497.7883 -3.8406 396.9234 400.7640 362.2980 499.3973 -3.8372 396.7331 400.5703 362.0955 501.0050 -3.8324 396.5242 400.3566 361.9083 502.5960 -3.8266 396.3177 400.1443 361.7132 504.2026 -3.8225 396.1161 399.9386 361.5080 505.7948 -3.8169 395.9162 399.7331 361.2871 507.4164 -3.8119 395.7076 399.5195 361.0848 509.0091 -3.8072 395.5007 399.3079 360.8663 510.6165 -3.8010 395.3053 399.1063 360.6539 512.2085 -3.7969 395.1018 398.8987 360.4342 513.8318 -3.7919 394.8982 398.6901 360.2380 515.4401 -3.7872 394.6911 398.4783 360.0215 517.0356 -3.7812 394.4935 398.2747 359.8051 518.6465 -3.7762 394.2748 398.0511 359.5968 520.2445 -3.7717 394.0683 397.8400 359.3660 521.8735 -3.7643 393.8793 397.6436 359.1584 523.4724 -3.7610 393.6716 397.4327 358.9491 525.0709 -3.7554 393.4800 397.2354 358.7488 526.6848 -3.7494 393.2699 397.0193 358.5359 528.2838 -3.7464 393.0618 396.8081 358.3445 529.8979 -3.7409 392.8633 396.6042 358.1051 531.5128 -3.7354 392.6540 396.3893 357.9138 533.1116 -3.7281 392.4596 396.1876 357.7064 534.7113 -3.7212 392.2604 395.9816 357.4838 536.3255 -3.7169 392.0443 395.7612 357.2622 537.9323 -3.7138 391.8395 395.5532 357.0615 539.5615 -3.7076 391.6411 395.3487 356.8532 541.1623 -3.7009 391.4444 395.1453 356.6386 542.7635 -3.6955 391.2341 394.9296 356.4346 544.3775 -3.6902 391.0206 394.7108 356.2244 545.9774 -3.6860 390.8114 394.4974 356.0140 547.6069 -3.6785 390.6034 394.2819 355.7928 549.2056 -3.6745 390.4107 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257.2654 258.4037 223.3726 1597.2316 -1.1374 257.0637 258.2011 223.2019 1598.8541 -1.1348 256.8585 257.9932 223.0240 1600.4464 -1.1336 256.6608 257.7944 222.8321 1602.0446 -1.1318 256.4717 257.6034 222.6470 1603.6584 -1.1296 256.2667 257.3964 222.4748 1605.2506 -1.1261 256.0908 257.2169 222.3054 1606.8728 -1.1223 255.8747 256.9970 222.1173 1608.4803 -1.1220 255.6799 256.8019 221.9480 1610.0725 -1.1205 255.4783 256.5988 221.7602 1611.6656 -1.1188 255.2909 256.4098 221.5827 1613.2894 -1.1149 255.1099 256.2248 221.3945 1614.8990 -1.1135 254.8999 256.0134 221.2190 1616.4975 -1.1123 254.6982 255.8105 221.0429 1618.1115 -1.1104 254.5082 255.6186 220.8612 1619.7105 -1.1095 254.3132 255.4227 220.6895 1621.3095 -1.1075 254.1134 255.2209 220.5057 1622.9395 -1.1039 253.9211 255.0250 220.3234 1624.5378 -1.1006 253.7074 254.8081 220.1501 1626.1366 -1.0993 253.5041 254.6034 219.9819 1627.7506 -1.0965 253.3239 254.4204 219.7981 1629.3504 -1.0922 253.1261 254.2183 219.6194 1630.9798 -1.0895 252.9429 254.0324 219.4433 1632.5731 -1.0873 252.7311 253.8184 219.2700 1634.1876 -1.0828 252.5454 253.6282 219.0935 1635.8016 -1.0801 252.3433 253.4234 218.9127 1637.4005 -1.0791 252.1484 253.2274 218.7535 1639.0145 -1.0788 251.9460 253.0248 218.5716 1640.6286 -1.0762 251.7652 252.8415 218.3906 1642.2285 -1.0759 251.5652 252.6410 218.2268 1643.8425 -1.0701 251.3669 252.4370 218.0445 1645.4413 -1.0679 251.1626 252.2306 217.8727 1647.0595 -1.0683 250.9775 252.0458 217.7041 1648.6739 -1.0678 250.7764 251.8442 217.5277