DTA measure 12. Date: 2024102:1036 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.30 s Mass = 956.900 mg data_number = 1582 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1278 -0.2163 245.5561 245.7723 266.2793 1.9470 -0.2115 245.7202 245.9317 266.2944 2.7060 -0.2054 245.8567 246.0621 266.3137 3.5553 -0.2002 246.0280 246.2282 266.3311 4.3448 -0.1934 246.1806 246.3739 266.3526 5.1353 -0.1901 246.3250 246.5152 266.3684 5.9550 -0.1842 246.4864 246.6706 266.3918 6.7448 -0.1794 246.6266 246.8060 266.4124 7.5643 -0.1758 246.7689 246.9447 266.4482 8.3553 -0.1735 246.9275 247.1010 266.4863 9.1460 -0.1721 247.0613 247.2334 266.5206 9.9673 -0.1646 247.2204 247.3850 266.5666 10.7585 -0.1638 247.3768 247.5406 266.6299 11.5790 -0.1591 247.5506 247.7097 266.6949 12.3700 -0.1563 247.6832 247.8396 266.7498 13.1635 -0.1531 247.8554 248.0085 266.8225 13.9965 -0.1492 247.9974 248.1466 266.9055 14.7705 -0.1463 248.1398 248.2861 266.9780 15.5928 -0.1425 248.2738 248.4163 267.0575 16.3845 -0.1374 248.4095 248.5469 267.1449 17.2068 -0.1337 248.5629 248.6966 267.2485 17.9990 -0.1352 248.7060 248.8412 267.3501 18.7925 -0.1440 248.8554 248.9994 267.4646 19.6145 -0.1397 249.0213 249.1610 267.5701 20.3765 -0.1405 249.1539 249.2944 267.6668 21.2305 -0.1284 249.3197 249.4481 267.7678 22.0245 -0.1194 249.4547 249.5741 267.8953 22.8175 -0.1181 249.6108 249.7289 268.0067 23.6395 -0.1260 249.7544 249.8804 268.1282 24.4058 -0.1261 249.8783 250.0044 268.2500 25.2603 -0.1216 250.0406 250.1621 268.3983 26.0238 -0.1252 250.1944 250.3196 268.5044 26.8495 -0.1110 250.3223 250.4333 268.6128 27.6425 -0.1040 250.4656 250.5695 268.7192 28.4355 -0.1043 250.5975 250.7018 268.8397 29.2580 -0.0997 250.7594 250.8591 268.9705 30.0505 -0.0984 250.8933 250.9917 269.0873 30.8718 -0.0961 251.0286 251.1246 269.2060 31.6640 -0.0945 251.1796 251.2741 269.3339 32.4858 -0.0942 251.3257 251.4200 269.4596 33.3095 -0.0918 251.4709 251.5627 269.5997 34.1018 -0.0924 251.6056 251.6980 269.7229 34.9095 -0.0924 251.7623 251.8547 269.8373 35.7318 -0.0913 251.9073 251.9986 269.9708 36.5540 -0.0878 252.0411 252.1289 270.1067 37.3455 -0.0881 252.1813 252.2694 270.2250 38.1678 -0.0884 252.3271 252.4155 270.3468 38.9318 -0.0864 252.4716 252.5579 270.4604 39.7868 -0.0860 252.6090 252.6950 270.6033 40.5788 -0.0862 252.7654 252.8516 270.7304 41.3705 -0.0852 252.9001 252.9853 270.8405 42.1925 -0.0849 253.0485 253.1334 270.9767 42.9545 -0.0848 253.1761 253.2610 271.0770 43.8085 -0.0841 253.3268 253.4109 271.2011 44.6005 -0.0835 253.4512 253.5346 271.3229 45.3925 -0.0843 253.5848 253.6691 271.4252 46.2145 -0.0826 253.7236 253.8062 271.5355 46.9765 -0.0799 253.8692 253.9492 271.6469 47.8305 -0.0867 254.0274 254.1142 271.7645 48.6225 -0.0878 254.1614 254.2493 271.8549 49.4118 -0.0912 254.2952 254.3864 271.9724 50.2300 -0.0881 254.4330 254.5211 272.0826 50.9878 -0.0892 254.5799 254.6691 272.1757 51.8360 -0.0894 254.7255 254.8149 272.2890 52.6238 -0.0894 254.8666 254.9561 272.4083 53.4120 -0.0886 254.9947 255.0833 272.5209 54.2305 -0.0886 255.1300 255.2186 272.6190 54.9900 -0.0893 255.2596 255.3489 272.7131 55.8380 -0.0812 255.4135 255.4947 272.8189 56.6260 -0.0897 255.5561 255.6458 272.9312 57.4150 -0.0928 255.6984 255.7912 273.0353 58.2338 -0.0929 255.8290 255.9219 273.1251 58.9928 -0.0881 255.9628 256.0509 273.2298 59.8418 -0.0864 256.1115 256.1979 273.3296 60.6305 -0.0879 256.2538 256.3416 273.4375 61.4210 -0.0882 256.3902 256.4784 273.5551 62.2393 -0.0897 256.5194 256.6091 273.6516 63.0280 -0.0879 256.6555 256.7434 273.7302 63.8468 -0.0886 256.7979 256.8866 273.8382 64.6385 -0.0911 256.9172 257.0083 273.9425 65.4360 -0.0942 257.0462 257.1404 274.0441 66.2588 -0.0959 257.2152 257.3112 274.1589 67.0170 -0.0944 257.3414 257.4358 274.2576 67.8668 -0.0902 257.4796 257.5697 274.3401 68.6568 -0.0945 257.6098 257.7043 274.4380 69.4460 -0.0992 257.7484 257.8476 274.5406 70.2680 -0.1081 257.8830 257.9911 274.6605 71.0273 -0.1051 258.0093 258.1144 274.7624 71.8775 -0.1045 258.1612 258.2657 274.8354 72.6688 -0.1060 258.3054 258.4114 274.9300 73.4593 -0.1140 258.4293 258.5433 275.0346 74.2808 -0.1180 258.5649 258.6829 275.1319 75.0785 -0.1203 258.7082 258.8285 275.2321 76.0670 -0.1117 258.8736 258.9852 275.3703 76.8888 -0.1063 259.0191 259.1254 275.4802 77.6808 -0.1069 259.1508 259.2577 275.5925 78.4725 -0.1063 259.2858 259.3921 275.6786 79.3248 -0.1055 259.4173 259.5228 275.7752 80.0865 -0.1084 259.5452 259.6536 275.8647 80.9085 -0.1111 259.6769 259.7880 275.9710 81.7005 -0.1113 259.8301 259.9414 276.0737 82.4925 -0.1148 259.9594 260.0742 276.1680 83.3445 -0.1169 260.0960 260.2130 276.2807 84.1068 -0.1184 260.2270 260.3454 276.3731 84.9295 -0.1183 260.3735 260.4918 276.4754 85.7215 -0.1188 260.5008 260.6196 276.5819 86.5135 -0.1212 260.6199 260.7411 276.6877 87.3355 -0.1245 260.7560 260.8805 276.8032 88.1275 -0.1262 260.8809 261.0070 276.9073 88.9493 -0.1296 261.0272 261.1569 277.0322 89.7410 -0.1335 261.1719 261.3053 277.1331 90.5325 -0.1378 261.3050 261.4428 277.2577 91.3850 -0.1394 261.4441 261.5835 277.3882 92.1465 -0.1399 261.5586 261.6985 277.4906 92.9688 -0.1409 261.7067 261.8476 277.6052 93.7608 -0.1429 261.8312 261.9741 277.7295 94.5525 -0.1441 261.9597 262.1038 277.8551 95.4048 -0.1437 262.1081 262.2518 277.9891 96.1548 -0.1427 262.2393 262.3820 278.0906 97.0128 -0.1481 262.3636 262.5117 278.2188 97.7745 -0.1511 262.4963 262.6473 278.3331 98.5968 -0.1517 262.6187 262.7705 278.4473 99.4188 -0.1564 262.7701 262.9265 278.5768 100.1805 -0.1593 262.8972 263.0565 278.6770 101.0325 -0.1602 263.0246 263.1848 278.7969 101.7945 -0.1605 263.1537 263.3141 278.8890 102.6165 -0.1635 263.2904 263.4539 279.0158 103.4385 -0.1661 263.4141 263.5801 279.1146 104.2005 -0.1693 263.5357 263.7050 279.2225 105.0525 -0.1707 263.6710 263.8417 279.3204 105.8145 -0.1756 263.7982 263.9739 279.4287 106.6365 -0.1752 263.9402 264.1154 279.5265 107.4585 -0.1774 264.0735 264.2509 279.6331 108.2205 -0.1787 264.1874 264.3661 279.7299 109.0730 -0.1814 264.3309 264.5122 279.8357 109.8360 -0.1841 264.4640 264.6481 279.9353 110.6578 -0.1852 264.5995 264.7847 280.0439 111.4800 -0.1874 264.7301 264.9174 280.1320 112.2415 -0.1886 264.8647 265.0534 280.2375 113.0930 -0.1914 264.9890 265.1804 280.3424 113.8513 -0.1935 265.1182 265.3116 280.4403 114.6693 -0.1955 265.2568 265.4523 280.5531 115.4873 -0.2003 265.3877 265.5880 280.6482 116.2450 -0.2057 265.5149 265.7206 280.7404 117.0938 -0.2064 265.6468 265.8532 280.8381 117.8513 -0.2083 265.7773 265.9856 280.9355 118.6690 -0.2127 265.8919 266.1047 281.0294 119.4885 -0.2152 266.0369 266.2521 281.1577 120.2485 -0.2112 266.1622 266.3734 281.2303 121.0980 -0.2138 266.2964 266.5102 281.3220 121.8560 -0.2148 266.4087 266.6235 281.4300 122.6750 -0.2161 266.5457 266.7619 281.5384 123.4935 -0.2192 266.6873 266.9064 281.6089 124.2520 -0.2211 266.7964 267.0175 281.7107 125.1018 -0.2253 266.9330 267.1582 281.8048 125.8900 -0.2268 267.0690 267.2957 281.8949 126.6888 -0.2278 267.1861 267.4138 281.9894 127.4870 -0.2318 267.3098 267.5416 282.1016 128.2760 -0.2344 267.4452 267.6796 282.2268 129.0953 -0.2397 267.5736 267.8134 282.3348 129.8840 -0.2404 267.7093 267.9496 282.4397 130.7035 -0.2424 267.8353 268.0777 282.5430 131.4925 -0.2455 267.9639 268.2094 282.6409 132.2828 -0.2469 268.0898 268.3368 282.7609 133.1318 -0.2478 268.2245 268.4724 282.8875 133.8903 -0.2519 268.3520 268.6040 282.9933 134.7108 -0.2523 268.4638 268.7161 283.1081 135.5310 -0.2522 268.5955 268.8477 283.2303 136.2908 -0.2553 268.7139 268.9692 283.3285 137.1603 -0.2585 268.8634 269.1219 283.4594 137.8983 -0.2619 268.9678 269.2297 283.5818 138.7493 -0.2644 269.1170 269.3815 283.6996 139.5425 -0.2658 269.2392 269.5049 283.8208 140.3355 -0.2639 269.3643 269.6283 283.9419 141.1575 -0.2716 269.5014 269.7730 284.0494 141.9195 -0.2727 269.6133 269.8860 284.1554 142.7715 -0.2738 269.7469 270.0207 284.3010 143.5335 -0.2793 269.8753 270.1546 284.3955 144.3555 -0.2832 270.0087 270.2919 284.5155 145.1775 -0.2814 270.1438 270.4251 284.6321 145.9390 -0.2860 270.2880 270.5740 284.7315 146.7913 -0.2889 270.4045 270.6934 284.8636 147.5395 -0.2890 270.5140 270.8030 284.9689 148.3930 -0.2934 270.6400 270.9334 285.0784 149.1848 -0.2967 270.7780 271.0748 285.1793 149.9765 -0.2969 270.8866 271.1835 285.2728 150.7978 -0.2963 271.0169 271.3132 285.3797 151.5895 -0.2973 271.1489 271.4462 285.4729 152.4118 -0.3062 271.2683 271.5745 285.5751 153.2045 -0.3107 271.3937 271.7045 285.6764 153.9965 -0.3120 271.5218 271.8338 285.7728 154.8198 -0.3159 271.6440 271.9599 285.8603 155.5825 -0.3190 271.7726 272.0916 285.9484 156.4348 -0.3200 271.9123 272.2324 286.0297 157.2713 -0.3216 272.0466 272.3682 286.1329 158.2300 -0.3264 272.1885 272.5149 286.2409 159.0225 -0.3277 272.2966 272.6243 286.3312 159.8445 -0.3283 272.4393 272.7676 286.4274 160.6365 -0.3309 272.5675 272.8984 286.5321 161.4585 -0.3349 272.6829 273.0178 286.6218 162.2505 -0.3367 272.8104 273.1471 286.7237 163.0425 -0.3393 272.9347 273.2739 286.8166 163.8945 -0.3443 273.0598 273.4041 286.9243 164.6585 -0.3480 273.1829 273.5309 287.0303 165.4805 -0.3497 273.3230 273.6727 287.1361 166.2725 -0.3410 273.4619 273.8030 287.2394 167.0645 -0.3449 273.5747 273.9197 287.3574 167.9328 -0.3515 273.7025 274.0540 287.4657 168.6645 -0.3564 273.8199 274.1763 287.5665 169.5170 -0.3605 273.9425 274.3030 287.6643 170.3090 -0.3616 274.0793 274.4409 287.7658 171.1005 -0.3595 274.2026 274.5621 287.8712 171.9228 -0.3558 274.3288 274.6846 287.9898 172.7145 -0.3599 274.4566 274.8165 288.1018 173.5368 -0.3648 274.5750 274.9398 288.1936 174.3288 -0.3657 274.6933 275.0591 288.3031 175.1205 -0.3675 274.8317 275.1993 288.4299 175.9428 -0.3734 274.9451 275.3185 288.5334 176.7345 -0.3770 275.0653 275.4423 288.6355 177.5568 -0.3796 275.1852 275.5648 288.7549 178.3380 -0.3835 275.3168 275.7004 288.8580 179.1560 -0.3874 275.4572 275.8446 288.9601 179.9443 -0.3913 275.5862 275.9775 289.0830 180.7320 -0.3895 275.6864 276.0758 289.1962 181.5808 -0.3896 275.8361 276.2257 289.2944 182.3395 -0.3885 275.9526 276.3411 289.4001 183.1580 -0.3965 276.0633 276.4598 289.5286 183.9463 -0.4026 276.1707 276.5732 289.6233 184.7350 -0.4089 276.2893 276.6982 289.7290 185.5830 -0.4097 276.4249 276.8346 289.8481 186.3410 -0.4100 276.5567 276.9667 289.9525 187.1598 -0.4133 276.6962 277.1096 290.0577 187.9553 -0.4152 276.8123 277.2275 290.1872 188.7520 -0.4125 276.9316 277.3441 290.3070 189.5715 -0.3965 277.0612 277.4577 290.4091 190.3310 -0.4019 277.1789 277.5808 290.4881 191.1800 -0.4101 277.3074 277.7175 290.5926 191.9693 -0.4196 277.4121 277.8316 290.7117 192.7588 -0.4234 277.5331 277.9565 290.8319 193.5783 -0.4271 277.6508 278.0779 290.9320 194.3390 -0.4251 277.7773 278.2024 291.0147 195.1885 -0.4218 277.9116 278.3334 291.1446 195.9790 -0.4326 278.0276 278.4603 291.2401 196.7693 -0.4383 278.1633 278.6016 291.3326 197.5893 -0.4445 278.2788 278.7233 291.4606 198.3598 -0.4491 278.3918 278.8409 291.5588 199.1928 -0.4558 278.5132 278.9690 291.6747 199.9545 -0.4544 278.6229 279.0773 291.7645 200.8038 -0.4542 278.7494 279.2036 291.8680 201.5950 -0.4610 278.8799 279.3409 291.9832 202.3865 -0.4634 279.0022 279.4656 292.0883 203.2085 -0.4622 279.1476 279.6098 292.1963 203.9698 -0.4659 279.2554 279.7212 292.2876 204.8220 -0.4667 279.3787 279.8454 292.4016 205.5840 -0.4699 279.4883 279.9582 292.5072 206.4058 -0.4760 279.6225 280.0985 292.6151 207.1980 -0.4767 279.7408 280.2175 292.7105 207.9895 -0.4798 279.8530 280.3328 292.8285 208.8583 -0.4823 279.9841 280.4665 292.9239 209.5905 -0.4674 280.1010 280.5683 293.0295 210.4428 -0.4810 280.2333 280.7143 293.1282 211.2048 -0.4875 280.3561 280.8436 293.2258 212.0268 -0.4881 280.4752 280.9632 293.3346 212.8488 -0.4935 280.5903 281.0838 293.4454 213.6105 -0.4941 280.6976 281.1917 293.5439 214.4628 -0.4970 280.8435 281.3405 293.6483 215.2245 -0.4997 280.9686 281.4683 293.7666 216.0475 -0.5050 281.0928 281.5978 293.8434 216.8398 -0.5071 281.2188 281.7259 293.9467 217.6315 -0.5097 281.3335 281.8433 294.0593 218.4535 -0.4938 281.4593 281.9531 294.1826 219.2318 -0.4831 281.5745 282.0576 294.2841 220.0845 -0.5103 281.7131 282.2233 294.3692 220.8465 -0.5158 281.8273 282.3431 294.4807 221.6685 -0.5210 281.9517 282.4727 294.5878 222.4605 -0.5252 282.0623 282.5875 294.6891 223.2525 -0.5274 282.1626 282.6900 294.7925 224.1045 -0.5274 282.2951 282.8225 294.9073 224.8665 -0.5295 282.4206 282.9501 295.0168 225.6893 -0.5332 282.5423 283.0755 295.1049 226.4815 -0.5340 282.6727 283.2067 295.2181 227.2728 -0.5360 282.8106 283.3465 295.3133 228.0965 -0.5404 282.9109 283.4513 295.4147 228.8888 -0.5447 283.0404 283.5851 295.5095 229.7108 -0.5470 283.1644 283.7113 295.6178 230.5033 -0.5523 283.2722 283.8245 295.7283 231.2955 -0.5542 283.3966 283.9508 295.8269 232.1178 -0.5563 283.5100 284.0664 295.9381 232.9095 -0.5548 283.6408 284.1956 296.0433 233.7325 -0.5553 283.7548 284.3101 296.1479 234.5258 -0.5586 283.8729 284.4315 296.2385 235.3185 -0.5602 284.0098 284.5700 296.3411 236.1408 -0.5650 284.1283 284.6934 296.4424 236.9025 -0.5666 284.2258 284.7924 296.5384 237.7568 -0.5699 284.3528 284.9226 296.6450 238.5485 -0.5711 284.4853 285.0565 296.7489 239.3535 -0.5705 284.6026 285.1731 296.8376 240.1300 -0.5745 284.7212 285.2958 296.9390 240.9535 -0.5797 284.8435 285.4232 297.0452 241.7753 -0.5813 284.9572 285.5385 297.1500 242.5340 -0.5817 285.0828 285.6646 297.2424 243.3850 -0.5848 285.2060 285.7908 297.3582 244.1438 -0.5865 285.3114 285.8979 297.4697 244.9648 -0.5884 285.4426 286.0310 297.5984 245.7530 -0.5908 285.5762 286.1670 297.6982 246.5410 -0.5940 285.6897 286.2837 297.8025 247.3610 -0.5961 285.8036 286.3996 297.9229 248.1503 -0.6004 285.9265 286.5268 298.0469 248.9708 -0.6027 286.0500 286.6527 298.1605 249.7593 -0.6054 286.1540 286.7594 298.2776 250.5490 -0.6077 286.2755 286.8831 298.3970 251.3678 -0.6099 286.4150 287.0249 298.5166 252.1270 -0.6122 286.5281 287.1404 298.6422 252.9778 -0.6155 286.6258 287.2413 298.7702 253.7660 -0.6196 286.7513 287.3709 298.8953 254.5550 -0.6214 286.8743 287.4957 299.0170 255.3733 -0.6224 286.9863 287.6087 299.1490 256.1320 -0.6244 287.1065 287.7309 299.2401 256.9833 -0.6295 287.2438 287.8732 299.3443 257.7723 -0.6309 287.3592 287.9901 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