DTA measure 1pbupdown3 Date: 2025226:912 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.26 s Mass = 944.800 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2060 -1.1739 239.3583 240.5322 269.2461 2.0668 -1.1702 239.5681 240.7383 269.1976 2.8340 -1.1665 239.7532 240.9197 269.1535 3.6633 -1.1628 239.9552 241.1180 269.1019 4.4310 -1.1599 240.1384 241.2983 269.0481 5.2603 -1.1563 240.3406 241.4969 268.9914 6.0483 -1.1523 240.5321 241.6844 268.9342 6.8465 -1.1482 240.7299 241.8781 268.8792 7.6760 -1.1440 240.9370 242.0810 268.8161 8.4433 -1.1404 241.1247 242.2651 268.7573 9.3038 -1.1353 241.3380 242.4733 268.6894 10.0608 -1.1318 241.5207 242.6526 268.6283 10.8900 -1.1271 241.7138 242.8408 268.5579 11.6885 -1.1228 241.9065 243.0292 268.4857 12.4870 -1.1182 242.1008 243.2190 268.4206 13.3058 -1.1138 242.3037 243.4175 268.3488 14.0833 -1.1092 242.4884 243.5976 268.2772 14.9338 -1.1049 242.6844 243.7893 268.2029 15.6905 -1.1007 242.8597 243.9604 268.1382 16.5303 -1.0959 243.0593 244.1552 268.0640 17.3183 -1.0912 243.2476 244.3388 267.9946 18.1170 -1.0868 243.4367 244.5235 267.9314 18.9358 -1.0819 243.6305 244.7124 267.8668 19.7033 -1.0773 243.8061 244.8834 267.8066 20.5635 -1.0723 244.0035 245.0759 267.7395 21.3208 -1.0679 244.1781 245.2459 267.6839 22.1500 -1.0630 244.3678 245.4308 267.6281 22.9378 -1.0590 244.5454 245.6045 267.5767 23.7258 -1.0539 244.7222 245.7761 267.5269 24.5550 -1.0486 244.9090 245.9575 267.4753 25.3220 -1.0444 245.0809 246.1252 267.4314 26.1725 -1.0400 245.2700 246.3100 267.3923 26.9398 -1.0360 245.4402 246.4762 267.3574 27.7588 -1.0318 245.6221 246.6538 267.3217 28.5570 -1.0275 245.7989 246.8263 267.2982 29.3450 -1.0240 245.9728 246.9968 267.2774 30.1848 -1.0197 246.1543 247.1740 267.2567 30.9418 -1.0156 246.3180 247.3336 267.2474 31.7608 -1.0118 246.5000 247.5118 267.2449 32.5283 -1.0082 246.6675 247.6756 267.2474 33.3783 -1.0037 246.8519 247.8556 267.2595 34.1560 -0.9994 247.0218 248.0212 267.2749 34.9753 -0.9957 247.1942 248.1899 267.2979 35.7630 -0.9923 247.3605 248.3528 267.3279 36.5618 -0.9890 247.5251 248.5141 267.3682 37.3808 -0.9859 247.6937 248.6796 267.4086 38.1583 -0.9824 247.8542 248.8366 267.4560 39.0083 -0.9792 248.0346 249.0138 267.5190 39.7650 -0.9768 248.1902 249.1669 267.5811 40.6050 -0.9746 248.3633 249.3379 267.6530 41.3930 -0.9711 248.5287 249.4998 267.7300 42.1913 -0.9677 248.6936 249.6613 267.8169 43.0103 -0.9648 248.8617 249.8264 267.9172 43.7880 -0.9634 249.0220 249.9853 268.0149 44.6378 -0.9610 249.1966 250.1575 268.1377 45.3948 -0.9582 249.3461 250.3044 268.2501 46.2345 -0.9555 249.5143 250.4697 268.3827 47.0228 -0.9538 249.6688 250.6226 268.5217 47.8210 -0.9525 249.8250 250.7775 268.6708 48.6398 -0.9515 249.9879 250.9394 268.8338 49.4173 -0.9503 250.1434 251.0937 268.9915 50.2673 -0.9490 250.3172 251.2661 269.1789 51.0248 -0.9480 250.4722 251.4202 269.3487 51.8643 -0.9462 250.6385 251.5847 269.5436 52.6520 -0.9449 250.7939 251.7388 269.7339 53.4608 -0.9438 250.9566 251.9003 269.9372 54.2798 -0.9430 251.1163 252.0593 270.1509 55.0470 -0.9427 251.2740 252.2167 270.3548 55.8973 -0.9426 251.4442 252.3867 270.5914 56.6750 -0.9421 251.5999 252.5420 270.8117 57.4940 -0.9418 251.7631 252.7049 271.0486 58.2820 -0.9415 251.9173 252.8588 271.2911 59.0908 -0.9416 252.0673 253.0089 271.5410 59.9100 -0.9420 252.2274 253.1694 271.7933 60.6773 -0.9435 252.3764 253.3199 272.0372 61.5273 -0.9447 252.5427 253.4874 272.3126 62.2740 -0.9455 252.6851 253.6305 272.5630 63.1243 -0.9468 252.8471 253.7939 272.8526 63.8810 -0.9485 252.9930 253.9415 273.1112 64.7208 -0.9509 253.1609 254.1118 273.4074 65.5088 -0.9533 253.3095 254.2627 273.6856 66.3173 -0.9558 253.4672 254.4230 273.9726 67.1365 -0.9574 253.6252 254.5826 274.2674 67.9040 -0.9593 253.7766 254.7359 274.5427 68.7640 -0.9610 253.9424 254.9034 274.8544 69.5313 -0.9633 254.0869 255.0502 275.1408 70.3508 -0.9661 254.2431 255.2092 275.4472 71.1593 -0.9695 254.3856 255.3551 275.7461 71.9473 -0.9726 254.5375 255.5101 276.0370 72.7668 -0.9757 254.7014 255.6770 276.3360 73.5443 -0.9792 254.8550 255.8342 276.6228 74.3940 -0.9831 255.0239 256.0070 276.9314 75.1618 -0.9867 255.1757 256.1624 277.2167 75.9810 -0.9908 255.3323 256.3230 277.5179 76.7895 -0.9946 255.4869 256.4816 277.8105 77.5778 -0.9988 255.6363 256.6351 278.0958 78.3863 -1.0032 255.7931 256.7963 278.3863 79.1743 -1.0074 255.9443 256.9516 278.6668 79.9933 -1.0123 256.1033 257.1156 278.9565 80.7710 -1.0173 256.2569 257.2742 279.2262 81.6210 -1.0214 256.4184 257.4399 279.5204 82.3988 -1.0250 256.5703 257.5953 279.7897 83.2178 -1.0300 256.7310 257.7611 280.0590 84.0160 -1.0357 256.8915 257.9271 280.3194 84.8043 -1.0400 257.0470 258.0870 280.5776 85.5920 -1.0445 257.2009 258.2454 280.8270 86.3903 -1.0491 257.3583 258.4074 281.0765 87.2095 -1.0539 257.5269 258.5808 281.3273 87.9665 -1.0584 257.6795 258.7379 281.5574 88.8270 -1.0643 257.8529 258.9171 281.8096 89.5838 -1.0700 258.0038 259.0738 282.0281 90.4135 -1.0758 258.1741 259.2499 282.2601 91.2013 -1.0808 258.3297 259.4105 282.4813 91.9998 -1.0858 258.4879 259.5737 282.6984 92.8290 -1.0908 258.6461 259.7369 282.9147 93.5860 -1.0955 258.7951 259.8906 283.1053 94.4360 -1.1021 258.9640 260.0662 283.3144 95.2138 -1.1080 259.1210 260.2290 283.5031 96.0328 -1.1137 259.2801 260.3938 283.6917 96.8000 -1.1191 259.4348 260.5539 283.8677 97.6193 -1.1249 259.6019 260.7268 284.0507 98.4280 -1.1306 259.7636 260.8942 284.2194 99.2158 -1.1358 259.9207 261.0564 284.3800 100.0348 -1.1422 260.0892 261.2314 284.5427 100.8123 -1.1479 260.2453 261.3932 284.6945 101.6623 -1.1535 260.4160 261.5695 284.8542 102.3990 -1.1585 260.5717 261.7302 284.9813 103.2488 -1.1637 260.7462 261.9098 285.1266 104.0263 -1.1687 260.9048 262.0735 285.2540 104.8458 -1.1734 261.0721 262.2455 285.3803 105.6338 -1.1778 261.2361 262.4139 285.4946 106.4423 -1.1819 261.4042 262.5861 285.6081 107.2610 -1.1868 261.5728 262.7596 285.7162 108.0285 -1.1915 261.7314 262.9229 285.8117 108.8788 -1.1963 261.9097 263.1060 285.9111 109.6563 -1.2002 262.0671 263.2673 286.0019 110.4753 -1.2049 262.2365 263.4414 286.0897 111.2633 -1.2089 262.3942 263.6031 286.1689 112.0723 -1.2136 262.5570 263.7705 286.2463 112.8910 -1.2176 262.7263 263.9439 286.3216 113.6583 -1.2220 262.8871 264.1091 286.3845 114.5083 -1.2271 263.0667 264.2937 286.4517 115.2863 -1.2317 263.2261 264.4578 286.5071 116.1053 -1.2366 263.3894 264.6259 286.5664 116.8623 -1.2405 263.5455 264.7860 286.6132 117.7023 -1.2444 263.7185 264.9629 286.6577 118.4900 -1.2477 263.8803 265.1280 286.6978 119.2883 -1.2515 264.0444 265.2959 286.7378 120.1075 -1.2550 264.2172 265.4722 286.7732 120.9163 -1.2576 264.3824 265.6400 286.8115 121.7353 -1.2603 264.5491 265.8094 286.8383 122.4920 -1.2632 264.7039 265.9671 286.8647 123.3320 -1.2659 264.8750 266.1409 286.8939 124.1510 -1.2687 265.0429 266.3116 286.9228 124.9183 -1.2710 265.1980 266.4690 286.9409 125.7683 -1.2743 265.3704 266.6447 286.9629 126.5463 -1.2762 265.5320 266.8082 286.9788 127.3653 -1.2786 265.6998 266.9784 286.9959 128.1530 -1.2817 265.8594 267.1411 287.0168 128.9618 -1.2844 266.0236 267.3080 287.0308 129.7810 -1.2879 266.1875 267.4754 287.0445 130.5483 -1.2895 266.3412 267.6307 287.0562 131.3983 -1.2921 266.5140 267.8061 287.0659 132.1760 -1.2950 266.6670 267.9620 287.0737 132.9948 -1.2977 266.8333 268.1310 287.0819 133.7828 -1.2995 266.9885 268.2880 287.0895 134.5918 -1.3009 267.1477 268.4486 287.0935 135.4105 -1.3031 267.3081 268.6112 287.1007 136.1778 -1.3046 267.4562 268.7608 287.1115 137.0380 -1.3060 267.6267 268.9327 287.1232 137.8053 -1.3076 267.7750 269.0827 287.1282 138.6243 -1.3093 267.9342 269.2435 287.1443 139.4330 -1.3117 268.0873 269.3989 287.1520 140.2210 -1.3139 268.2424 269.5562 287.1657 141.0400 -1.3155 268.4010 269.7166 287.1776 141.8178 -1.3172 268.5497 269.8669 287.1929 142.6680 -1.3190 268.7138 270.0328 287.2150 143.4455 -1.3200 268.8637 270.1838 287.2358 144.2648 -1.3214 269.0203 270.3417 287.2630 145.0630 -1.3225 269.1736 270.4960 287.2961 145.8508 -1.3233 269.3277 270.6510 287.3286 146.6905 -1.3247 269.4885 270.8132 287.3642 147.4475 -1.3258 269.6421 270.9679 287.4022 148.2978 -1.3281 269.8033 271.1314 287.4546 149.0340 -1.3295 269.9466 271.2761 287.4965 149.8838 -1.3312 270.1096 271.4408 287.5490 150.6410 -1.3327 270.2527 271.5855 287.5991 151.4805 -1.3336 270.4129 271.7465 287.6622 152.2688 -1.3346 270.5626 271.8972 287.7251 153.0670 -1.3365 270.7128 272.0493 287.7914 153.8860 -1.3380 270.8697 272.2076 287.8622 154.6430 -1.3391 271.0131 272.3522 287.9343 155.4723 -1.3408 271.1684 272.5092 288.0154 156.2398 -1.3422 271.3122 272.6544 288.1016 157.0898 -1.3441 271.4673 272.8114 288.1971 157.8573 -1.3449 271.6069 272.9517 288.2886 158.6760 -1.3465 271.7546 273.1011 288.3911 159.4743 -1.3484 271.9004 273.2488 288.4920 160.2728 -1.3500 272.0524 273.4024 288.6010 161.1020 -1.3507 272.2051 273.5558 288.7171 161.8590 -1.3512 272.3417 273.6929 288.8255 162.7088 -1.3523 272.4967 273.8489 288.9565 163.4868 -1.3529 272.6423 273.9952 289.0802 164.3058 -1.3541 272.7945 274.1485 289.2180 165.0730 -1.3558 272.9323 274.2881 289.3499 165.8920 -1.3580 273.0794 274.4374 289.4915 166.7008 -1.3592 273.2233 274.5824 289.6392 167.4888 -1.3606 273.3645 274.7251 289.7859 168.3078 -1.3618 273.5071 274.8689 289.9466 169.0853 -1.3632 273.6493 275.0125 290.1076 169.9350 -1.3650 273.8058 275.1708 290.2838 170.7023 -1.3666 273.9486 275.3153 290.4471 171.5218 -1.3690 274.0948 275.4638 290.6327 172.3303 -1.3720 274.2366 275.6087 290.8137 173.1183 -1.3742 274.3759 275.7501 290.9983 173.9375 -1.3771 274.5258 275.9030 291.1920 174.7153 -1.3806 274.6640 276.0446 291.3796 175.5340 -1.3832 274.8152 276.1985 291.5826 176.3013 -1.3871 274.9523 276.3394 291.7746 177.1513 -1.3906 275.1045 276.4951 291.9941 177.9293 -1.3933 275.2461 276.6394 292.2000 178.7483 -1.3966 275.3942 276.7909 292.4186 179.5360 -1.3994 275.5335 276.9329 292.6276 180.3450 -1.4017 275.6767 277.0784 292.8406 181.1850 -1.4046 275.8270 277.2316 293.0697 181.9418 -1.4088 275.9624 277.3712 293.2819 182.7608 -1.4120 276.1127 277.5247 293.5110 183.5388 -1.4152 276.2543 277.6695 293.7281 184.3888 -1.4195 276.4062 277.8257 293.9715 185.1663 -1.4233 276.5490 277.9722 294.1941 185.9850 -1.4278 276.6973 278.1251 294.4277 186.7833 -1.4319 276.8427 278.2746 294.6619 187.5713 -1.4360 276.9870 278.4231 294.8900 188.4110 -1.4400 277.1335 278.5736 295.1377 189.1683 -1.4445 277.2611 278.7055 295.3630 190.0388 -1.4493 277.4129 278.8622 295.6191 190.7648 -1.4534 277.5416 278.9950 295.8263 191.6250 -1.4582 277.6944 279.1526 296.0726 192.3928 -1.4630 277.8314 279.2945 296.2918 193.2118 -1.4685 277.9737 279.4422 296.5325 194.0203 -1.4736 278.1185 279.5921 296.7676 194.8083 -1.4788 278.2647 279.7435 296.9936 195.6380 -1.4842 278.4146 279.8988 297.2281 196.4050 -1.4884 278.5511 280.0395 297.4425 197.2655 -1.4943 278.7085 280.2028 297.6918 198.0228 -1.4989 278.8403 280.3392 297.9086 198.8520 -1.5042 278.9931 280.4973 298.1417 199.6508 -1.5095 279.1397 280.6492 298.3601 200.4388 -1.5148 279.2805 280.7954 298.5776 201.2680 -1.5199 279.4299 280.9498 298.8039 202.0358 -1.5250 279.5688 281.0938 299.0125 202.8960 -1.5301 279.7202 281.2504 299.2392 203.6630 -1.5347 279.8615 281.3962 299.4371 204.4928 -1.5398 280.0167 281.5565 299.6517 205.2498 -1.5445 280.1552 281.6997 299.8415 206.0790 -1.5503 280.3042 281.8545 300.0488 206.8773 -1.5561 280.4520 282.0081 300.2444 207.6653 -1.5614 280.5950 282.1563 300.4287 208.5053 -1.5676 280.7463 282.3139 300.6248 209.2620 -1.5726 280.8817 282.4544 300.8062 210.1223 -1.5781 281.0426 282.6207 301.0053 210.8898 -1.5832 281.1834 282.7667 301.1829 211.7190 -1.5882 281.3363 282.9245 301.3697 212.5073 -1.5940 281.4806 283.0746 301.5404 213.2950 -1.5986 281.6270 283.2257 301.7068 214.1243 -1.6041 281.7832 283.3873 301.8836 214.8813 -1.6093 281.9259 283.5351 302.0345 215.7318 -1.6144 282.0811 283.6955 302.1988 216.4783 -1.6191 282.2229 283.8420 302.3414 217.3283 -1.6239 282.3768 284.0007 302.4995 218.0960 -1.6287 282.5182 284.1470 302.6403 218.9148 -1.6345 282.6713 284.3058 302.7853 219.7030 -1.6396 282.8182 284.4578 302.9283 220.5013 -1.6445 282.9696 284.6142 303.0632 221.3203 -1.6491 283.1324 284.7815 303.1943 222.0980 -1.6540 283.2840 284.9380 303.3213 222.9480 -1.6598 283.4492 285.1090 303.4559 223.7050 -1.6643 283.5940 285.2583 303.5696 224.5343 -1.6697 283.7494 285.4191 303.6933 225.3328 -1.6751 283.8980 285.5731 303.8055 226.1310 -1.6798 284.0458 285.7256 303.9154 226.9498 -1.6846 284.1994 285.8840 304.0233 227.7170 -1.6891 284.3450 286.0341 304.1210 228.5773 -1.6944 284.5068 286.2013 304.2285 229.3035 -1.6988 284.6434 286.3422 304.3217 230.1640 -1.7035 284.8076 286.5111 304.4203 230.9310 -1.7078 284.9512 286.6590 304.5062 231.7603 -1.7120 285.1070 286.8189 304.5958 232.5485 -1.7156 285.2547 286.9703 304.6793 233.3468 -1.7194 285.4074 287.1268 304.7584 234.1763 -1.7235 285.5623 287.2858 304.8409 234.9330 -1.7272 285.7023 287.4295 304.9107 235.7933 -1.7314 285.8687 287.6001 304.9905 236.5608 -1.7342 286.0118 287.7460 305.0578 237.3903 -1.7377 286.1675 287.9052 305.1258 238.1783 -1.7409 286.3196 288.0605 305.1887 238.9765 -1.7445 286.4730 288.2175 305.2448 239.8060 -1.7476 286.6341 288.3817 305.3057 240.5630 -1.7509 286.7801 288.5310 305.3646 241.4338 -1.7545 286.9442 288.6987 305.4306 242.1700 -1.7580 287.0820 288.8400 305.4841 243.0305 -1.7615 287.2484 289.0099 305.5433 243.7878 -1.7645 287.3914 289.1559 305.5973 244.6170 -1.7673 287.5440 289.3114 305.6529 245.4150 -1.7702 287.6976 289.4679 305.7067 246.2135 -1.7726 287.8470 289.6196 305.7570 247.0328 -1.7755 288.0034 289.7789 305.8105 247.8000 -1.7777 288.1435 289.9213 305.8604 248.6603 -1.7811 288.3047 290.0858 305.9139 249.4178 -1.7837 288.4460 290.2297 305.9604 250.2573 -1.7860 288.6044 290.3904 306.0102 251.0453 -1.7884 288.7551 290.5435 306.0587 251.8435 -1.7910 288.9052 290.6962 306.1118 252.6625 -1.7937 289.0544 290.8481 306.1690 253.4403 -1.7963 289.1931 290.9894 306.2219 254.2903 -1.7988 289.3501 291.1489 306.2775 255.0575 -1.8007 289.4876 291.2883 306.3310 255.8870 -1.8035 289.6384 291.4420 306.3862 256.6750 -1.8053 289.7786 291.5840 306.4415 257.4838 -1.8072 289.9290 291.7362 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