DTA measure 1pbupdown4 Date: 2025226:1025 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.81 s Mass = 944.800 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4805 -0.9329 216.6978 217.6307 209.6457 4.0939 -0.9343 216.6988 217.6331 209.7091 5.6966 -0.9352 216.7008 217.6360 209.7669 7.3046 -0.9359 216.7071 217.6431 209.8204 8.9283 -0.9367 216.7094 217.6462 209.8655 10.5260 -0.9387 216.7047 217.6434 209.9073 12.1340 -0.9385 216.7117 217.6502 209.9412 13.7423 -0.9385 216.7258 217.6643 209.9718 15.3453 -0.9394 216.7367 217.6760 210.0048 16.9583 -0.9404 216.7554 217.6958 210.0293 18.5613 -0.9414 216.7632 217.7046 210.0585 20.1746 -0.9420 216.7662 217.7082 210.0925 21.7826 -0.9421 216.7822 217.7243 210.1132 23.3908 -0.9423 216.7947 217.7371 210.1396 24.9989 -0.9424 216.8040 217.7464 210.1651 26.6068 -0.9429 216.8128 217.7557 210.1927 28.2096 -0.9426 216.8251 217.7676 210.2201 29.8231 -0.9426 216.8347 217.7773 210.2561 31.4261 -0.9419 216.8444 217.7863 210.2985 33.0341 -0.9423 216.8536 217.7959 210.3422 34.6581 -0.9417 216.8564 217.7981 210.3895 36.2661 -0.9410 216.8681 217.8091 210.4450 37.8791 -0.9412 216.8853 217.8265 210.5103 39.4871 -0.9415 216.8962 217.8377 210.5891 41.0901 -0.9406 216.9036 217.8443 210.6679 42.7034 -0.9404 216.9157 217.8560 210.7615 44.3063 -0.9403 216.9357 217.8760 210.8668 45.9299 -0.9397 216.9588 217.8984 210.9809 47.5383 -0.9395 216.9771 217.9167 211.1105 49.1463 -0.9400 216.9933 217.9332 211.2520 50.7439 -0.9406 217.0026 217.9432 211.4003 52.3520 -0.9399 217.0287 217.9686 211.5575 53.9600 -0.9397 217.0439 217.9836 211.7397 55.5683 -0.9397 217.0642 218.0039 211.9267 57.1761 -0.9407 217.0794 218.0201 212.1277 58.7946 -0.9420 217.1006 218.0426 212.3443 60.4081 -0.9431 217.1263 218.0693 212.5608 62.0111 -0.9455 217.1495 218.0950 212.7871 63.6244 -0.9473 217.1701 218.1174 213.0279 65.2273 -0.9479 217.1888 218.1367 213.2864 66.8351 -0.9492 217.2160 218.1652 213.5591 68.4431 -0.9521 217.2453 218.1973 213.8395 70.0619 -0.9542 217.2733 218.2275 214.1344 71.6751 -0.9564 217.3059 218.2623 214.4349 73.2781 -0.9599 217.3315 218.2914 214.7418 74.8914 -0.9630 217.3597 218.3228 215.0582 76.5045 -0.9650 217.3955 218.3605 215.3783 78.0919 -0.9675 217.4314 218.3990 215.6989 79.7155 -0.9691 217.4708 218.4399 216.0333 81.3391 -0.9711 217.5080 218.4791 216.3689 82.9423 -0.9741 217.5422 218.5163 216.7082 84.5556 -0.9779 217.5871 218.5650 217.0466 86.1588 -0.9818 217.6326 218.6145 217.3853 87.7720 -0.9861 217.6759 218.6620 217.7260 89.3749 -0.9891 217.7250 218.7141 218.0707 90.9830 -0.9926 217.7705 218.7631 218.4101 92.6116 -0.9981 217.8189 218.8170 218.7642 94.2196 -1.0032 217.8705 218.8736 219.1024 95.8225 -1.0077 217.9260 218.9337 219.4309 97.3891 -1.0122 217.9792 218.9914 219.7486 98.9611 -1.0165 218.0314 219.0479 220.0634 100.5431 -1.0213 218.0866 219.1079 220.3736 102.1203 -1.0263 218.1454 219.1717 220.6767 103.7176 -1.0308 218.2046 219.2354 220.9801 105.3155 -1.0350 218.2713 219.3063 221.2723 106.8976 -1.0380 218.3293 219.3673 221.5524 108.4904 -1.0416 218.3877 219.4292 221.8263 110.1140 -1.0452 218.4570 219.5022 222.1034 111.7168 -1.0483 218.5206 219.5688 222.3644 113.2991 -1.0521 218.5962 219.6483 222.6165 114.9021 -1.0561 218.6737 219.7298 222.8605 116.5155 -1.0592 218.7496 219.8088 223.0951 118.1131 -1.0623 218.8291 219.8914 223.3193 119.7264 -1.0654 218.9060 219.9715 223.5364 121.3293 -1.0683 218.9922 220.0605 223.7417 122.9219 -1.0718 219.0772 220.1490 223.9353 124.5455 -1.0735 219.1672 220.2407 224.1248 126.1539 -1.0758 219.2518 220.3276 224.3153 127.7620 -1.0786 219.3462 220.4248 224.4888 129.3493 -1.0809 219.4307 220.5115 224.6589 130.9470 -1.0833 219.5230 220.6063 224.8228 132.5499 -1.0853 219.6216 220.7070 224.9751 134.1528 -1.0861 219.7122 220.7983 225.1198 135.7608 -1.0862 219.8082 220.8944 225.2566 137.3635 -1.0861 219.9025 220.9887 225.3914 138.9718 -1.0864 219.9994 221.0858 225.5156 140.5798 -1.0869 220.0965 221.1834 225.6408 142.1881 -1.0873 220.1861 221.2734 225.7609 143.7959 -1.0878 220.2844 221.3722 225.8812 145.3989 -1.0877 220.3874 221.4751 226.0006 147.0121 -1.0878 220.4977 221.5855 226.1130 148.6149 -1.0864 220.6047 221.6911 226.2202 150.2386 -1.0866 220.7110 221.7977 226.3288 151.8466 -1.0862 220.8127 221.8989 226.4249 153.4546 -1.0844 220.9179 222.0023 226.5224 155.0628 -1.0836 221.0340 222.1175 226.6311 156.6656 -1.0834 221.1513 222.2347 226.7405 158.2789 -1.0816 221.2615 222.3430 226.8478 159.8766 -1.0797 221.3774 222.4572 226.9575 161.4951 -1.0766 221.4965 222.5731 227.0688 163.0930 -1.0744 221.6031 222.6775 227.1829 164.7061 -1.0721 221.7154 222.7874 227.3058 166.3040 -1.0701 221.8214 222.8915 227.4310 167.9015 -1.0692 221.9264 222.9957 227.5576 169.5044 -1.0672 222.0351 223.1023 227.6938 171.1228 -1.0656 222.1427 223.2083 227.8386 172.7153 -1.0641 222.2538 223.3179 227.9903 174.3389 -1.0615 222.3718 223.4334 228.1464 175.9416 -1.0593 222.4937 223.5530 228.3122 177.5551 -1.0571 222.6195 223.6766 228.4845 179.1580 -1.0540 222.7357 223.7897 228.6599 180.7713 -1.0509 222.8569 223.9079 228.8384 182.3743 -1.0484 222.9764 224.0248 229.0244 183.9823 -1.0461 223.0916 224.1376 229.2238 185.6060 -1.0446 223.2179 224.2625 229.4347 187.2090 -1.0436 223.3479 224.3915 229.6493 188.8221 -1.0414 223.4688 224.5102 229.8644 190.4251 -1.0399 223.5919 224.6318 230.0824 192.0384 -1.0387 223.7090 224.7478 230.3089 193.6363 -1.0374 223.8271 224.8646 230.5387 195.2391 -1.0363 223.9524 224.9888 230.7853 196.8318 -1.0357 224.0755 225.1112 231.0355 198.4501 -1.0353 224.2004 225.2357 231.3014 200.0374 -1.0346 224.3226 225.3572 231.5689 201.6456 -1.0351 224.4525 225.4876 231.8365 203.2536 -1.0352 224.5885 225.6237 232.1089 204.8564 -1.0353 224.7217 225.7570 232.3855 206.4696 -1.0355 224.8640 225.8995 232.6613 208.0569 -1.0362 225.0076 226.0439 232.9391 209.6700 -1.0372 225.1381 226.1753 233.2237 211.2730 -1.0376 225.2715 226.3091 233.5082 212.8966 -1.0377 225.4131 226.4508 233.7941 214.5046 -1.0387 225.5499 226.5885 234.0840 216.0921 -1.0390 225.6819 226.7209 234.3684 217.7055 -1.0394 225.8189 226.8583 234.6490 219.3085 -1.0391 225.9608 227.0000 234.9303 220.9219 -1.0410 226.1118 227.1528 235.2196 222.5250 -1.0420 226.2546 227.2966 235.5051 224.1383 -1.0425 226.4010 227.4435 235.7877 225.7411 -1.0444 226.5408 227.5853 236.0644 227.3439 -1.0459 226.6795 227.7254 236.3368 228.9469 -1.0477 226.8334 227.8812 236.6122 230.5443 -1.0493 226.9864 228.0356 236.8763 232.1370 -1.0495 227.1355 228.1850 237.1464 233.7398 -1.0505 227.2848 228.3353 237.4173 235.3529 -1.0518 227.4368 228.4886 237.6817 236.9559 -1.0528 227.5914 228.6443 237.9348 238.5589 -1.0533 227.7486 228.8019 238.1825 240.1824 -1.0537 227.9058 228.9595 238.4348 241.7905 -1.0555 228.0633 229.1188 238.6764 243.3776 -1.0571 228.2174 229.2746 238.9059 244.9908 -1.0583 228.3695 229.4278 239.1360 246.5988 -1.0598 228.5214 229.5812 239.3538 248.2071 -1.0624 228.6848 229.7471 239.5666 249.8204 -1.0635 228.8502 229.9137 239.7769 251.4233 -1.0653 229.0149 230.0802 239.9928 253.0470 -1.0663 229.1824 230.2487 240.2066 254.6551 -1.0659 229.3482 230.4141 240.4031 256.2578 -1.0672 229.5124 230.5796 240.5889 257.8609 -1.0684 229.6797 230.7481 240.7743 259.4639 -1.0692 229.8464 230.9157 240.9554 261.0563 -1.0691 230.0140 231.0831 241.1312 262.6540 -1.0705 230.1798 231.2503 241.3013 264.2568 -1.0720 230.3509 231.4229 241.4641 265.8804 -1.0736 230.5310 231.6046 241.6233 267.4833 -1.0744 230.6946 231.7691 241.7780 269.0914 -1.0733 230.8628 231.9361 241.9339 270.6941 -1.0738 231.0412 232.1150 242.0875 272.3073 -1.0752 231.2154 232.2906 242.2361 273.9100 -1.0761 231.3828 232.4590 242.3913 275.5234 -1.0761 231.5539 232.6300 242.5493 277.1470 -1.0767 231.7295 232.8062 242.7043 278.7496 -1.0774 231.9003 232.9776 242.8550 280.3629 -1.0771 232.0705 233.1476 242.9981 281.9655 -1.0766 232.2345 233.3111 243.1386 283.5736 -1.0765 232.4073 233.4838 243.2919 285.1819 -1.0758 232.5758 233.6516 243.4460 286.7901 -1.0756 232.7469 233.8225 243.5895 288.4136 -1.0752 232.9212 233.9965 243.7439 290.0165 -1.0735 233.0969 234.1704 243.9002 291.6140 -1.0719 233.2726 234.3445 244.0552 293.2170 -1.0708 233.4529 234.5237 244.2109 294.8301 -1.0698 233.6347 234.7045 244.3773 296.4123 -1.0687 233.8114 234.8801 244.5375 298.0153 -1.0669 233.9824 235.0493 244.7003 299.6231 -1.0660 234.1618 235.2277 244.8677 301.2468 -1.0663 234.3453 235.4116 245.0479 302.8546 -1.0660 234.5192 235.5851 245.2296 304.4625 -1.0649 234.6935 235.7583 245.4174 306.0654 -1.0630 234.8724 235.9354 245.6006 307.6630 -1.0622 235.0526 236.1147 245.7917 309.2659 -1.0625 235.2357 236.2981 245.9924 310.8741 -1.0626 235.4249 236.4875 246.2018 312.4821 -1.0622 235.6130 236.6752 246.4104 314.0950 -1.0624 235.7942 236.8566 246.6253 315.7034 -1.0628 235.9648 237.0276 246.8429 317.3115 -1.0631 236.1415 237.2047 247.0626 318.9195 -1.0633 236.3190 237.3823 247.2830 320.5274 -1.0642 236.5054 237.5696 247.5132 322.1096 -1.0644 236.6876 237.7520 247.7375 323.7230 -1.0649 236.8724 237.9373 247.9697 325.3260 -1.0646 237.0568 238.1214 248.2047 326.9081 -1.0657 237.2361 238.3019 248.4412 328.5211 -1.0669 237.4197 238.4866 248.6890 330.1345 -1.0671 237.6036 238.6707 248.9410 331.7476 -1.0682 237.7957 238.8639 249.1994 333.3504 -1.0701 237.9843 239.0543 249.4522 334.9481 -1.0712 238.1658 239.2370 249.7117 336.5560 -1.0709 238.3500 239.4209 249.9687 338.1589 -1.0726 238.5352 239.6078 250.2240 339.7720 -1.0751 238.7204 239.7954 250.4949 341.3749 -1.0782 238.9034 239.9816 250.7592 342.9985 -1.0820 239.0975 240.1795 251.0200 344.6065 -1.0850 239.2970 240.3820 251.2873 346.1990 -1.0885 239.4926 240.5811 251.5432 347.8073 -1.0917 239.6833 240.7751 251.8014 349.4203 -1.0947 239.8742 240.9689 252.0652 351.0283 -1.0986 240.0609 241.1595 252.3291 352.6364 -1.1037 240.2549 241.3586 252.5851 354.2340 -1.1064 240.4445 241.5509 252.8419 355.8528 -1.1102 240.6407 241.7509 253.0979 357.4504 -1.1144 240.8322 241.9466 253.3466 359.0638 -1.1174 241.0289 242.1463 253.5926 360.6459 -1.1198 241.2258 242.3455 253.8346 362.2488 -1.1227 241.4237 242.5464 254.0723 363.8620 -1.1255 241.6241 242.7496 254.3134 365.4650 -1.1287 241.8242 242.9529 254.5481 367.0729 -1.1312 242.0192 243.1505 254.7810 368.6965 -1.1337 242.2197 243.3534 255.0166 370.2995 -1.1357 242.4210 243.5567 255.2437 371.9126 -1.1373 242.6283 243.7656 255.4630 373.5154 -1.1404 242.8238 243.9642 255.6882 375.1285 -1.1443 243.0180 244.1623 255.9011 376.7315 -1.1481 243.2217 244.3698 256.1058 378.3396 -1.1510 243.4249 244.5758 256.3139 379.9631 -1.1538 243.6273 244.7812 256.5180 381.5661 -1.1565 243.8335 244.9900 256.7167 383.1795 -1.1585 244.0387 245.1972 256.9151 384.7824 -1.1593 244.2362 245.3956 257.1103 386.3955 -1.1603 244.4418 245.6020 257.3023 387.9933 -1.1621 244.6446 245.8067 257.4891 389.5754 -1.1630 244.8465 246.0095 257.6655 391.1784 -1.1648 245.0547 246.2194 257.8406 392.8019 -1.1662 245.2666 246.4329 258.0244 394.4044 -1.1658 245.4721 246.6379 258.1976 396.0126 -1.1671 245.6756 246.8427 258.3749 397.6106 -1.1701 245.8791 247.0492 258.5503 399.2135 -1.1731 246.0814 247.2545 258.7256 400.8164 -1.1751 246.2829 247.4579 258.9026 402.4299 -1.1745 246.4896 247.6640 259.0740 404.0328 -1.1749 246.6998 247.8747 259.2419 405.6563 -1.1769 246.9225 248.0994 259.4098 407.2645 -1.1781 247.1302 248.3082 259.5747 408.8675 -1.1800 247.3375 248.5175 259.7397 410.4861 -1.1818 247.5523 248.7341 259.9052 412.0943 -1.1842 247.7622 248.9464 260.0712 413.7024 -1.1869 247.9689 249.1557 260.2326 415.2948 -1.1889 248.1710 249.3599 260.3980 416.9030 -1.1909 248.3848 249.5757 260.5748 418.5110 -1.1920 248.5927 249.7847 260.7481 420.1346 -1.1935 248.8040 249.9975 260.9184 421.7428 -1.1968 249.0104 250.2071 261.0923 423.3459 -1.1986 249.2147 250.4133 261.2673 424.9594 -1.1988 249.4238 250.6225 261.4468 426.5723 -1.1990 249.6331 250.8321 261.6293 428.1753 -1.1998 249.8356 251.0354 261.8181 429.7834 -1.2003 250.0367 251.2370 262.0064 431.4070 -1.2011 250.2496 251.4507 262.1994 433.0151 -1.2006 250.4566 251.6572 262.4008 434.6235 -1.2018 250.6613 251.8630 262.6089 436.2369 -1.2035 250.8677 252.0712 262.8114 437.8396 -1.2069 251.0786 252.2854 263.0165 439.4526 -1.2090 251.2843 252.4933 263.2291 441.0556 -1.2098 251.4893 252.6990 263.4408 442.6795 -1.2121 251.7040 252.9162 263.6614 444.2925 -1.2130 251.9127 253.1257 263.8814 445.8954 -1.2145 252.1267 253.3412 264.1076 447.5084 -1.2172 252.3388 253.5560 264.3392 449.1113 -1.2185 252.5492 253.7677 264.5763 450.7194 -1.2211 252.7585 253.9796 264.8206 452.3274 -1.2242 252.9706 254.1948 265.0679 453.9459 -1.2272 253.1828 254.4099 265.3097 455.5591 -1.2306 253.3975 254.6281 265.5597 457.1621 -1.2335 253.6043 254.8379 265.8072 458.7754 -1.2362 253.8091 255.0453 266.0589 460.3784 -1.2401 254.0206 255.2607 266.3148 461.9915 -1.2446 254.2367 255.4814 266.5674 463.5998 -1.2488 254.4538 255.7025 266.8208 465.2231 -1.2524 254.6707 255.9231 267.0772 466.8261 -1.2551 254.8704 256.1254 267.3249 468.4395 -1.2581 255.0717 256.3298 267.5791 470.0423 -1.2622 255.2823 256.5445 267.8254 471.6400 -1.2662 255.4979 256.7642 268.0737 473.2533 -1.2699 255.7137 256.9837 268.3213 474.8563 -1.2733 255.9273 257.2007 268.5697 476.4643 -1.2778 256.1410 257.4188 268.8187 478.0880 -1.2819 256.3554 257.6373 269.0652 479.7013 -1.2853 256.5704 257.8557 269.3096 481.3039 -1.2899 256.7892 258.0791 269.5484 482.9171 -1.2940 257.0097 258.3037 269.7874 484.5201 -1.2960 257.2245 258.5205 270.0191 486.1334 -1.2992 257.4483 258.7475 270.2491 487.7364 -1.3018 257.6595 258.9613 270.4736 489.3600 -1.3042 257.8738 259.1780 270.7056 490.9683 -1.3068 258.0914 259.3982 270.9314 492.5711 -1.3098 258.3074 259.6172 271.1643 494.1635 -1.3132 258.5169 259.8301 271.3865 495.7510 -1.3182 258.7313 260.0495 271.5971 497.3281 -1.3217 258.9490 260.2708 271.8042 498.9255 -1.3260 259.1637 260.4897 272.0156 500.5078 -1.3293 259.3739 260.7032 272.2265 502.0955 -1.3328 259.5869 260.9196 272.4270 503.7139 -1.3372 259.8031 261.1403 272.6319 505.3115 -1.3405 260.0159 261.3564 272.8298 506.9196 -1.3438 260.2343 261.5781 273.0288 508.5225 -1.3460 260.4503 261.7963 273.2217 510.1253 -1.3498 260.6661 262.0158 273.4186 511.7388 -1.3529 260.8854 262.2383 273.6189 513.3414 -1.3560 261.0980 262.4540 273.8067 514.9649 -1.3591 261.3173 262.6765 273.9937 516.5730 -1.3625 261.5358 262.8983 274.1830 518.1759 -1.3663 261.7657 263.1320 274.3727 519.7891 -1.3701 261.9939 263.3640 274.5601 521.3919 -1.3732 262.2150 263.5882 274.7454 523.0050 -1.3764 262.4401 263.8165 274.9312 524.6080 -1.3790 262.6611 264.0400 275.1111 526.2316 -1.3809 262.8843 264.2652 275.2935 527.8291 -1.3820 263.1041 264.4861 275.4708 529.4165 -1.3848 263.3191 264.7039 275.6476 531.0298 -1.3881 263.5378 264.9259 275.8275 532.6276 -1.3892 263.7521 265.1413 275.9990 534.2255 -1.3903 263.9635 265.3538 276.1664 535.8335 -1.3944 264.1893 265.5838 276.3447 537.4414 -1.3976 264.4185 265.8161 276.5254 539.0650 -1.4027 264.6438 266.0464 276.7006 540.6678 -1.4064 264.8627 266.2691 276.8768 542.2810 -1.4105 265.0870 266.4975 277.0601 543.8839 -1.4150 265.3060 266.7211 277.2487 545.4916 -1.4181 265.5226 266.9407 277.4266 547.0999 -1.4201 265.7416 267.1616 277.6120 548.7079 -1.4238 265.9590 267.3828 277.7963 550.3314 -1.4269 266.1815 267.6084 277.9873 551.9343 -1.4315 266.4014 267.8329 278.1707 553.5474 -1.4351 266.6230 268.0581 278.3589 555.1606 -1.4378 266.8465 268.2843 278.5502 556.7634 -1.4410 267.0650 268.5059 278.7528 558.3714 -1.4440 267.2820 268.7261 278.9487 559.9740 -1.4475 267.4979 268.9454 279.1537 561.5718 -1.4503 267.7170 269.1673 279.3596 563.1800 -1.4529 267.9334 269.3863 279.5657 564.7828 -1.4560 268.1534 269.6093 279.7770 566.3856 -1.4589 268.3733 269.8323 279.9963 567.9989 -1.4620 268.5975 270.0595 280.2188 569.5966 -1.4645 268.8169 270.2814 280.4326 571.2096 -1.4674 269.0367 270.5041 280.6510 572.8126 -1.4692 269.2558 270.7250 280.8649 574.4365 -1.4717 269.4782 270.9500 281.0859 576.0290 -1.4745 269.6890 271.1635 281.3063 577.6370 -1.4766 269.9034 271.3800 281.5430 579.2451 -1.4792 270.1207 271.5998 281.7763 580.8481 -1.4829 270.3416 271.8245 282.0061 582.4616 -1.4868 270.5632 272.0500 282.2402 584.0644 -1.4899 270.7811 272.2710 282.4784 585.6726 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431.4447 428.4739 1699.6789 -5.1383 426.5292 431.6675 428.6712 1701.2764 -5.1435 426.7462 431.8897 428.8649 1702.9000 -5.1487 426.9733 432.1220 429.0668 1704.5029 -5.1551 427.1914 432.3465 429.2612 1706.1160 -5.1610 427.4162 432.5772 429.4697 1707.7189 -5.1681 427.6358 432.8039 429.6773 1709.3319 -5.1736 427.8613 433.0349 429.8807 1710.9346 -5.1791 428.0878 433.2669 430.0908 1712.5426 -5.1848 428.3122 433.4970 430.3031 1714.1660 -5.1912 428.5362 433.7274 430.5157 1715.7686 -5.1979 428.7534 433.9513 430.7347 1717.3821 -5.2050 428.9694 434.1745 430.9575 1718.9849 -5.2113 429.1915 434.4028 431.1768 1720.5981 -5.2176 429.4127 434.6303 431.4001 1722.2013 -5.2239 429.6345 434.8584 431.6278 1723.8093 -5.2305 429.8549 435.0854 431.8587