DTA measure 3pbupdown3 Date: 2025226:941 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1647.97 s Mass = 944.800 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3424 -5.0999 436.8577 441.9576 419.7441 3.9340 -5.1049 436.9021 442.0070 419.7601 5.5358 -5.1112 436.9482 442.0594 419.8131 7.1325 -5.1177 436.9918 442.1095 419.9036 8.7398 -5.1247 437.0287 442.1535 420.0272 10.3573 -5.1314 437.0694 442.2008 420.1736 11.9595 -5.1390 437.0957 442.2347 420.3464 13.5511 -5.1476 437.1225 442.2701 420.5451 15.1533 -5.1574 437.1517 442.3091 420.7684 16.7553 -5.1680 437.1795 442.3476 421.0020 18.3623 -5.1793 437.1969 442.3762 421.2467 19.9694 -5.1900 437.2229 442.4130 421.4979 21.5766 -5.2016 437.2443 442.4459 421.7523 23.1838 -5.2133 437.2708 442.4841 422.0119 24.7909 -5.2255 437.2904 442.5159 422.2765 26.3981 -5.2373 437.3179 442.5551 422.5276 28.0053 -5.2492 437.3457 442.5948 422.7607 29.6074 -5.2611 437.3701 442.6312 422.9772 31.2198 -5.2724 437.3983 442.6707 423.1836 32.8066 -5.2854 437.4243 442.7096 423.3693 34.4189 -5.2984 437.4487 442.7471 423.5351 36.0208 -5.3115 437.4740 442.7855 423.6800 37.6436 -5.3239 437.5044 442.8283 423.8103 39.2510 -5.3346 437.5403 442.8748 423.9151 40.8533 -5.3463 437.5748 442.9210 423.9852 42.4658 -5.3568 437.6033 442.9601 424.0349 44.0678 -5.3668 437.6316 442.9984 424.0566 45.6803 -5.3752 437.6602 443.0354 424.0532 47.2824 -5.3835 437.6942 443.0777 424.0265 48.9051 -5.3927 437.7282 443.1209 423.9655 50.5125 -5.4011 437.7573 443.1584 423.8793 52.1145 -5.4097 437.7874 443.1971 423.7666 53.7113 -5.4177 437.8280 443.2456 423.6198 55.3238 -5.4245 437.8553 443.2797 423.4451 56.9309 -5.4316 437.8788 443.3104 423.2491 58.5381 -5.4369 437.9076 443.3445 423.0419 60.1503 -5.4420 437.9287 443.3707 422.8112 61.7678 -5.4463 437.9501 443.3964 422.5502 63.3751 -5.4494 437.9748 443.4242 422.2775 64.9720 -5.4525 437.9949 443.4474 421.9899 66.5741 -5.4554 438.0124 443.4678 421.6888 68.1709 -5.4571 438.0316 443.4887 421.3672 69.7730 -5.4584 438.0482 443.5066 421.0305 71.3750 -5.4599 438.0567 443.5166 420.6725 72.9668 -5.4607 438.0627 443.5235 420.3004 74.5793 -5.4608 438.0692 443.5300 419.9214 76.1865 -5.4599 438.0803 443.5402 419.5258 77.7885 -5.4588 438.0864 443.5452 419.1308 79.3908 -5.4568 438.0899 443.5466 418.7197 81.0031 -5.4543 438.0810 443.5353 418.2971 82.5999 -5.4524 438.0749 443.5273 417.8810 84.1969 -5.4497 438.0683 443.5181 417.4547 85.7985 -5.4482 438.0646 443.5128 417.0259 87.4213 -5.4462 438.0479 443.4941 416.5780 89.0336 -5.4431 438.0293 443.4724 416.1379 90.6354 -5.4397 438.0043 443.4441 415.6931 92.2323 -5.4360 437.9700 443.4060 415.2496 93.8448 -5.4324 437.9339 443.3663 414.8068 95.4518 -5.4287 437.8884 443.3172 414.3609 97.0590 -5.4251 437.8536 443.2788 413.9221 98.6663 -5.4215 437.8057 443.2272 413.4888 100.2890 -5.4176 437.7537 443.1712 413.0567 101.8910 -5.4139 437.6950 443.1089 412.6327 103.5035 -5.4104 437.6335 443.0439 412.2135 105.1058 -5.4069 437.5706 442.9774 411.8141 106.7180 -5.4029 437.5027 442.9056 411.4212 108.3203 -5.3995 437.4277 442.8273 411.0489 109.9328 -5.3966 437.3518 442.7484 410.6795 111.5555 -5.3934 437.2763 442.6697 410.3127 113.1628 -5.3907 437.1850 442.5757 409.9693 114.7650 -5.3872 437.0990 442.4863 409.6403 116.3774 -5.3849 437.0169 442.4018 409.3260 117.9795 -5.3838 436.9326 442.3163 409.0206 119.5919 -5.3822 436.8369 442.2191 408.7249 121.1939 -5.3808 436.7351 442.1160 408.4426 122.8219 -5.3798 436.6241 442.0039 408.1731 124.4290 -5.3770 436.5154 441.8924 407.9243 126.0361 -5.3751 436.4070 441.7820 407.6894 127.6228 -5.3740 436.2959 441.6699 407.4695 129.2251 -5.3742 436.1770 441.5512 407.2666 130.8271 -5.3742 436.0667 441.4409 407.0780 132.4343 -5.3748 435.9492 441.3241 406.9089 134.0313 -5.3749 435.8259 441.2009 406.7458 135.6175 -5.3750 435.7111 441.0861 406.5952 137.2403 -5.3757 435.5838 440.9596 406.4600 138.8424 -5.3761 435.4511 440.8271 406.3363 140.4496 -5.3767 435.3164 440.6932 406.2262 142.0518 -5.3782 435.1848 440.5630 406.1234 143.6536 -5.3795 435.0537 440.4332 406.0280 145.2504 -5.3810 434.9232 440.3042 405.9431 146.8524 -5.3837 434.7892 440.1729 405.8615 148.4594 -5.3849 434.6572 440.0421 405.7868 150.0821 -5.3874 434.5188 439.9062 405.7147 151.6840 -5.3900 434.3830 439.7730 405.6548 153.2963 -5.3922 434.2452 439.6374 405.5924 154.8983 -5.3936 434.1095 439.5031 405.5413 156.4951 -5.3956 433.9737 439.3693 405.4811 158.0970 -5.3973 433.8359 439.2332 405.4193 159.7044 -5.3994 433.6997 439.0991 405.3626 161.3115 -5.4019 433.5684 438.9703 405.3060 162.9291 -5.4049 433.4258 438.8307 405.2477 164.5414 -5.4060 433.2808 438.6868 405.1804 166.1435 -5.4077 433.1358 438.5435 405.1142 167.7558 -5.4090 432.9934 438.4024 405.0348 169.3633 -5.4121 432.8579 438.2700 404.9492 170.9550 -5.4144 432.7175 438.1319 404.8618 172.5621 -5.4165 432.5774 437.9938 404.7736 174.1696 -5.4181 432.4423 437.8604 404.6789 175.7873 -5.4202 432.2912 437.7114 404.5661 177.3995 -5.4206 432.1485 437.5691 404.4466 179.0120 -5.4216 432.0135 437.4351 404.3250 180.6140 -5.4217 431.8722 437.2939 404.1899 182.2264 -5.4213 431.7334 437.1547 404.0413 183.8285 -5.4210 431.5995 437.0205 403.8847 185.4359 -5.4206 431.4655 436.8861 403.7190 187.0481 -5.4207 431.3241 436.7448 403.5375 188.6554 -5.4215 431.1817 436.6032 403.3505 190.2629 -5.4225 431.0411 436.4636 403.1535 191.8701 -5.4217 430.9071 436.3289 402.9522 193.4721 -5.4205 430.7742 436.1947 402.7449 195.0689 -5.4189 430.6355 436.0544 402.5377 196.6816 -5.4171 430.4947 435.9118 402.3174 198.2784 -5.4157 430.3565 435.7722 402.0877 199.8961 -5.4145 430.2206 435.6351 401.8445 201.4876 -5.4133 430.0786 435.4919 401.5956 203.0896 -5.4103 429.9377 435.3480 401.3418 204.6968 -5.4077 429.7869 435.1946 401.0869 206.2988 -5.4058 429.6405 435.0463 400.8203 207.9010 -5.4025 429.5014 434.9039 400.5531 209.5133 -5.3992 429.3616 434.7608 400.2788 211.1151 -5.3963 429.2137 434.6100 400.0038 212.7379 -5.3920 429.0532 434.4452 399.7246 214.3349 -5.3888 428.9029 434.2916 399.4444 215.9473 -5.3856 428.7517 434.1372 399.1527 217.5493 -5.3816 428.6026 433.9843 398.8694 219.1618 -5.3778 428.4525 433.8303 398.5816 220.7640 -5.3732 428.2901 433.6633 398.2909 222.3714 -5.3688 428.1308 433.4996 398.0025 223.9941 -5.3651 427.9721 433.3372 397.7072 225.5960 -5.3611 427.8220 433.1831 397.4129 227.2083 -5.3562 427.6673 433.0234 397.1134 228.8105 -5.3511 427.5116 432.8627 396.8212 230.4229 -5.3472 427.3489 432.6960 396.5291 232.0250 -5.3421 427.1835 432.5256 396.2395 233.6323 -5.3372 427.0186 432.3558 395.9498 235.2549 -5.3337 426.8566 432.1903 395.6599 236.8569 -5.3300 426.6847 432.0146 395.3710 238.4693 -5.3252 426.5146 431.8398 395.0954 240.0713 -5.3208 426.3424 431.6632 394.8236 241.6835 -5.3147 426.1732 431.4880 394.5520 243.2855 -5.3094 426.0000 431.3094 394.2781 244.8824 -5.3052 425.8303 431.1355 394.0082 246.4896 -5.2995 425.6564 430.9559 393.7510 248.1121 -5.2945 425.4745 430.7690 393.4953 249.7246 -5.2895 425.2990 430.5885 393.2350 251.3264 -5.2850 425.1258 430.4109 392.9885 252.9389 -5.2805 424.9421 430.2226 392.7455 254.5255 -5.2760 424.7592 430.0352 392.5182 256.1380 -5.2708 424.5834 429.8542 392.2926 257.7403 -5.2658 424.4129 429.6786 392.0702 259.3371 -5.2615 424.2333 429.4948 391.8580 260.9549 -5.2570 424.0517 429.3087 391.6395 262.5520 -5.2524 423.8714 429.1238 391.4350 264.1594 -5.2478 423.6924 428.9402 391.2294 265.7561 -5.2438 423.5093 428.7531 391.0355 267.3429 -5.2397 423.3298 428.5696 390.8362 268.9554 -5.2356 423.1395 428.3751 390.6480 270.5521 -5.2316 422.9520 428.1836 390.4663 272.1594 -5.2274 422.7620 427.9895 390.2909 273.7616 -5.2229 422.5732 427.7960 390.1206 275.3690 -5.2183 422.3815 427.5998 389.9475 276.9763 -5.2129 422.1946 427.4076 389.7789 278.5834 -5.2076 422.0020 427.2096 389.6170 280.1859 -5.2042 421.8101 427.0143 389.4550 281.7976 -5.2025 421.6251 426.8276 389.2960 283.3996 -5.1994 421.4363 426.6357 389.1329 285.0070 -5.1958 421.2388 426.4346 388.9785 286.6299 -5.1926 421.0479 426.2405 388.8266 288.2371 -5.1896 420.8613 426.0509 388.6711 289.8289 -5.1862 420.6721 425.8583 388.5119 291.4311 -5.1831 420.4860 425.6690 388.3562 293.0434 -5.1790 420.2986 425.4776 388.1971 294.6455 -5.1761 420.1154 425.2915 388.0405 296.2528 -5.1728 419.9277 425.1005 387.8888 297.8599 -5.1693 419.7440 424.9133 387.7379 299.4826 -5.1659 419.5548 424.7207 387.5769 301.0900 -5.1631 419.3680 424.5311 387.4229 302.6921 -5.1600 419.1768 424.3368 387.2650 304.3045 -5.1561 418.9782 424.1344 387.0972 305.9064 -5.1528 418.7908 423.9436 386.9282 307.5138 -5.1493 418.6023 423.7516 386.7601 309.1263 -5.1454 418.4102 423.5555 386.5885 310.7489 -5.1419 418.2135 423.3554 386.4131 312.3561 -5.1404 418.0221 423.1625 386.2456 313.9636 -5.1380 417.8358 422.9738 386.0710 315.5710 -5.1341 417.6519 422.7859 385.8912 317.1780 -5.1299 417.4717 422.6016 385.7070 318.7901 -5.1257 417.2904 422.4161 385.5148 320.3924 -5.1219 417.1032 422.2251 385.3276 322.0153 -5.1181 416.9203 422.0384 385.1259 323.6173 -5.1142 416.7350 421.8492 384.9267 325.2144 -5.1103 416.5426 421.6529 384.7327 326.8063 -5.1048 416.3543 421.4592 384.5323 328.4081 -5.0997 416.1657 421.2654 384.3258 330.0103 -5.0945 415.9778 421.0724 384.1111 331.6124 -5.0898 415.7938 420.8836 383.8910 333.2145 -5.0840 415.6104 420.6944 383.6761 334.8321 -5.0801 415.4182 420.4983 383.4584 336.4394 -5.0760 415.2285 420.3045 383.2433 338.0465 -5.0721 415.0468 420.1189 383.0224 339.6538 -5.0679 414.8630 419.9309 382.8016 341.2556 -5.0640 414.6847 419.7487 382.5765 342.8581 -5.0591 414.4939 419.5530 382.3571 344.4653 -5.0538 414.3026 419.3564 382.1354 346.0880 -5.0489 414.1083 419.1572 381.9047 347.6798 -5.0445 413.9201 418.9646 381.6802 349.2869 -5.0391 413.7321 418.7713 381.4504 350.8940 -5.0345 413.5421 418.5767 381.2154 352.5011 -5.0289 413.3509 418.3798 380.9877 354.1136 -5.0236 413.1551 418.1787 380.7585 355.7154 -5.0178 412.9627 417.9805 380.5285 357.3228 -5.0127 412.7712 417.7839 380.2945 358.9454 -5.0062 412.5847 417.5909 380.0654 360.5370 -5.0008 412.3926 417.3934 379.8373 362.1441 -4.9954 412.1973 417.1928 379.6016 363.7565 -4.9893 412.0088 416.9981 379.3631 365.3584 -4.9833 411.8137 416.7970 379.1251 366.9709 -4.9780 411.6096 416.5876 378.8855 368.5731 -4.9716 411.4165 416.3880 378.6542 370.1854 -4.9643 411.2205 416.1848 378.4240 371.7928 -4.9594 411.0288 415.9881 378.1930 373.4050 -4.9530 410.8360 415.7890 377.9539 375.0121 -4.9468 410.6471 415.5939 377.7217 376.6194 -4.9406 410.4548 415.3954 377.4865 378.2318 -4.9339 410.2650 415.1990 377.2441 379.8338 -4.9284 410.0684 414.9967 377.0091 381.4410 -4.9231 409.8672 414.7903 376.7809 383.0380 -4.9179 409.6748 414.5927 376.5511 384.6451 -4.9127 409.4790 414.3918 376.3195 386.2625 -4.9082 409.2793 414.1874 376.0953 387.8643 -4.9029 409.0863 413.9892 375.8807 389.4614 -4.8970 408.8892 413.7862 375.6523 391.0634 -4.8907 408.6895 413.5802 375.4257 392.6705 -4.8851 408.4872 413.3723 375.2033 394.2570 -4.8800 408.2863 413.1663 374.9826 395.8593 -4.8743 408.0843 412.9586 374.7623 397.4666 -4.8688 407.8822 412.7509 374.5379 399.0789 -4.8631 407.6872 412.5503 374.3211 400.6911 -4.8572 407.4863 412.3436 374.1043 402.2933 -4.8507 407.2855 412.1362 373.8921 403.9003 -4.8448 407.0877 411.9325 373.6740 405.5024 -4.8401 406.8926 411.7327 373.4618 407.1148 -4.8339 406.6930 411.5269 373.2460 408.7169 -4.8292 406.4874 411.3167 373.0334 410.3086 -4.8246 406.2860 411.1106 372.8239 411.9314 -4.8191 406.0789 410.8980 372.6154 413.5388 -4.8129 405.8722 410.6852 372.4133 415.1461 -4.8078 405.6640 410.4718 372.2178 416.7481 -4.8038 405.4629 410.2667 372.0142 418.3606 -4.7987 405.2557 410.0544 371.8108 419.9626 -4.7925 405.0480 409.8405 371.6228 421.5700 -4.7878 404.8457 409.6335 371.4387 423.1930 -4.7815 404.6461 409.4276 371.2493 424.8001 -4.7755 404.4418 409.2173 371.0593 426.3919 -4.7706 404.2414 409.0120 370.8654 427.9990 -4.7653 404.0367 408.8021 370.6830 429.6061 -4.7602 403.8398 408.6001 370.5012 431.2186 -4.7556 403.6406 408.3962 370.3029 432.8206 -4.7502 403.4447 408.1949 370.1057 434.4281 -4.7459 403.2388 407.9847 369.9145 436.0510 -4.7414 403.0282 407.7697 369.7260 437.6635 -4.7371 402.8254 407.5625 369.5395 439.2705 -4.7323 402.6262 407.3585 369.3452 440.8778 -4.7273 402.4201 407.1474 369.1555 442.4800 -4.7214 402.2173 406.9387 368.9786 444.0921 -4.7161 402.0178 406.7339 368.7962 445.6946 -4.7110 401.8134 406.5244 368.6173 447.3173 -4.7065 401.6056 406.3121 368.4387 448.9296 -4.7022 401.4053 406.1076 368.2535 450.5160 -4.6973 401.2072 405.9045 368.0661 452.1126 -4.6923 401.0139 405.7062 367.8758 453.7149 -4.6871 400.8128 405.4999 367.6876 455.3221 -4.6821 400.6138 405.2959 367.4963 456.9240 -4.6769 400.4063 405.0832 367.3082 458.5261 -4.6715 400.2037 404.8752 367.1150 460.1179 -4.6659 400.0060 404.6719 366.9182 461.7304 -4.6603 399.8027 404.4629 366.7193 463.3429 -4.6549 399.5983 404.2532 366.5242 464.9448 -4.6489 399.3937 404.0426 366.3296 466.5571 -4.6438 399.1880 403.8318 366.1232 468.1538 -4.6383 398.9863 403.6246 365.9175 469.7661 -4.6328 398.7897 403.4225 365.7080 471.3680 -4.6276 398.5894 403.2170 365.5018 472.9908 -4.6212 398.3828 403.0040 365.2903 474.5981 -4.6158 398.1817 402.7975 365.0814 476.1949 -4.6113 397.9799 402.5912 364.8733 477.8021 -4.6064 397.7798 402.3862 364.6690 479.4093 -4.6016 397.5788 402.1804 364.4605 481.0165 -4.5967 397.3701 401.9668 364.2484 482.6239 -4.5918 397.1619 401.7537 364.0396 484.2311 -4.5860 396.9584 401.5444 363.8334 485.8485 -4.5797 396.7577 401.3374 363.6170 487.4610 -4.5736 396.5578 401.1314 363.4051 489.0630 -4.5670 396.3590 400.9261 363.1897 490.6754 -4.5614 396.1586 400.7200 362.9740 492.2878 -4.5567 395.9599 400.5166 362.7605 493.8898 -4.5509 395.7649 400.3158 362.5492 495.5019 -4.5461 395.5652 400.1113 362.3364 497.1246 -4.5410 395.3665 399.9076 362.1239 498.7318 -4.5352 395.1726 399.7078 361.9115 500.3341 -4.5297 394.9689 399.4986 361.6931 501.9465 -4.5241 394.7647 399.2888 361.4723 503.5486 -4.5192 394.5676 399.0868 361.2559 505.1609 -4.5135 394.3728 398.8863 361.0415 506.7629 -4.5072 394.1699 398.6772 360.8253 508.3856 -4.5011 393.9554 398.4565 360.6083 509.9930 -4.4953 393.7554 398.2507 360.3930 511.5953 -4.4901 393.5570 398.0470 360.1775 513.2078 -4.4851 393.3541 397.8392 359.9639 514.8098 -4.4801 393.1472 397.6273 359.7504 516.4068 -4.4744 392.9379 397.4124 359.5319 518.0086 -4.4690 392.7346 397.2036 359.3178 519.6260 -4.4631 392.5292 396.9923 359.1013 521.2333 -4.4570 392.3298 396.7868 358.8939 522.8198 -4.4511 392.1377 396.5888 358.6875 524.4371 -4.4460 391.9357 396.3817 358.4791 526.0236 -4.4403 391.7402 396.1806 358.2696 527.6260 -4.4347 391.5302 395.9649 358.0545 529.2333 -4.4299 391.3270 395.7570 357.8444 530.8353 -4.4239 391.1241 395.5480 357.6312 532.4476 -4.4177 390.9227 395.3405 357.4150 534.0653 -4.4118 390.7116 395.1234 357.1973 535.6725 -4.4069 390.5103 394.9172 356.9831 537.2795 -4.4013 390.3061 394.7074 356.7783 538.8819 -4.3954 390.1065 394.5019 356.5673 540.4788 -4.3907 389.9027 394.2934 356.3552 542.0808 -4.3850 389.6986 394.0836 356.1446 543.6933 -4.3796 389.4986 393.8782 355.9341 545.2956 -4.3735 389.3030 393.6765 355.7352 546.9184 -4.3686 389.0976 393.4661 355.5281 548.5255 -4.3614 388.8941 393.2555 355.3231 550.1273 -4.3553 388.6875 393.0429 355.1111 551.7396 -4.3498 388.4816 392.8314 354.9057 553.3415 -4.3441 388.2759 392.6200 354.7003 554.9538 -4.3394 388.0668 392.4062 354.4972 556.5559 -4.3338 387.8652 392.1991 354.2876 558.1786 -4.3284 387.6638 391.9922 354.0800 559.7861 -4.3227 387.4655 391.7882 353.8754 561.3986 -4.3160 387.2609 391.5769 353.6738 563.0008 -4.3103 387.0625 391.3728 353.4632 564.5975 -4.3049 386.8640 391.1689 353.2547 566.2096 -4.2995 386.6634 390.9629 353.0437 567.8165 -4.2945 386.4668 390.7613 352.8289 569.4238 -4.2892 386.2639 390.5530 352.6200 571.0466 -4.2838 386.0564 390.3402 352.4040 572.6538 -4.2776 385.8513 390.1290 352.1948 574.2609 -4.2728 385.6555 389.9282 351.9787 575.8734 -4.2675 385.4513 389.7189 351.7716 577.4805 -4.2625 385.2465 389.5090 351.5650 579.0825 -4.2579 385.0435 389.3014 351.3689 580.6690 -4.2531 384.8403 389.0934 351.1561 582.2713 -4.2476 384.6366 388.8842 350.9400 583.8835 -4.2425 384.4320 388.6745 350.7288 585.4908 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