DTA measure 11.meres Date: 2026225:99 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.73 s Mass = 1153.500 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2728 -23.2236 162.3218 185.5454 246.6544 2.0393 -23.1831 162.5631 185.7462 246.5554 2.8668 -23.1439 162.8286 185.9724 246.4574 3.6225 -23.1047 163.0790 186.1837 246.3896 4.4915 -23.0640 163.3734 186.4374 246.3225 5.2473 -23.0228 163.6400 186.6628 246.2460 6.0748 -22.9752 163.9511 186.9263 246.1483 6.8720 -22.9293 164.1968 187.1261 246.0764 7.6688 -22.8879 164.4424 187.3303 246.0128 8.4860 -22.8403 164.7104 187.5507 245.9675 9.2525 -22.7965 164.9526 187.7490 245.9116 10.1108 -22.7482 165.2509 187.9991 245.8230 10.8768 -22.7034 165.4981 188.2016 245.7814 11.6945 -22.6517 165.7348 188.3865 245.7513 12.5013 -22.6047 166.0068 188.6116 245.6881 13.2880 -22.5524 166.2598 188.8123 245.6459 14.1160 -22.5018 166.5151 189.0169 245.5739 14.8818 -22.4531 166.7811 189.2342 245.5618 15.7403 -22.3984 167.0595 189.4579 245.5534 16.4965 -22.3470 167.3264 189.6734 245.5204 17.3238 -22.2893 167.5829 189.8722 245.4856 18.1208 -22.2298 167.8386 190.0685 245.4480 18.9180 -22.1723 168.1237 190.2960 245.4189 19.7350 -22.1097 168.4097 190.5194 245.3912 20.5115 -22.0537 168.6732 190.7269 245.3837 21.3600 -21.9903 168.9864 190.9767 245.3744 22.1258 -21.9331 169.2469 191.1799 245.3656 22.9535 -21.8714 169.5207 191.3921 245.3450 23.7508 -21.8073 169.7948 191.6021 245.3581 24.5473 -21.7456 170.0496 191.7952 245.3644 25.3648 -21.6818 170.3381 192.0199 245.3843 26.1415 -21.6268 170.6038 192.2305 245.4158 26.9895 -21.5699 170.8786 192.4485 245.4706 27.7555 -21.5119 171.1396 192.6515 245.5014 28.5835 -21.4548 171.4092 192.8640 245.5230 29.3808 -21.3963 171.6620 193.0583 245.5901 30.1770 -21.3348 171.9577 193.2925 245.6547 30.9948 -21.2669 172.2175 193.4845 245.7357 31.7715 -21.2061 172.4578 193.6639 245.8430 32.6190 -21.1334 172.6921 193.8255 245.9183 33.3855 -21.0659 172.9128 193.9787 246.0494 34.2135 -20.9910 173.1846 194.1755 246.1346 35.0100 -20.9244 173.4867 194.4110 246.2261 35.8070 -20.8557 173.7375 194.5932 246.3208 36.6248 -20.7851 174.0087 194.7938 246.4497 37.4010 -20.7184 174.2409 194.9592 246.5262 38.2593 -20.6442 174.5099 195.1540 246.6091 39.0258 -20.5772 174.7957 195.3729 246.7325 39.8428 -20.5091 175.0566 195.5657 246.8526 40.6500 -20.4405 175.3206 195.7610 246.9764 41.4370 -20.3762 175.6034 195.9796 247.1152 42.2640 -20.3047 175.8918 196.1965 247.2663 43.0305 -20.2352 176.1370 196.3722 247.4185 43.8893 -20.1582 176.4118 196.5699 247.5733 44.6550 -20.0943 176.6847 196.7790 247.7469 45.4725 -20.0251 176.9881 197.0132 247.9316 46.2800 -19.9575 177.2735 197.2310 248.1187 47.0660 -19.8870 177.5507 197.4377 248.2415 47.9248 -19.8095 177.8514 197.6609 248.4368 48.6913 -19.7425 178.0793 197.8218 248.6162 49.5188 -19.6714 178.3467 198.0181 248.8348 50.3155 -19.6013 178.6089 198.2101 249.0311 51.1025 -19.5311 178.8649 198.3961 249.2353 51.9403 -19.4556 179.1618 198.6174 249.4347 52.6960 -19.3889 179.4256 198.8144 249.6084 53.5548 -19.3158 179.6994 199.0153 249.8317 54.3205 -19.2509 179.9940 199.2449 250.0038 55.1483 -19.1838 180.2388 199.4227 250.1905 55.9353 -19.1122 180.4806 199.5928 250.3557 56.7320 -19.0398 180.7371 199.7769 250.5336 57.5288 -18.9717 180.9662 199.9379 250.7293 58.3158 -18.9025 181.2221 200.1246 250.9095 59.1433 -18.8275 181.5103 200.3377 251.1110 59.8990 -18.7640 181.7786 200.5425 251.2526 60.7475 -18.6916 182.0812 200.7727 251.4608 61.5238 -18.6247 182.3459 200.9706 251.6490 62.3410 -18.5608 182.6436 201.2044 251.8302 63.1075 -18.4978 182.9003 201.3981 252.0003 63.9353 -18.4269 183.1768 201.6038 252.2210 64.7215 -18.3618 183.4088 201.7706 252.3983 65.5188 -18.2918 183.6799 201.9716 252.5850 66.3463 -18.2200 183.9403 202.1602 252.7483 67.1020 -18.1538 184.1916 202.3454 252.9550 67.9608 -18.0744 184.4973 202.5718 253.1552 68.6965 -18.0042 184.7769 202.7812 253.3118 69.5440 -17.9276 185.0408 202.9685 253.4901 70.3105 -17.8584 185.2842 203.1426 253.6704 71.1385 -17.7880 185.5441 203.3322 253.8833 71.9350 -17.7204 185.8162 203.5367 254.0763 72.7320 -17.6518 186.0816 203.7334 254.2584 73.5498 -17.5814 186.3352 203.9166 254.4550 74.3258 -17.5138 186.5781 204.0919 254.6293 75.1740 -17.4428 186.8547 204.2975 254.7882 75.9098 -17.3820 187.0720 204.4540 254.9287 76.7678 -17.3097 187.3033 204.6129 255.1259 77.5340 -17.2521 187.5776 204.8297 255.3186 78.3620 -17.1805 187.8478 205.0283 255.5013 79.1483 -17.1098 188.1125 205.2223 255.6573 79.9555 -17.0391 188.3966 205.4357 255.8584 80.7733 -16.9716 188.6766 205.6482 256.0063 81.5395 -16.9105 188.9431 205.8537 256.1593 82.3975 -16.8374 189.2417 206.0791 256.3571 83.1640 -16.7719 189.4922 206.2641 256.5203 83.9918 -16.6997 189.7761 206.4758 256.6632 84.7473 -16.6401 189.9959 206.6360 256.8101 85.5855 -16.5694 190.2668 206.8363 256.9767 86.3725 -16.5035 190.5390 207.0425 257.1102 87.1790 -16.4380 190.8144 207.2524 257.2575 87.9968 -16.3755 191.0744 207.4499 257.4144 88.7735 -16.3138 191.2809 207.5946 257.5822 89.6005 -16.2452 191.5539 207.7991 257.7206 90.3670 -16.1867 191.7716 207.9583 257.8862 91.2155 -16.1197 192.0553 208.1750 258.0325 91.9913 -16.0580 192.3324 208.3904 258.1763 92.8090 -15.9917 192.6020 208.5937 258.3189 93.6063 -15.9247 192.8597 208.7844 258.4528 94.4028 -15.8613 193.1110 208.9723 258.5714 95.2305 -15.7956 193.3821 209.1777 258.7276 95.9970 -15.7373 193.6167 209.3540 258.8768 96.8548 -15.6690 193.8608 209.5298 258.9947 97.5905 -15.6083 194.1010 209.7093 259.0396 98.4595 -15.5380 194.3549 209.8929 259.1623 99.2148 -15.4770 194.6117 210.0888 259.3092 100.0428 -15.4134 194.8732 210.2865 259.4455 100.8400 -15.3485 195.1400 210.4884 259.5995 101.6363 -15.2848 195.4100 210.6948 259.7311 102.4643 -15.2219 195.6858 210.9077 259.8411 103.2205 -15.1636 195.9469 211.1105 259.9550 104.0890 -15.0959 196.2114 211.3073 260.0304 104.8448 -15.0434 196.4471 211.4905 260.1199 105.6728 -14.9799 196.6983 211.6781 260.2800 106.4700 -14.9203 196.9572 211.8775 260.4158 107.2663 -14.8567 197.2023 212.0590 260.5192 108.0943 -14.7876 197.4607 212.2483 260.6584 108.8505 -14.7280 197.7024 212.4303 260.8089 109.7190 -14.6672 197.9650 212.6321 260.9321 110.4748 -14.6133 198.2120 212.8254 261.0500 111.3130 -14.5451 198.5120 213.0571 261.1445 112.0993 -14.4835 198.7819 213.2654 261.2361 112.9065 -14.4252 199.0168 213.4421 261.3322 113.7243 -14.3624 199.2274 213.5898 261.4565 114.4903 -14.3041 199.4454 213.7495 261.5587 115.3485 -14.2438 199.7154 213.9592 261.6500 116.1150 -14.1935 199.9464 214.1399 261.7325 116.9428 -14.1362 200.2415 214.3778 261.8287 117.7290 -14.0798 200.4941 214.5739 261.9168 118.5365 -14.0247 200.7743 214.7989 262.0296 119.3543 -13.9637 201.0282 214.9919 262.1639 120.1098 -13.9138 201.2656 215.1794 262.2965 120.9683 -13.8551 201.5269 215.3820 262.3804 121.7245 -13.8044 201.7824 215.5868 262.4833 122.5515 -13.7430 202.0508 215.7938 262.5859 123.3488 -13.6856 202.2827 215.9684 262.6783 124.1358 -13.6268 202.5009 216.1277 262.7613 124.9628 -13.5666 202.7578 216.3244 262.8401 125.7190 -13.5155 202.9833 216.4988 262.9421 126.5470 -13.4583 203.2106 216.6690 263.0680 127.3130 -13.4061 203.4601 216.8662 263.2084 128.1610 -13.3523 203.7632 217.1156 263.3260 128.9275 -13.2991 204.0104 217.3095 263.4438 129.7555 -13.2459 204.2513 217.4972 263.5425 130.5723 -13.1922 204.5119 217.7041 263.6938 131.3388 -13.1415 204.7430 217.8844 263.7898 132.1668 -13.0854 204.9875 218.0729 263.9242 132.9323 -13.0310 205.2300 218.2609 264.0352 133.7808 -12.9813 205.5124 218.4937 264.2023 134.5473 -12.9306 205.6896 218.6201 264.3245 135.3743 -12.8687 205.9459 218.8146 264.4373 136.1715 -12.8155 206.1894 219.0049 264.5605 136.9585 -12.7644 206.4054 219.1699 264.6461 137.7958 -12.7127 206.6171 219.3297 264.7769 138.5520 -12.6639 206.8419 219.5058 264.9142 139.4108 -12.6068 207.0882 219.6949 265.0372 140.1765 -12.5553 207.2980 219.8533 265.1504 141.0043 -12.5066 207.5123 220.0190 265.2644 141.7913 -12.4594 207.7456 220.2050 265.4078 142.5880 -12.4096 207.9640 220.3736 265.5350 143.4155 -12.3523 208.2276 220.5799 265.6688 144.1820 -12.3018 208.4719 220.7737 265.7879 145.0303 -12.2495 208.7438 220.9933 265.9076 145.8063 -12.2037 208.9881 221.1918 266.0541 146.6240 -12.1532 209.2589 221.4121 266.2120 147.4210 -12.1049 209.4694 221.5743 266.3656 148.2175 -12.0566 209.6838 221.7404 266.4927 149.0455 -12.0036 209.9009 221.9045 266.6390 149.8115 -11.9575 210.0955 222.0530 266.7692 150.6698 -11.9105 210.3237 222.2343 266.9128 151.4363 -11.8703 210.5412 222.4114 267.0385 152.2635 -11.8186 210.7972 222.6159 267.1289 153.0605 -11.7717 211.0188 222.7905 267.2345 153.8475 -11.7253 211.2383 222.9636 267.3359 154.6848 -11.6791 211.4545 223.1336 267.5024 155.4410 -11.6369 211.6464 223.2833 267.6516 156.2998 -11.5868 211.8920 223.4788 267.7669 157.0658 -11.5465 212.1027 223.6492 267.8887 157.8933 -11.4973 212.3153 223.8126 267.9890 158.6905 -11.4538 212.5193 223.9731 268.1472 159.4973 -11.4129 212.7359 224.1488 268.3310 160.3148 -11.3737 212.9996 224.3732 268.4564 161.0915 -11.3317 213.1857 224.5174 268.6127 161.9085 -11.2853 213.4074 224.6927 268.7548 162.6748 -11.2415 213.6395 224.8810 268.8908 163.5335 -11.2006 213.8951 225.0957 269.0188 164.2993 -11.1609 214.0980 225.2589 269.1673 165.1270 -11.1122 214.3269 225.4391 269.2847 165.9140 -11.0697 214.5468 225.6165 269.4061 166.7210 -11.0275 214.7746 225.8020 269.5446 167.5383 -10.9848 215.0012 225.9860 269.6543 168.3048 -10.9452 215.1974 226.1425 269.7784 169.1633 -10.9053 215.4564 226.3617 269.9261 169.9393 -10.8643 215.6677 226.5320 270.0903 170.7570 -10.8230 215.9000 226.7230 270.2753 171.5543 -10.7839 216.0919 226.8758 270.4359 172.3505 -10.7436 216.3148 227.0584 270.5677 173.1785 -10.7013 216.5348 227.2361 270.7178 173.9450 -10.6606 216.7474 227.4079 270.8619 174.8030 -10.6159 216.9488 227.5647 271.0062 175.5385 -10.5795 217.1787 227.7582 271.1390 176.3970 -10.5377 217.4059 227.9435 271.3389 177.1628 -10.4975 217.6321 228.1296 271.4947 177.9805 -10.4554 217.8894 228.3448 271.6241 178.7878 -10.4130 218.1410 228.5540 271.7881 179.5843 -10.3731 218.3907 228.7639 271.9351 180.4123 -10.3302 218.6150 228.9453 272.0518 181.1683 -10.2997 218.7887 229.0885 272.1942 182.0365 -10.2560 219.0193 229.2753 272.3592 182.7825 -10.2259 219.1804 229.4063 272.4698 183.6308 -10.1935 219.4244 229.6178 272.6134 184.3863 -10.1571 219.6528 229.8098 272.7207 185.2143 -10.1206 219.8724 229.9931 272.8999 186.0013 -10.0842 220.0591 230.1433 273.0372 186.7975 -10.0476 220.3217 230.3692 273.1934 187.6255 -10.0055 220.5755 230.5810 273.3794 188.3818 -9.9746 220.7956 230.7702 273.5238 189.2398 -9.9404 221.0068 230.9472 273.6698 189.9753 -9.9021 221.1775 231.0796 273.7818 190.8340 -9.8659 221.3914 231.2573 273.9211 191.5898 -9.8340 221.6001 231.4341 274.0362 192.4173 -9.7967 221.8364 231.6331 274.1598 193.2145 -9.7563 222.0370 231.7933 274.2815 194.0010 -9.7231 222.2366 231.9597 274.4143 194.7978 -9.6931 222.4624 232.1554 274.5246 195.5950 -9.6610 222.6848 232.3458 274.6809 196.4123 -9.6296 222.8767 232.5064 274.8307 197.1885 -9.5976 223.0695 232.6671 274.9762 198.0370 -9.5668 223.3009 232.8677 275.1173 198.8030 -9.5365 223.4993 233.0358 275.2416 199.6305 -9.5060 223.6990 233.2050 275.4173 200.4278 -9.4750 223.8973 233.3722 275.5714 201.2248 -9.4413 224.0787 233.5200 275.7168 202.0418 -9.4088 224.2895 233.6984 275.8734 202.8185 -9.3715 224.4905 233.8620 275.9885 203.6358 -9.3423 224.7061 234.0483 276.1159 204.4018 -9.3106 224.9031 234.2137 276.2390 205.2605 -9.2770 225.1105 234.3875 276.3689 206.0265 -9.2490 225.2806 234.5297 276.5161 206.8540 -9.2211 225.5220 234.7431 276.6150 207.6410 -9.1921 225.7227 234.9148 276.7354 208.4483 -9.1579 225.9404 235.0983 276.8888 209.2653 -9.1247 226.1450 235.2697 277.0276 210.0318 -9.0960 226.3544 235.4504 277.1714 210.8903 -9.0637 226.6204 235.6841 277.3175 211.6253 -9.0390 226.7944 235.8333 277.4262 212.4840 -9.0083 226.9917 236.0001 277.5502 213.2403 -8.9825 227.1760 236.1584 277.6774 214.0775 -8.9513 227.3965 236.3478 277.7925 214.8645 -8.9240 227.6019 236.5259 277.9325 215.6618 -8.8971 227.8141 236.7112 278.0488 216.4888 -8.8678 228.0453 236.9131 278.1808 217.2655 -8.8359 228.1980 237.0338 278.3110 218.1140 -8.8026 228.4499 237.2525 278.4302 218.8795 -8.7738 228.6716 237.4454 278.5355 219.7075 -8.7456 228.8753 237.6210 278.6698 220.5048 -8.7211 229.0397 237.7608 278.8069 221.3010 -8.6918 229.2217 237.9135 278.9074 222.1188 -8.6639 229.4264 238.0903 279.0156 222.8955 -8.6396 229.6397 238.2793 279.1613 223.7430 -8.6153 229.8730 238.4883 279.2601 224.5095 -8.5955 230.0776 238.6732 279.3649 225.3375 -8.5685 230.2755 238.8439 279.5099 226.1340 -8.5430 230.4540 238.9970 279.6440 226.9310 -8.5217 230.6487 239.1705 279.7632 227.7488 -8.4952 230.8111 239.3064 279.8682 228.5253 -8.4701 230.9592 239.4292 279.9639 229.3730 -8.4447 231.1649 239.6096 280.0977 230.1395 -8.4181 231.3571 239.7752 280.2322 230.9673 -8.3865 231.5490 239.9355 280.3181 231.7638 -8.3628 231.7379 240.1007 280.4181 232.5610 -8.3383 231.9106 240.2489 280.5437 233.3788 -8.3163 232.1369 240.4532 280.7104 234.1545 -8.2930 232.3142 240.6071 280.8112 235.0030 -8.2716 232.5365 240.8081 280.9544 235.7693 -8.2432 232.7124 240.9556 281.1044 236.5965 -8.2159 232.9364 241.1523 281.2460 237.4040 -8.1889 233.1315 241.3204 281.3758 238.1910 -8.1687 233.3385 241.5073 281.4935 239.0183 -8.1425 233.5436 241.6861 281.5695 239.7845 -8.1245 233.7337 241.8582 281.6861 240.6433 -8.0979 233.9521 242.0500 281.7722 241.4090 -8.0769 234.1693 242.2461 281.8725 242.2368 -8.0508 234.3696 242.4204 281.9612 243.0033 -8.0284 234.5525 242.5809 282.0625 243.8303 -8.0057 234.7349 242.7406 282.1974 244.6275 -7.9880 234.9336 242.9216 282.3475 245.4145 -7.9711 235.1122 243.0833 282.5070 246.2830 -7.9500 235.3345 243.2846 282.6744 247.0388 -7.9287 235.5213 243.4501 282.8192 247.8565 -7.9093 235.6846 243.5940 282.9965 248.6330 -7.8930 235.8176 243.7106 283.1278 249.4500 -7.8697 236.0399 243.9095 283.2651 250.2370 -7.8457 236.2429 244.0886 283.3711 251.0343 -7.8203 236.4488 244.2691 283.4733 251.8513 -7.7962 236.6474 244.4436 283.5885 252.6175 -7.7709 236.8396 244.6106 283.7046 253.4763 -7.7520 237.0317 244.7838 283.8120 254.2320 -7.7312 237.2029 244.9341 283.9146 255.0595 -7.7082 237.3505 245.0586 284.0505 255.8568 -7.6880 237.5349 245.2229 284.1929 256.6535 -7.6678 237.7412 245.4090 284.2718 257.4708 -7.6432 237.9351 245.5782 284.3934 258.2373 -7.6211 238.0856 245.7067 284.5246 259.0955 -7.5997 238.3130 245.9127 284.6598 259.8513 -7.5869 238.4984 246.0853 284.7849 260.6793 -7.5709 238.6983 246.2692 284.9249 261.4758 -7.5485 238.9043 246.4528 285.0599 262.2625 -7.5325 239.1216 246.6542 285.2015 263.0598 -7.5190 239.3570 246.8760 285.3268 263.8565 -7.4956 239.5157 247.0113 285.4539 264.6738 -7.4748 239.6335 247.1083 285.6099 265.4505 -7.4605 239.8217 247.2822 285.7531 266.2988 -7.4414 240.0279 247.4693 285.9000 267.0645 -7.4209 240.1782 247.5991 286.0182 267.8925 -7.3965 240.3549 247.7514 286.1424 268.6895 -7.3789 240.5604 247.9392 286.2679 269.4860 -7.3654 240.7532 248.1186 286.3830 270.3038 -7.3429 240.9429 248.2858 286.5079 271.0803 -7.3256 241.1271 248.4527 286.6516 271.9280 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289.5870 290.4115 -6.9381 245.4937 252.4318 289.7295 291.1883 -6.9225 245.6569 252.5794 289.8440 292.0163 -6.9130 245.8160 252.7290 289.9565 292.7818 -6.8983 245.9446 252.8429 290.0443 293.6098 -6.8843 246.1012 252.9855 290.1640 294.4070 -6.8736 246.2718 253.1454 290.3093 295.2035 -6.8545 246.4213 253.2758 290.4707 296.0313 -6.8322 246.5951 253.4273 290.6536 296.7875 -6.8169 246.7588 253.5757 290.8037 297.6558 -6.7994 246.9651 253.7645 290.9427 298.4118 -6.7890 247.1287 253.9177 291.0931 299.2398 -6.7722 247.2788 254.0511 291.2358 300.0363 -6.7595 247.4389 254.1984 291.3829 300.8333 -6.7502 247.6408 254.3909 291.5406 301.6613 -6.7362 247.8033 254.5394 291.6676 302.4373 -6.7274 247.9874 254.7148 291.7553 303.2548 -6.7143 248.1588 254.8731 291.8753 304.0315 -6.7011 248.3423 255.0433 291.9933 304.8793 -6.6889 248.5552 255.2441 292.1426 305.6455 -6.6738 248.7466 255.4205 292.2895 306.4735 -6.6605 248.9452 255.6057 292.4461 307.2805 -6.6471 249.1064 255.7535 292.6035 308.0670 -6.6341 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