DTA measure 2pb4 Date: 2026225:104 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.23 s Mass = 1153.500 mg data_number = 1570 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2113 -2.0389 220.4678 222.5067 249.0116 2.0495 -2.0578 220.5384 222.5962 248.9808 2.8365 -2.0760 220.6133 222.6893 248.9242 3.6338 -2.0917 220.6857 222.7774 248.9007 4.4618 -2.1043 220.7610 222.8653 248.8898 5.2283 -2.1160 220.8744 222.9903 248.8747 6.0768 -2.1318 220.9824 223.1142 248.8665 6.8435 -2.1473 221.0690 223.2163 248.8185 7.6620 -2.1609 221.1331 223.2939 248.7726 8.4285 -2.1796 221.1968 223.3764 248.7421 9.2565 -2.1954 221.2580 223.4534 248.7060 10.0435 -2.2095 221.2942 223.5038 248.6694 10.8305 -2.2185 221.3898 223.6083 248.6328 11.6688 -2.2292 221.4953 223.7245 248.5794 12.4250 -2.2365 221.5946 223.8312 248.5298 13.2735 -2.2447 221.6826 223.9273 248.4679 14.0503 -2.2550 221.7563 224.0114 248.4543 14.8680 -2.2691 221.8379 224.1070 248.4529 15.6555 -2.2765 221.9280 224.2045 248.4210 16.4633 -2.2879 222.0071 224.2950 248.3916 17.2810 -2.2944 222.0882 224.3826 248.3791 18.0478 -2.3004 222.1711 224.4715 248.3418 18.8758 -2.3119 222.2405 224.5524 248.3413 19.6730 -2.3198 222.3146 224.6344 248.2933 20.4908 -2.3298 222.4025 224.7323 248.2888 21.2675 -2.3346 222.4966 224.8311 248.2948 22.0853 -2.3419 222.5987 224.9406 248.2898 22.8723 -2.3491 222.6689 225.0181 248.2810 23.7108 -2.3539 222.7585 225.1124 248.3103 24.4670 -2.3608 222.8097 225.1704 248.3075 25.2948 -2.3660 222.8616 225.2277 248.3130 26.0923 -2.3706 222.9301 225.3007 248.3245 26.8893 -2.3819 223.0361 225.4181 248.3211 27.7175 -2.3891 223.1003 225.4894 248.3333 28.4738 -2.3972 223.1476 225.5449 248.3557 29.3435 -2.4020 223.2370 225.6390 248.3742 30.0990 -2.4073 223.3240 225.7313 248.4009 30.9278 -2.4134 223.3855 225.7989 248.4367 31.7248 -2.4221 223.4652 225.8872 248.4546 32.5223 -2.4290 223.5160 225.9450 248.4897 33.3503 -2.4380 223.6056 226.0436 248.5326 34.1065 -2.4468 223.6789 226.1257 248.5777 34.9755 -2.4536 223.7634 226.2171 248.6241 35.7318 -2.4567 223.8399 226.2966 248.6702 36.5598 -2.4643 223.9170 226.3814 248.7598 37.3570 -2.4710 224.0056 226.4766 248.8346 38.1543 -2.4780 224.0816 226.5595 248.8950 38.9515 -2.4807 224.1638 226.6446 248.9643 39.7385 -2.4847 224.2290 226.7137 249.0321 40.5775 -2.4936 224.3087 226.8023 249.1117 41.3340 -2.5035 224.3838 226.8873 249.1944 42.1928 -2.5083 224.4859 226.9942 249.2663 42.9593 -2.5132 224.5438 227.0569 249.3537 43.7873 -2.5233 224.6384 227.1618 249.4114 44.5845 -2.5274 224.7389 227.2663 249.4807 45.3715 -2.5291 224.8160 227.3451 249.5641 46.2098 -2.5292 224.8926 227.4218 249.6616 46.9660 -2.5330 224.9682 227.5011 249.7416 47.8248 -2.5360 225.1047 227.6407 249.8838 48.5918 -2.5428 225.1840 227.7268 249.9846 49.4203 -2.5468 225.2480 227.7948 250.0544 50.2175 -2.5534 225.3284 227.8818 250.1870 51.0045 -2.5623 225.3918 227.9541 250.3098 51.8428 -2.5666 225.5007 228.0673 250.4334 52.5990 -2.5714 225.5400 228.1115 250.5297 53.4578 -2.5763 225.6193 228.1956 250.6094 54.2243 -2.5821 225.7155 228.2976 250.7286 55.0625 -2.5862 225.8046 228.3908 250.8882 55.8495 -2.5930 225.8633 228.4563 251.0263 56.6468 -2.5988 225.9386 228.5374 251.1762 57.4748 -2.6040 226.0120 228.6160 251.3149 58.2413 -2.6144 226.0569 228.6713 251.4078 59.1005 -2.6193 226.0972 228.7165 251.5660 59.8573 -2.6251 226.1398 228.7648 251.6835 60.6955 -2.6270 226.2656 228.8926 251.8015 61.4825 -2.6287 226.3637 228.9924 251.9604 62.2798 -2.6351 226.4878 229.1228 252.0774 63.1078 -2.6398 226.5901 229.2299 252.2049 63.8845 -2.6428 226.6569 229.2997 252.3274 64.7330 -2.6437 226.7188 229.3625 252.4450 65.4998 -2.6429 226.7948 229.4378 252.5738 66.3285 -2.6449 226.9311 229.5760 252.7086 67.1258 -2.6511 227.0006 229.6517 252.8457 67.9230 -2.6606 227.0706 229.7313 253.0030 68.7408 -2.6650 227.1442 229.8093 253.1770 69.5175 -2.6689 227.1929 229.8618 253.3119 70.3455 -2.6732 227.3007 229.9739 253.4904 71.1120 -2.6736 227.3917 230.0653 253.6486 71.9605 -2.6814 227.4889 230.1702 253.7865 72.7270 -2.6851 227.5823 230.2674 253.9434 73.5448 -2.6920 227.6563 230.3483 254.0571 74.3113 -2.7025 227.7112 230.4137 254.2038 75.1290 -2.7105 227.7821 230.4926 254.3560 75.9263 -2.7117 227.8163 230.5280 254.5002 76.7235 -2.7150 227.9328 230.6478 254.6358 77.5420 -2.7236 228.0436 230.7672 254.7928 78.3088 -2.7242 228.1217 230.8459 254.9495 79.1675 -2.7290 228.1935 230.9225 255.0574 79.8930 -2.7345 228.2675 231.0019 255.1844 80.7518 -2.7390 228.3555 231.0944 255.3180 81.5183 -2.7455 228.4451 231.1906 255.4579 82.3463 -2.7488 228.5585 231.3073 255.5781 83.1333 -2.7530 228.6401 231.3931 255.6915 83.9305 -2.7539 228.7297 231.4836 255.8280 84.7585 -2.7562 228.8041 231.5602 255.9662 85.5250 -2.7636 228.8622 231.6259 256.0816 86.3735 -2.7720 228.9228 231.6949 256.2367 87.1400 -2.7810 229.0197 231.8007 256.3489 87.9680 -2.7857 229.1232 231.9089 256.5087 88.7550 -2.7891 229.2413 232.0304 256.6899 89.5625 -2.7958 229.3398 232.1356 256.8456 90.3598 -2.8000 229.4487 232.2486 256.9690 91.1570 -2.8086 229.5431 232.3516 257.0890 91.9750 -2.8127 229.6188 232.4315 257.1886 92.7525 -2.8149 229.6990 232.5140 257.2805 93.6010 -2.8169 229.7933 232.6102 257.3889 94.3675 -2.8208 229.8602 232.6811 257.4985 95.1955 -2.8344 229.9277 232.7621 257.6398 95.9518 -2.8373 229.9648 232.8022 257.7342 96.7798 -2.8387 230.0331 232.8718 257.8651 97.5770 -2.8405 230.1040 232.9445 257.9649 98.3743 -2.8428 230.2195 233.0623 258.0791 99.2023 -2.8489 230.3225 233.1714 258.1978 99.9585 -2.8537 230.3824 233.2360 258.2962 100.8285 -2.8565 230.5163 233.3728 258.4113 101.5848 -2.8621 230.6000 233.4621 258.5333 102.4128 -2.8737 230.6684 233.5421 258.6405 103.2100 -2.8795 230.7392 233.6187 258.7406 104.0073 -2.8818 230.8190 233.7009 258.8700 104.8353 -2.8919 230.9202 233.8121 258.9755 105.5915 -2.8967 231.0119 233.9086 259.0747 106.4605 -2.9013 231.1129 234.0141 259.2149 107.2168 -2.9055 231.2619 234.1674 259.3145 108.0455 -2.9097 231.3733 234.2830 259.4460 108.8123 -2.9139 231.4421 234.3560 259.5117 109.6403 -2.9142 231.5246 234.4388 259.6198 110.4375 -2.9173 231.6250 234.5423 259.7005 111.2245 -2.9232 231.7336 234.6568 259.7766 112.0628 -2.9260 231.7916 234.7175 259.8589 112.8190 -2.9312 231.8757 234.8069 259.9495 113.6778 -2.9372 231.9510 234.8882 260.0841 114.4443 -2.9388 232.0527 234.9915 260.1653 115.2723 -2.9450 232.1589 235.1039 260.2440 116.0705 -2.9492 232.2168 235.1660 260.3499 116.8575 -2.9550 232.2863 235.2414 260.4286 117.6958 -2.9608 232.3793 235.3401 260.4691 118.4520 -2.9637 232.4604 235.4240 260.5547 119.3108 -2.9699 232.5860 235.5559 260.6891 120.0773 -2.9812 232.6743 235.6555 260.7995 120.9053 -2.9870 232.7695 235.7565 260.8778 121.7025 -2.9885 232.8617 235.8502 260.9655 122.4895 -2.9911 232.9631 235.9542 261.0612 123.3288 -2.9920 233.0270 236.0190 261.1788 124.0850 -2.9916 233.1053 236.0968 261.3009 124.9438 -2.9861 233.1958 236.1819 261.4650 125.7103 -2.9949 233.2944 236.2893 261.5728 126.5383 -3.0002 233.4009 236.4011 261.6765 127.3355 -3.0037 233.4731 236.4768 261.7694 128.1225 -3.0084 233.5474 236.5558 261.8342 128.9608 -3.0135 233.5931 236.6066 261.9178 129.7170 -3.0198 233.6584 236.6782 262.0000 130.5758 -3.0282 233.7643 236.7925 262.1062 131.3428 -3.0334 233.8526 236.8860 262.1971 132.1815 -3.0447 233.9665 237.0112 262.3063 132.9685 -3.0509 234.0547 237.1056 262.4051 133.7658 -3.0563 234.1455 237.2018 262.4894 134.5938 -3.0556 234.2399 237.2954 262.5463 135.3500 -3.0581 234.3560 237.4141 262.6305 136.1678 -3.0599 234.4599 237.5197 262.7222 136.9445 -3.0617 234.5600 237.6217 262.8127 137.7930 -3.0693 234.6806 237.7499 262.9156 138.5493 -3.0715 234.8043 237.8758 263.0078 139.3773 -3.0751 234.9070 237.9821 263.0971 140.1745 -3.0775 234.9690 238.0465 263.1617 140.9620 -3.0839 234.9993 238.0832 263.2553 141.7905 -3.0886 235.0861 238.1747 263.3748 142.5570 -3.0953 235.2144 238.3097 263.4709 143.4055 -3.1014 235.3079 238.4093 263.5799 144.1720 -3.1084 235.4002 238.5085 263.6934 145.0000 -3.1098 235.5020 238.6118 263.8151 145.7870 -3.1123 235.6003 238.7126 263.9085 146.5843 -3.1125 235.6844 238.7970 264.0129 147.4123 -3.1164 235.7859 238.9022 264.1117 148.1685 -3.1205 235.8648 238.9853 264.1955 149.0068 -3.1194 235.9894 239.1088 264.2726 149.7630 -3.1255 236.0786 239.2041 264.3642 150.6218 -3.1338 236.1527 239.2865 264.5003 151.3883 -3.1376 236.1832 239.3209 264.5824 152.2163 -3.1399 236.2865 239.4264 264.6559 153.0135 -3.1454 236.4003 239.5457 264.7360 153.8005 -3.1497 236.4884 239.6382 264.8261 154.6388 -3.1544 236.5684 239.7228 264.9438 155.3950 -3.1583 236.6770 239.8353 265.0331 156.2538 -3.1616 236.8063 239.9679 265.0873 157.0203 -3.1665 236.8714 240.0379 265.1673 157.8483 -3.1686 236.9661 240.1348 265.2538 158.6460 -3.1689 237.0790 240.2480 265.3319 159.4335 -3.1713 237.1753 240.3466 265.4305 160.2718 -3.1698 237.3179 240.4878 265.5319 161.0280 -3.1706 237.3735 240.5441 265.6705 161.8560 -3.1729 237.4468 240.6197 265.7800 162.6225 -3.1766 237.5376 240.7141 265.8414 163.4813 -3.1842 237.6383 240.8224 265.8831 164.2478 -3.1909 237.7364 240.9273 265.9500 165.0655 -3.1920 237.8198 241.0118 266.0677 165.8730 -3.1956 237.9201 241.1157 266.1707 166.6600 -3.2029 238.0473 241.2502 266.2613 167.4888 -3.2083 238.1202 241.3285 266.3381 168.2555 -3.2068 238.1977 241.4045 266.4472 169.1143 -3.2058 238.3093 241.5151 266.5366 169.8808 -3.2105 238.3952 241.6057 266.6748 170.6985 -3.2148 238.4835 241.6983 266.7798 171.5060 -3.2213 238.6005 241.8219 266.8747 172.2930 -3.2229 238.7181 241.9410 266.9811 173.1210 -3.2258 238.8090 242.0348 267.0738 173.8875 -3.2280 238.9065 242.1346 267.1409 174.7463 -3.2231 238.9653 242.1884 267.2465 175.4820 -3.2266 239.0177 242.2443 267.3235 176.3313 -3.2315 239.1437 242.3752 267.4229 177.1083 -3.2364 239.2399 242.4763 267.5458 177.9260 -3.2427 239.3265 242.5692 267.6286 178.7233 -3.2457 239.4023 242.6480 267.7239 179.5205 -3.2487 239.4891 242.7378 267.8101 180.3485 -3.2551 239.5653 242.8204 267.9013 181.1150 -3.2626 239.6628 242.9254 268.0204 181.9635 -3.2627 239.8117 243.0744 268.1446 182.7403 -3.2628 239.9192 243.1821 268.2485 183.5580 -3.2577 240.0186 243.2764 268.3565 184.3553 -3.2643 240.1117 243.3760 268.4478 185.1533 -3.2667 240.1977 243.4645 268.5528 185.9815 -3.2678 240.3074 243.5752 268.6580 186.7480 -3.2757 240.4015 243.6773 268.7587 187.5658 -3.2812 240.5045 243.7857 268.8658 188.3425 -3.2839 240.6029 243.8868 268.9517 189.1910 -3.2869 240.7249 244.0118 269.0806 189.9575 -3.2918 240.7889 244.0808 269.1681 190.7855 -3.2974 240.9046 244.2020 269.2770 191.5835 -3.2965 240.9999 244.2964 269.3915 192.3810 -3.2980 241.1014 244.3994 269.5056 193.1988 -3.2986 241.1768 244.4754 269.5917 193.9755 -3.3001 241.2782 244.5783 269.7041 194.8240 -3.3055 241.3917 244.6971 269.8151 195.5905 -3.3073 241.4758 244.7830 269.9128 196.4185 -3.3108 241.5726 244.8834 270.0550 197.2158 -3.3145 241.6124 244.9269 270.1806 198.0135 -3.3171 241.7352 245.0523 270.2421 198.8318 -3.3182 241.8464 245.1646 270.3601 199.5983 -3.3246 241.9493 245.2739 270.4682 200.4468 -3.3288 242.0281 245.3570 270.6135 201.1825 -3.3327 242.1170 245.4497 270.6996 202.0310 -3.3358 242.2237 245.5595 270.7745 202.7873 -3.3396 242.3063 245.6459 270.8580 203.6460 -3.3425 242.3903 245.7328 270.9997 204.3818 -3.3457 242.4887 245.8344 271.0921 205.2405 -3.3457 242.6028 245.9485 271.2226 206.0070 -3.3493 242.6916 246.0409 271.3476 206.8248 -3.3556 242.7874 246.1430 271.4619 207.6225 -3.3629 242.8962 246.2591 271.5723 208.4203 -3.3658 242.9996 246.3654 271.6532 209.2380 -3.3665 243.0552 246.4217 271.8114 210.0045 -3.3667 243.1261 246.4928 271.9371 210.8633 -3.3684 243.2345 246.6028 272.0604 211.6195 -3.3707 243.3178 246.6885 272.1395 212.4475 -3.3707 243.4125 246.7832 272.2571 213.2243 -3.3701 243.4647 246.8348 272.3705 214.0625 -3.3702 243.5774 246.9475 272.5001 214.8495 -3.3739 243.6910 247.0649 272.5740 215.6375 -3.3788 243.8115 247.1903 272.6858 216.4758 -3.3859 243.9116 247.2975 272.8080 217.2320 -3.3881 244.0046 247.3927 272.8857 218.0600 -3.3863 244.0815 247.4678 272.9582 218.8265 -3.3891 244.1640 247.5531 273.0608 219.6853 -3.3896 244.2968 247.6864 273.1488 220.4518 -3.3928 244.3752 247.7680 273.2576 221.2695 -3.3989 244.4504 247.8493 273.3806 222.0668 -3.4042 244.5623 247.9665 273.4897 222.8640 -3.4084 244.6714 248.0797 273.5811 223.6818 -3.4106 244.7870 248.1975 273.6547 224.4800 -3.4121 244.8900 248.3021 273.7472 225.2978 -3.4108 244.9836 248.3943 273.8571 226.0745 -3.4111 245.0897 248.5007 273.9908 226.9230 -3.4149 245.2039 248.6188 274.1330 227.6588 -3.4167 245.2761 248.6929 274.2372 228.5175 -3.4208 245.3825 248.8033 274.3496 229.2943 -3.4277 245.4584 248.8862 274.4510 230.1120 -3.4288 245.5990 249.0278 274.5870 230.9093 -3.4302 245.6764 249.1067 274.6723 231.7065 -3.4329 245.7862 249.2191 274.7250 232.5345 -3.4308 245.9030 249.3338 274.8389 233.3010 -3.4330 245.9603 249.3932 274.9277 234.1495 -3.4333 246.0488 249.4820 275.0225 234.9270 -3.4340 246.1826 249.6166 275.1080 235.7450 -3.4386 246.2847 249.7233 275.2042 236.5423 -3.4419 246.4076 249.8495 275.3135 237.3395 -3.4473 246.5047 249.9520 275.4203 238.1675 -3.4515 246.5580 250.0095 275.5309 238.9340 -3.4545 246.6412 250.0957 275.6355 239.7825 -3.4586 246.7421 250.2007 275.7494 240.5593 -3.4621 246.8049 250.2670 275.8342 241.3770 -3.4697 246.8750 250.3448 275.9607 242.1743 -3.4717 246.9611 250.4328 276.0768 242.9715 -3.4687 247.0861 250.5548 276.1720 243.7995 -3.4688 247.1773 250.6461 276.2925 244.5660 -3.4725 247.2849 250.7575 276.3820 245.4153 -3.4765 247.3939 250.8704 276.4907 246.1923 -3.4798 247.5136 250.9934 276.5885 247.0100 -3.4818 247.6336 251.1154 276.6309 247.8073 -3.4836 247.7303 251.2139 276.7218 248.6045 -3.4826 247.8407 251.3233 276.8011 249.4325 -3.4834 247.9421 251.4256 276.8954 250.1990 -3.4877 248.0301 251.5178 277.0234 251.0475 -3.4902 248.1378 251.6280 277.1417 251.8243 -3.4914 248.2092 251.7006 277.2275 252.6420 -3.4960 248.3066 251.8026 277.3245 253.4400 -3.4984 248.4206 251.9190 277.4356 254.2375 -3.4986 248.4881 251.9868 277.5195 255.0655 -3.5032 248.5858 252.0890 277.6033 255.8320 -3.5053 248.6871 252.1924 277.6732 256.6805 -3.5029 248.7925 252.2954 277.7741 257.4573 -3.5036 248.8774 252.3810 277.8255 258.2750 -3.5065 249.0056 252.5120 277.9115 259.0728 -3.5102 249.0747 252.5849 277.9974 259.8705 -3.5158 249.1396 252.6554 278.1166 260.6985 -3.5172 249.2322 252.7494 278.2110 261.4650 -3.5210 249.3053 252.8263 278.3051 262.3135 -3.5232 249.3971 252.9203 278.3965 263.0903 -3.5260 249.4899 253.0159 278.4573 263.9080 -3.5271 249.5754 253.1024 278.5325 264.6950 -3.5303 249.6911 253.2214 278.6452 265.4923 -3.5278 249.8164 253.3442 278.7646 266.2895 -3.5319 249.9327 253.4646 278.8448 267.0765 -3.5377 250.0473 253.5850 278.9232 267.9045 -3.5412 250.1307 253.6719 279.0607 268.6710 -3.5441 250.2381 253.7822 279.1506 269.5205 -3.5458 250.3766 253.9224 279.2986 270.2870 -3.5482 250.4902 254.0384 279.4037 271.1150 -3.5510 250.6151 254.1661 279.4923 271.9020 -3.5554 250.7161 254.2716 279.6030 272.6993 -3.5531 250.7977 254.3508 279.7001 273.5273 -3.5547 250.8909 254.4456 279.8101 274.2835 -3.5571 250.9952 254.5523 279.9409 275.1115 -3.5593 251.1061 254.6654 280.0651 275.8783 -3.5621 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