DTA measure 1gyors Date: 2026310:1050 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.65 s Mass = 1164.400 mg data_number = 1343 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1383 1.4757 236.2070 234.7312 275.5763 1.9040 1.4756 236.4823 235.0067 275.4777 2.7518 1.4761 236.7755 235.2994 275.3545 3.5280 1.4779 237.0313 235.5535 275.2513 4.3450 1.4799 237.3085 235.8286 275.1109 5.1415 1.4770 237.5885 236.1114 274.9483 5.9383 1.4730 237.8538 236.3807 274.7688 6.7450 1.4760 238.1437 236.6677 274.5679 7.5315 1.4764 238.3915 236.9151 274.3649 8.3590 1.4775 238.6788 237.2013 274.1795 9.1245 1.4766 238.9418 237.4652 274.0298 9.9930 1.4733 239.1788 237.7056 273.8681 10.7488 1.4733 239.4261 237.9527 273.7421 11.5760 1.4764 239.6907 238.2143 273.6197 12.3730 1.4744 239.9286 238.4543 273.5280 13.1693 1.4701 240.1830 238.7129 273.4483 13.9968 1.4678 240.4291 238.9613 273.4173 14.7628 1.4652 240.6931 239.2279 273.4213 15.6208 1.4639 240.9936 239.5297 273.4572 16.3868 1.4659 241.2699 239.8041 273.5134 17.2140 1.4663 241.5187 240.0524 273.6618 18.0003 1.4678 241.7703 240.3025 273.7968 18.8075 1.4646 242.0313 240.5667 273.9617 19.6038 1.4668 242.2678 240.8009 274.1637 20.4005 1.4619 242.5339 241.0720 274.3856 21.2178 1.4560 242.8030 241.3470 274.6404 21.9938 1.4574 243.0108 241.5533 274.9676 22.8418 1.4560 243.2591 241.8031 275.3594 23.6075 1.4526 243.4988 242.0463 275.7001 24.4350 1.4480 243.7344 242.2864 276.1017 25.2318 1.4468 243.9666 242.5198 276.5190 26.0178 1.4566 244.2067 242.7501 276.9318 26.8455 1.4762 244.4532 242.9770 277.3550 27.6113 1.4695 244.7003 243.2309 277.7626 28.4693 1.4540 244.9845 243.5305 278.2143 29.2248 1.4466 245.2214 243.7748 278.5908 30.0625 1.4434 245.4983 244.0549 278.9907 30.8488 1.4384 245.7510 244.3126 279.3481 31.6455 1.4282 245.9724 244.5442 279.6798 32.4420 1.4235 246.1824 244.7589 279.9844 33.2385 1.4203 246.4204 245.0001 280.2813 34.0660 1.4287 246.6454 245.2166 280.5516 34.8215 1.4226 246.8706 245.4480 280.7812 35.6898 1.4082 247.1315 245.7233 281.0094 36.4458 1.3970 247.3549 245.9579 281.1463 37.2728 1.3857 247.5844 246.1987 281.2544 38.0698 1.3758 247.8389 246.4631 281.3598 38.8663 1.3658 248.0808 246.7150 281.4402 39.6938 1.3556 248.3677 247.0121 281.4794 40.4598 1.3476 248.6291 247.2815 281.4875 41.3175 1.3406 248.9025 247.5619 281.4727 42.0838 1.3342 249.1154 247.7812 281.4658 42.9110 1.3271 249.3135 247.9864 281.4213 43.7078 1.3206 249.5904 248.2699 281.3377 44.5045 1.3142 249.8264 248.5122 281.2589 45.3315 1.3102 250.0536 248.7433 281.1737 46.0975 1.3051 250.2762 248.9711 281.0719 46.9455 1.2989 250.5355 249.2366 280.9677 47.7215 1.2947 250.7497 249.4550 280.8720 48.5388 1.2888 250.9746 249.6858 280.7381 49.3353 1.2823 251.2064 249.9241 280.6574 50.1318 1.2746 251.4389 250.1643 280.5649 50.9695 1.2682 251.6580 250.3898 280.4949 51.7250 1.2629 251.8825 250.6196 280.4371 52.5830 1.2613 252.1431 250.8818 280.3863 53.3493 1.2571 252.3422 251.0851 280.3605 54.1865 1.2513 252.5840 251.3327 280.3777 54.9730 1.2474 252.8032 251.5558 280.4274 55.7595 1.2411 253.0033 251.7622 280.5019 56.5865 1.2360 253.2229 251.9869 280.5868 57.3528 1.2261 253.4770 252.2509 280.7091 58.2005 1.2183 253.7317 252.5135 280.8894 58.9765 1.2142 253.9426 252.7283 281.0871 59.7938 1.2073 254.1754 252.9681 281.2720 60.5903 1.2059 254.4017 253.1958 281.4897 61.3870 1.1996 254.6189 253.4193 281.7743 62.2043 1.1948 254.8607 253.6659 282.1189 62.9700 1.1874 255.0626 253.8753 282.4339 63.8285 1.1852 255.3031 254.1179 282.7820 64.5940 1.1821 255.5265 254.3445 283.1380 65.4215 1.1735 255.7627 254.5892 283.5048 66.2080 1.1644 255.9623 254.7979 283.8709 67.0145 1.1592 256.1803 255.0211 284.2301 67.8320 1.1516 256.4075 255.2559 284.5860 68.5978 1.1435 256.6229 255.4794 284.9323 69.4560 1.1344 256.8420 255.7076 285.2749 70.2220 1.1263 257.0339 255.9077 285.5676 71.0490 1.1197 257.2306 256.1108 285.8630 71.8358 1.1124 257.4491 256.3366 286.1413 72.6425 1.1095 257.6864 256.5770 286.3809 73.4595 1.1028 257.9125 256.8097 286.6183 74.2255 1.0974 258.1320 257.0347 286.8450 75.0835 1.0897 258.3679 257.2782 287.0467 75.8495 1.0858 258.5857 257.4999 287.1976 76.6770 1.0749 258.8362 257.7613 287.3669 77.4735 1.0670 259.0713 258.0043 287.4796 78.2703 1.0574 259.3007 258.2433 287.5686 79.0975 1.0495 259.5158 258.4663 287.6279 79.8633 1.0410 259.6848 258.6438 287.6593 80.7115 1.0330 259.9001 258.8670 287.6732 81.4873 1.0287 260.1070 259.0783 287.6611 82.3048 1.0203 260.3501 259.3298 287.6600 83.1115 1.0110 260.5662 259.5552 287.6216 83.8978 1.0052 260.7732 259.7680 287.5776 84.7358 1.0024 260.9794 259.9770 287.5159 85.4910 1.0003 261.1722 260.1720 287.4446 86.3495 0.9938 261.3940 260.4002 287.3568 87.0845 0.9899 261.5976 260.6077 287.2874 87.9425 0.9789 261.7951 260.8162 287.2089 88.6983 0.9721 261.9870 261.0150 287.1561 89.5255 0.9665 262.2119 261.2455 287.1028 90.3223 0.9596 262.4207 261.4610 287.0483 91.1088 0.9548 262.6163 261.6615 287.0193 91.9358 0.9480 262.7981 261.8500 287.0337 92.7018 0.9420 263.0071 262.0651 287.0589 93.5600 0.9369 263.2426 262.3057 287.1393 94.3155 0.9339 263.4336 262.4996 287.2219 95.1430 0.9239 263.6497 262.7259 287.3504 95.9088 0.9170 263.8400 262.9230 287.4545 96.7258 0.9119 264.0354 263.1235 287.5725 97.5330 0.9103 264.2450 263.3346 287.7361 98.3193 0.9025 264.4523 263.5499 287.9083 99.1470 0.8962 264.6873 263.7911 288.1078 99.9125 0.8888 264.8861 263.9974 288.3245 100.7708 0.8795 265.1175 264.2379 288.6191 101.5368 0.8691 265.2996 264.4305 288.8648 102.3538 0.8629 265.4646 264.6017 289.1541 103.1608 0.8552 265.6581 264.8030 289.4621 103.9470 0.8473 265.8564 265.0091 289.7711 104.7435 0.8365 266.0238 265.1873 290.0886 105.5403 0.8296 266.2213 265.3917 290.4221 106.3675 0.8225 266.4327 265.6102 290.7611 107.1335 0.8175 266.6409 265.8234 291.0636 107.9815 0.8155 266.8481 266.0327 291.3871 108.7573 0.8108 267.0454 266.2346 291.6702 109.5850 0.7990 267.2494 266.4505 291.9882 110.3815 0.7899 267.4585 266.6686 292.2629 111.1678 0.7790 267.6588 266.8798 292.5181 112.0055 0.7739 267.8725 267.0987 292.7689 112.7610 0.7675 268.0722 267.3047 292.9514 113.6295 0.7583 268.2944 267.5361 293.1617 114.3853 0.7515 268.4772 267.7257 293.3178 115.2225 0.7431 268.6944 267.9513 293.4642 116.0093 0.7372 268.9145 268.1773 293.5818 116.8160 0.7321 269.1058 268.3737 293.6803 117.6023 0.7252 269.2832 268.5580 293.7709 118.4093 0.7171 269.4849 268.7679 293.8340 119.2263 0.7100 269.6879 268.9779 293.8808 119.9923 0.7052 269.8903 269.1851 293.9117 120.8505 0.6902 270.1149 269.4247 293.9411 121.6060 0.6783 270.3094 269.6311 293.9394 122.4233 0.6712 270.5188 269.8476 293.9150 123.2300 0.6678 270.7229 270.0550 293.8881 124.0165 0.6598 270.9054 270.2456 293.8567 124.8338 0.6555 271.0921 270.4366 293.8193 125.6095 0.6463 271.2512 270.6049 293.7847 126.4578 0.6371 271.4558 270.8187 293.7231 127.2235 0.6288 271.6210 270.9921 293.6973 128.0508 0.6231 271.8088 271.1857 293.6763 128.8168 0.6182 271.9903 271.3721 293.6862 129.6440 0.6145 272.2035 271.5890 293.7077 130.4303 0.6108 272.4235 271.8126 293.7487 131.2375 0.6053 272.6445 272.0391 293.7723 132.0543 0.5967 272.8461 272.2495 293.8130 132.8203 0.5900 273.0108 272.4207 293.8903 133.6785 0.5811 273.2166 272.6355 293.9345 134.4443 0.5749 273.3921 272.8172 294.0298 135.2718 0.5705 273.6200 273.0495 294.1629 136.0580 0.5681 273.7994 273.2313 294.3022 136.8650 0.5602 274.0046 273.4443 294.4627 137.6823 0.5534 274.2020 273.6486 294.6782 138.4478 0.5455 274.3719 273.8264 294.8684 139.3063 0.5387 274.5918 274.0531 295.1191 140.0720 0.5359 274.7874 274.2516 295.3190 140.8995 0.5303 274.9919 274.4616 295.5864 141.6860 0.5224 275.1540 274.6316 295.8403 142.4925 0.5135 275.3364 274.8229 296.1194 143.3200 0.5102 275.5396 275.0294 296.4328 144.0860 0.5067 275.7029 275.1961 296.7100 144.9338 0.5001 275.8750 275.3749 297.0322 145.7100 0.4902 276.0626 275.5725 297.3133 146.5270 0.4831 276.2660 275.7828 297.6263 147.3235 0.4760 276.4431 275.9671 297.9188 148.1205 0.4707 276.6239 276.1532 298.1844 148.9475 0.4642 276.7964 276.3321 298.4555 149.7135 0.4581 276.9653 276.5072 298.6703 150.5718 0.4509 277.1603 276.7093 298.9226 151.3375 0.4431 277.3337 276.8906 299.1055 152.1648 0.4372 277.5287 277.0915 299.2919 152.9513 0.4285 277.7149 277.2864 299.4568 153.7475 0.4189 277.9513 277.5324 299.6269 154.5750 0.4136 278.1571 277.7435 299.7773 155.3410 0.4075 278.3321 277.9246 299.8814 156.1888 0.3992 278.5099 278.1107 299.9868 156.9650 0.3941 278.6552 278.2612 300.0670 157.7820 0.3858 278.8374 278.4515 300.1129 158.5683 0.3794 279.0152 278.6357 300.1607 159.3753 0.3715 279.2073 278.8358 300.2167 160.1923 0.3623 279.3892 279.0269 300.2407 160.9580 0.3542 279.5724 279.2182 300.2478 161.8163 0.3463 279.7706 279.4244 300.2686 162.5820 0.3408 279.9598 279.6189 300.2633 163.4093 0.3348 280.1423 279.8075 300.2562 164.1958 0.3303 280.3268 279.9965 300.2544 165.0025 0.3274 280.5095 280.1821 300.2370 165.8093 0.3223 280.6865 280.3641 300.2068 166.5958 0.3190 280.8500 280.5310 300.1871 167.4230 0.3129 281.0585 280.7456 300.1882 168.1890 0.3046 281.2297 280.9251 300.1931 169.0473 0.2989 281.4437 281.1448 300.1926 169.8130 0.2960 281.6156 281.3196 300.2111 170.6303 0.2905 281.8284 281.5379 300.2612 171.4370 0.2860 282.0108 281.7248 300.3198 172.2235 0.2821 282.1825 281.9004 300.4208 173.0510 0.2750 282.3633 282.0883 300.5290 173.8165 0.2696 282.5317 282.2620 300.6735 174.6748 0.2619 282.7382 282.4764 300.8195 175.4715 0.2584 282.8990 282.6406 300.9775 176.2578 0.2525 283.0719 282.8194 301.1519 177.0958 0.2452 283.2633 283.0181 301.3680 177.8510 0.2396 283.4216 283.1820 301.5542 178.7198 0.2308 283.6096 283.3788 301.7998 179.4753 0.2253 283.7820 283.5567 302.0154 180.3128 0.2166 284.0132 283.7965 302.2349 181.0995 0.2093 284.1938 283.9844 302.4940 181.9060 0.2039 284.3424 284.1384 302.7799 182.7233 0.1966 284.4978 284.3012 303.0745 183.4995 0.1904 284.6702 284.4798 303.3455 184.3163 0.1871 284.8577 284.6706 303.6463 185.0823 0.1798 285.0413 284.8615 303.9192 185.9200 0.1726 285.2060 285.0334 304.1997 186.6855 0.1682 285.3655 285.1973 304.4355 187.5440 0.1581 285.5346 285.3765 304.7026 188.2790 0.1512 285.7077 285.5565 304.9235 189.1268 0.1472 285.8682 285.7210 305.1608 189.9033 0.1389 286.0321 285.8933 305.3595 190.7200 0.1316 286.2103 286.0787 305.5515 191.5065 0.1234 286.3718 286.2484 305.7056 192.3135 0.1165 286.5550 286.4385 305.8513 193.1303 0.1105 286.7405 286.6301 305.9888 193.8965 0.1058 286.9167 286.8110 306.1059 194.7545 0.0900 287.1101 287.0202 306.2300 195.4895 0.0810 287.2893 287.2083 306.3257 196.3580 0.0743 287.4815 287.4072 306.4015 197.1238 0.0682 287.6459 287.5777 306.4501 197.9408 0.0603 287.8157 287.7554 306.4925 198.7480 0.0507 288.0275 287.9768 306.5380 199.5340 0.0472 288.2262 288.1790 306.5635 200.3618 0.0416 288.4166 288.3750 306.5778 201.1275 0.0394 288.5648 288.5255 306.5961 201.9855 0.0312 288.7529 288.7217 306.6171 202.7518 0.0268 288.9291 288.9023 306.6024 203.5788 0.0244 289.0938 289.0694 306.5797 204.3448 0.0210 289.2594 289.2384 306.5863 205.1723 0.0187 289.4500 289.4313 306.6173 205.9685 0.0133 289.6044 289.5911 306.6417 206.7755 0.0045 289.7914 289.7870 306.6419 207.5928 0.0014 289.9618 289.9604 306.6643 208.3688 -0.0017 290.1337 290.1355 306.6962 209.1963 -0.0073 290.3038 290.3111 306.8026 209.9620 -0.0133 290.4501 290.4634 306.8774 210.8095 -0.0197 290.6275 290.6472 306.9842 211.5860 -0.0247 290.7793 290.8040 307.1083 212.4030 -0.0232 290.9276 290.9508 307.2330 213.2098 -0.0189 291.1175 291.1364 307.3744 213.9965 -0.0188 291.2773 291.2962 307.5226 214.8338 -0.0163 291.4548 291.4710 307.7073 215.5895 -0.0121 291.6133 291.6254 307.8729 216.4478 -0.0130 291.8129 291.8259 308.0850 217.2133 -0.0203 291.9671 291.9873 308.2938 218.0308 -0.0230 292.1352 292.1581 308.5394 218.8273 -0.0278 292.2903 292.3181 308.7815 219.6238 -0.0261 292.4597 292.4858 309.0286 220.4205 -0.0274 292.6398 292.6672 309.2526 221.2170 -0.0366 292.8390 292.8756 309.4856 222.0343 -0.0423 293.0012 293.0435 309.7473 222.8003 -0.0457 293.1329 293.1787 310.0000 223.6583 -0.0452 293.3171 293.3624 310.3009 224.4140 -0.0526 293.4776 293.5303 310.5527 225.2515 -0.0597 293.6456 293.7053 310.8021 226.0380 -0.0626 293.8234 293.8860 311.0192 226.8348 -0.0675 294.0005 294.0681 311.2411 227.6310 -0.0728 294.2030 294.2757 311.4673 228.4278 -0.0738 294.3734 294.4472 311.6594 229.2553 -0.0778 294.5744 294.6522 311.8598 230.0105 -0.0808 294.7118 294.7925 312.0083 230.8793 -0.0839 294.8714 294.9553 312.1962 231.6450 -0.0986 295.0534 295.1520 312.3399 232.4723 -0.1173 295.2475 295.3648 312.4465 233.2590 -0.1344 295.4311 295.5655 312.5301 234.0655 -0.1489 295.5667 295.7156 312.6237 234.8828 -0.1580 295.7273 295.8853 312.6921 235.6590 -0.1688 295.8952 296.0640 312.7341 236.5065 -0.1779 296.0863 296.2642 312.7914 237.2828 -0.1889 296.2936 296.4825 312.8267 238.1000 -0.1965 296.4777 296.6742 312.8501 238.8963 -0.2010 296.6630 296.8640 312.8754 239.6930 -0.2100 296.8499 297.0599 312.9036 240.5000 -0.2116 297.0310 297.2426 312.9284 241.2860 -0.1898 297.1753 297.3652 312.9555 242.1135 -0.1885 297.3533 297.5419 312.9781 242.8795 -0.1999 297.5245 297.7244 313.0027 243.7478 -0.2148 297.7142 297.9290 313.0268 244.5035 -0.2254 297.8715 298.0969 313.0369 245.3308 -0.2235 298.0526 298.2760 313.0618 246.1275 -0.1904 298.2296 298.4200 313.1237 246.9345 -0.1983 298.4087 298.6070 313.1750 247.7515 -0.2171 298.5648 298.7820 313.2357 248.5175 -0.2322 298.7021 298.9343 313.3158 249.3755 -0.2435 298.8816 299.1251 313.4133 250.1313 -0.2507 299.0108 299.2615 313.4969 250.9588 -0.2597 299.1641 299.4238 313.5957 251.7550 -0.2680 299.3115 299.5795 313.7309 252.5415 -0.2787 299.4469 299.7257 313.8855 253.3690 -0.2865 299.6134 299.8999 314.0557 254.1348 -0.2897 299.7921 300.0818 314.2047 254.9625 -0.2949 299.9598 300.2547 314.4021 255.7280 -0.2987 300.1480 300.4468 314.5996 256.5760 -0.3079 300.3349 300.6428 314.8379 257.3523 -0.3136 300.4981 300.8116 315.0603 258.1690 -0.3126 300.6828 300.9954 315.3055 258.9658 -0.3159 300.8333 301.1493 315.5386 259.7625 -0.3151 300.9958 301.3109 315.8015 260.5895 -0.3121 301.1861 301.4982 316.0738 261.3558 -0.3212 301.3367 301.6579 316.3167 262.2035 -0.3336 301.4954 301.8290 316.5577 262.9795 -0.3398 301.6634 302.0032 316.7861 263.7968 -0.3500 301.8064 302.1564 317.0305 264.6035 -0.3585 301.9630 302.3215 317.2745 265.3898 -0.3638 302.1232 302.4870 317.4890 266.2275 -0.3717 302.3155 302.6872 317.7212 266.9830 -0.3638 302.4848 302.8486 317.9110 267.8413 -0.3290 302.6799 303.0089 318.1202 268.6073 -0.2970 302.8329 303.1299 318.2942 269.4343 -0.3018 302.9843 303.2861 318.4536 270.2310 -0.3154 303.1301 303.4454 318.5985 271.0175 -0.3351 303.2924 303.6275 318.7302 271.8550 -0.3494 303.4559 303.8053 318.8500 272.6210 -0.3308 303.6166 303.9474 318.9535 273.4790 -0.3105 303.7907 304.1012 319.0722 274.2348 -0.3284 303.9374 304.2658 319.1292 275.0725 -0.3536 304.1290 304.4826 319.1621 275.8585 -0.3726 304.2807 304.6533 319.2046 276.6655 -0.3898 304.4582 304.8480 319.2402 277.4828 -0.4047 304.6277 305.0324 319.2802 278.2588 -0.4185 304.7808 305.1993 319.2874 279.1070 -0.4329 304.9457 305.3785 319.3036 279.8725 -0.4416 305.0815 305.5231 319.3189 280.7000 -0.4515 305.2562 305.7077 319.3506 281.4968 -0.4603 305.4446 305.9049 319.3697 282.2933 -0.4673 305.5951 306.0623 319.4056 283.1105 -0.4759 305.7605 306.2365 319.4580 283.8763 -0.4860 305.9199 306.4059 319.4961 284.7345 -0.4912 306.0842 306.5755 319.5574 285.4903 -0.4937 306.2479 306.7416 319.6226 286.3275 -0.4979 306.4097 306.9076 319.6962 287.1143 -0.5045 306.5659 307.0704 319.7875 287.9108 -0.5115 306.7260 307.2375 319.8891 288.7380 -0.5232 306.8909 307.4141 319.9646 289.5040 -0.5247 307.0475 307.5723 320.0804 290.3518 -0.5246 307.2261 307.7508 320.2376 291.1175 -0.5318 307.4123 307.9441 320.3861 291.9450 -0.5380 307.5879 308.1259 320.5479 292.7108 -0.5415 307.7529 308.2944 320.7264 293.5280 -0.5488 307.9136 308.4624 320.9356 294.3658 -0.5515 308.0765 308.6280 321.1489 295.1210 -0.5558 308.2081 308.7639 321.3789 295.9795 -0.5592 308.3838 308.9431 321.5891 296.7145 -0.5630 308.5473 309.1104 321.7825 297.5725 -0.5681 308.7532 309.3213 322.0464 298.3388 -0.5686 308.8857 309.4543 322.2437 299.1555 -0.5722 309.0398 309.6120 322.4902 299.9628 -0.5776 309.1897 309.7673 322.7339 300.7490 -0.5871 309.3425 309.9295 322.9518 301.5763 -0.5873 309.5317 310.1190 323.1849 302.3733 -0.5892 309.6942 310.2834 323.4092 303.2003 -0.5960 309.8371 310.4331 323.6325 303.9663 -0.5995 309.9928 310.5924 323.8216 304.7835 -0.6055 310.1601 310.7656 324.0298 305.6210 -0.6129 310.3470 310.9599 324.2159 306.3768 -0.6173 310.5021 311.1194 324.3865 307.2450 -0.6168 310.6897 311.3065 324.5620 308.0005 -0.6210 310.8533 311.4743 324.7019 308.8383 -0.6297 311.0438 311.6735 324.8667 309.6245 -0.6346 311.2022 311.8368 324.9856 310.4313 -0.6375 311.3509 311.9884 325.1046 311.2180 -0.6405 311.5040 312.1445 325.2225 312.0245 -0.6485 311.6611 312.3097 325.3564 312.8418 -0.6570 311.8348 312.4918 325.4536 313.6078 -0.6629 311.9762 312.6391 325.5339 314.4655 -0.6701 312.1750 312.8451 325.6008 315.2213 -0.6704 312.3437 313.0141 325.6457 316.0385 -0.6724 312.5017 313.1741 325.6905 316.8450 -0.6786 312.6592 313.3378 325.7231 317.6315 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