DTA measure 1lassu Date: 2026310:120 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.73 s Mass = 1164.400 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4978 0.0299 231.5056 231.4757 215.9896 4.1124 0.0250 231.5491 231.5241 215.7098 5.7171 0.0218 231.6001 231.5783 215.4543 7.3265 0.0316 231.6396 231.6080 215.2251 8.9154 0.0578 231.6714 231.6137 215.0271 10.5201 0.0597 231.6803 231.6206 214.8741 12.1300 0.0674 231.6579 231.5905 214.7828 13.7499 0.0829 231.6461 231.5632 214.7540 15.3591 0.1045 231.6321 231.5276 214.8193 16.9638 0.1702 231.6371 231.4670 214.9968 18.5736 0.1845 231.6624 231.4779 215.2334 20.1784 0.1468 231.6568 231.5100 215.5610 21.7828 0.1305 231.6470 231.5165 215.9960 23.3920 0.1097 231.6675 231.5579 216.4515 25.0121 0.1002 231.6761 231.5758 216.9495 26.6220 0.1015 231.6914 231.5899 217.4462 28.2268 0.0991 231.7050 231.6059 217.9856 29.8365 0.0861 231.6717 231.5857 218.5209 31.4404 0.0773 231.6617 231.5844 218.9990 33.0451 0.0960 231.6668 231.5708 219.4877 34.6499 0.0898 231.6693 231.5795 219.9389 36.2700 0.1018 231.6855 231.5837 220.2958 37.8693 0.1034 231.6695 231.5660 220.6045 39.4580 0.0833 231.6696 231.5863 220.8678 41.0576 0.0697 231.6810 231.6113 221.0430 42.6573 0.0845 231.6800 231.5955 221.1953 44.2663 0.0835 231.6973 231.6138 221.2398 45.8709 0.0626 231.7087 231.6460 221.2826 47.4808 0.0467 231.7154 231.6687 221.3001 49.0955 0.0357 231.7526 231.7169 221.3065 50.6995 0.0264 231.7735 231.7471 221.2793 52.3094 0.0247 231.7936 231.7689 221.2281 53.9090 0.0443 231.7712 231.7269 221.2073 55.5131 0.0444 231.7689 231.7245 221.2174 57.1073 0.0525 231.7755 231.7230 221.2544 58.7120 0.0371 231.7950 231.7579 221.2836 60.3219 0.0242 231.8089 231.7847 221.3786 61.9414 0.0212 231.8669 231.8457 221.5263 63.5509 0.0320 231.9084 231.8764 221.7301 65.1556 0.0247 231.9139 231.8892 221.9555 66.7604 0.0182 231.9625 231.9443 222.1872 68.3694 0.0075 231.9616 231.9541 222.4931 69.9740 0.0131 231.9486 231.9355 222.8360 71.5839 0.0143 231.9947 231.9804 223.2006 73.2039 0.0047 232.0015 231.9968 223.5702 74.8129 -0.0074 232.0317 232.0390 223.9692 76.4176 -0.0065 232.0443 232.0507 224.3663 78.0224 0.0059 232.1019 232.0960 224.7539 79.6314 -0.0034 232.1466 232.1500 225.1089 81.2360 -0.0161 232.1588 232.1748 225.4505 82.8459 -0.0285 232.1562 232.1848 225.7618 84.4656 -0.0399 232.2074 232.2474 226.0100 86.0749 -0.0485 232.2911 232.3396 226.2480 87.6796 -0.0573 232.3148 232.3721 226.4865 89.2844 -0.0625 232.3338 232.3964 226.6562 90.8938 -0.0646 232.3645 232.4292 226.7608 92.4980 -0.0551 232.4059 232.4610 226.8407 94.1079 -0.0445 232.4199 232.4643 226.9125 95.7126 -0.0567 232.4277 232.4844 226.9817 97.3276 -0.0502 232.4304 232.4806 227.0219 98.9315 -0.0578 232.4582 232.5160 227.0786 100.5259 -0.0710 232.5613 232.6322 227.1750 102.1358 -0.0686 232.6475 232.7162 227.2641 103.7148 -0.0677 232.7041 232.7718 227.3669 105.3186 -0.0813 232.7682 232.8495 227.5328 106.9234 -0.0895 232.7996 232.8891 227.7073 108.5281 -0.0468 232.7986 232.8454 227.8724 110.1424 -0.0174 232.8206 232.8380 228.1015 111.7366 0.0032 232.8494 232.8463 228.3540 113.3363 0.0349 232.8910 232.8561 228.6287 114.9408 0.0580 232.9617 232.9037 228.8733 116.5448 0.0360 233.0371 233.0011 229.1837 118.1495 0.0628 233.0664 233.0037 229.5170 119.7594 0.0497 233.1066 233.0569 229.8592 121.3635 0.0146 233.2074 233.1928 230.1567 122.9833 -0.0077 233.2719 233.2796 230.4623 124.5931 0.0039 233.3549 233.3510 230.7853 126.1825 0.0082 233.4460 233.4377 231.0474 127.7923 -0.0215 233.4917 233.5132 231.2872 129.3961 -0.0525 233.5708 233.6233 231.5289 131.0060 -0.0763 233.6242 233.7005 231.7615 132.6108 -0.0917 233.6726 233.7643 231.9693 134.2153 -0.0926 233.7247 233.8174 232.1577 135.8398 -0.0964 233.7528 233.8492 232.3434 137.4445 -0.0809 233.8560 233.9369 232.5181 139.0544 -0.0794 233.9334 234.0129 232.6590 140.6584 -0.0931 234.0202 234.1133 232.7981 142.2680 -0.0885 234.0879 234.1764 232.9661 143.8728 -0.0634 234.1536 234.2170 233.0830 145.4774 -0.0666 234.2308 234.2973 233.1723 147.1018 -0.0676 234.3152 234.3827 233.2811 148.7065 -0.0713 234.4055 234.4769 233.4072 150.3215 0.0119 234.4964 234.4845 233.5488 151.9260 0.0665 234.5584 234.4919 233.7011 153.5351 0.0705 234.6517 234.5812 233.8668 155.1450 0.0333 234.7193 234.6860 234.0600 156.7549 0.0019 234.8051 234.8032 234.2583 158.3741 -0.0343 234.8996 234.9339 234.5046 159.9839 -0.0516 235.0022 235.0537 234.7688 161.5886 -0.0541 235.0672 235.1213 235.0566 163.1883 -0.0829 235.1792 235.2621 235.3848 164.7980 -0.1071 235.2840 235.3910 235.7053 166.3763 -0.1124 235.3822 235.4946 235.9856 167.9759 -0.0972 235.5276 235.6248 236.3185 169.5858 -0.0939 235.5889 235.6827 236.5865 171.1848 -0.0931 235.6719 235.7651 236.8798 172.7891 -0.0852 235.7844 235.8697 237.1470 174.3939 -0.0949 235.8709 235.9658 237.3958 175.9935 -0.0969 235.9737 236.0707 237.6245 177.5821 -0.0942 236.1149 236.2091 237.8590 179.1918 -0.0975 236.1725 236.2700 238.0367 180.7965 -0.0953 236.2778 236.3731 238.2097 182.4064 -0.0775 236.3621 236.4396 238.4055 184.0104 -0.0511 236.4572 236.5083 238.5770 185.6303 -0.0581 236.6022 236.6603 238.7142 187.2248 -0.0670 236.6528 236.7198 238.8176 188.8295 -0.0847 236.7450 236.8297 238.9134 190.4385 -0.0961 236.9072 237.0032 238.9930 192.0431 -0.0929 237.0177 237.1106 239.1350 193.6530 -0.0902 237.1235 237.2137 239.3235 195.2578 -0.0890 237.2221 237.3111 239.4956 196.8468 -0.0891 237.3549 237.4440 239.6543 198.4560 -0.0791 237.4951 237.5742 239.8325 200.0761 -0.0631 237.6115 237.6746 240.0225 201.6860 -0.0579 237.7387 237.7966 240.2491 203.2903 -0.0678 237.8561 237.9239 240.4798 204.8996 -0.0796 237.9822 238.0617 240.7182 206.5044 -0.0761 238.0860 238.1621 240.9878 208.1091 -0.0858 238.2224 238.3082 241.2404 209.7184 -0.0953 238.3555 238.4508 241.5768 211.3279 -0.0950 238.4909 238.5859 241.8960 212.9378 -0.0707 238.5685 238.6392 242.1915 214.5425 -0.0323 238.7061 238.7383 242.4654 216.1524 -0.0106 238.8681 238.8787 242.7234 217.7561 -0.0087 239.0217 239.0304 243.0261 219.3660 -0.0295 239.1662 239.1957 243.2965 220.9708 -0.0326 239.3049 239.3375 243.5003 222.5754 0.0124 239.4465 239.4341 243.6702 224.2000 -0.0199 239.6069 239.6268 243.8703 225.8045 -0.0449 239.7353 239.7802 244.0896 227.4144 -0.0360 239.8606 239.8966 244.2209 229.0086 -0.0013 239.9785 239.9798 244.3229 230.6075 -0.0198 240.0966 240.1164 244.4655 232.2123 -0.0334 240.2389 240.2723 244.6238 233.8170 -0.0283 240.3887 240.4170 244.7749 235.4011 -0.0160 240.5299 240.5459 244.8801 237.0204 -0.0054 240.6523 240.6577 245.0260 238.6251 0.0084 240.7902 240.7817 245.2035 240.2299 -0.0122 240.9371 240.9493 245.3953 241.8389 -0.0234 241.0967 241.1201 245.5692 243.4384 -0.0263 241.2522 241.2785 245.8010 245.0431 -0.0299 241.4303 241.4603 246.0166 246.6373 -0.0270 241.5730 241.6000 246.2678 248.2414 -0.0362 241.7207 241.7569 246.5292 249.8615 -0.0418 241.8402 241.8820 246.7980 251.4663 -0.0506 241.9736 242.0242 247.0483 253.0710 -0.0483 242.1457 242.1940 247.3400 254.6801 -0.0313 242.3017 242.3330 247.5790 256.2846 -0.0279 242.4193 242.4472 247.8607 257.8945 -0.0264 242.5572 242.5836 248.1117 259.4993 -0.0330 242.7051 242.7381 248.3607 261.1243 -0.0404 242.8764 242.9168 248.5985 262.7334 -0.0406 243.0453 243.0859 248.8377 264.3433 -0.0382 243.2135 243.2517 249.0573 265.9480 -0.0122 243.4140 243.4262 249.2434 267.5526 -0.0017 243.5802 243.5819 249.4394 269.1616 -0.0175 243.7362 243.7537 249.6340 270.7664 -0.0213 243.8958 243.9171 249.7960 272.3916 0.0277 244.0428 244.0152 249.9448 273.9964 0.0151 244.2142 244.1991 250.1090 275.6053 0.0077 244.3592 244.3515 250.2781 277.2100 0.0075 244.5481 244.5405 250.4520 278.8148 0.0102 244.7068 244.6966 250.6202 280.4244 -0.0048 244.8166 244.8214 250.7832 282.0284 0.0119 244.9676 244.9556 250.9302 283.6536 0.0926 245.1592 245.0665 251.1045 285.2584 0.0886 245.3404 245.2518 251.3277 286.8681 0.0545 245.5170 245.4625 251.5221 288.4720 0.0627 245.6525 245.5899 251.7180 290.0768 0.0572 245.8001 245.7429 251.9285 291.6815 0.0720 245.9871 245.9151 252.1416 293.2811 0.1106 246.1886 246.0780 252.4099 294.8799 0.0793 246.3824 246.3030 252.7117 296.4896 0.0567 246.5460 246.4893 252.9950 298.0893 0.0692 246.7001 246.6309 253.2905 299.6888 0.1090 246.8866 246.7777 253.5650 301.2978 0.1304 247.0531 246.9227 253.8681 302.8871 0.1152 247.2123 247.0971 254.1614 304.4970 0.1520 247.3932 247.2412 254.4200 306.1008 0.1550 247.5485 247.3935 254.6420 307.7004 0.1496 247.7256 247.5761 254.8472 309.3103 0.1467 247.9292 247.7825 255.0245 310.9140 0.1722 248.1462 247.9740 255.1904 312.5239 0.1782 248.3432 248.1650 255.3498 314.1286 0.1738 248.5149 248.3410 255.4712 315.7330 0.1775 248.6979 248.5203 255.6371 317.3423 0.1337 248.8824 248.7487 255.8023 318.9470 0.1361 249.0446 248.9084 255.9779 320.5569 0.0920 249.2025 249.1105 256.1422 322.1610 0.1107 249.3829 249.2722 256.2827 323.7705 0.0878 249.5666 249.4788 256.5042 325.3753 0.0739 249.7488 249.6749 256.7020 326.9896 0.0478 249.9621 249.9143 256.9119 328.5940 0.0628 250.1330 250.0701 257.1041 330.1988 0.0775 250.3071 250.2296 257.3306 331.8138 0.0656 250.5100 250.4444 257.5387 333.4021 0.0849 250.7006 250.6157 257.7912 335.0120 0.1219 250.8482 250.7263 258.0510 336.6321 0.1163 251.0403 250.9239 258.3162 338.2420 0.0944 251.2306 251.1362 258.5790 339.8509 0.0660 251.4314 251.3653 258.8059 341.4608 0.0427 251.6304 251.5877 259.0740 343.0655 0.0287 251.7924 251.7636 259.3437 344.6749 0.0166 252.0075 251.9910 259.6057 346.2791 0.0110 252.2184 252.2074 259.8203 347.8993 0.0087 252.4265 252.4178 260.0367 349.5143 0.0026 252.6181 252.6156 260.2307 351.1185 0.0239 252.8257 252.8018 260.4465 352.7279 0.0197 253.0209 253.0012 260.6470 354.3326 0.0067 253.2125 253.2057 260.8299 355.9425 -0.0008 253.3923 253.3931 261.0131 357.5369 -0.0062 253.6154 253.6217 261.2074 359.1561 -0.0056 253.7922 253.7978 261.3594 360.7558 -0.0054 253.9890 253.9944 261.5316 362.3605 -0.0048 254.1697 254.1745 261.7049 363.9496 -0.0080 254.3542 254.3622 261.8794 365.5485 -0.0104 254.5225 254.5329 262.0724 367.1533 -0.0107 254.7305 254.7412 262.2648 368.7528 -0.0082 254.9447 254.9529 262.4589 370.3618 -0.0085 255.0996 255.1082 262.6740 371.9819 -0.0149 255.3232 255.3381 262.8984 373.5866 -0.0176 255.4926 255.5102 263.1288 375.1963 -0.0200 255.7213 255.7413 263.3383 376.7951 -0.0213 255.9446 255.9659 263.5870 378.4050 -0.0277 256.1617 256.1894 263.8180 380.0098 -0.0284 256.3306 256.3590 264.0825 381.6145 -0.0293 256.5001 256.5294 264.3148 383.2390 -0.0299 256.7465 256.7764 264.5767 384.8435 -0.0263 256.9902 257.0165 264.8141 386.4534 -0.0256 257.1577 257.1833 265.0428 388.0580 -0.0165 257.3414 257.3579 265.2629 389.6670 -0.0243 257.5395 257.5638 265.4586 391.2718 -0.0274 257.7756 257.8030 265.6707 392.8765 -0.0268 257.9582 257.9850 265.8692 394.5015 -0.0266 258.1704 258.1971 266.0732 396.0901 -0.0281 258.3887 258.4168 266.2549 397.7000 -0.0280 258.5587 258.5867 266.4726 399.3098 -0.0266 258.7356 258.7622 266.6775 400.9188 -0.0287 258.9469 258.9756 266.9000 402.5235 -0.0260 259.1601 259.1862 267.1051 404.1334 -0.0284 259.4047 259.4330 267.3133 405.7379 -0.0304 259.6018 259.6322 267.5171 407.3573 -0.0297 259.8233 259.8530 267.7423 408.9671 -0.0327 260.0229 260.0557 267.9399 410.5719 -0.0337 260.2221 260.2557 268.1156 412.1818 -0.0326 260.3848 260.4174 268.2813 413.7856 -0.0322 260.5886 260.6208 268.4689 415.3954 -0.0372 260.8363 260.8735 268.6667 417.0001 -0.0397 261.0727 261.1124 268.8357 418.6203 -0.0355 261.3028 261.3383 269.0134 420.2301 -0.0345 261.5280 261.5624 269.2393 421.8296 -0.0330 261.7275 261.7605 269.4805 423.4233 -0.0309 261.9246 261.9556 269.6982 425.0331 -0.0305 262.1246 262.1551 269.9394 426.6328 -0.0265 262.3525 262.3790 270.1888 428.2324 -0.0251 262.5635 262.5885 270.4462 429.8519 -0.0301 262.7434 262.7736 270.7068 431.4563 -0.0312 262.9512 262.9824 270.9153 433.0559 -0.0329 263.1915 263.2244 271.1102 434.6658 -0.0360 263.3864 263.4224 271.3580 436.2703 -0.0377 263.6152 263.6528 271.5739 437.8640 -0.0400 263.8388 263.8788 271.7662 439.4739 -0.0500 264.0941 264.1441 271.9374 441.0838 -0.0567 264.2880 264.3447 272.1365 442.7031 -0.0629 264.4822 264.5451 272.3444 444.3076 -0.0640 264.7059 264.7698 272.5684 445.9175 -0.0650 264.8899 264.9549 272.7905 447.5219 -0.0682 265.0967 265.1649 272.9904 449.1311 -0.0727 265.2957 265.3684 273.2270 450.7359 -0.0756 265.5299 265.6055 273.4613 452.3458 -0.0780 265.7624 265.8404 273.6827 453.9650 -0.0805 265.9605 266.0410 273.8792 455.5543 -0.0797 266.1924 266.2721 274.0729 457.1795 -0.0735 266.4343 266.5078 274.2886 458.7689 -0.0827 266.6596 266.7423 274.4666 460.3830 -0.0864 266.8945 266.9808 274.6718 461.9876 -0.0888 267.1220 267.2108 274.8699 463.5975 -0.0919 267.3319 267.4238 275.0616 465.2021 -0.0938 267.5400 267.6338 275.3293 466.8265 -0.0944 267.7606 267.8549 275.5335 468.4313 -0.0990 267.9861 268.0850 275.7616 470.0360 -0.1049 268.1963 268.3011 275.9741 471.6459 -0.1099 268.4108 268.5208 276.1825 473.2496 -0.1079 268.6391 268.7470 276.3631 474.8595 -0.1114 268.8550 268.9664 276.5589 476.4643 -0.1090 269.0544 269.1634 276.7298 478.0886 -0.1106 269.2305 269.3411 276.9329 479.6933 -0.1133 269.4754 269.5887 277.1726 481.3134 -0.1176 269.7096 269.8272 277.3917 482.9181 -0.1239 269.9241 270.0481 277.6193 484.5220 -0.1252 270.1133 270.2385 277.8242 486.1215 -0.1214 270.3463 270.4678 278.0039 487.7211 -0.1186 270.5546 270.6732 278.2469 489.3361 -0.1201 270.7718 270.8919 278.4824 490.9453 -0.1301 270.9775 271.1077 278.6845 492.5446 -0.1089 271.2116 271.3206 278.9331 494.1443 -0.0730 271.4248 271.4978 279.1777 495.7541 -0.0835 271.6599 271.7434 279.4246 497.3589 -0.0941 271.8677 271.9618 279.6519 498.9583 -0.1015 272.0838 272.1853 279.8790 500.5674 -0.0894 272.3129 272.4023 280.0739 502.1721 -0.1081 272.5522 272.6603 280.2954 503.7820 -0.1194 272.7830 272.9024 280.5219 505.3863 -0.1235 272.9907 273.1142 280.7495 506.9956 -0.1249 273.2523 273.3773 280.9343 508.6004 -0.1037 273.4626 273.5663 281.1676 510.2103 -0.1141 273.6650 273.7791 281.3896 511.8196 -0.0908 273.8656 273.9564 281.5579 513.4393 -0.0910 274.1119 274.2030 281.7479 515.0491 -0.0983 274.3390 274.4373 281.9536 516.6533 -0.0756 274.5652 274.6408 282.1259 518.2525 -0.1084 274.7738 274.8821 282.2867 519.8573 -0.1369 275.0307 275.1676 282.4128 521.4671 -0.1570 275.2824 275.4394 282.5879 523.0714 -0.1777 275.5228 275.7005 282.8263 524.6808 -0.1842 275.7253 275.9095 283.0545 526.3009 -0.1882 275.9531 276.1414 283.2864 527.9056 -0.1612 276.1787 276.3399 283.5556 529.5300 -0.1307 276.3983 276.5290 283.7916 531.1346 -0.1544 276.5823 276.7367 284.0016 532.7445 -0.1733 276.7837 276.9571 284.2337 534.3490 -0.1891 277.0121 277.2012 284.5164 535.9735 -0.1987 277.2270 277.4257 284.7647 537.5783 -0.2116 277.4445 277.6561 284.9954 539.1933 -0.2187 277.6565 277.8752 285.2695 540.7976 -0.2228 277.8810 278.1039 285.5134 542.4018 -0.2282 278.1459 278.3742 285.6780 544.0116 -0.2347 278.4028 278.6375 285.8736 545.6164 -0.2139 278.5934 278.8073 286.0942 547.2410 -0.2185 278.8055 279.0239 286.2957 548.8351 -0.2344 279.0409 279.2753 286.5204 550.4399 -0.2429 279.2517 279.4946 286.7112 552.0446 -0.2493 279.4877 279.7370 286.8735 553.6434 -0.2276 279.7440 279.9715 287.0214 555.2429 -0.2351 279.9888 280.2239 287.1845 556.8528 -0.2334 280.2112 280.4447 287.3776 558.4524 -0.2365 280.4222 280.6587 287.5805 560.0571 -0.2499 280.6592 280.9091 287.7556 561.6660 -0.2635 280.9228 281.1863 287.9496 563.2656 -0.2717 281.1114 281.3831 288.1422 564.8703 -0.2718 281.3169 281.5887 288.3575 566.4793 -0.2794 281.5228 281.8022 288.5699 568.0840 -0.2867 281.7524 282.0392 288.7386 569.6734 -0.2746 281.9893 282.2639 288.9942 571.2781 -0.2859 282.3004 282.5863 289.2514 572.8974 -0.2852 282.5340 282.8192 289.4934 574.5686 -0.2905 282.7517 283.0422 289.7032 576.2349 -0.3009 282.9737 283.2746 289.9740 577.8448 -0.3062 283.1928 283.4990 290.2283 579.4490 -0.3121 283.4227 283.7347 290.5129 581.0584 -0.3166 283.6753 283.9919 290.7863 582.6631 -0.3204 283.9119 284.2323 291.0302 584.2833 -0.3287 284.1539 284.4826 291.2921 585.8925 -0.3340 284.3958 284.7298 291.5117 587.4969 -0.3325 284.6562 284.9887 291.7205 589.1068 -0.3363 284.8803 285.2166 291.9302 590.7114 -0.3456 285.0976 285.4432 292.1394 592.3101 -0.3450 285.3130 285.6580 292.3610 593.9149 -0.3464 285.5189 285.8654 292.5389 595.5248 -0.3478 285.7373 286.0851 292.7105 597.1603 -0.3472 286.0042 286.3514 292.8674 598.7493 -0.3519 286.2684 286.6204 293.0118 600.3790 -0.3567 286.4999 286.8566 293.1452 601.9684 -0.3649 286.7126 287.0775 293.3016 603.5834 -0.3681 286.9515 287.3196 293.4765 605.1871 -0.3770 287.1658 287.5428 293.6660 606.7970 -0.3867 287.4006 287.7873 293.8449 608.4171 -0.3947 287.6546 288.0493 294.0712 610.0264 -0.3997 287.8695 288.2692 294.2863 611.6359 -0.4063 288.0907 288.4970 294.5361 613.2458 -0.4051 288.2912 288.6963 294.7642 614.8399 -0.4077 288.4773 288.8850 295.0139 616.4389 -0.4118 288.6886 289.1004 295.2826 618.0436 -0.4142 288.9432 289.3574 295.5533 619.6586 -0.4198 289.2086 289.6284 295.8327 621.2624 -0.4234 289.4915 289.9149 296.1095 622.8569 -0.4276 289.7314 290.1591 296.3694 624.4668 -0.4293 289.9360 290.3653 296.6044 626.0711 -0.4327 290.1296 290.5623 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