DTA measure 2gyors Date: 2026310:1121 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.21 s Mass = 1164.400 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4045 -5.4838 467.3954 472.8791 432.5532 4.0128 -5.4888 467.3199 472.8087 432.7576 5.6214 -5.4951 467.2335 472.7286 432.9654 7.2146 -5.5044 467.1629 472.6672 433.1830 8.8281 -5.5003 467.0613 472.5616 433.3027 10.4315 -5.5142 466.9640 472.4782 433.3421 12.0400 -5.5249 466.8688 472.3937 433.2894 13.6639 -5.5347 466.8058 472.3405 433.2065 15.2724 -5.5390 466.7083 472.2473 433.0327 16.8755 -5.5442 466.6200 472.1642 432.7521 18.4841 -5.5241 466.5352 472.0593 432.4286 20.0926 -5.5265 466.4513 471.9778 432.0510 21.6805 -5.5319 466.3742 471.9061 431.6465 23.2789 -5.5237 466.2599 471.7836 431.1777 24.8821 -5.5248 466.1871 471.7119 430.7343 26.5060 -5.5306 466.1228 471.6534 430.2553 28.1094 -5.5234 466.0529 471.5763 429.7932 29.7179 -5.5210 465.9587 471.4797 429.3692 31.3214 -5.5235 465.8448 471.3683 428.9720 32.9245 -5.5231 465.7558 471.2789 428.6094 34.5331 -5.5201 465.6492 471.1694 428.2848 36.1418 -5.5152 465.5690 471.0842 428.0062 37.7348 -5.5073 465.4875 470.9948 427.7888 39.3588 -5.5066 465.3776 470.8843 427.6511 40.9674 -5.5093 465.2583 470.7677 427.5392 42.5705 -5.5061 465.1174 470.6234 427.4556 44.1791 -5.5046 464.9949 470.4995 427.4086 45.7876 -5.5021 464.8841 470.3862 427.4491 47.3961 -5.4952 464.7808 470.2760 427.4317 49.0048 -5.4964 464.7160 470.2124 427.4210 50.6286 -5.5020 464.6310 470.1329 427.3706 52.2319 -5.5051 464.5172 470.0223 427.3084 53.8303 -5.5061 464.3920 469.8981 427.2098 55.4335 -5.4915 464.2558 469.7473 427.0738 57.0370 -5.4873 464.1156 469.6029 426.8833 58.6453 -5.4856 463.9823 469.4679 426.6718 60.2486 -5.4896 463.9102 469.3998 426.4081 61.8468 -5.4853 463.7804 469.2657 426.1364 63.4654 -5.4816 463.6424 469.1239 425.8162 65.0689 -5.4806 463.4997 468.9803 425.4708 66.6773 -5.4796 463.3982 468.8778 425.1076 68.2859 -5.4796 463.3202 468.7998 424.7525 69.8945 -5.4761 463.1635 468.6396 424.4213 71.4978 -5.4725 463.0400 468.5125 424.0734 73.0960 -5.4666 462.9043 468.3709 423.7460 74.7148 -5.4656 462.8040 468.2696 423.4245 76.3284 -5.4443 462.6503 468.0946 423.1580 77.9370 -5.4341 462.5073 467.9414 422.9503 79.5505 -5.4332 462.3833 467.8165 422.7911 81.1539 -5.4315 462.2476 467.6791 422.6078 82.7471 -5.4238 462.1330 467.5568 422.4376 84.3506 -5.4219 461.9865 467.4083 422.3220 85.9540 -5.4254 461.8688 467.2942 422.2185 87.5575 -5.4227 461.7167 467.1395 422.1607 89.1454 -5.4211 461.5962 467.0173 422.0415 90.7693 -5.4216 461.4605 466.8822 421.9030 92.3729 -5.4167 461.3100 466.7267 421.7663 93.9658 -5.3731 461.1755 466.5487 421.6000 95.5693 -5.2827 461.0189 466.3016 421.4031 97.1779 -5.3083 460.8422 466.1505 421.2324 98.7863 -5.2817 460.6970 465.9787 421.0790 100.3948 -5.3058 460.5608 465.8667 420.8612 101.9981 -5.3276 460.3787 465.7062 420.6330 103.6014 -5.3339 460.2353 465.5692 420.4107 105.2203 -5.3375 460.0978 465.4352 420.1702 106.8336 -5.3322 459.9136 465.2458 419.8854 108.4371 -5.3327 459.7624 465.0951 419.5804 110.0508 -5.3365 459.6225 464.9591 419.2801 111.6439 -5.3327 459.5016 464.8343 418.9906 113.2575 -5.3369 459.3483 464.6852 418.7572 114.8659 -5.3370 459.1886 464.5256 418.4788 116.4745 -5.3375 459.0242 464.3617 418.2362 118.0780 -5.3340 458.8626 464.1966 418.0065 119.6813 -5.3320 458.7311 464.0631 417.8282 121.2796 -5.3302 458.5524 463.8826 417.5803 122.8831 -5.3304 458.3899 463.7204 417.3748 124.4761 -5.3054 458.2171 463.5225 417.1849 126.0950 -5.2922 458.0806 463.3728 417.0181 127.6883 -5.2886 457.9344 463.2231 416.8441 129.2915 -5.2899 457.7855 463.0754 416.6789 130.8950 -5.2918 457.6403 462.9321 416.5218 132.5240 -5.2876 457.4644 462.7520 416.3875 134.1170 -5.2921 457.2923 462.5844 416.2210 135.7306 -5.2908 457.1376 462.4284 416.0460 137.3390 -5.2872 456.9451 462.2323 415.8817 138.9476 -5.2839 456.7147 461.9986 415.6927 140.5563 -5.2785 456.5430 461.8215 415.5026 142.1594 -5.2833 456.3905 461.6738 415.2999 143.7680 -5.2937 456.2391 461.5328 415.0974 145.3916 -5.2940 456.0628 461.3568 414.8753 147.0053 -5.2940 455.8898 461.1837 414.6276 148.6085 -5.2960 455.7005 460.9965 414.3847 150.1914 -5.2952 455.5524 460.8476 414.1377 151.8000 -5.2891 455.3958 460.6849 413.8697 153.3980 -5.2709 455.2304 460.5013 413.6304 155.0066 -5.2447 455.0507 460.2954 413.3802 156.5945 -5.2069 454.9038 460.1107 413.1052 158.1979 -5.1845 454.7256 459.9101 412.8830 159.8219 -5.1617 454.5472 459.7089 412.6603 161.4251 -5.1484 454.3617 459.5101 412.4621 163.0338 -5.1366 454.1763 459.3129 412.2277 164.6373 -5.1385 453.9836 459.1221 412.0085 166.2456 -5.1367 453.8254 458.9621 411.8160 167.8543 -5.1367 453.6537 458.7904 411.6081 169.4578 -5.1327 453.4257 458.5584 411.4071 171.0866 -5.1597 453.2039 458.3636 411.2090 172.6901 -5.1819 453.0478 458.2298 411.0130 174.2988 -5.1921 452.9086 458.1007 410.8366 175.9020 -5.1981 452.7338 457.9319 410.6437 177.5158 -5.1988 452.5549 457.7537 410.4613 179.1193 -5.1976 452.3775 457.5751 410.2698 180.7328 -5.1978 452.2013 457.3991 410.0852 182.3158 -5.1958 452.0178 457.2136 409.9196 183.9295 -5.1939 451.8546 457.0486 409.7227 185.5379 -5.1943 451.6659 456.8602 409.5154 187.1363 -5.1886 451.4821 456.6707 409.3327 188.7296 -5.1780 451.3217 456.4997 409.1405 190.3328 -5.1724 451.1331 456.3055 408.9269 191.9363 -5.1666 450.9287 456.0953 408.7480 193.5450 -5.1585 450.7201 455.8787 408.5132 195.1535 -5.1586 450.5652 455.7238 408.2689 196.7465 -5.1539 450.3655 455.5194 408.0408 198.3655 -5.1468 450.1886 455.3355 407.7865 199.9791 -5.1437 449.9903 455.1339 407.5803 201.5824 -5.1345 449.8003 454.9348 407.3434 203.1808 -5.1282 449.6324 454.7607 407.0970 204.7840 -5.1229 449.4327 454.5556 406.8485 206.3978 -5.1201 449.2315 454.3516 406.6087 208.0013 -5.1172 449.0063 454.1235 406.3641 209.6148 -5.1154 448.8064 453.9218 406.1604 211.2336 -5.1130 448.6223 453.7354 405.9360 212.8423 -5.1075 448.4484 453.5559 405.7150 214.4301 -5.1054 448.2621 453.3676 405.5188 216.0285 -5.1008 448.0628 453.1636 405.3212 217.6320 -5.0976 447.8915 452.9891 405.0769 219.2354 -5.0996 447.6833 452.7829 404.8681 220.8439 -5.0923 447.4861 452.5784 404.6879 222.4474 -5.0883 447.2995 452.3878 404.4836 224.0455 -5.0899 447.1398 452.2297 404.3060 225.6644 -5.0849 446.9410 452.0259 404.1293 227.2679 -5.0737 446.7392 451.8130 403.9567 228.8763 -5.0623 446.5387 451.6010 403.7715 230.4798 -5.0559 446.3017 451.3577 403.5707 232.0884 -5.0541 446.1003 451.1543 403.3500 233.6916 -5.0502 445.9464 450.9966 403.1713 235.3054 -5.0418 445.7779 450.8197 403.0088 236.9240 -5.0399 445.5571 450.5970 402.7998 238.5325 -5.0363 445.3542 450.3905 402.5355 240.1411 -5.0338 445.1592 450.1930 402.3052 241.7498 -5.0329 444.9526 449.9855 402.1114 243.3583 -5.0283 444.7725 449.8009 401.8787 244.9515 -5.0172 444.6107 449.6280 401.6620 246.5499 -5.0132 444.4192 449.4324 401.4471 248.1531 -5.0039 444.2243 449.2282 401.2156 249.7720 -4.9926 444.0108 449.0034 400.9872 251.3755 -4.9933 443.8056 448.7988 400.7905 252.9788 -4.9828 443.6125 448.5953 400.5405 254.5874 -4.9752 443.4096 448.3848 400.2992 256.1909 -4.9719 443.2058 448.1777 400.1107 257.7993 -4.9701 443.0157 447.9857 399.8882 259.4028 -4.9648 442.7979 447.7627 399.6586 261.0268 -4.9566 442.6053 447.5619 399.4735 262.6300 -4.9481 442.3821 447.3302 399.2464 264.2388 -4.9408 442.1717 447.1125 399.0658 265.8474 -4.9395 441.9740 446.9135 398.8890 267.4508 -4.9339 441.7791 446.7131 398.6665 269.0593 -4.9292 441.5704 446.4997 398.4724 270.6628 -4.9281 441.3655 446.2936 398.2755 272.2918 -4.9236 441.1574 446.0810 398.0580 273.8951 -4.9186 440.9681 445.8867 397.8489 275.5089 -4.9112 440.7760 445.6872 397.6200 277.1123 -4.9063 440.5950 445.5013 397.4009 278.7208 -4.8973 440.3822 445.2796 397.1913 280.3243 -4.8920 440.1754 445.0674 396.9903 281.9225 -4.8825 439.9581 444.8406 396.8318 283.5155 -4.8776 439.7574 444.6351 396.6030 285.1293 -4.8735 439.5687 444.4421 396.3733 286.7379 -4.8657 439.3891 444.2547 396.1746 288.3411 -4.8629 439.1808 444.0437 395.9846 289.9294 -4.8586 438.9536 443.8123 395.7690 291.5376 -4.8478 438.7732 443.6211 395.5715 293.1413 -4.8539 438.5414 443.3953 395.3663 294.7499 -4.8497 438.3434 443.1931 395.1472 296.3584 -4.8421 438.1302 442.9724 394.9370 297.9566 -4.8349 437.9470 442.7819 394.7354 299.5806 -4.8278 437.7018 442.5296 394.5130 301.1891 -4.8206 437.5217 442.3423 394.3192 302.7925 -4.8136 437.3230 442.1366 394.1097 304.4011 -4.8077 437.1008 441.9084 393.8259 306.0044 -4.8014 436.8856 441.6870 393.5880 307.6129 -4.7920 436.6931 441.4851 393.3703 309.2164 -4.7878 436.4850 441.2728 393.1382 310.8350 -4.7819 436.3045 441.0864 392.9368 312.4231 -4.7720 436.0695 440.8415 392.7208 314.0266 -4.7654 435.8877 440.6531 392.4975 315.6349 -4.7563 435.6575 440.4138 392.3359 317.2384 -4.7465 435.4564 440.2029 392.1476 318.8366 -4.7403 435.2524 439.9927 391.9250 320.4451 -4.7425 435.0446 439.7871 391.7006 322.0333 -4.7416 434.8556 439.5971 391.5241 323.6469 -4.7326 434.6268 439.3594 391.3468 325.2655 -4.7243 434.4296 439.1538 391.1546 326.8741 -4.7158 434.1955 438.9113 390.9417 328.4825 -4.7132 434.0052 438.7184 390.7253 330.0911 -4.7072 433.7936 438.5008 390.5241 331.6946 -4.7019 433.5996 438.3016 390.2818 333.2926 -4.6948 433.3686 438.0634 390.0760 334.8961 -4.6852 433.1690 437.8543 389.8616 336.5046 -4.6762 433.0054 437.6816 389.6124 338.1284 -4.6717 432.8260 437.4977 389.3837 339.7319 -4.6666 432.5594 437.2260 389.1855 341.3454 -4.6588 432.3666 437.0254 388.9855 342.9438 -4.6583 432.1885 436.8467 388.7804 344.5471 -4.6532 431.9394 436.5927 388.5892 346.1504 -4.6494 431.7295 436.3789 388.3810 347.7486 -4.6446 431.5002 436.1448 388.1957 349.3573 -4.6370 431.2809 435.9179 387.9644 350.9605 -4.6317 431.0821 435.7138 387.7278 352.5691 -4.6292 430.8843 435.5136 387.4924 354.1724 -4.6208 430.6728 435.2936 387.2977 355.7759 -4.6084 430.4559 435.0643 387.0951 357.3898 -4.5947 430.2517 434.8464 386.9230 358.9930 -4.5867 430.0771 434.6639 386.6865 360.6015 -4.5919 429.8825 434.4744 386.4691 362.2204 -4.5838 429.7080 434.2918 386.2382 363.8340 -4.5845 429.4711 434.0556 386.0322 365.4375 -4.5761 429.2594 433.8355 385.8056 367.0513 -4.5720 429.0504 433.6223 385.5994 368.6494 -4.5650 428.8357 433.4007 385.4191 370.2579 -4.5572 428.6312 433.1883 385.2555 371.8666 -4.5501 428.4302 432.9803 385.0441 373.4750 -4.5428 428.2455 432.7883 384.8512 375.0938 -4.5346 428.0206 432.5553 384.6385 376.6973 -4.5345 427.8012 432.3357 384.3905 378.3005 -4.5318 427.5579 432.0897 384.1488 379.8989 -4.5311 427.3579 431.8889 383.9183 381.5075 -4.5240 427.1237 431.6477 383.6884 383.0954 -4.5140 426.9143 431.4284 383.5061 384.7040 -4.5016 426.7063 431.2080 383.2915 386.3075 -4.4926 426.5055 430.9982 383.0734 387.9313 -4.4898 426.3427 430.8325 382.8636 389.5349 -4.4801 426.1252 430.6053 382.6373 391.1384 -4.4707 425.9219 430.3926 382.4074 392.7519 -4.4639 425.7077 430.1716 382.2024 394.3553 -4.4578 425.4634 429.9213 382.0185 395.9639 -4.4552 425.2311 429.6863 381.8169 397.5671 -4.4484 425.0236 429.4719 381.5999 399.1809 -4.4413 424.8244 429.2657 381.3807 400.7844 -4.4342 424.6025 429.0367 381.1848 402.3979 -4.4237 424.4180 428.8418 380.9913 404.0014 -4.4184 424.2084 428.6268 380.8023 405.6100 -4.4143 423.9861 428.4003 380.5757 407.2135 -4.4071 423.8221 428.2292 380.3542 408.8169 -4.3996 423.6310 428.0306 380.1491 410.4203 -4.3917 423.4254 427.8170 379.9295 412.0339 -4.3831 423.2118 427.5948 379.7268 413.6424 -4.3748 422.9821 427.3569 379.5194 415.2459 -4.3708 422.7486 427.1195 379.2995 416.8439 -4.3594 422.5219 426.8813 379.0758 418.4526 -4.3494 422.3337 426.6831 378.8934 420.0508 -4.3427 422.1232 426.4658 378.6939 421.6593 -4.3370 421.9108 426.2478 378.4519 423.2679 -4.3342 421.6705 426.0047 378.1863 424.8916 -4.3339 421.4551 425.7890 377.9715 426.4950 -4.3281 421.2448 425.5728 377.7689 428.1036 -4.3182 421.0472 425.3654 377.5783 429.7119 -4.3181 420.8360 425.1541 377.4002 431.3205 -4.3092 420.5998 424.9090 377.1684 432.9288 -4.3008 420.3338 424.6346 376.9422 434.5373 -4.2921 420.1348 424.4269 376.7430 436.1561 -4.2862 419.9334 424.2196 376.5258 437.7645 -4.2818 419.7088 423.9906 376.2928 439.3629 -4.2770 419.5178 423.7948 376.0702 440.9663 -4.2675 419.3074 423.5748 375.8421 442.5748 -4.2639 419.1098 423.3736 375.6018 444.1731 -4.2603 418.9265 423.1868 375.3994 445.7765 -4.2548 418.6898 422.9446 375.2045 447.3953 -4.2456 418.4679 422.7136 374.9967 448.9988 -4.2359 418.2270 422.4629 374.8278 450.5970 -4.2261 418.0211 422.2472 374.6183 452.2005 -4.2152 417.8617 422.0769 374.4535 453.8091 -4.2115 417.6606 421.8721 374.2305 455.4124 -4.2086 417.4296 421.6383 374.0224 457.0158 -4.2017 417.1763 421.3780 373.8342 458.6245 -4.1991 416.9696 421.1687 373.6339 460.2536 -4.1954 416.7347 420.9302 373.4639 461.8620 -4.1873 416.5220 420.7093 373.2460 463.4706 -4.1878 416.3262 420.5140 373.0278 465.0793 -4.1849 416.1153 420.3001 372.7884 466.6824 -4.1771 415.9021 420.0792 372.5844 468.2911 -4.1711 415.6821 419.8533 372.3574 469.8998 -4.1608 415.4626 419.6234 372.1583 471.5184 -4.1440 415.2678 419.4119 371.9170 473.1219 -4.1346 415.0675 419.2020 371.6762 474.7048 -4.1295 414.8703 418.9998 371.4714 476.3131 -4.1235 414.6061 418.7296 371.2446 477.9166 -4.1190 414.3813 418.5003 371.0627 479.5251 -4.1166 414.1662 418.2828 370.8628 481.1285 -4.1107 413.9729 418.0836 370.6465 482.7371 -4.1076 413.7510 417.8587 370.3889 484.3556 -4.1041 413.5440 417.6481 370.1774 485.9591 -4.0979 413.3331 417.4310 369.9807 487.5678 -4.0899 413.1622 417.2521 369.7920 489.1710 -4.0825 412.9482 417.0307 369.5810 490.7796 -4.0815 412.7399 416.8214 369.3593 492.3883 -4.0715 412.5454 416.6169 369.1691 493.9966 -4.0632 412.3330 416.3962 368.9628 495.6154 -4.0635 412.0888 416.1523 368.7580 497.2290 -4.0556 411.8721 415.9278 368.5232 498.8324 -4.0500 411.6835 415.7335 368.3202 500.4411 -4.0487 411.4695 415.5182 368.1055 502.0599 -4.0449 411.2473 415.2922 367.8692 503.6631 -4.0407 411.0193 415.0601 367.6568 505.2820 -4.0322 410.8088 414.8410 367.4713 506.8854 -4.0237 410.5679 414.5916 367.2781 508.4733 -4.0171 410.3332 414.3502 367.0562 510.0768 -4.0067 410.1266 414.1333 366.8460 511.6954 -4.0007 409.9319 413.9326 366.6490 513.3039 -3.9939 409.7011 413.6949 366.4402 514.9073 -3.9842 409.4898 413.4740 366.2372 516.5311 -3.9780 409.2984 413.2764 366.0266 518.1346 -3.9694 409.0417 413.0110 365.8096 519.7380 -3.9635 408.8405 412.8040 365.6160 521.3465 -3.9577 408.6200 412.5777 365.3891 522.9500 -3.9491 408.4026 412.3518 365.2034 524.5635 -3.9488 408.2136 412.1624 364.9547 526.1669 -3.9391 408.0225 411.9616 364.7274 527.7909 -3.9331 407.8199 411.7530 364.4846 529.3941 -3.9302 407.6479 411.5781 364.2308 531.0078 -3.9233 407.4214 411.3447 363.9811 532.6111 -3.9170 407.2022 411.1192 363.7781 534.2248 -3.9094 406.9859 410.8953 363.5919 535.8283 -3.9036 406.7893 410.6930 363.3811 537.4316 -3.8961 406.5466 410.4427 363.1623 539.0504 -3.8865 406.2814 410.1680 362.9692 540.6486 -3.8855 406.0816 409.9671 362.7692 542.2573 -3.8801 405.8890 409.7690 362.5570 543.8605 -3.8650 405.6820 409.5470 362.3697 545.4640 -3.8574 405.4684 409.3258 362.1782 547.0573 -3.8432 405.2625 409.1057 361.9828 548.6605 -3.8416 405.0588 408.9005 361.7787 550.2846 -3.8451 404.8144 408.6596 361.5946 551.9034 -3.8309 404.5527 408.3836 361.3793 553.5119 -3.7825 404.3425 408.1250 361.1759 555.1154 -3.7087 404.0935 407.8022 360.9866 556.7188 -3.6786 403.9085 407.5871 360.7934 558.3273 -3.6667 403.7140 407.3807 360.5979 559.9359 -3.6892 403.5137 407.2030 360.3330 561.5598 -3.7107 403.3102 407.0208 360.1088 563.1631 -3.7284 403.1150 406.8434 359.9008 564.7719 -3.7366 402.8757 406.6122 359.6678 566.3804 -3.7348 402.6579 406.3926 359.4447 567.9888 -3.7342 402.4480 406.1821 359.2166 569.5923 -3.7337 402.2249 405.9586 358.9939 571.1749 -3.7294 402.0045 405.7339 358.7637 572.7835 -3.7242 401.7940 405.5182 358.5511 574.3970 -3.7257 401.5946 405.3203 358.3461 576.0055 -3.7256 401.3494 405.0750 358.1167 577.6089 -3.7254 401.0922 404.8176 357.9105 579.2121 -3.7179 400.8846 404.6025 357.6906 580.8209 -3.7113 400.6901 404.4014 357.4977 582.4243 -3.7059 400.4809 404.1868 357.2963 584.0223 -3.7025 400.3080 404.0104 357.0853 585.6258 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