DTA measure 1DTA1_PB4 Date: 202623:141 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.87 s Mass = 1173.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3744 -0.2898 237.9468 238.2366 219.8221 3.9843 -0.2784 237.9394 238.2178 219.5525 5.5890 -0.2648 237.9266 238.1913 219.2585 7.1935 -0.2492 237.9494 238.1986 218.9518 8.8078 -0.2368 237.9610 238.1977 218.6412 10.4125 -0.2231 237.9732 238.1964 218.3566 12.0224 -0.2088 237.9686 238.1773 218.0525 13.6218 -0.2010 237.9678 238.1688 217.8105 15.2206 -0.1911 237.9396 238.1307 217.5754 16.8305 -0.1809 237.9046 238.0855 217.3054 18.4301 -0.1724 237.8789 238.0513 217.0934 20.0339 -0.1615 237.8858 238.0473 216.8972 21.6386 -0.1551 237.8704 238.0255 216.7762 23.2434 -0.1492 237.8470 237.9962 216.6740 24.8679 -0.1415 237.8438 237.9853 216.6243 26.4570 -0.1377 237.8506 237.9883 216.6507 28.0669 -0.1315 237.8082 237.9398 216.7223 29.6715 -0.1275 237.7809 237.9084 216.8983 31.2754 -0.1190 237.7653 237.8843 217.1680 32.8853 -0.1137 237.7771 237.8909 217.5477 34.4900 -0.1157 237.7363 237.8520 217.9461 36.0996 -0.1181 237.7485 237.8666 218.4345 37.7190 -0.1136 237.7395 237.8531 218.9354 39.3340 -0.1113 237.7091 237.8204 219.4608 40.9388 -0.1163 237.6502 237.7665 219.9970 42.5486 -0.1203 237.5999 237.7201 220.5229 44.1473 -0.1207 237.5797 237.7004 220.9833 45.7469 -0.1274 237.5465 237.6739 221.3929 47.3516 -0.1340 237.4980 237.6320 221.7827 48.9718 -0.1394 237.4461 237.5855 222.1202 50.5705 -0.1458 237.4326 237.5784 222.3863 52.1751 -0.1492 237.4173 237.5665 222.5798 53.7799 -0.1508 237.4165 237.5674 222.7340 55.3846 -0.1493 237.3937 237.5429 222.8242 56.9938 -0.1514 237.3742 237.5256 222.8667 58.5983 -0.1580 237.3410 237.4990 222.9464 60.2235 -0.1686 237.3375 237.5061 223.0013 61.8279 -0.1739 237.3423 237.5162 222.9945 63.4320 -0.1773 237.3212 237.4985 223.0062 65.0316 -0.1803 237.3051 237.4854 223.0110 66.6466 -0.1854 237.3300 237.5153 223.0403 68.2505 -0.1953 237.2987 237.4940 223.0764 69.8551 -0.1966 237.2952 237.4917 223.1222 71.4650 -0.2037 237.2778 237.4815 223.1829 73.0851 -0.2047 237.2444 237.4491 223.2760 74.6950 -0.2139 237.2044 237.4184 223.4319 76.2998 -0.2173 237.2084 237.4256 223.6486 77.8940 -0.2162 237.2123 237.4285 223.8909 79.5031 -0.2210 237.2419 237.4629 224.1564 81.1079 -0.2239 237.2417 237.4656 224.4440 82.7075 -0.2303 237.2074 237.4377 224.7528 84.3169 -0.2369 237.2035 237.4404 225.0832 85.9211 -0.2411 237.1827 237.4238 225.4478 87.5310 -0.2431 237.1680 237.4111 225.8015 89.1358 -0.2534 237.1475 237.4009 226.1178 90.7455 -0.2606 237.1603 237.4209 226.4525 92.3494 -0.2655 237.1837 237.4492 226.7922 93.9388 -0.2733 237.1884 237.4617 227.0940 95.5538 -0.2870 237.2178 237.5048 227.3975 97.1575 -0.2967 237.2549 237.5516 227.6944 98.7828 -0.2993 237.2518 237.5512 227.9254 100.3875 -0.3086 237.2286 237.5372 228.1330 101.9974 -0.3085 237.2228 237.5312 228.3009 103.6063 -0.3100 237.2417 237.5517 228.4201 105.2008 -0.3100 237.2391 237.5490 228.5322 106.8055 -0.3229 237.2571 237.5800 228.6571 108.4154 -0.3296 237.2796 237.6093 228.7886 110.0143 -0.3292 237.2777 237.6069 228.9109 111.6341 -0.3352 237.2773 237.6125 228.9982 113.2389 -0.3419 237.3366 237.6784 229.0674 114.8385 -0.3488 237.3488 237.6976 229.1589 116.4431 -0.3559 237.3285 237.6844 229.2969 118.0521 -0.3614 237.3347 237.6961 229.4430 119.6415 -0.3634 237.3323 237.6956 229.5952 121.2514 -0.3658 237.3833 237.7491 229.7418 122.8553 -0.3699 237.4349 237.8048 229.9495 124.4753 -0.3724 237.4603 237.8327 230.1502 126.0851 -0.3756 237.4972 237.8728 230.4101 127.6894 -0.3814 237.5296 237.9110 230.6829 129.2988 -0.3836 237.5346 237.9182 230.9659 130.8933 -0.3860 237.5671 237.9531 231.2798 132.5031 -0.3845 237.6243 238.0087 231.5917 134.1128 -0.3892 237.6643 238.0535 231.9047 135.7219 -0.3900 237.6812 238.0712 232.1986 137.3471 -0.3896 237.7219 238.1116 232.4476 138.9570 -0.4027 237.7749 238.1776 232.7258 140.5618 -0.4080 237.8160 238.2240 232.9927 142.1504 -0.4107 237.8534 238.2641 233.2324 143.7498 -0.4115 237.9164 238.3279 233.4265 145.3545 -0.4150 237.9317 238.3467 233.6281 146.9590 -0.4209 237.9635 238.3844 233.8739 148.5630 -0.4200 238.0144 238.4344 234.0971 150.1831 -0.4225 238.0526 238.4750 234.2514 151.7930 -0.4300 238.1079 238.5378 234.4275 153.3971 -0.4273 238.1488 238.5760 234.5685 155.0066 -0.4264 238.2174 238.6439 234.7223 156.6114 -0.4324 238.2567 238.6891 234.8519 158.2159 -0.4350 238.2725 238.7075 234.9458 159.8250 -0.4369 238.3055 238.7423 235.0584 161.4451 -0.4362 238.4059 238.8421 235.1938 163.0550 -0.4393 238.5033 238.9426 235.3656 164.6596 -0.4366 238.5459 238.9825 235.5164 166.2686 -0.4393 238.6330 239.0722 235.7184 167.8734 -0.4365 238.7090 239.1455 235.9412 169.4781 -0.4328 238.7585 239.1913 236.1562 171.0880 -0.4329 238.8409 239.2739 236.3605 172.7081 -0.4372 238.8979 239.3351 236.6259 174.3068 -0.4396 239.0080 239.4475 236.8923 175.9115 -0.4432 239.0955 239.5387 237.1572 177.5111 -0.4446 239.1582 239.6028 237.4156 179.1056 -0.4456 239.2057 239.6513 237.6895 180.7094 -0.4472 239.2573 239.7045 237.9243 182.3141 -0.4520 239.3170 239.7690 238.1747 183.9189 -0.4526 239.4133 239.8659 238.4586 185.5236 -0.4559 239.4973 239.9533 238.7221 187.1331 -0.4550 239.5611 240.0161 238.9490 188.7475 -0.4559 239.6374 240.0933 239.1902 190.3574 -0.4582 239.7051 240.1633 239.4054 191.9468 -0.4575 239.8220 240.2795 239.5918 193.5565 -0.4555 239.9358 240.3913 239.8165 195.1604 -0.4565 240.0377 240.4942 240.0267 196.7754 -0.4604 240.1306 240.5910 240.2323 198.3801 -0.4572 240.2240 240.6813 240.4456 200.0001 -0.4559 240.3050 240.7609 240.5999 201.6095 -0.4569 240.4261 240.8830 240.7757 203.2139 -0.4585 240.5157 240.9742 240.9479 204.8238 -0.4575 240.5992 241.0567 241.1256 206.4131 -0.4547 240.6713 241.1260 241.2610 208.0125 -0.4531 240.7603 241.2133 241.4399 209.6165 -0.4596 240.8558 241.3154 241.6066 211.2213 -0.4587 240.9652 241.4239 241.7728 212.8260 -0.4552 241.0512 241.5064 241.9671 214.4356 -0.4496 241.1618 241.6114 242.1384 216.0396 -0.4503 241.2893 241.7396 242.3565 217.6495 -0.4511 241.3748 241.8259 242.5697 219.2543 -0.4498 241.4910 241.9408 242.7981 220.8631 -0.4495 241.5772 242.0266 243.0449 222.4679 -0.4523 241.6520 242.1043 243.2548 224.0778 -0.4471 241.7565 242.2036 243.4872 225.6820 -0.4448 241.8575 242.3024 243.7089 227.3016 -0.4474 241.9710 242.4184 243.9711 228.8961 -0.4517 242.1023 242.5541 244.2567 230.5009 -0.4526 242.2485 242.7011 244.4958 232.1108 -0.4541 242.3889 242.8430 244.7516 233.7151 -0.4526 242.5315 242.9841 244.9943 235.3244 -0.4543 242.6499 243.1041 245.2368 236.9291 -0.4559 242.7852 243.2411 245.4661 238.5490 -0.4588 242.9082 243.3670 245.7029 240.1581 -0.4579 243.0095 243.4674 245.9179 241.7578 -0.4501 243.1333 243.5835 246.1121 243.3625 -0.4492 243.2553 243.7045 246.2975 244.9673 -0.4466 243.3680 243.8146 246.5131 246.5664 -0.4521 243.4905 243.9426 246.6741 248.1758 -0.4538 243.6247 244.0785 246.8818 249.7959 -0.4535 243.7689 244.2224 247.0604 251.4006 -0.4446 243.8797 244.3243 247.1943 252.9948 -0.4368 244.0201 244.4569 247.4121 254.5989 -0.4390 244.1531 244.5921 247.5933 256.2241 -0.4398 244.2544 244.6942 247.7570 257.8135 -0.4378 244.3638 244.8016 247.9261 259.4384 -0.4385 244.4637 244.9022 248.1169 261.0476 -0.4374 244.6048 245.0422 248.2960 262.6575 -0.4372 244.7508 245.1880 248.4826 264.2776 -0.4394 244.9320 245.3714 248.6689 265.8823 -0.4335 245.0403 245.4738 248.8803 267.4913 -0.4295 245.1916 245.6211 249.0907 269.1011 -0.4263 245.3060 245.7322 249.3056 270.7059 -0.4269 245.4218 245.8487 249.5819 272.2899 -0.4225 245.5932 246.0157 249.8621 273.9041 -0.4206 245.7636 246.1842 250.0708 275.5140 -0.4199 245.9361 246.3560 250.3475 277.1136 -0.4191 246.0860 246.5051 250.6237 278.7184 -0.4189 246.1793 246.5981 250.8669 280.3176 -0.4227 246.3116 246.7343 251.1051 281.9269 -0.4208 246.4327 246.8535 251.3676 283.5316 -0.4190 246.5988 247.0179 251.5837 285.1409 -0.4208 246.7413 247.1620 251.8114 286.7453 -0.4194 246.8949 247.3143 252.0443 288.3705 -0.4148 247.0971 247.5119 252.2121 289.9749 -0.4134 247.2816 247.6951 252.3724 291.5790 -0.4152 247.4256 247.8408 252.5642 293.1889 -0.4171 247.5567 247.9738 252.7621 294.7988 -0.4181 247.7279 248.1460 252.8989 296.3926 -0.4154 247.8854 248.3008 253.0458 297.9970 -0.4145 248.0019 248.4165 253.2245 299.6069 -0.4133 248.1216 248.5349 253.4224 301.2270 -0.4134 248.3142 248.7276 253.5953 302.8318 -0.4165 248.5009 248.9174 253.7866 304.4365 -0.4173 248.6760 249.0933 253.9679 306.0198 -0.4153 248.8504 249.2658 254.1829 307.6245 -0.4146 249.0085 249.4232 254.4198 309.2293 -0.4102 249.1581 249.5684 254.6579 310.8335 -0.4075 249.3269 249.7344 254.9210 312.4429 -0.4089 249.4558 249.8646 255.1401 314.0323 -0.4082 249.6386 250.0469 255.3322 315.6575 -0.4110 249.8002 250.2113 255.6032 317.2613 -0.4136 249.9813 250.3949 255.8588 318.8660 -0.4111 250.1264 250.5375 256.1190 320.4810 -0.4136 250.2843 250.6980 256.3610 322.0704 -0.4149 250.4324 250.8473 256.6238 323.6803 -0.4166 250.6097 251.0263 256.8578 325.2844 -0.4174 250.7808 251.1982 257.0790 326.8990 -0.4166 250.9715 251.3881 257.2729 328.5191 -0.4153 251.1567 251.5720 257.4925 330.1290 -0.4154 251.3632 251.7786 257.7223 331.7331 -0.4190 251.5151 251.9341 257.9082 333.3478 -0.4198 251.6918 252.1117 258.0619 334.9423 -0.4185 251.8846 252.3031 258.2532 336.5419 -0.4163 252.0211 252.4374 258.4176 338.1459 -0.4175 252.2022 252.6197 258.5713 339.7658 -0.4196 252.4020 252.8216 258.7333 341.3654 -0.4132 252.5975 253.0106 258.9011 342.9648 -0.4145 252.7534 253.1680 259.0873 344.5790 -0.4154 252.9255 253.3409 259.2360 346.1735 -0.4138 253.0953 253.5091 259.4361 347.7783 -0.4109 253.2865 253.6974 259.6234 349.3880 -0.4078 253.4883 253.8961 259.8681 350.9919 -0.4092 253.6371 254.0463 260.1157 352.6069 -0.4150 253.8295 254.2444 260.3620 354.2270 -0.4146 253.9680 254.3826 260.5946 355.8369 -0.4149 254.1826 254.5976 260.8686 357.4408 -0.4105 254.3700 254.7805 261.1448 359.0454 -0.4117 254.5748 254.9865 261.4123 360.6553 -0.4118 254.7341 255.1458 261.6867 362.2600 -0.4112 254.8933 255.3044 261.9421 363.8693 -0.4121 255.0780 255.4901 262.1795 365.4890 -0.4116 255.2422 255.6538 262.3947 367.0938 -0.4165 255.4341 255.8506 262.6326 368.6985 -0.4173 255.6471 256.0644 262.8355 370.2980 -0.4187 255.8666 256.2853 263.0244 371.8866 -0.4200 256.0394 256.4594 263.1758 373.4913 -0.4190 256.2438 256.6629 263.3249 375.0960 -0.4169 256.4347 256.8516 263.4749 376.7049 -0.4215 256.6216 257.0431 263.6880 378.3250 -0.4186 256.7998 257.2184 263.8735 379.9349 -0.4211 256.9860 257.4071 264.0813 381.5394 -0.4263 257.1686 257.5949 264.2421 383.1434 -0.4284 257.3592 257.7876 264.4272 384.7533 -0.4298 257.5399 257.9697 264.6117 386.3580 -0.4301 257.7487 258.1788 264.8163 387.9679 -0.4254 257.9486 258.3739 265.0119 389.5876 -0.4220 258.1295 258.5514 265.2192 391.1969 -0.4250 258.3190 258.7439 265.4276 392.7863 -0.4268 258.4938 258.9205 265.6118 394.4013 -0.4272 258.6582 259.0855 265.8504 396.0154 -0.4307 258.9024 259.3331 266.1103 397.6200 -0.4280 259.0786 259.5066 266.3472 399.2196 -0.4273 259.2827 259.7101 266.5984 400.8244 -0.4332 259.4822 259.9154 266.8508 402.4236 -0.4389 259.6846 260.1235 267.0641 404.0278 -0.4458 259.8861 260.3320 267.3022 405.6376 -0.4454 260.0636 260.5091 267.5708 407.2371 -0.4461 260.2943 260.7404 267.8080 408.8410 -0.4476 260.4922 260.9397 268.0237 410.4509 -0.4469 260.7121 261.1590 268.2382 412.0556 -0.4466 260.8941 261.3407 268.4663 413.6655 -0.4475 261.0708 261.5183 268.6890 415.2695 -0.4507 261.2641 261.7148 268.8933 416.8945 -0.4532 261.4410 261.8942 269.0745 418.4993 -0.4521 261.6522 262.1043 269.2452 420.1040 -0.4486 261.8754 262.3240 269.4295 421.7139 -0.4492 262.0443 262.4936 269.6076 423.3180 -0.4483 262.2436 262.6919 269.7804 424.9326 -0.4488 262.4341 262.8829 269.9973 426.5374 -0.4532 262.6320 263.0852 270.1667 428.1626 -0.4534 262.8826 263.3360 270.3439 429.7674 -0.4587 263.0705 263.5293 270.5737 431.3714 -0.4610 263.3065 263.7675 270.7903 432.9708 -0.4566 263.5404 263.9970 270.9741 434.5755 -0.4539 263.7600 264.2139 271.2197 436.1751 -0.4588 263.9593 264.4181 271.4441 437.7841 -0.4576 264.1688 264.6264 271.6497 439.3990 -0.4571 264.3338 264.7910 271.8718 441.0089 -0.4604 264.5296 264.9900 272.1138 442.6133 -0.4678 264.7559 265.2236 272.3586 444.2174 -0.4703 264.9698 265.4400 272.5650 445.8119 -0.4740 265.1996 265.6736 272.7985 447.4166 -0.4786 265.3970 265.8755 273.0516 449.0256 -0.4774 265.5989 266.0763 273.2877 450.6303 -0.4746 265.7897 266.2643 273.5105 452.2555 -0.4741 266.0044 266.4785 273.7304 453.8755 -0.4739 266.2052 266.6791 273.9405 455.4743 -0.4784 266.4344 266.9128 274.1523 457.0790 -0.4793 266.6451 267.1244 274.3506 458.6838 -0.4806 266.8441 267.3247 274.5511 460.2986 -0.4779 267.0538 267.5317 274.7823 461.9025 -0.4761 267.2365 267.7126 274.9814 463.5226 -0.4769 267.4520 267.9289 275.1525 465.1223 -0.4790 267.6632 268.1421 275.3688 466.7213 -0.4850 267.8440 268.3290 275.5597 468.3308 -0.4877 268.0788 268.5665 275.7357 469.9355 -0.4916 268.2864 268.7780 275.9328 471.5403 -0.4942 268.4747 268.9690 276.1526 473.1441 -0.4995 268.6937 269.1932 276.3550 474.7641 -0.5034 268.9278 269.4312 276.5941 476.3740 -0.5035 269.1322 269.6357 276.7785 477.9788 -0.5089 269.3501 269.8591 276.9681 479.5879 -0.5149 269.5615 270.0764 277.1957 481.1924 -0.5133 269.7780 270.2914 277.3768 482.7971 -0.5136 270.0062 270.5198 277.5980 484.4069 -0.5123 270.2195 270.7318 277.8291 486.0313 -0.5155 270.4334 270.9489 278.0284 487.6411 -0.5137 270.6554 271.1691 278.2511 489.2456 -0.5161 270.8555 271.3717 278.4303 490.8548 -0.5211 271.0548 271.5760 278.6615 492.4595 -0.5206 271.2670 271.7876 278.9065 494.0694 -0.5228 271.4636 271.9864 279.1709 495.6741 -0.5254 271.6983 272.2237 279.4248 497.2934 -0.5299 271.9608 272.4907 279.6883 498.8980 -0.5294 272.1888 272.7181 279.9658 500.5028 -0.5331 272.4145 272.9476 280.1967 502.1024 -0.5333 272.6494 273.1827 280.4329 503.6914 -0.5388 272.8589 273.3977 280.6590 505.2955 -0.5393 273.0710 273.6103 280.8391 506.9054 -0.5416 273.2997 273.8413 281.0523 508.5101 -0.5437 273.5199 274.0636 281.2557 510.1300 -0.5496 273.7104 274.2600 281.4509 511.7391 -0.5528 273.9111 274.4640 281.6251 513.3439 -0.5607 274.1285 274.6892 281.7979 514.9538 -0.5618 274.3672 274.9290 281.9549 516.5585 -0.5608 274.5744 275.1352 282.1029 518.1679 -0.5612 274.8043 275.3655 282.2796 519.7721 -0.5647 274.9899 275.5546 282.4916 521.3923 -0.5691 275.1853 275.7545 282.6695 523.0021 -0.5767 275.4486 276.0254 282.8423 524.6061 -0.5769 275.6615 276.2384 283.0393 526.2158 -0.5777 275.8863 276.4640 283.2301 527.8205 -0.5809 276.0873 276.6682 283.4473 529.4253 -0.5867 276.3102 276.8969 283.6891 531.0241 -0.5911 276.5705 277.1616 283.9144 532.6389 -0.5918 276.7984 277.3902 284.1527 534.2436 -0.5894 277.0521 277.6414 284.3963 535.8529 -0.5873 277.2780 277.8653 284.6733 537.4419 -0.5883 277.4916 278.0800 284.9112 539.0518 -0.5938 277.6928 278.2866 285.1792 540.6560 -0.5985 277.9399 278.5384 285.4542 542.2654 -0.6027 278.1590 278.7617 285.7055 543.8701 -0.6110 278.4060 279.0170 285.9507 545.4903 -0.6143 278.6279 279.2422 286.1929 547.0994 -0.6215 278.8427 279.4642 286.3979 548.7039 -0.6246 279.0560 279.6806 286.6264 550.3138 -0.6249 279.2754 279.9003 286.8624 551.9180 -0.6267 279.5307 280.1574 287.0605 553.5274 -0.6285 279.7680 280.3965 287.2113 555.1321 -0.6313 280.0027 280.6340 287.3912 556.7523 -0.6383 280.2439 280.8822 287.5407 558.3621 -0.6416 280.4993 281.1409 287.7105 559.9659 -0.6472 280.7227 281.3698 287.8716 561.5706 -0.6550 280.9251 281.5801 288.0261 563.1703 -0.6546 281.1210 281.7756 288.1613 564.7743 -0.6568 281.3073 281.9640 288.3204 566.3788 -0.6525 281.4952 282.1476 288.5028 567.9835 -0.6531 281.6951 282.3482 288.6941 569.6036 -0.6609 281.8972 282.5581 288.9053 571.2074 -0.6650 282.1067 282.7717 289.1007 572.8121 -0.6676 282.3493 283.0169 289.2996 574.4220 -0.6719 282.5841 283.2561 289.5188 576.0165 -0.6741 282.8111 283.4852 289.7582 577.6255 -0.6783 283.0277 283.7061 290.0802 579.2301 -0.6817 283.2312 283.9129 290.3921 580.8503 -0.6843 283.4467 284.1311 290.6975 582.4601 -0.6835 283.7089 284.3924 290.9830 584.0641 -0.6870 283.9596 284.6466 291.2656 585.6738 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