DTA measure 1gyors Date: 2026224:112 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.05 s Mass = 968.000 mg data_number = 1262 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1990 -0.7482 286.5553 287.3035 274.1171 1.9958 -0.7438 286.6166 287.3603 273.9204 2.7925 -0.7375 286.6523 287.3898 273.7588 3.6095 -0.7319 286.6858 287.4177 273.6047 4.3755 -0.7277 286.7018 287.4295 273.4804 5.2335 -0.7197 286.7522 287.4719 273.3747 5.9995 -0.7179 286.7701 287.4880 273.2977 6.8270 -0.7148 286.8083 287.5232 273.1862 7.6133 -0.7159 286.8207 287.5366 273.1326 8.4203 -0.7136 286.8336 287.5472 273.1324 9.2065 -0.7073 286.8218 287.5291 273.1690 10.0030 -0.7035 286.8050 287.5085 273.2402 10.8305 -0.7001 286.8479 287.5480 273.3255 11.5963 -0.6968 286.9082 287.6049 273.4527 12.4543 -0.6903 286.9384 287.6287 273.6582 13.2100 -0.6918 286.9873 287.6791 273.8224 14.0475 -0.6867 287.0197 287.7065 274.0779 14.8338 -0.6811 287.0730 287.7540 274.3575 15.6305 -0.6775 287.1194 287.7969 274.7001 16.4578 -0.6738 287.1276 287.8014 275.0782 17.2340 -0.6726 287.1295 287.8021 275.4134 18.0820 -0.6717 287.1715 287.8433 275.8040 18.8475 -0.6723 287.1871 287.8594 276.1371 19.6750 -0.6684 287.1998 287.8682 276.5454 20.4718 -0.6676 287.2172 287.8847 276.9449 21.2680 -0.6676 287.2659 287.9335 277.3370 22.0853 -0.6671 287.3295 287.9966 277.7645 22.8615 -0.6646 287.3500 288.0146 278.1577 23.7093 -0.6705 287.3571 288.0276 278.5525 24.4855 -0.6735 287.3619 288.0354 278.9128 25.3025 -0.6767 287.4032 288.0799 279.2800 26.1093 -0.6740 287.3872 288.0612 279.6066 26.8958 -0.6705 287.3899 288.0605 279.8993 27.7333 -0.6754 287.4289 288.1043 280.1708 28.4890 -0.6732 287.4974 288.1706 280.3740 29.3575 -0.6728 287.5338 288.2066 280.6111 30.1128 -0.6708 287.5618 288.2326 280.7791 30.9508 -0.6716 287.6073 288.2790 280.9400 31.7063 -0.6736 287.6314 288.3050 281.0485 32.5438 -0.6736 287.6858 288.3594 281.1279 33.3613 -0.6734 287.7110 288.3844 281.2168 34.1268 -0.6714 287.7525 288.4239 281.2393 34.9543 -0.6730 287.7923 288.4654 281.2484 35.7100 -0.6735 287.8246 288.4981 281.2273 36.5575 -0.6724 287.8533 288.5257 281.2097 37.3340 -0.6742 287.9007 288.5750 281.1820 38.1510 -0.6777 287.9265 288.6042 281.1624 38.9478 -0.6780 287.9728 288.6508 281.1188 39.7445 -0.6779 288.0137 288.6916 281.0657 40.5715 -0.6788 288.0418 288.7206 280.9891 41.3375 -0.6756 288.0770 288.7526 280.9086 42.1855 -0.6750 288.1031 288.7781 280.8815 42.9305 -0.6749 288.1471 288.8220 280.8058 43.7788 -0.6743 288.1894 288.8637 280.7088 44.5445 -0.6748 288.2162 288.8910 280.6540 45.3718 -0.6753 288.2452 288.9205 280.6092 46.1685 -0.6755 288.2840 288.9595 280.5759 46.9650 -0.6763 288.3332 289.0095 280.5686 47.7820 -0.6780 288.3757 289.0536 280.5558 48.5580 -0.6772 288.4138 289.0910 280.5571 49.4060 -0.6733 288.4548 289.1281 280.5764 50.1718 -0.6728 288.5048 289.1776 280.6127 50.9993 -0.6719 288.5633 289.2352 280.6767 51.7958 -0.6733 288.6054 289.2787 280.7418 52.5923 -0.6767 288.6364 289.3131 280.8499 53.4198 -0.6806 288.6862 289.3668 280.9812 54.1855 -0.6793 288.7207 289.4000 281.1415 55.0435 -0.6793 288.7369 289.4162 281.3464 55.8095 -0.6858 288.7569 289.4427 281.5088 56.6368 -0.6866 288.7837 289.4703 281.7509 57.4333 -0.6872 288.8155 289.5027 281.9692 58.2403 -0.6854 288.8547 289.5402 282.2539 59.0573 -0.6832 288.8620 289.5452 282.4995 59.8230 -0.6833 288.8794 289.5627 282.7678 60.6813 -0.6806 288.9288 289.6094 283.1332 61.4573 -0.6809 288.9856 289.6665 283.4427 62.2743 -0.6820 289.0058 289.6878 283.7575 63.0403 -0.6783 289.0529 289.7312 284.0749 63.8675 -0.6707 289.1198 289.7905 284.4010 64.6643 -0.6749 289.1920 289.8669 284.7122 65.4610 -0.6766 289.2452 289.9218 285.0079 66.2778 -0.6795 289.3166 289.9961 285.3055 67.0438 -0.6832 289.3227 290.0059 285.5737 67.8918 -0.6878 289.3486 290.0364 285.8356 68.6573 -0.6863 289.3840 290.0703 286.0550 69.4848 -0.6833 289.4262 290.1096 286.2918 70.2815 -0.6858 289.4583 290.1442 286.4847 71.0678 -0.6884 289.5070 290.1954 286.6515 71.8955 -0.6895 289.5648 290.2543 286.8313 72.6610 -0.6882 289.6322 290.3204 287.0023 73.5090 -0.6897 289.6792 290.3689 287.1159 74.2545 -0.6905 289.7369 290.4275 287.2051 75.1023 -0.6907 289.7601 290.4508 287.2915 75.8683 -0.6949 289.7851 290.4799 287.3591 76.6955 -0.6985 289.8572 290.5557 287.4210 77.4920 -0.7000 289.9247 290.6247 287.4808 78.2888 -0.7001 289.9692 290.6693 287.5081 79.1058 -0.6999 290.0129 290.7128 287.5130 79.8820 -0.7007 290.0750 290.7757 287.4891 80.7300 -0.7022 290.1337 290.8359 287.4818 81.4955 -0.7006 290.1648 290.8654 287.4696 82.3233 -0.7007 290.2281 290.9288 287.4812 83.1300 -0.7044 290.2734 290.9778 287.4682 83.9163 -0.7043 290.3259 291.0302 287.4649 84.7438 -0.7068 290.3752 291.0820 287.4148 85.5095 -0.7056 290.4271 291.1327 287.3658 86.3470 -0.7046 290.4782 291.1828 287.3516 87.1030 -0.7069 290.5325 291.2394 287.3591 87.9608 -0.7070 290.5979 291.3049 287.3828 88.7268 -0.7084 290.6593 291.3677 287.4119 89.5543 -0.7072 290.7331 291.4404 287.4239 90.3508 -0.7058 290.7789 291.4846 287.4713 91.1373 -0.7052 290.8505 291.5557 287.5418 91.9748 -0.7053 290.9119 291.6172 287.6490 92.7405 -0.7055 290.9623 291.6678 287.7331 93.5988 -0.7065 290.9846 291.6911 287.8675 94.3543 -0.7040 291.0497 291.7537 287.9908 95.1920 -0.7028 291.0951 291.7979 288.1321 95.9888 -0.6984 291.1615 291.8599 288.3050 96.7850 -0.6945 291.2323 291.9268 288.4994 97.6023 -0.6921 291.2953 291.9874 288.7253 98.3683 -0.6851 291.3368 292.0219 288.9458 99.2263 -0.6769 291.3927 292.0696 289.2197 99.9513 -0.6684 291.4394 292.1078 289.4412 100.8093 -0.6606 291.4921 292.1526 289.7188 101.5750 -0.6597 291.5558 292.2154 289.9349 102.3923 -0.6555 291.6021 292.2577 290.2048 103.1888 -0.6498 291.6602 292.3100 290.4693 103.9858 -0.6444 291.7309 292.3753 290.7321 104.8028 -0.6415 291.7982 292.4397 290.9965 105.5788 -0.6533 291.8488 292.5021 291.2616 106.4270 -0.6693 291.9301 292.5994 291.5392 107.1925 -0.6778 292.0051 292.6829 291.7980 108.0200 -0.6829 292.0630 292.7458 292.0421 108.8168 -0.6907 292.1160 292.8067 292.2360 109.6130 -0.6995 292.1960 292.8955 292.4562 110.4305 -0.7036 292.2847 292.9883 292.6422 111.2065 -0.7102 292.3318 293.0420 292.8134 112.0543 -0.7204 292.4177 293.1381 293.0141 112.8305 -0.7275 292.4918 293.2193 293.1603 113.6475 -0.7287 292.5458 293.2745 293.2958 114.4235 -0.7292 292.5945 293.3236 293.4227 115.2510 -0.7346 292.6532 293.3878 293.5368 116.0475 -0.7376 292.7393 293.4769 293.6341 116.8340 -0.7401 292.8262 293.5663 293.7040 117.6718 -0.7435 292.8961 293.6396 293.7815 118.4270 -0.7436 292.9671 293.7107 293.8332 119.2953 -0.7418 293.0367 293.7785 293.8913 120.0510 -0.7419 293.0925 293.8344 293.9201 120.8885 -0.7426 293.1338 293.8765 293.9427 121.6748 -0.7402 293.1910 293.9312 293.9392 122.4818 -0.7438 293.2704 294.0142 293.9423 123.2988 -0.7433 293.3443 294.0876 293.9488 124.0748 -0.7399 293.4461 294.1860 293.9606 124.9228 -0.7361 293.4958 294.2320 293.9646 125.6885 -0.7401 293.5549 294.2949 293.9832 126.5160 -0.7450 293.6528 294.3978 293.9918 127.3230 -0.7457 293.7326 294.4783 294.0076 128.1090 -0.7489 293.7980 294.5470 294.0473 128.9365 -0.7576 293.9074 294.6651 294.0829 129.7025 -0.7596 293.9747 294.7343 294.1524 130.5500 -0.7550 294.0223 294.7773 294.2381 131.3160 -0.7552 294.0829 294.8381 294.3142 132.1435 -0.7543 294.1535 294.9078 294.4270 132.9295 -0.7533 294.2012 294.9546 294.5179 133.7265 -0.7518 294.2744 295.0262 294.6130 134.5538 -0.7507 294.3285 295.0792 294.7723 135.3195 -0.7478 294.4236 295.1714 294.9011 136.1675 -0.7471 294.5120 295.2591 295.0512 136.9333 -0.7477 294.5810 295.3287 295.2401 137.7605 -0.7484 294.6307 295.3792 295.4451 138.5573 -0.7480 294.7222 295.4702 295.6516 139.3435 -0.7496 294.7988 295.5484 295.8650 140.1810 -0.7513 294.8762 295.6276 296.0918 140.9370 -0.7534 294.9446 295.6979 296.2926 141.7948 -0.7543 295.0194 295.7737 296.5534 142.5608 -0.7560 295.0840 295.8400 296.7670 143.3985 -0.7557 295.1544 295.9101 297.0204 144.1848 -0.7521 295.2266 295.9787 297.2621 144.9815 -0.7529 295.3182 296.0711 297.4991 145.8088 -0.7538 295.4133 296.1671 297.7297 146.5848 -0.7576 295.5016 296.2592 297.9659 147.4330 -0.7548 295.5726 296.3273 298.2169 148.1985 -0.7583 295.6391 296.3974 298.4444 149.0258 -0.7597 295.7250 296.4847 298.6570 149.8228 -0.7579 295.8038 296.5617 298.8762 150.6190 -0.7568 295.8857 296.6426 299.0747 151.4363 -0.7556 295.9876 296.7433 299.2420 152.2125 -0.7522 296.0698 296.8220 299.4042 153.0603 -0.7559 296.1666 296.9225 299.5867 153.8263 -0.7589 296.2177 296.9766 299.7278 154.6535 -0.7545 296.2744 297.0289 299.8554 155.4298 -0.7541 296.3525 297.1066 299.9457 156.2470 -0.7523 296.4496 297.2019 300.0625 157.0433 -0.7522 296.5240 297.2763 300.1632 157.8400 -0.7522 296.6049 297.3571 300.2385 158.6778 -0.7553 296.6870 297.4423 300.3229 159.4330 -0.7610 296.7768 297.5378 300.3905 160.2913 -0.7636 296.9030 297.6665 300.4500 161.0573 -0.7616 297.0009 297.7625 300.4569 161.8843 -0.7601 297.0989 297.8590 300.4898 162.6810 -0.7588 297.2004 297.9592 300.5122 163.4675 -0.7594 297.2701 298.0295 300.5502 164.2948 -0.7609 297.3464 298.1073 300.5906 165.0608 -0.7611 297.4289 298.1900 300.6214 165.8880 -0.7607 297.5198 298.2805 300.6480 166.6538 -0.7654 297.6102 298.3755 300.6831 167.5018 -0.7627 297.7168 298.4795 300.7206 168.2675 -0.7623 297.7904 298.5527 300.7589 169.0948 -0.7611 297.8388 298.5999 300.8280 169.8918 -0.7581 297.9448 298.7029 300.8885 170.6880 -0.7573 298.0328 298.7901 300.9555 171.4848 -0.7584 298.1023 298.8607 301.0547 172.2815 -0.7538 298.1745 298.9284 301.1342 173.1085 -0.7520 298.2804 299.0324 301.2610 173.8745 -0.7533 298.3628 299.1161 301.3795 174.7223 -0.7551 298.4726 299.2278 301.5508 175.4983 -0.7540 298.5785 299.3325 301.6888 176.3155 -0.7564 298.6816 299.4380 301.8268 177.1123 -0.7545 298.7723 299.5268 301.9748 177.9085 -0.7554 298.8555 299.6109 302.1347 178.7358 -0.7563 298.9694 299.7257 302.3455 179.5018 -0.7537 299.0594 299.8131 302.5346 180.3495 -0.7532 299.1639 299.9171 302.7727 181.0950 -0.7556 299.2492 300.0048 302.9759 181.9430 -0.7546 299.3321 300.0866 303.2218 182.7188 -0.7559 299.4080 300.1639 303.4471 183.5360 -0.7554 299.5129 300.2683 303.6978 184.3428 -0.7542 299.5963 300.3505 303.9331 185.1290 -0.7546 299.6952 300.4498 304.1701 185.9565 -0.7560 299.8143 300.5703 304.4135 186.7225 -0.7562 299.9028 300.6590 304.6133 187.5905 -0.7554 300.0314 300.7868 304.8575 188.3465 -0.7535 300.1010 300.8545 305.0435 189.1738 -0.7577 300.1854 300.9431 305.2372 189.9703 -0.7553 300.2852 301.0405 305.4349 190.7673 -0.7538 300.3673 301.1211 305.6136 191.5943 -0.7519 300.4521 301.2040 305.7705 192.3603 -0.7523 300.5656 301.3178 305.9232 193.2185 -0.7558 300.6957 301.4514 306.0606 193.9533 -0.7562 300.7696 301.5258 306.1886 194.8118 -0.7544 300.8696 301.6241 306.3188 195.5673 -0.7563 300.9605 301.7168 306.4070 196.3945 -0.7582 301.0676 301.8258 306.5158 197.1915 -0.7562 301.1584 301.9145 306.6303 197.9775 -0.7556 301.2542 302.0099 306.7171 198.8050 -0.7537 301.3851 302.1388 306.7692 199.5710 -0.7526 301.5067 302.2593 306.8245 200.4185 -0.7589 301.5927 302.3516 306.8798 201.1950 -0.7594 301.6823 302.4417 306.9288 202.0120 -0.7586 301.7690 302.5276 306.9669 202.7778 -0.7573 301.8654 302.6226 307.0280 203.6055 -0.7581 301.9596 302.7177 307.0692 204.4018 -0.7590 302.0760 302.8351 307.0937 205.1983 -0.7600 302.1818 302.9418 307.1264 206.0158 -0.7610 302.2887 303.0497 307.1411 206.7915 -0.7596 302.3664 303.1260 307.1780 207.6395 -0.7575 302.4615 303.2191 307.2216 208.4055 -0.7561 302.5770 303.3331 307.2910 209.2325 -0.7525 302.6871 303.4396 307.3806 210.0293 -0.7495 302.7850 303.5344 307.4738 210.8260 -0.7482 302.8950 303.6432 307.5836 211.6428 -0.7463 303.0015 303.7478 307.6917 212.4190 -0.7479 303.0954 303.8433 307.7918 213.2773 -0.7473 303.1771 303.9243 307.9130 214.0428 -0.7463 303.2706 304.0168 308.0334 214.8600 -0.7482 303.4010 304.1492 308.1805 215.6670 -0.7443 303.5120 304.2563 308.3590 216.4635 -0.7430 303.6077 304.3507 308.5317 217.2603 -0.7469 303.7174 304.4643 308.7203 218.0465 -0.7472 303.8320 304.5793 308.9137 218.8840 -0.7506 303.9280 304.6786 309.1039 219.6500 -0.7494 304.0145 304.7640 309.2918 220.5080 -0.7472 304.1373 304.8845 309.5111 221.2635 -0.7496 304.2477 304.9973 309.7291 222.1015 -0.7504 304.3474 305.0978 309.9673 222.8978 -0.7541 304.4420 305.1961 310.1822 223.6943 -0.7562 304.5283 305.2845 310.4036 224.5115 -0.7526 304.6262 305.3788 310.6313 225.2875 -0.7507 304.7468 305.4975 310.8444 226.1455 -0.7484 304.8679 305.6164 311.0365 226.9013 -0.7487 304.9746 305.7233 311.1999 227.7285 -0.7499 305.0868 305.8367 311.4112 228.5250 -0.7493 305.1864 305.9357 311.5990 229.3115 -0.7507 305.2793 306.0300 311.7716 230.1388 -0.7495 305.4076 306.1571 311.9691 230.9045 -0.7522 305.5324 306.2847 312.1166 231.7628 -0.7514 305.6445 306.3958 312.2913 232.5183 -0.7495 305.7521 306.5016 312.4139 233.3455 -0.7505 305.8687 306.6192 312.5671 234.1423 -0.7519 305.9715 306.7233 312.7062 234.9285 -0.7514 306.0588 306.8101 312.8085 235.7660 -0.7470 306.1414 306.8884 312.9236 236.5218 -0.7448 306.2664 307.0112 312.9992 237.3798 -0.7440 306.4106 307.1546 313.0910 238.1458 -0.7473 306.4967 307.2440 313.1954 238.9733 -0.7552 306.5892 307.3444 313.2566 239.7695 -0.7590 306.7150 307.4740 313.3157 240.5563 -0.7566 306.8453 307.6019 313.3610 241.3938 -0.7541 306.9543 307.7084 313.4072 242.1495 -0.7500 307.0455 307.7955 313.4314 243.0180 -0.7515 307.1490 307.9004 313.4966 243.7733 -0.7537 307.2718 308.0255 313.5274 244.6113 -0.7496 307.3782 308.1278 313.6017 245.3668 -0.7466 307.5038 308.2504 313.6576 246.2043 -0.7468 307.6302 308.3769 313.7126 246.9908 -0.7541 307.7696 308.5238 313.7698 247.7975 -0.7541 307.8598 308.6139 313.8447 248.6148 -0.7547 307.9807 308.7353 313.9267 249.3910 -0.7538 308.0584 308.8122 314.0208 250.2385 -0.7536 308.1401 308.8937 314.1434 251.0148 -0.7528 308.2425 308.9953 314.2474 251.8320 -0.7494 308.3739 309.1233 314.3653 252.6285 -0.7482 308.5169 309.2651 314.4896 253.4253 -0.7466 308.6267 309.3733 314.6271 254.2628 -0.7456 308.7421 309.4876 314.7582 255.0183 -0.7427 308.8420 309.5847 314.9004 255.8765 -0.7422 308.9784 309.7206 315.1101 256.6423 -0.7474 309.0840 309.8314 315.2570 257.4800 -0.7503 309.2154 309.9657 315.4575 258.2665 -0.7515 309.3342 310.0857 315.6385 259.0628 -0.7523 309.4220 310.1743 315.8173 259.8903 -0.7547 309.5340 310.2887 316.0082 260.6460 -0.7533 309.6481 310.4014 316.1801 261.4628 -0.7560 309.7728 310.5288 316.3753 262.2390 -0.7585 309.8803 310.6388 316.5647 263.0870 -0.7586 310.0280 310.7866 316.7843 263.8525 -0.7586 310.1357 310.8943 316.9686 264.6800 -0.7583 310.2455 311.0038 317.2020 265.4665 -0.7599 310.3396 311.0996 317.4108 266.2628 -0.7582 310.4656 311.2238 317.6107 267.0905 -0.7587 310.6056 311.3643 317.8332 267.8563 -0.7574 310.7269 311.4842 318.0420 268.7143 -0.7577 310.8387 311.5965 318.2522 269.4393 -0.7576 310.9372 311.6949 318.4201 270.3075 -0.7572 311.0524 311.8096 318.6271 271.0633 -0.7589 311.1563 311.9152 318.7916 271.8908 -0.7597 311.2919 312.0516 318.9648 272.6873 -0.7625 311.4211 312.1835 319.1150 273.4945 -0.7678 311.5117 312.2795 319.2368 274.3113 -0.7668 311.6583 312.4251 319.3455 275.0775 -0.7679 311.7609 312.5288 319.4365 275.9355 -0.7708 311.9067 312.6776 319.5347 276.6808 -0.7719 312.0321 312.8040 319.6020 277.5288 -0.7729 312.1905 312.9633 319.6943 278.2945 -0.7721 312.3117 313.0838 319.7710 279.1220 -0.7724 312.4452 313.2175 319.8422 279.9188 -0.7740 312.5751 313.3491 319.8914 280.7153 -0.7724 312.6818 313.4542 319.9173 281.5325 -0.7738 312.7849 313.5587 319.9489 282.3085 -0.7798 312.8815 313.6613 319.9731 283.1665 -0.7833 312.9912 313.7745 320.0445 283.9325 -0.7862 313.0903 313.8765 320.0744 284.7495 -0.7864 313.2117 313.9981 320.1361 285.5563 -0.7867 313.3417 314.1284 320.1909 286.3533 -0.7880 313.4660 314.2540 320.2560 287.1495 -0.7882 313.5492 314.3374 320.3451 287.9360 -0.7842 313.6593 314.4434 320.4403 288.7738 -0.7798 313.8007 314.5805 320.5262 289.5293 -0.7777 313.9093 314.6870 320.6125 290.3873 -0.7799 314.0901 314.8701 320.7493 291.1533 -0.7852 314.2074 314.9926 320.8623 291.9805 -0.7873 314.3355 315.1229 321.0054 292.7670 -0.7867 314.4659 315.2527 321.1521 293.5635 -0.7878 314.6109 315.3987 321.2900 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