DTA measure 1lassu Date: 2026224:125 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.54 s Mass = 968.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3478 -0.1542 247.3113 247.4654 223.7246 3.9513 -0.1434 247.2697 247.4132 223.4828 5.5751 -0.1341 247.2281 247.3622 223.2119 7.1839 -0.1328 247.1985 247.3312 222.9416 8.7769 -0.1231 247.1587 247.2818 222.6887 10.3804 -0.1207 247.0707 247.1914 222.4364 11.9890 -0.1184 247.0527 247.1712 222.1671 13.5978 -0.1132 247.0523 247.1655 221.9233 15.2063 -0.1061 247.0409 247.1470 221.6481 16.8150 -0.0993 246.9626 247.0619 221.3787 18.4390 -0.0918 246.8840 246.9757 221.1536 20.0476 -0.0860 246.8499 246.9359 220.9316 21.6561 -0.0831 246.8016 246.8847 220.6931 23.2649 -0.0818 246.7556 246.8374 220.4354 24.8735 -0.0835 246.6758 246.7593 220.1928 26.4770 -0.0823 246.5733 246.6555 219.9738 28.0855 -0.0782 246.4769 246.5551 219.7323 29.7096 -0.0804 246.4049 246.4853 219.5270 31.3183 -0.0807 246.3114 246.3921 219.3092 32.9268 -0.0852 246.2180 246.3032 219.0764 34.5199 -0.0856 246.1686 246.2542 218.9591 36.1286 -0.0834 246.0769 246.1603 218.8699 37.7371 -0.0851 245.9941 246.0791 218.8220 39.3456 -0.0916 245.9542 246.0458 218.8083 40.9543 -0.0935 245.8709 245.9643 218.8320 42.5731 -0.0944 245.8104 245.9048 218.9659 44.1715 -0.0948 245.7402 245.8350 219.1599 45.7800 -0.0918 245.6131 245.7049 219.4438 47.3733 -0.0880 245.5268 245.6147 219.8329 48.9768 -0.0922 245.4318 245.5240 220.2493 50.5801 -0.0964 245.3696 245.4660 220.6965 52.1836 -0.1027 245.2945 245.3971 221.1267 53.7719 -0.1126 245.2172 245.3298 221.6051 55.3958 -0.1170 245.1034 245.2204 222.0875 56.9991 -0.1259 245.0351 245.1609 222.5305 58.6079 -0.1443 245.0026 245.1469 222.9526 60.1960 -0.1502 244.9439 245.0941 223.3390 61.8046 -0.1565 244.8633 245.0198 223.6840 63.4081 -0.1665 244.7843 244.9508 223.9694 65.0116 -0.1739 244.6704 244.8442 224.2417 66.6203 -0.1820 244.5736 244.7557 224.4366 68.2389 -0.1961 244.4960 244.6921 224.5508 69.8476 -0.2092 244.4164 244.6256 224.6887 71.4513 -0.2157 244.3288 244.5445 224.7644 73.0599 -0.2210 244.2637 244.4847 224.8468 74.6634 -0.2274 244.2088 244.4362 224.8892 76.2515 -0.2325 244.1247 244.3572 224.9662 77.8603 -0.2363 244.0958 244.3321 225.0181 79.4638 -0.2385 244.0352 244.2737 225.0400 81.0879 -0.2465 243.9655 244.2120 225.1210 82.6914 -0.2553 243.9047 244.1601 225.2005 84.2999 -0.2618 243.8285 244.0903 225.2649 85.9034 -0.2744 243.7381 244.0125 225.3873 87.5170 -0.2756 243.6535 243.9292 225.5073 89.1205 -0.2791 243.5649 243.8440 225.7025 90.7291 -0.2664 243.5024 243.7688 225.9088 92.3533 -0.2633 243.4735 243.7367 226.1498 93.9414 -0.2724 243.4599 243.7323 226.3823 95.5550 -0.2796 243.4097 243.6893 226.6466 97.1638 -0.2881 243.3488 243.6369 226.9227 98.7724 -0.2953 243.3057 243.6010 227.1892 100.3861 -0.2992 243.2622 243.5614 227.5102 101.9895 -0.3078 243.2408 243.5487 227.8271 103.5879 -0.3141 243.2006 243.5147 228.1676 105.1914 -0.3192 243.1451 243.4643 228.4812 106.8104 -0.3325 243.0864 243.4189 228.7764 108.4138 -0.3399 243.0339 243.3737 229.0529 110.0173 -0.3434 243.0024 243.3458 229.3178 111.6105 -0.3555 242.9455 243.3010 229.5521 113.2191 -0.3648 242.9248 243.2896 229.7725 114.8174 -0.3716 242.9188 243.2904 229.9830 116.4158 -0.3733 242.9059 243.2791 230.1645 118.0399 -0.3803 242.8631 243.2433 230.3466 119.6431 -0.3831 242.8534 243.2365 230.5174 121.2364 -0.3803 242.8035 243.1837 230.6478 122.8400 -0.3827 242.7623 243.1450 230.7514 124.4435 -0.3860 242.7342 243.1202 230.8854 126.0520 -0.3946 242.7173 243.1119 231.0033 127.6555 -0.3998 242.6894 243.0892 231.1150 129.2641 -0.4012 242.6499 243.0511 231.2895 130.8830 -0.4006 242.6088 243.0094 231.4530 132.4915 -0.4016 242.6127 243.0143 231.5780 134.0951 -0.4036 242.5785 242.9821 231.7135 135.6986 -0.4060 242.5721 242.9781 231.8795 137.3074 -0.4069 242.5854 242.9923 232.0856 138.9108 -0.4104 242.5901 243.0005 232.2766 140.5194 -0.4169 242.6018 243.0188 232.4832 142.1384 -0.4153 242.5968 243.0121 232.7111 143.7469 -0.4152 242.6086 243.0238 233.0099 145.3504 -0.4161 242.6245 243.0406 233.2996 146.9539 -0.4147 242.6254 243.0401 233.5584 148.5678 -0.4197 242.5988 243.0185 233.8358 150.1711 -0.4174 242.6120 243.0294 234.0914 151.7798 -0.4197 242.6143 243.0341 234.3822 153.3986 -0.4199 242.6122 243.0321 234.6618 155.0073 -0.4198 242.5992 243.0190 234.9388 156.6160 -0.4236 242.6130 243.0366 235.2250 158.2245 -0.4205 242.6263 243.0468 235.4633 159.8280 -0.4106 242.6747 243.0854 235.6915 161.4418 -0.4104 242.6812 243.0916 235.9073 163.0451 -0.4185 242.6895 243.1080 236.1036 164.6589 -0.4195 242.7141 243.1336 236.2783 166.2623 -0.4161 242.6990 243.1151 236.4706 167.8760 -0.4159 242.7252 243.1411 236.5921 169.4691 -0.4119 242.7510 243.1629 236.7514 171.0829 -0.4121 242.7484 243.1605 236.8799 172.6811 -0.4106 242.8059 243.2165 236.9954 174.2845 -0.4098 242.8458 243.2556 237.1330 175.8880 -0.4099 242.8922 243.3021 237.2775 177.4711 -0.4057 242.9203 243.3259 237.4248 179.0796 -0.4076 242.9830 243.3907 237.5792 180.6985 -0.4061 243.0239 243.4299 237.7849 182.3020 -0.4012 243.0505 243.4516 238.0139 183.8954 -0.3973 243.0493 243.4466 238.2181 185.4935 -0.3999 243.1067 243.5066 238.4164 187.1023 -0.3950 243.1524 243.5474 238.6554 188.7059 -0.3887 243.2113 243.6000 238.8762 190.3094 -0.3862 243.2579 243.6441 239.1220 191.9178 -0.3885 243.2572 243.6457 239.3825 193.5214 -0.3904 243.2942 243.6846 239.6550 195.1301 -0.3914 243.3613 243.7527 239.9269 196.7338 -0.3869 243.4360 243.8228 240.1849 198.3424 -0.3810 243.5430 243.9240 240.4299 199.9459 -0.3815 243.6258 244.0073 240.6573 201.5495 -0.3775 243.7251 244.1026 240.9262 203.1583 -0.3742 243.7569 244.1310 241.2021 204.7618 -0.3731 243.8446 244.2177 241.4540 206.3856 -0.3633 243.8912 244.2545 241.6425 207.9891 -0.3596 243.9662 244.3257 241.8681 209.6029 -0.3610 244.0040 244.3650 242.0739 211.2064 -0.3620 244.0445 244.4064 242.2781 212.8201 -0.3610 244.1172 244.4782 242.4714 214.4235 -0.3614 244.1748 244.5362 242.6488 216.0173 -0.3575 244.2627 244.6202 242.8149 217.6211 -0.3545 244.3401 244.6946 242.9623 219.2413 -0.3492 244.4336 244.7828 243.1158 220.8511 -0.3418 244.5292 244.8711 243.2600 222.4558 -0.3383 244.6278 244.9661 243.4479 224.0801 -0.3335 244.7402 245.0737 243.6255 225.6849 -0.3333 244.8184 245.1517 243.8087 227.2948 -0.3226 244.8888 245.2114 243.9881 228.9200 -0.3179 244.9283 245.2462 244.1762 230.5138 -0.3154 245.0363 245.3517 244.3538 232.1234 -0.3154 245.1338 245.4491 244.5683 233.7281 -0.3179 245.2063 245.5242 244.7864 235.3278 -0.3137 245.3036 245.6173 245.0180 236.9316 -0.3109 245.4215 245.7325 245.3050 238.5260 -0.3007 245.5135 245.8142 245.5457 240.1359 -0.2982 245.5914 245.8896 245.8056 241.7500 -0.2984 245.6807 245.9791 246.0811 243.3546 -0.2917 245.7815 246.0732 246.3282 244.9645 -0.2943 245.8601 246.1544 246.5538 246.5533 -0.2936 245.9462 246.2398 246.8180 248.1628 -0.2878 246.0476 246.3354 247.0721 249.7624 -0.2868 246.1737 246.4604 247.3001 251.3665 -0.2839 246.3063 246.5902 247.5368 252.9760 -0.2873 246.4518 246.7391 247.7764 254.5961 -0.2865 246.5422 246.8287 247.9903 256.2058 -0.2795 246.6479 246.9274 248.1694 257.7944 -0.2760 246.7603 247.0363 248.3436 259.4043 -0.2636 246.8661 247.1297 248.5050 261.0090 -0.2593 246.9595 247.2188 248.6792 262.6138 -0.2615 247.0704 247.3319 248.8509 264.2230 -0.2557 247.1803 247.4360 249.0222 265.8274 -0.2528 247.2810 247.5338 249.1993 267.4373 -0.2487 247.3919 247.6406 249.3306 269.0420 -0.2496 247.5152 247.7649 249.4932 270.6515 -0.2438 247.6431 247.8869 249.6779 272.2556 -0.2416 247.7418 247.9833 249.8421 273.8604 -0.2366 247.8873 248.1239 250.0021 275.4700 -0.2345 248.0676 248.3021 250.1839 277.0740 -0.2281 248.1836 248.4117 250.3878 278.6839 -0.2256 248.2896 248.5152 250.6084 280.3040 -0.2224 248.4302 248.6526 250.8599 281.9139 -0.2223 248.5862 248.8084 251.1044 283.5026 -0.2160 248.6646 248.8807 251.3478 285.1121 -0.2145 248.7252 248.9398 251.6380 286.7220 -0.2093 248.8465 249.0558 251.9416 288.3268 -0.2024 248.9776 249.1800 252.2261 289.9363 -0.1972 249.0974 249.2945 252.5009 291.5404 -0.1933 249.1997 249.3930 252.7739 293.1708 -0.1947 249.3573 249.5520 253.0331 294.7755 -0.1888 249.5144 249.7032 253.2754 296.3846 -0.1873 249.6778 249.8651 253.4738 297.9789 -0.1820 249.8508 250.0328 253.6789 299.5785 -0.1796 249.9826 250.1621 253.8565 301.1773 -0.1818 250.1018 250.2835 254.0254 302.7819 -0.1782 250.2115 250.3897 254.2191 304.3815 -0.1711 250.3512 250.5223 254.3923 306.0013 -0.1704 250.5356 250.7060 254.5469 307.5900 -0.1674 250.6662 250.8336 254.7097 309.1896 -0.1659 250.8073 250.9732 254.8667 310.7993 -0.1633 250.9379 251.1012 255.0027 312.4033 -0.1595 251.0519 251.2115 255.1438 314.0080 -0.1576 251.1670 251.3247 255.3078 315.6128 -0.1576 251.3286 251.4861 255.4688 317.2174 -0.1576 251.4803 251.6380 255.6976 318.8418 -0.1520 251.6663 251.8183 255.9364 320.4414 -0.1503 251.7931 251.9434 256.1368 322.0513 -0.1438 251.9607 252.1045 256.3493 323.6556 -0.1375 252.1375 252.2749 256.5890 325.2598 -0.1354 252.3032 252.4386 256.8455 326.8696 -0.1320 252.4866 252.6186 257.0864 328.4738 -0.1276 252.6695 252.7971 257.3181 330.0986 -0.1244 252.8275 252.9519 257.5688 331.7034 -0.1166 252.9927 253.1093 257.8378 333.3133 -0.1145 253.1591 253.2737 258.1199 334.9178 -0.1121 253.2859 253.3980 258.4012 336.5218 -0.1100 253.4377 253.5477 258.6563 338.1316 -0.1092 253.6043 253.7135 258.9104 339.7364 -0.1089 253.7681 253.8769 259.1315 341.3663 -0.1059 253.9229 254.0288 259.3538 342.9705 -0.0980 254.0389 254.1369 259.5749 344.5804 -0.0941 254.1715 254.2655 259.7741 346.1903 -0.0922 254.3682 254.4604 259.9369 347.7996 -0.0963 254.5416 254.6379 260.0667 349.4039 -0.0927 254.6947 254.7873 260.2502 351.0138 -0.0929 254.8785 254.9714 260.4105 352.6339 -0.0928 255.0128 255.1056 260.5954 354.2284 -0.0938 255.1601 255.2539 260.7720 355.8379 -0.0906 255.3712 255.4617 260.9279 357.4523 -0.0849 255.5489 255.6338 261.0655 359.0570 -0.0789 255.7574 255.8363 261.2398 360.6618 -0.0783 255.9137 255.9920 261.4407 362.2768 -0.0780 256.0949 256.1729 261.6419 363.8810 -0.0775 256.2464 256.3239 261.8410 365.4699 -0.0749 256.4192 256.4940 262.0756 367.0849 -0.0781 256.5806 256.6588 262.3237 368.6844 -0.0755 256.7700 256.8455 262.5428 370.2934 -0.0723 256.9616 257.0339 262.7951 371.8930 -0.0695 257.1345 257.2040 263.0787 373.4773 -0.0681 257.3251 257.3932 263.3208 375.0760 -0.0738 257.4991 257.5730 263.6071 376.6806 -0.0714 257.6673 257.7387 263.8840 378.2905 -0.0622 257.8233 257.8855 264.1351 379.8900 -0.0585 257.9934 258.0519 264.3719 381.4939 -0.0545 258.1889 258.2434 264.6206 383.1038 -0.0537 258.4000 258.4537 264.8231 384.7085 -0.0530 258.6214 258.6744 265.0506 386.3174 -0.0583 258.7989 258.8573 265.2279 387.9221 -0.0543 258.9774 259.0316 265.3822 389.5320 -0.0529 259.1631 259.2160 265.5698 391.1206 -0.0486 259.3358 259.3843 265.7585 392.7251 -0.0483 259.4936 259.5419 265.9458 394.3350 -0.0516 259.6672 259.7188 266.1260 395.9551 -0.0497 259.8474 259.8971 266.2680 397.5644 -0.0442 260.0047 260.0488 266.4086 399.1688 -0.0430 260.2045 260.2475 266.5850 400.7786 -0.0416 260.4246 260.4662 266.7712 402.3834 -0.0397 260.6046 260.6444 266.9307 403.9871 -0.0407 260.7826 260.8234 267.1076 405.5970 -0.0388 260.9689 261.0077 267.3166 407.2171 -0.0416 261.1963 261.2379 267.5143 408.8270 -0.0421 261.3895 261.4316 267.7906 410.4363 -0.0395 261.5584 261.5980 268.0265 412.0458 -0.0390 261.7492 261.7883 268.2888 413.6505 -0.0353 261.9397 261.9750 268.5508 415.2604 -0.0375 262.1145 262.1521 268.8192 416.8648 -0.0333 262.3066 262.3399 269.1085 418.4843 -0.0344 262.4804 262.5149 269.3766 420.0941 -0.0275 262.6721 262.6995 269.6646 421.6989 -0.0321 262.8703 262.9023 269.9284 423.3139 -0.0349 263.0595 263.0944 270.1637 424.9176 -0.0359 263.2604 263.2963 270.3327 426.5275 -0.0348 263.5141 263.5489 270.5101 428.1271 -0.0303 263.7049 263.7351 270.6800 429.7421 -0.0285 263.8987 263.9271 270.8665 431.3515 -0.0346 264.0745 264.1091 271.0675 432.9455 -0.0340 264.2781 264.3121 271.2583 434.5503 -0.0334 264.5099 264.5433 271.4335 436.1339 -0.0320 264.7020 264.7340 271.5764 437.7485 -0.0305 264.9009 264.9314 271.7071 439.3533 -0.0241 265.1069 265.1310 271.8912 440.9631 -0.0241 265.3199 265.3441 272.0683 442.5619 -0.0260 265.5371 265.5631 272.2658 444.1665 -0.0256 265.7115 265.7371 272.4615 445.7969 -0.0250 265.9006 265.9257 272.6668 447.4015 -0.0259 266.1037 266.1296 272.8728 449.0054 -0.0280 266.2498 266.2778 273.1014 450.6101 -0.0220 266.4723 266.4943 273.3649 452.2200 -0.0238 266.6928 266.7167 273.6184 453.8243 -0.0172 266.9174 266.9346 273.8806 455.4285 -0.0206 267.1130 267.1336 274.1560 457.0538 -0.0154 267.3474 267.3628 274.4072 458.6585 -0.0114 267.5795 267.5909 274.6598 460.2681 -0.0138 267.7930 267.8068 274.9280 461.8721 -0.0180 267.9690 267.9870 275.1711 463.4820 -0.0200 268.1587 268.1787 275.4300 465.0868 -0.0247 268.3293 268.3539 275.6445 466.6909 -0.0229 268.5181 268.5409 275.8208 468.3158 -0.0201 268.7445 268.7646 275.9919 469.9205 -0.0185 268.9498 268.9683 276.1859 471.5353 -0.0209 269.1711 269.1920 276.3767 473.1393 -0.0221 269.3778 269.3999 276.5535 474.7491 -0.0259 269.6083 269.6342 276.7597 476.3539 -0.0316 269.8049 269.8365 276.9203 477.9634 -0.0355 270.0059 270.0414 277.0789 479.5880 -0.0345 270.2114 270.2458 277.2748 481.1825 -0.0332 270.4334 270.4666 277.4547 482.7923 -0.0311 270.6359 270.6670 277.6386 484.4013 -0.0324 270.8321 270.8645 277.8439 486.0060 -0.0331 271.0299 271.0630 278.0429 487.6108 -0.0305 271.2434 271.2738 278.2533 489.2204 -0.0252 271.4986 271.5238 278.4623 490.8551 -0.0259 271.7230 271.7489 278.6738 492.4394 -0.0309 271.9338 271.9647 278.8843 494.0441 -0.0358 272.1770 272.2127 279.0916 495.6483 -0.0391 272.3897 272.4289 279.2973 497.2475 -0.0419 272.5772 272.6191 279.5667 498.8471 -0.0430 272.7793 272.8224 279.8619 500.4365 -0.0457 272.9827 273.0284 280.1452 502.0459 -0.0487 273.2041 273.2528 280.4101 503.6501 -0.0483 273.4313 273.4796 280.6582 505.2549 -0.0501 273.6366 273.6868 280.9114 506.8596 -0.0468 273.8311 273.8780 281.1746 508.4635 -0.0505 274.0330 274.0835 281.4490 510.0733 -0.0555 274.2284 274.2839 281.6396 511.6780 -0.0551 274.4506 274.5057 281.8239 513.2825 -0.0600 274.6823 274.7423 281.9835 514.8916 -0.0673 274.9023 274.9696 282.1310 516.4964 -0.0692 275.1544 275.2236 282.2759 518.1216 -0.0684 275.3684 275.4369 282.4304 519.7258 -0.0690 275.5469 275.6159 282.6026 521.3353 -0.0724 275.7670 275.8394 282.7699 522.9246 -0.0719 275.9875 276.0594 282.9365 524.5290 -0.0688 276.1902 276.2590 283.1226 526.1383 -0.0734 276.3914 276.4648 283.3029 527.7430 -0.0818 276.5895 276.6713 283.5140 529.3529 -0.0850 276.8347 276.9196 283.7295 530.9728 -0.0876 277.0800 277.1675 283.9208 532.5819 -0.0893 277.3194 277.4086 284.1651 534.1918 -0.0939 277.5631 277.6570 284.4165 535.8016 -0.0927 277.7936 277.8863 284.6438 537.4061 -0.0944 278.0352 278.1295 284.8808 539.0101 -0.0916 278.2268 278.3184 285.1539 540.6251 -0.0930 278.4599 278.5529 285.3863 542.2453 -0.0958 278.6394 278.7352 285.6020 543.8394 -0.0957 278.8484 278.9441 285.8620 545.4435 -0.0997 279.0563 279.1560 286.1084 547.0534 -0.1010 279.2799 279.3809 286.3712 548.6633 -0.1043 279.4780 279.5823 286.6326 550.2730 -0.1111 279.6859 279.7971 286.8327 551.8769 -0.1193 279.9352 280.0545 287.0695 553.4868 -0.1228 280.1738 280.2966 287.2762 555.1069 -0.1232 280.4327 280.5559 287.5076 556.7116 -0.1219 280.6416 280.7635 287.7092 558.3154 -0.1194 280.8548 280.9742 287.8996 559.9150 -0.1256 281.0691 281.1948 288.0761 561.4993 -0.1304 281.2697 281.4001 288.2219 563.1085 -0.1318 281.4986 281.6304 288.4195 564.7026 -0.1283 281.7453 281.8736 288.5853 566.3074 -0.1285 281.9415 282.0700 288.7700 567.9268 -0.1297 282.1497 282.2794 288.9379 569.5313 -0.1327 282.3772 282.5099 289.1021 571.1360 -0.1377 282.5895 282.7273 289.2885 572.7458 -0.1467 282.8508 282.9975 289.4980 574.3343 -0.1529 283.0622 283.2151 289.6979 575.9441 -0.1583 283.2157 283.3739 289.8909 577.5489 -0.1585 283.4358 283.5943 290.0812 579.1578 -0.1578 283.6747 283.8326 290.2869 580.7625 -0.1576 283.9423 284.0999 290.5360 582.3673 -0.1623 284.1786 284.3409 290.7821 583.9765 -0.1659 284.3938 284.5597 291.0235 585.5809 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446.3704 450.6181 438.6397 1699.4065 -4.2563 446.6100 450.8662 438.8328 1701.0318 -4.2632 446.8412 451.1044 439.0149 1702.6365 -4.2725 447.0963 451.3688 439.1575 1704.2461 -4.2772 447.3249 451.6021 439.2968 1705.8501 -4.2858 447.5284 451.8141 439.4544 1707.4651 -4.2970 447.7366 452.0336 439.5874 1709.0696 -4.3029 447.9920 452.2950 439.7051 1710.6788 -4.3089 448.2071 452.5160 439.8354 1712.2989 -4.3151 448.4139 452.7291 439.9974 1713.8985 -4.3238 448.6680 452.9918 440.1365 1715.5024 -4.3308 448.9034 453.2342 440.3340 1717.1019 -4.3357 449.1495 453.4852 440.5780 1718.7066 -4.3407 449.3806 453.7214 440.8507 1720.3114 -4.3491 449.6220 453.9711 441.1347 1721.9154 -4.3595 449.8505 454.2100 441.4291 1723.5353 -4.3695 450.0688 454.4383 441.7447